CN203291543U - Device of flow adjustable separation plate collection and redistribution device - Google Patents
Device of flow adjustable separation plate collection and redistribution device Download PDFInfo
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- CN203291543U CN203291543U CN2013203227268U CN201320322726U CN203291543U CN 203291543 U CN203291543 U CN 203291543U CN 2013203227268 U CN2013203227268 U CN 2013203227268U CN 201320322726 U CN201320322726 U CN 201320322726U CN 203291543 U CN203291543 U CN 203291543U
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Abstract
The utility model relates to a device of a flow adjustable separation plate collection and redistribution device. A separation plate is placed in the middle of a placing tower and the flow of liquid on one side is flexibly adjusted by a flow controller outside the tower; collection channels on the two sides are connected by a liquid-phase balance pipe so as to guarantee that the compositions of the liquid on the two sides of the separation plate and the heights of liquid levels of the channels are the same and the liquid on the two sides flows down at the same flow speed; an inclined angle is formed between each liquid guide pipe which is led out of the tower and the horizontal plane, and the liquid guide pipes and the horizontal plane are in smooth transition so as to reduce the liquid flowing resistance; the flowing of the liquid takes the height of the liquid level on the disc as a driving force; collection boxes on the two sides are fixed on the tower wall and uniformly-distributed small holes are formed in the bottom so as to have a liquid buffering effect, uniformly distribute the liquid, prevent from impacts of large-liquid-amount fluid to the liquid level of the liquid collection and redistribution device, and guarantee the operation stability of the device. The utility model provides a simple and stable method for adjusting a flow distribution ratio of the liquid on the two sides of the separation plate in a distillation tower. Static equipment is used so that extra energies including electricity, high-pressure steam and the like do not need to be consumed.
Description
Technical field
The utility model relates to a kind of dividing wall column liquid distribution trough, and the partition plate liquid that particularly relates to a kind of adjustable-flow is collected apparatus for redistributing.
Background technology
Rectifying is the industrial liquid mixture lock out operation that is widely used in most, rectifying why can separating mixture, key is the application that refluxes, but necessary lot of energy refluxes, except selecting the reflux ratio of economical rationality, developed some energy-saving rectifying columns both at home and abroad, improve the thermodynamic efficiency of rectifying column, reduce energy consumption, such as heat pump distillation, differential pressure heat coupling rectification, dividing plate rectifying etc.
Yet less for the research of dividing wall column both at home and abroad, dividing plate rectifying is, in rectifying column inside, one vertical partition plate is set, rectifying feed zone and middle extraction section four parts that rectifying column is divided into to public rectifying section, public stripping section, is separated by dividing plate.Because dividing wall column can reduce the material back mixing, than traditional cascade towers flow process is energy-conservation, reach as high as 60%, and can save 30% equipment investment, the most obvious to separating 3 component system power savings advantages.
The phase assignment of traffic of dividing wall column median septum both sides is key technologies of dividing plate rectifying.In dividing plate one side, be provided with charging aperture, opposite side is provided with discharging opening, the vapour phase flow of controlling the dividing plate both sides mainly completes by the pressure drop of both sides.Both sides vapour phase flow is uniformly distributed, need makes the pressure drop of dividing plate both sides consistent.If dividing plate one side liquid phase load is greater than opposite side, gas will flow into the little side of liquid phase load in a large number, and it is inhomogeneous that this will cause the vapour phase of both sides to be unworthy of, and can not carry out normal activity.Because charging aperture and discharging opening are located at the dividing plate both sides, therefore, consistent in order to guarantee both sides liquid phase load, the liquid that gets off from public rectifying section flow into the flow of feed side need be less than the flow of exit side.
Make dividing plate both sides liquid phase flow unequal, two kinds of methods are generally arranged: 1, dividing plate is not placed in the middle of tower; 2, flow distributor of design is controlled fluid flow above dividing plate.Adopt first method, can only be for fixing separation operating mode, if operating condition changes, the expense of follow-up transformation partitioned column is large, complicated operation.Adopt second method to have obvious advantage, can regulate flexibly dividing plate both sides liquid phase distribution ratio of liquid flow according to actual condition.
CN102872609 discloses and a kind ofly can regulate the liquid backflow distribution ratio of dividing plate both sides and the method for gas distribution ratio, this method comprises a liquid backflow system: dividing plate upper end liquid is all extracted out, again it is back to respectively to the dividing plate both sides in proportion, can cause extracting out like this temperature change of liquid, and then can affect separating effect, and need stage casing backflow surge tank and stage casing reflux pump are installed, invest more; This patent has also been announced a gas distributor: adopts moving equipment, and it is arranged on to rectifying column inside, and complex structure, wayward, on engineering, vapour phase is distributed to more difficult realization.
In the US5755933 patent, point out, by dividing plate being extended to bottom or the top of dividing wall column, by reboiler and condenser, carry out the distribution ratio of adjustments of gas and liquid.But the improved rectifying column of this method has not been traditional dividing wall column.
In the US7267746 patent, point out, by detecting respectively the temperature of uprising gas at the bottom of overhead reflux liquid and tower, come dynamic adjustments to enter the distribution ratio of dividing plate both sides liquid.This method complicated operation, equipment is more, is applicable to produce alkylated aromatic hydrocarbon.
Summary of the invention
The purpose of this utility model is to provide a kind of device of adjustable partition plate liquid distributor, liquid phase flow-rate ratio that can flexible modulation dividing plate both sides.The static equipment device that uses the utility model to provide, the position without changing dividing plate, can facilitate, the fluid flow distribution ratio on stable adjusting dividing plate both sides.
The technical solution of the utility model is as follows:
A kind of adjustable-flow dividing plate is collected the device of redistributor, comprises public rectifying section filler (1), rises gas cap (2), riser (3), base plate (4), collects in canal (5), liquid equilibrium pipe (6), tower catheter (7-1) and tower catheter (7-2), tower external flux controller (8), distributor disk (9), liquid collection redistributor (10), dividing plate (11), filler (12) outward; It is characterized in that, in public stripping section filler (1) below, a base plate (4) is set, base plate (4) top arranges equally distributed riser (3), and riser (3) top arranges and rises gas cap (2); In base plate (4) both sides, a collection canal (5) is set respectively, collects canal (5) and connect by liquid equilibrium pipe (6); In both sides, collect canal (5) below and be provided with catheter (7-2) outside catheter in tower (7-1) and tower, the outer catheter (7-2) of the tower of feed side is led to outside tower, the outer catheter (7-2) of tower has downward angle of inclination with horizontal plane, on the outer catheter of tower, be provided with tower external flux controller (8), outer catheter (7-2) outlet of tower connects distributor disk (9); In tower, catheter (7-1) is vertically installed, and in tower, catheter (7-1) outlet connects distributor disk (9); Distributor disk (9) both sides are fixed on Ta Bishang, and the duct of even size is offered in its bottom; In distributor disk (9) below, a liquid collection redistributor (10) is set, its below arranges the filler (12) that is separated by dividing plate (11).
The method for designing of the outer catheter (7-2) of catheter (7-1) and tower is in tower of the present utility model: in the bottom opening of both sides collection canal, connect catheter below hole.The both sides the number of openings respectively is advisable for 5-10, in actual condition, according to outer catheter (7-2) number of factor design perforate number, duct size and the towers such as liquid load in tray diameter, tower.
The number of the outer catheter (7-2) of the tower of feed side is generally less than the number of catheter (7-1) in tower, and the preferred number of the outer catheter (7-2) of tower is advisable with 2-4.
The operating process that the adjustable-flow partition plate liquid is collected redistributor is as follows:
Liquid mixture flows down and enters base plate (4) from public rectifying section filler (1), then imports in the collection canal (5) of both sides; Vapour mixture out enters public rectifying section filler (1) from riser (3), rises gas cap (2) and stops liquid to flow into riser (3); Liquid enrichment in collecting canal (5), both sides are collected canal (5) and are connected by liquid equilibrium pipe (6); Exit side liquid directly flows down and enters in distributor disk (9) by catheter (7-1) in tower; Feed side liquid partly directly flows down and enters in distributor disk (9) by catheter (7-1) in tower, partially liq flows out to outside tower by the outer catheter (7-2) of tower, after controlling uninterrupted, tower external flux controller (8) flows in distributor disk (9) again, liquid comes together in the distributor disk (9) of both sides, aperture by disposable box (9) bottom flows down again, enters into following liquid collection redistributor (10); Final liquid enters in the filler (12) of dividing plate (11) both sides and separates.So just, realized the control to the different distribution ratios of dividing plate both sides fluid flow.
So characteristics of the present utility model are in a kind of method of simple and easy, stable adjusting dividing wall column median septum both sides fluid flow distribution ratio.Innovation is: use be static equipment, without consuming extra electricity, high steam homenergic; Partition position is placed on the centre of tower, by tower external flux controller flexible modulation one side fluid flow; The collection canal of both sides is connected by the liquid equilibrium pipe, to guarantee that on dividing plate both sides liquid composition and canal, liquid level is consistent, the liquid of both sides is flowed down with identical flow velocity; Drawing the outer catheter of tower and horizontal plane has individual inclination angle and round and smooth excessive, has reduced liquid flowing resistance, and on liquid flow dependence dish, liquid level is as motive force; The both sides disposable box is fixed on Ta Bishang, and equally distributed aperture is opened in bottom, plays a fluid cushion effect, can make the liquid distributed uniform, prevents the impact of large liquid measure fluid to following liquid collection redistributor liquid level, the stability of assurance device operation.
The accompanying drawing explanation
Fig. 1: a kind of easy, stable adjustable-flow dividing plate of the present utility model is collected the redistributor structural representation.
Fig. 2: a kind of easy, stable adjustable-flow dividing plate of the present utility model is collected the redistributor top view.
Fig. 3: feed side is collected the catheter structure simplified schematic diagram of canal bottom.
The specific embodiment
Below in conjunction with Fig. 1, Fig. 2, Fig. 3, the utility model is described in further detail
A kind of device of adjustable partition plate liquid distributor, comprise public rectifying section filler (1), rise gas cap (2), riser (3), base plate (4), collect in canal (5), liquid equilibrium pipe (6), tower catheter (7-1) and tower catheter (7-2), tower external flux controller (8), distributor disk (9), liquid collection redistributor (10), dividing plate (11), filler (12) outward; It is characterized in that, in public stripping section filler (1) below, a base plate (4) is set, base plate (4) top arranges equally distributed riser (3), and riser (3) top arranges and rises gas cap (2); In base plate (4) both sides, a collection canal (5) is set respectively, collects canal (5) and connect by liquid equilibrium pipe (6); In both sides, collect canal (5) below and be provided with catheter (7-2) outside catheter in tower (7-1) and tower, the outer catheter (7-2) of the tower of feed side is led to outside tower, the outer catheter (7-2) of tower has angle of inclination with horizontal plane, on the outer catheter of tower, be provided with tower external flux controller (8), outer catheter (7-2) outlet of tower connects distributor disk (9); In tower, catheter (7-1) is vertically installed, and in tower, catheter (7-1) outlet connects distributor disk (9); Distributor disk (9) both sides are fixed on Ta Bishang, and the duct of even size is offered in its bottom; In distributor disk (9) below, a liquid collection redistributor (10) is set, its below arranges the filler (12) that is separated by dividing plate (11).
A kind of adjustable-flow dividing plate of the present utility model is collected the redistributor device, and its concrete implementation step is:
Liquid mixture flows down and enters base plate (4) from public rectifying section filler (1), then imports in the collection canal (5) of both sides; Vapour mixture out enters public rectifying section filler (1) from riser (3), rises gas cap (2) and stops liquid to flow into riser (3); Liquid enrichment in collecting canal (5), both sides are collected canal (5) and are connected by liquid equilibrium pipe (6); Exit side liquid directly flows down and enters in distributor disk (9) by catheter (7-1) in tower; Feed side liquid partly directly flows down and enters in distributor disk (9) by catheter (7-1) in tower, partially liq flows out to outside tower by the outer catheter (7-2) of tower, after controlling uninterrupted, tower external flux controller (8) flows in distributor disk (9) again, liquid comes together in the distributor disk (9) of both sides, aperture by disposable box (9) bottom flows down again, enters into following liquid collection redistributor (10); Final liquid enters in the filler (12) of dividing plate (11) both sides and separates.So just, realized the control to the different distribution ratios of dividing plate both sides fluid flow.
In actual condition, by calculating, enter dividing plate both sides fluid flow ratio, then set the number of catheter (7-1), (7-2), set again tower external flux controller opening degree, can be different so that flow to the fluid flow of distributor disk, in distributor disk, the ratio of fluid flow is the ratio of dividing plate both sides fluid flow, can facilitate like this, regulate flexibly dividing plate both sides fluid flow distribution ratio.
Below illustrate:
1), make dividing plate both sides fluid flow than being 4:7.As shown in the top view of figure bis-, both sides are collected canal (5) bottom and are all opened 7 holes, below hole, be catheter (7-1) and the outer catheter (7-2) of tower in the catheter tower, the outer catheter (7-2) of 3 towers of feed side is drawn out to the outer flow controller (8) of tower, and in tower, catheter (7-1) is vertically installed.It is 0(that is complete shut-down that tower external flux controller (8) is set flow), the both sides fluid flow is than being 4:7.
2), make dividing plate both sides fluid flow than being 5:7.As shown in the top view of figure bis-, both sides are collected canal (5) bottom and are all opened 7 holes, below hole, be catheter (7-1) or the outer catheter (7-2) of tower in tower, the outer catheter (7-2) of 3 towers of feed side is drawn out to the outer flow controller (8) of tower, in tower, catheter (7-1) is vertically installed.It is the flow of a catheter that tower external flux controller (8) is set flow, and the both sides fluid flow is than being 5:7.
3), make dividing plate both sides fluid flow than being 1:1.As shown in the top view of figure bis-, both sides are collected canal (5) bottom and are all opened 7 holes, below hole, be catheter (7-1) or the outer catheter (7-2) of tower in tower, the outer catheter (7-2) of 3 towers of feed side is drawn out to the outer flow controller (8) of tower, in tower, catheter (7-1) is vertically installed.It is the flow (that is standard-sized sheet) of 3 catheters that tower external flux controller (8) is set flow, and the both sides fluid flow is than being 1:1.
Collecting the number of openings of canal both sides is advisable at 5-10, outer catheter (7-2) number of tower generally is less than catheter (7-1) number in tower, the outer catheter (7-2) of tower is advisable with 2-4, above-mentioned example is only preferred embodiment of the present utility model, can not be considered to be used to limiting practical range of the present utility model.
So characteristics of the present utility model are in a kind of method of simple and easy, stable adjusting dividing wall column median septum both sides fluid flow distribution ratio.Innovation is: use be static equipment, without consuming extra electricity, high steam homenergic; Partition position is placed the centre of tower, by tower external flux controller flexible modulation one side fluid flow; The collection canal of both sides is connected by the liquid equilibrium pipe, to guarantee that on dividing plate both sides liquid composition and canal, liquid level is consistent, the liquid of both sides is flowed down with identical flow velocity; Drawing the outer catheter of tower and horizontal plane has individual inclination angle and round and smooth excessive, has reduced liquid flowing resistance, and on liquid flow dependence dish, liquid level is as motive force; The both sides disposable box is fixed on Ta Bishang, and equally distributed aperture is opened in bottom, plays a fluid cushion effect, can make the liquid distributed uniform, prevents the impact of large liquid measure fluid to following liquid collection redistributor liquid level, the stability of assurance device operation.
Claims (3)
1. an adjustable-flow dividing plate is collected the device of redistributor, comprises public rectifying section filler (1), rises gas cap (2), riser (3), base plate (4), collects in canal (5), liquid equilibrium pipe (6), tower catheter (7-1) and tower catheter (7-2), tower external flux controller (8), distributor disk (9), liquid collection redistributor (10), dividing plate (11), filler (12) outward; It is characterized in that, in public stripping section filler (1) below, a base plate (4) is set, base plate (4) top arranges equally distributed riser (3), and riser (3) top arranges and rises gas cap (2); In base plate (4) both sides, a collection canal (5) is set respectively, collects canal (5) and connect by liquid equilibrium pipe (6); In both sides, collect canal (5) below and be provided with catheter (7-2) outside catheter in tower (7-1) and tower, the outer catheter (7-2) of the tower of feed side is led to outside tower, the outer catheter (7-2) of tower has downward angle of inclination with horizontal plane, on the outer catheter of tower, be provided with tower external flux controller (8), outer catheter (7-2) outlet of tower connects distributor disk (9); In tower, catheter (7-1) is vertically installed, and in tower, catheter (7-1) outlet connects distributor disk (9); Distributor disk (9) both sides are fixed on Ta Bishang, and the duct of even size is offered in its bottom; In distributor disk (9) below, a liquid collection redistributor (10) is set, its below arranges the filler (12) that is separated by dividing plate (11).
2. device as claimed in claim 1, is characterized in that outer catheter (7-2) number of tower is less than catheter (7-1) number in tower.
3. device as claimed in claim 1, is characterized in that the outer catheter (7-2) of tower is 2-4.
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CN2013203227268U CN203291543U (en) | 2013-06-05 | 2013-06-05 | Device of flow adjustable separation plate collection and redistribution device |
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CN2013203227268U CN203291543U (en) | 2013-06-05 | 2013-06-05 | Device of flow adjustable separation plate collection and redistribution device |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109357543A (en) * | 2018-12-13 | 2019-02-19 | 北京国电龙源环保工程有限公司 | New structural vertical column liquid trap |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN109357543A (en) * | 2018-12-13 | 2019-02-19 | 北京国电龙源环保工程有限公司 | New structural vertical column liquid trap |
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