CN203144515U - Device to prepare coatings, films or composite materials - Google Patents
Device to prepare coatings, films or composite materials Download PDFInfo
- Publication number
- CN203144515U CN203144515U CN 201220600651 CN201220600651U CN203144515U CN 203144515 U CN203144515 U CN 203144515U CN 201220600651 CN201220600651 CN 201220600651 CN 201220600651 U CN201220600651 U CN 201220600651U CN 203144515 U CN203144515 U CN 203144515U
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- matrix material
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Abstract
The utility model is applicable in the preparation filed of films, coatings or composite materials, and discloses a device to make coatings, films and composite materials which comprises a solution tank, a cooling device of solution to be settled, a deposition tank, an HP circulating pump, a cooling tank, an electrode generating device and an ultrasonic generating device. An outlet tube is provided between the solution tank and the cooling device of solution to be settled; an inlet tube is provided between the cooling device of solution to be settled and the deposition tank; a reflux tube is provided between the deposition tank and the solution tank; and the HP circulating pump is set on the reflux tube. An electrode generating device is set inside the deposition tank, and an ultrasonic generating device is set inside the cooling tank. The coating or films prepared in the utility model is provided with ample compositions, structures and figures, and higher binding force with products.
Description
Technical field
The utility model relates to a kind of apparatus and method that prepare coating, film or matrix material, more particularly, relates to a kind of apparatus and method of utilizing the ultrasonic electric heating deposition of jet preparation coating, film or matrix material.
Background technology
The hot basal body method is that the electro-conductive material that will have certain resistivity places to contain and remains deposited coatings or film and form ion solution, heat by alternating-current then, its surface temperature of this electro-conductive material raises, realize the preparation (KensukeKuroda of coating or film with the Gibbs free energy that reduces the formation of coating or film, MikikoMoriyama, RyoichiIchino, MasazumiOkido, AzusaSeki.Formationand Osteoconductivity of Hydroxyapatite/Collagen Composite Films Usinga Thermal Substrate Method in Aqueous Solutions, Materials Transactions, 2009,50(5): 1190-1195).Though this method can be controlled composition, structure, pattern and the thickness of coating or film, the bonding force of this method is very poor, does not satisfy the mechanical property requirements of coating.
Application number is that 200810011621.4 Chinese patent " a kind of preparation method of carbon nanotube/carbon fiber multi-dimension mixing composite material " has announced that the method for utilizing ultrasonic wave assisted electrochemical deposition prepares the technology of nanofiber precast body, and this technology can make shearing resistance, impact resistance, the specific conductivity of matrix material all improve a lot.Application number is that 201010540770.7 Chinese patent " preparation method of a kind of carbon-carbon composite/hydroxyapatite/polylactic acid biomaterial " utilizes hyperacoustic concussion cavitation effect to solve the not enough problem of coating's adhesion that is deposited on matrix surface.Above-mentioned two patents all improve the not enough problem of matrix surface coating bonding force that is deposited on ultrasonic technology, and still, only the result who solves such problem with ultrasonic technology obviously is not very desirable.Application number is that 200510041821.0 Chinese patent " Hall ion source actuated magnetron sputtering enhancing type multi-arc ion plating film method " has been announced another technology: utilize Hall source forcing magnetic technology to improve the ionization level of reaction process, by the adjustable mechanical filter structure Design of bias voltage, guarantee film and high base strength.But there is complicated in mechanical structure in this technology, the shortcoming that cost is high.
The utility model content
Technical problem to be solved in the utility model is to provide a kind of device for preparing coating, film or matrix material.
This device is specific as follows:
A kind of device for preparing coating, film or matrix material comprises: splendid attire remain deposit solution solution tank, treat deposit solution refrigerating unit, sedimentation tank, be loaded with the cooling tank of cooling fluid; Described solution tank and described treating are connected with output tube between the deposit solution refrigerating unit, and described treating is connected with liquid-inlet pipe between deposit solution refrigerating unit and the described sedimentation tank, and described sedimentation tank and described solution tank are connected with return line; This return line pipeline is provided with high-pressure circulation pump, and described sedimentation tank is arranged in the described cooling tank, also is provided with the electrode generating unit in the described sedimentation tank, also is provided with ultrasonic generator in the described cooling tank.
Further, described electrode generating unit comprises product, two electrodes, and two electrodes are electrically connected with AC power by lead.
Further, described ultrasonic generator comprises ultrasonic vibration plate and ultrasonic generator, and described ultrasonic vibration plate places outside the cooling tank and with described ultrasonic generator and is connected.
Further, the described deposit solution refrigerating unit for the treatment of comprises cooling-water machine, cooling tube and first pipe connecting, and described first pipe connecting connects described cooling-water machine and described cooling tube, and the two ends of described cooling tube connect described output tube and described liquid-inlet pipe respectively.
Further, described cooling tank and described cooling-water machine also are connected with second pipe connecting.
Further, described cooling fluid is water.
Further, described AC power is alternating current steady voltage plug.
The device of preparation coating, film or matrix material that the utility model provides and the beneficial effect of prior art are: by adding cooling fluid and ultrasonic unit in the cooling tank, the energy that ultrasonic vibration is produced passes to by cooling fluid treats deposit solution, further accelerate to treat the collision of deposit solution and product surface, make the coating that is combined in product surface or the binding ability enhancing of film; By with solution tank, output tube, treat that deposit solution refrigerating unit, liquid-inlet pipe, sedimentation tank, high-pressure circulation pump are according to necessarily being linked in sequence, allow and treat that deposit solution circulates in aforesaid device, make the coating sedimentary dynamics change surface reaction control into by the diffusion way of traditional hot deposition, can also make the stronger particle of adhesive capacity in the deposit solution for the treatment of in the sedimentation tank form strong uniform coating or the film of bonding force at product surface simultaneously; The binding ability of using the coating can make product surface or film in the time of these two kinds of patterns is stronger.
Description of drawings
A kind of device synoptic diagram for preparing coating, film or matrix material that Fig. 1 provides for the utility model embodiment.
Embodiment
In order to make technical problem to be solved in the utility model, technical scheme and beneficial effect clearer, below in conjunction with drawings and Examples, the utility model is further described.Should be appreciated that specific embodiment described herein only in order to explaining the utility model, and be not used in restriction the utility model.
Please refer to Fig. 1, the apparatus and method that show preparation coating, film or matrix material that the utility model is provided describe.
Whole device of the present utility model is made up of following each several part: solution tank 1, treat deposit solution refrigerating unit, sedimentation tank 11 and high-pressure circulation pump 2, cooling tank 4, electrode generating unit and ultrasonic generator.Treat that the deposit solution refrigerating unit is made up of cooling tube 12, first pipe connecting 32 and cooling-water machine 13.Be connected with output tube 31 between cooling tube 12 and the solution tank 1.Be connected with liquid-inlet pipe 33 between cooling tube 12 and the sedimentation tank 11.Cooling tube 12 is connected by first pipe connecting 32 with cooling-water machine 13.Be connected with second pipe connecting 34 between cooling-water machine 13 and the cooling tank 4.Be connected with return line 3 between sedimentation tank 11 and the solution tank 1.High-pressure circulation pump 2 is arranged on the return line 3.
Be placed with the electrode generating unit in the sedimentation tank 11.The electrode generating unit comprises: product 6, two electrodes 8, lead 10 and AC power 9.The same utmost point of the two ends of product 6 and two electrodes 8 links to each other respectively.Another utmost point of two electrodes 8 is electrically connected by lead 10 and AC power 9 respectively.Product 6, two electrodes 8, lead 10, AC power 9 form the loop line.
After the connection of finishing above-mentioned all parts, begin to prepare the said preparation of the ultrasonic electric heating deposition of jet coating, film or the matrix material of utilizing of the utility model, concrete steps are as follows:
1) opens cooling-water machine 13, respectively cooling tube 12 and cooling tank 4 are cooled off;
2) prepare according to the composition of the coating of required preparation or film and correlation parameter and treat deposit solution, and will treat that deposit solution puts into solution tank 1;
3) open sedimentation tank 11, product 6 is clamped between two electrodes 8, build the sealing cover of sedimentation tank 11 then;
4) start high-pressure circulation pump 2, make and treat that deposit solution constantly circulates between solution tank 1, output tube 31, cooling tube 12, liquid-inlet pipe 33, sedimentation tank 11, high-pressure circulation pump 2, return line 3 and solution tank 1; Simultaneously cooling fluid is poured into cooling tank 4, guaranteed that cooling fluid floods oscillating plate 5 and sedimentation tank 11 outer walls, but can not make cooling fluid pour into the deposit solution for the treatment of in the sedimentation tank 11.In addition, the deposit solution for the treatment of in the sedimentation tank 11 need guarantee to flood the lower end of product 6 and electrode 8.
5) open ultrasonic generator 7, ultrasonic vibration plate 5 is started working, and ultrasonic vibration plate 5 constantly vibrates cooling fluid, cooling fluid vibration sedimentation tank 11 outer walls, the deposit solution for the treatment of in the sedimentation tank 11 also and then constantly vibrates, thereby constantly washes away the outside surface of product 6.Like this, treat that the solution particle that adhesive capacity is strong in the deposit solution just evenly is attached to the outside surface of product 6, formation coating or film.
6) open AC power 9, set oscillating current and the depositing time of required preparation coating or film, carry out coating or thin film deposition.
After when 7) waiting to reach required deposition, at first close AC power 9, deposition process is stopped; After close high-pressure circulation pump 2, take out product 6, product is carried out ultrasonic cleaning, drying, obtained preparing the matrix product of coating or film.
Product 6 also can be matrix material, treats that then the solution particle that adhesive capacity is strong in the deposit solution enters the gap between the molecule in the matrix material, forms new matrix material.
So far, the whole preparation process of the preparation of the ultrasonic electric heating deposition of jet coating, film or matrix material of utilizing is finished.
Because in coating or depositing of thin film process, product 6 is in the Vltrasonic device, during ultrasonic cleaning, under action of ultrasonic waves, treating in the deposit solution in the sedimentation tank 11 passed in mechanical vibration, make the vibration for the treatment of alternately to occur in the deposit solution density interphase, treat that deposit solution is constantly stretched and compresses.The place of dredging is stretched, and forms microbubble (hole); Close place is compressed.Stretch continually and compress owing to treat deposit solution inside to be subjected to hyperacoustic vibration, the result constantly produces microbubble and constantly breaks.During microbubbles rupture, the deposit solution for the treatment of on every side stretches to the center of bubble from all directions with huge speed, produce water attack, cause coating to combine more closely with product 6, hyperacoustic energy has participated in surface chemical reaction simultaneously, so coating has abundanter composition, structure and pattern.In addition, because under the effect of high-pressure pump, what flow fast treats deposit solution just as the water cutter, and coating has been formed very strong cutting force, be not easy to adhere in conjunction with particle a little less than this makes, this also is the major cause that the coating bonding force increases substantially.In addition, the coating sedimentation model is subjected to surface reaction control by the dispersal pattern transformation of traditional hot deposition, also is that coating obtains high major reason of making a concerted effort.
In the present embodiment, said cooling fluid is preferably water, and said AC power 9 is alternating current steady voltage plug.
The utility model has been owing to added jet and ultrasonic field in coating or film deposition process, so manufactured coating or film composition, structure, pattern are abundanter, and bonding force is higher.
The above only is preferred embodiment of the present utility model; not in order to limit the utility model; all any modifications of within spirit of the present utility model and principle, doing, be equal to and replace and improvement etc., all should be included within the protection domain of the present utility model.
Claims (7)
1. a device for preparing coating, film or matrix material is characterized in that, comprising: splendid attire remain deposit solution solution tank, treat deposit solution refrigerating unit, sedimentation tank, be loaded with the cooling tank of cooling fluid; Described solution tank and described treating are connected with output tube between the deposit solution refrigerating unit, and described treating is connected with liquid-inlet pipe between deposit solution refrigerating unit and the described sedimentation tank, and described sedimentation tank and described solution tank are connected with return line; This return line pipeline is provided with high-pressure circulation pump, and described sedimentation tank is arranged in the described cooling tank, also is provided with the electrode generating unit in the described sedimentation tank, also is provided with ultrasonic generator in the described cooling tank.
2. the device of preparation coating as claimed in claim 1, film or matrix material is characterized in that, described electrode generating unit comprises product, two electrodes, and two electrodes are electrically connected with AC power by lead.
3. the device of preparation coating as claimed in claim 1, film or matrix material, it is characterized in that, described ultrasonic generator comprises ultrasonic vibration plate and ultrasonic generator, and described ultrasonic vibration plate places outside the cooling tank and with described ultrasonic generator and is connected.
4. the device of preparation coating as claimed in claim 1, film or matrix material, it is characterized in that, the described deposit solution refrigerating unit for the treatment of comprises cooling-water machine, cooling tube and first pipe connecting, described first pipe connecting connects described cooling-water machine and described cooling tube, and the two ends of described cooling tube connect described output tube and described liquid-inlet pipe respectively.
5. the device of preparation coating as claimed in claim 4, film or matrix material is characterized in that, is connected with second pipe connecting between described cooling tank and the described cooling-water machine.
6. the device of preparation coating as claimed in claim 1, film or matrix material is characterized in that, described cooling fluid is water.
7. the device of preparation coating as claimed in claim 2, film or matrix material is characterized in that, described AC power is alternating current steady voltage plug.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201220600651 CN203144515U (en) | 2012-11-14 | 2012-11-14 | Device to prepare coatings, films or composite materials |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201220600651 CN203144515U (en) | 2012-11-14 | 2012-11-14 | Device to prepare coatings, films or composite materials |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203144515U true CN203144515U (en) | 2013-08-21 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201220600651 Expired - Fee Related CN203144515U (en) | 2012-11-14 | 2012-11-14 | Device to prepare coatings, films or composite materials |
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| Country | Link |
|---|---|
| CN (1) | CN203144515U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108939929A (en) * | 2018-08-13 | 2018-12-07 | 清华大学 | The coating modified filter membrane of graphene oxide and its preparation and bond strength appraisal procedure |
-
2012
- 2012-11-14 CN CN 201220600651 patent/CN203144515U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108939929A (en) * | 2018-08-13 | 2018-12-07 | 清华大学 | The coating modified filter membrane of graphene oxide and its preparation and bond strength appraisal procedure |
| CN108939929B (en) * | 2018-08-13 | 2021-06-08 | 清华大学 | Graphene oxide coating modified filter membrane and preparation method and bonding strength evaluation method thereof |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20130821 Termination date: 20141114 |
|
| EXPY | Termination of patent right or utility model |