A kind of efficient rhodium reaction heating elevator furnace
Technical field
The utility model relates to a kind of heating reaction furnace, the especially a kind of reaction of rhodium efficiently heating elevator furnace.
Background technology
Metal current rhodium powder transforms rhodium ion, and two kinds of methods are arranged usually, and first method is mixed back feeding chlorine with rhodium with potassium chloride and carried out chlorination; Second method is mixed the back heating with rhodium with potassium acid sulfate and is reacted.First method need be led to chlorine, yet chlorine is a kind of toxic gas, causes chlorine leakage if deal with improperly, causes life danger can for operating personnel and personnel on every side, so seldom use now.The main now second method of using is about to rhodium and reacts with the potassium acid sulfate Hybrid Heating, and method is simple, and does not need chlorine.Yet in the second approach; The firing equipment that uses at present all is common Muffle furnace, and this makes rhodium follow the mixture of the potassium acid sulfate inequality of being heated, and it is low to cause rhodium to follow metal rhodium to change into the conversion ratio of rhodium ion; And it is temperature required to need the operating personnel regularly to regulate, troublesome poeration.In addition, this Muffle furnace poor air-tightness is unfavorable for the saving of the temperature control and the energy.
The utility model content
To existing technical deficiency; The inner crisscross layout of heating element heater that adopts of the burner hearth of the utility model; Make rhodium follow the potassium acid sulfate mixture to obtain fully and equably heating, solved above-described effectively because of heating the inhomogeneous low technical problem of conversion ratio that causes.
The technical scheme that the utility model is taked is:
A kind of efficient rhodium reaction heating elevator furnace comprises body of heater, has flame-proof thermal insulation material in the said body of heater and heating element heater is housed, and wherein said heating element heater is the resistance-type heating rod, and the crisscross top that is distributed in said body of heater; Said body of heater also has the lifting pedestal that the inner chamber of shape and said body of heater is complementary; Said lifting pedestal liftably is linked at body of heater inside and constitutes the heating chamber that seals with said body of heater through the up-down power transmission chain, and building on the said lifting pedestal has insulating brick and be provided with a plurality of charge piers that hold the rhodium reaction material.
The beneficial effect of the utility model is:
The utility model discloses a kind of heating elevator furnace to the rhodium reaction; The crisscross layout of heating element heater that burner hearth is inner; Form the space of a plurality of squares; Make rhodium follow the potassium acid sulfate mixture to obtain fully and equably heating in the space of said square, improved the rhodium conversion ratio so widely.This heating elevator furnace employing burner hearth bottom goes up and down, and its liftable bottom and fire door kiss is joined material employing flame-proof thermal insulation material in combination and its stove when closing, thereby has improved sealing, reduces thermal loss, energy savings.
Description of drawings
Below in conjunction with accompanying drawing and embodiment the utility model is described further.
Fig. 1 is the front view of the utility model;
Fig. 2 is the vertical view of the utility model.
The specific embodiment
As illustrated in fig. 1 and 2, the utility model provides a kind of efficient rhodium reaction heating elevator furnace, it comprises resistant to elevated temperatures body of heater 1, the inwall of body of heater 1 is with one deck flame-proof thermal insulation material 2, to reduce the thermal loss of burner hearth.The heating element heater 3 that is used to heat the rhodium reaction material also is equipped with in the inside of body of heater 1, and in the utility model, heating element heater 3 is selected the resistance-type heating rod for use, and with the crisscross top that is distributed in body of heater 1 of these heating rods, forms the space of a plurality of squares.
The utility model also has a liftable lifting pedestal 4; The cavity shape of its shape and body of heater 1 is complementary; This lifting pedestal 4 liftably is linked at body of heater 1 inside through up-down power transmission chain 5, when lifting pedestal 4 is risen and body of heater 1 constituted the burner hearth of a sealing.In addition, building on the lifting pedestal 4 has insulating brick 6, and is provided with a plurality of charge piers 7 that hold the rhodium reaction material.
When using this heating elevator furnace, at first the mixture of rhodium with potassium acid sulfate evenly is placed in the charge pier 7, again lifting pedestal 4 risen heating in the charge pier 7 insertion heating element heaters 3.Like this, rhodium obtains fully and equably heating with the potassium acid sulfate mixture in the square space that heating element heater 3 is constituted, and the rhodium conversion ratio is able to improve effectively.In addition, this heating elevator furnace adopts burner hearth bottom to go up and down, and liftable base 4 and fire door (being the inner chamber of body of heater) kiss is joined combination, and material is a flame-proof thermal insulation material in the stove, thereby has improved sealing, reduces thermal loss, has reached the purpose of energy savings.
The heating elevator furnace of the utility model can adopt the adjustable intelligent instrument as its supporting temperature control part, can work out a plurality of blocks, the sintering procedure of precisely control product, and can realize overcurrent, current limliting, defencive function such as overheated.
The above be the utility model preferred embodiment, it does not constitute the restriction to the utility model protection domain, so long as realize that with essentially identical means the purpose of the utility model all should belong to the protection domain of the utility model.