CN202128934U - Acetate recovery distillation column with heater - Google Patents

Acetate recovery distillation column with heater Download PDF

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Publication number
CN202128934U
CN202128934U CN201120250913U CN201120250913U CN202128934U CN 202128934 U CN202128934 U CN 202128934U CN 201120250913 U CN201120250913 U CN 201120250913U CN 201120250913 U CN201120250913 U CN 201120250913U CN 202128934 U CN202128934 U CN 202128934U
Authority
CN
China
Prior art keywords
heater
steam
column
steam heater
distribution
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201120250913U
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Chinese (zh)
Inventor
叶四华
李帆
汪尚飞
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
JIANGMEN HANDSOME CHEMICAL DEVELOPMENT Co Ltd
Original Assignee
JIANGMEN HANDSOME CHEMICAL DEVELOPMENT Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by JIANGMEN HANDSOME CHEMICAL DEVELOPMENT Co Ltd filed Critical JIANGMEN HANDSOME CHEMICAL DEVELOPMENT Co Ltd
Priority to CN201120250913U priority Critical patent/CN202128934U/en
Application granted granted Critical
Publication of CN202128934U publication Critical patent/CN202128934U/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Abstract

The utility model discloses an acetate recovery distillation column with a heater, which comprises a column body and the heater arranged inside the column body. The heater is a steam heater which is arranged above the bottom of the column. The steam heater comprises at least one steam distribution pipe. One end of the steam heater penetrates through the lateral side of the column body and is provided with a steam inlet. Openings which correspond to materials in the column are arranged on the steam distribution pipe. The conventional heater in the prior art is omitted, and a predesigned steam heater is introduced to replace the original heater. Steam enters the steam heater through the steam inlet and jet out through the openings of the steam heater so that the steam directly contacts with materials in the recovery distillation column to carry out heat and mass exchanges, namely, to carry out mixing direct heat exchange. The steam heater is simple in manufacture, low in cost and mainly made of stainless pipes, welding rods and the like. The use of the steam heater not only guarantees normal or better running of the acetate recovery distillation column but lowers the cost thereof greatly.

Description

A kind of acetate that has heater reclaims rectifying column
Technical field
The utility model relates to the firing equipment of organic wastewater recovery centrifugal station in a kind of acetate industry, relates in particular to a kind of recovery rectifying column that has heater that is specifically designed to.
Background technology
The heater that uses in the existing recovery rectifying column roughly is divided into three kinds of dividing wall type, hybrid, heat accumulating types.Reclaim rectifying and generally adopt the dividing wall type heater, and the dividing wall type heater is the most general with shell-and-tube heat exchanger (reboiler), submerged coil heat exchanger.Characteristic according to institute adaptive technique field; It is water that acetate reclaims the most of composition of the handled material of rectifier unit, adopts the direct contact heat-exchanging mode of dividing wall type heater feasible, even even more ideal; But; Existing dividing wall type heater, in textural more complicated, and the price of this type of heater is comparatively expensive like shell-and-tube heat exchanger, submerged coil heat exchanger.
Summary of the invention
The utility model is in order to overcome the deficiency of prior art; Provide a kind of acetate that has heater to reclaim rectifying column; Especially to reclaiming the transformation of the heater in the rectifying column, be intended to production cost and input cost in order to reduce acetate, the recovery rectifying column of the utility model is being guaranteed under the prerequisite of unit normal run; Design a steam heater simple in structure, easily manufactured and replaced original shell-and-tube heat exchanger and submerged coil heat exchanger.
The utility model solves the technical scheme that its technical problem adopted: a kind of acetate that has heater reclaims rectifying column; Comprise the heater that is provided with in tower body and the tower body; Wherein aforesaid heater is a steam heater of being located at top at the bottom of the tower; Steam heater is made up of at least one distribution of steam pipe, and an end of steam heater passes the tower body sidepiece and is provided with the steam inlet, and the distribution of steam pipe is provided with the opening of material in the corresponding tower.The utility model is through removing heater of the prior art; Introduce a pre-designed steam heater in the tower body middle and lower part and replace original heater; Steam gets into steam heater through the steam inlet; Steam directly contacts from the opening ejection of the steam heater material inner with reclaiming rectifying column and carries out heat exchange, matter exchange, promptly carries out hybrid direct heat transfer.
As the further design to the aforementioned techniques scheme: aforesaid steam heater is made up of cross two or four distribution of steam pipes, the bottom of every distribution of steam pipe evenly is provided with the corresponding material of opening.Promptly sidewall has been installed cross steam heater in the left and right sides of tower body, and the material of distribution of steam pipe is a stainless steel, and the pipe end of every distribution of steam pipe is fixed on tower body and gets on the outer wall.In rectifying column, be provided with liquid distribution trough above the steam heater, when producing, the noise that steam heater produced is very little, and the noise that sends than the reboiler of esterification column is little a lot.
The external diameter of aforesaid distribution of steam pipe is 159mm, and the width of opening is 50mm, and the distance between the adjacent apertures is 160mm.
Aforesaid steam heater is located on the position apart from 200mm at the bottom of the tower.
In sum; It is to replace original dividing wall type heat exchanger (shell-and-tube or submerged coil heat exchanger) with a steam heater that the acetate of the utility model reclaims the heater that is provided with in the rectifying column; Steam heater is made simple, and main material is stainless steel tube, welding rod etc., and cost is low.The use of steam heater can normally or better move by ensuring equipment, greatly reduces equipment cost again.In addition; Owing to reclaim rectifying column heat exchange method is changed to hybrid direct contact heat-exchanging by wall-type heat exchange; Satisfy the requirement of heat exchange fully, the low-grade flash steam that produces in the time of can rationally utilizing acetate system high-temperature condensation water to reclaim carries out heat supply, and can reduce equipment cost again; Can make the low-grade energy of by-product be fully used energy efficiency again.
Description of drawings
Fig. 1 is the structural representation of steam heater in reclaiming rectifying column of the utility model embodiment;
Fig. 2 is the structural representation of distribution of steam pipe;
Fig. 3 is that A-A among Fig. 2 is to profile.
The specific embodiment
Below in conjunction with accompanying drawing the embodiment of the utility model is done further to describe explanation.
Embodiment 1
The concrete scheme of present embodiment is: a kind of acetate that has heater reclaims rectifying column; Like Fig. 1, Fig. 2, shown in Figure 3; Comprise the heater 2 that is provided with in tower body 1 and the tower body; Heater is a steam heater of being located at top at the bottom of the tower, and steam heater is welded into cross by four distribution of steam pipes 3, and the bottom of every distribution of steam pipe evenly is provided with opening 5 corresponding materials.A distribution of steam Guan Yiduan in the steam heater passes the tower body sidepiece and is provided with steam inlet 4, and the bottom of every distribution of steam pipe all evenly is provided with many openings of material in the corresponding tower, and the pipe end of every distribution of steam pipe is fixed on tower body and gets on the outer wall.The utility model is through removing heater of the prior art; Introduce a pre-designed steam heater in the tower body middle and lower part and replace original heater; Steam gets into steam heater through the steam inlet; Steam directly contacts from the opening ejection of the steam heater material inner with reclaiming rectifying column and carries out heat exchange, matter exchange, promptly carries out hybrid direct heat transfer.
The external diameter of aforesaid distribution of steam pipe is 159mm, and the width of opening is 50mm, and the distance between the adjacent apertures is 160mm.
Except that the embodiment of above structure, every and solvent sampler the utility model structural similarity falls within the protection domain of the utility model too.

Claims (4)

1. an acetate that has heater reclaims rectifying column; Comprise the heater (2) that is provided with in tower body (1) and the tower body; It is characterized in that: described heater is a steam heater of being located at top at the bottom of the tower; Steam heater is made up of at least one distribution of steam pipe (3), and an end of steam heater passes the tower body sidepiece and is provided with steam inlet (4), and the distribution of steam pipe is provided with the opening (5) of material in the corresponding tower.
2. recovery rectifying column according to claim 1 is characterized in that: described steam heater is made up of cross two or four distribution of steam pipes, the bottom of every distribution of steam pipe evenly is provided with the corresponding material of opening.
3. recovery rectifying column according to claim 2 is characterized in that: the external diameter of described distribution of steam pipe is 159mm, and the width of opening is 50mm, and the distance between the adjacent apertures is 160mm.
4. recovery rectifying column according to claim 3 is characterized in that: described steam heater is located on the position apart from 200mm at the bottom of the tower.
CN201120250913U 2011-07-16 2011-07-16 Acetate recovery distillation column with heater Expired - Fee Related CN202128934U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201120250913U CN202128934U (en) 2011-07-16 2011-07-16 Acetate recovery distillation column with heater

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201120250913U CN202128934U (en) 2011-07-16 2011-07-16 Acetate recovery distillation column with heater

Publications (1)

Publication Number Publication Date
CN202128934U true CN202128934U (en) 2012-02-01

Family

ID=45517720

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201120250913U Expired - Fee Related CN202128934U (en) 2011-07-16 2011-07-16 Acetate recovery distillation column with heater

Country Status (1)

Country Link
CN (1) CN202128934U (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105417605A (en) * 2015-12-29 2016-03-23 北京华福工程有限公司 Coal chemical industry wastewater steam stripping, deacidifying, and deaminating tower directly heated by steam

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105417605A (en) * 2015-12-29 2016-03-23 北京华福工程有限公司 Coal chemical industry wastewater steam stripping, deacidifying, and deaminating tower directly heated by steam

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Legal Events

Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20120201

Termination date: 20180716

CF01 Termination of patent right due to non-payment of annual fee