CN201981022U - Stannous chloride solution dynamic crystallizing device - Google Patents
Stannous chloride solution dynamic crystallizing device Download PDFInfo
- Publication number
- CN201981022U CN201981022U CN2011200939168U CN201120093916U CN201981022U CN 201981022 U CN201981022 U CN 201981022U CN 2011200939168 U CN2011200939168 U CN 2011200939168U CN 201120093916 U CN201120093916 U CN 201120093916U CN 201981022 U CN201981022 U CN 201981022U
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- crystallizer
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- stannous chloride
- chloride solution
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Abstract
The utility model relates to a solution crystallizing device, in particular to a stannous chloride solution dynamic crystallizing device, which comprises a rotary crystallizer driven by a rotary crystallizer driving system and a refrigerating system, wherein the refrigerating system comprises a refrigerating machine unit, a cooling tower and a buffer tank which are matched with the refrigerating machine unit. The rotary crystallizer is a double-cone rotary device provided with a clamping sleeve, and the cooling tower is communicated with the refrigerating machine unit respectively through a cooling-tower water inlet pipeline and a cooling-tower water outlet pipeline. The refrigerating machine unit is communicated with the buffer tank respectively through a machine-unit water outlet pipeline and a machine-unit water return pipeline, and the buffer tank is communicated with the clamping sleeve of the rotary crystallizer through a buffer-tank water outlet pipeline and a buffer-tank water return pipeline. The stannous chloride solution dynamic crystallizing device changes the an existing static crystallizing manner of stannous chloride solution into a dynamic crystallizing manner, has the advantages of being high in production efficiency and crystallizing rate, enabling grain diameters of stannous chloride crystals to be even, simplifying production process of the crystals, and the like.
Description
Technical field
The utility model relates to a kind of solution crystallization device, particularly a kind of stannous chloride solution dynamic crystallization device.
Background technology
All the time, in the crystallisation by cooling operation of preparation tin protochloride process, all be to adopt static crystallization mode, promptly be stannous chloride solution to be packed into put into freezer behind the plastic tank, rely on freezer that stannous chloride solution is carried out crystallisation by cooling.Stationary crystallization needs lower Tc (5～10 ℃), long crystallization time (48h), and the product hardness that crystallizes out is big, and reduction ratio is difficulty, and product granularity is inhomogeneous, and outward appearance is bad.Simultaneously the heat transfer efficiency of freezer is low, and it is big to take up room, and hydrochloric acid is very big to the corrosion on freezer equipment and ground, causes that production efficiency is low, cost is high.
Summary of the invention
The technical problems to be solved in the utility model is: provide a kind of stationary crystallization that stannous chloride solution is original to change dynamic crystallization mode, production efficiency height into, the percent crystallization in massecuite height, the all even stannous chloride solution dynamic crystallization device of having simplified the crystallization Production Flow Chart of tin protochloride crystal particle diameter is to overcome above-mentioned the deficiencies in the prior art part.
The technical scheme that solves the problems of the technologies described above is: a kind of stannous chloride solution dynamic crystallization device, comprise the revolution crystallizer and the refrigeration system that drive by revolution crystallizer drive system, refrigeration system comprises unit cooler, with supporting cooling tower and the buffer tank of unit cooler, described revolution crystallizer is the double cone-shaped equipment applies that has chuck, described cooling tower is communicated with unit cooler by cooling tower inlet channel and cooling tower outlet conduit respectively, unit cooler is communicated with buffer tank by unit outlet conduit and unit water return pipeline respectively, and buffer tank is communicated with the chuck of revolution crystallizer by buffer tank outlet conduit and buffer tank water return pipeline.
The rotating speed of described revolution crystallizer is 2～5r/min.
Described revolution crystallizer inwall is that the salt tolerant acid corrosion material of liner enamel, poly-tetrafluoro or PE is made, and revolution crystallizer outside surface carries out the glass reinforced plastic rotproofing, and revolution crystallizer discharge port also adds lining fluorine dish valve.
Described revolution crystallizer adopts the glass lining double conic rotary drying machine.
The utility model adopts double cone-shaped equipment applies as the revolution crystallizer, promptly be to adopt the dynamic crystallization technology, the tin protochloride concentrated solution of an amount of volume is joined in the revolution crystallizer, start revolution crystallizer and unit cooler, the control stannous chloride solution temperature and the refrigerant temperature difference that is arranged in revolution crystallizer chuck, the rotating speed of crystallizer is controlled in 2～5r/min scope, drop to certain temperature up to solution temperature, crystallization this moment is finished, close refrigeration system, the slurry crystalline substance is put in the whizzer and dries, and promptly gets product through packing again.Revolution crystallizer inwall is salt tolerant acid corrosions such as liner enamel, poly-tetrafluoro, PE, and heat conductivility is material preferably, has accelerated the rate of heat exchange of stannous chloride solution and refrigerant.
The utility model changes original stationary crystallization into dynamic crystallization, also has following beneficial effect:
1, crystalline rate improves greatly, and crystallization time obviously shortens, and it is 48 hours that stationary crystallization needs crystallization time, and the dynamic rotation crystallization only needs 20 hours, and production efficiency obviously raises.
2, the percent crystallization in massecuite of dynamic crystallization further improves.The percent crystallization in massecuite of stationary crystallization method is generally about 55%, and dynamic rotation crystallization process percent crystallization in massecuite on average can reach more than 75%, and this helps further improving the product direct yield.
3, the tin protochloride crystal particle diameter of dynamic crystallization output is even, and outward appearance is better; The product cut size of stationary crystallization output is inhomogeneous, and macrobead is many, and outward appearance is bad.
4, dynamic crystallization has been simplified Production Flow Chart, cancelled extensive works such as tin protochloride concentrated solution warehouse-in, outbound, crystallization fragmentation, so dynamic crystallization technology is lower than stationary crystallization technology labour intensity.
Below, the technical characterictic to the stannous chloride solution dynamic crystallization device of the utility model is further described in conjunction with the accompanying drawings and embodiments.
Description of drawings
The stannous chloride solution dynamic crystallization apparatus structure synoptic diagram of Fig. 1: the utility model embodiment one.
Among the figure: the 1-cooling tower, 11-cooling tower inlet channel, 12-cooling tower outlet conduit, 121-cooling-water pump, 13-moisturizing pipeline, the 2-unit cooler, 21-unit outlet conduit, 211-vent valve, the 212-water discharge valve, 22-unit water return pipeline, 221-freeze cycle water pump, 3-buffer tank, 31-buffer tank outlet conduit, the 311-cooling water circulating pump, 312-entrance of cooling water PP ball valve, 32-buffer tank water return pipeline, 321-cooling water outlet PP ball valve, 4-turns round crystallizer, 41-lining fluorine dish valve, 5-revolution crystallizer drive system.
Arrow is represented water (flow) direction among the figure.
Embodiment
Embodiment one: a kind of stannous chloride solution dynamic crystallization device (referring to Fig. 1), this device comprises revolution crystallizer 4 and the refrigeration system that is driven by revolution crystallizer drive system 5, refrigeration system comprise unit cooler 2, with supporting cooling tower 1 and the buffer tank 3 of unit cooler, described revolution crystallizer 4 is the glass lining double conic rotary drying machines that have chuck.Described cooling tower 1 is communicated with unit cooler 2 by cooling tower inlet channel 11 and cooling tower outlet conduit 12 respectively, unit cooler 2 is communicated with buffer tank 3 by unit outlet conduit 21 and unit water return pipeline 22 respectively, and buffer tank 3 is communicated with the chuck of revolution crystallizer 4 by buffer tank outlet conduit 31 and buffer tank water return pipeline 32.Revolution crystallizer 4 inwalls are that salt tolerant acid corrosion materials such as liner enamel, poly-tetrafluoro or PE are made, revolution crystallizer outside surface carries out the glass reinforced plastic rotproofing, revolution crystallizer discharge port also adds lining fluorine dish valve 41, and the rotating speed of described revolution crystallizer is 2～5r/min.
The supporting parts such as cooling-water pump, freeze cycle water pump, valve and thermometer that are equipped with on the corresponding pipeline of the present utility model, its concrete structure and mounting means, installation site belong to known technology, repeat no more herein.
Claims (4)
1. stannous chloride solution dynamic crystallization device, it is characterized in that: this device comprises revolution crystallizer (4) and the refrigeration system that is driven by revolution crystallizer drive system (5), refrigeration system comprises unit cooler (2), with supporting cooling tower (1) and the buffer tank (3) of unit cooler, described revolution crystallizer (4) is the double cone-shaped equipment applies that has chuck, described cooling tower (1) is communicated with unit cooler (2) by cooling tower inlet channel (11) and cooling tower outlet conduit (12) respectively, unit cooler (2) is communicated with buffer tank (3) by unit outlet conduit (21) and unit water return pipeline (22) respectively, and buffer tank (3) is communicated with the chuck of revolution crystallizer (4) by buffer tank outlet conduit (31) and buffer tank water return pipeline (32).
2. stannous chloride solution dynamic crystallization device according to claim 1 is characterized in that: the rotating speed of described revolution crystallizer is 2～5r/min.
3. stannous chloride solution dynamic crystallization device according to claim 1 and 2, it is characterized in that: described revolution crystallizer (4) inwall is that the salt tolerant acid corrosion material of liner enamel, poly-tetrafluoro or PE is made, revolution crystallizer outside surface carries out the glass reinforced plastic rotproofing, and revolution crystallizer discharge port also adds lining fluorine dish valve (41).
4. stannous chloride solution dynamic crystallization device according to claim 3 is characterized in that: described revolution crystallizer adopts the glass lining double conic rotary drying machine.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011200939168U CN201981022U (en) | 2011-03-28 | 2011-04-01 | Stannous chloride solution dynamic crystallizing device |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201120084577 | 2011-03-28 | ||
| CN201120084577.7 | 2011-03-28 | ||
| CN2011200939168U CN201981022U (en) | 2011-03-28 | 2011-04-01 | Stannous chloride solution dynamic crystallizing device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN201981022U true CN201981022U (en) | 2011-09-21 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2011200939168U Expired - Lifetime CN201981022U (en) | 2011-03-28 | 2011-04-01 | Stannous chloride solution dynamic crystallizing device |
Country Status (1)
| Country | Link |
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| CN (1) | CN201981022U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102120609A (en) * | 2011-03-28 | 2011-07-13 | 柳州百韧特先进材料有限公司 | Dynamic crystallization technological method and device for stannous chloride solution |
| CN113845506A (en) * | 2021-10-18 | 2021-12-28 | 惠州市宙邦化工有限公司 | Dynamic crystallization purification method of ethylene carbonate |
-
2011
- 2011-04-01 CN CN2011200939168U patent/CN201981022U/en not_active Expired - Lifetime
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102120609A (en) * | 2011-03-28 | 2011-07-13 | 柳州百韧特先进材料有限公司 | Dynamic crystallization technological method and device for stannous chloride solution |
| CN102120609B (en) * | 2011-03-28 | 2012-11-07 | 柳州百韧特先进材料有限公司 | Dynamic crystallization technological method and device for stannous chloride solution |
| CN113845506A (en) * | 2021-10-18 | 2021-12-28 | 惠州市宙邦化工有限公司 | Dynamic crystallization purification method of ethylene carbonate |
| US11958820B2 (en) | 2021-10-18 | 2024-04-16 | Shenzhen Capchem Technology Co., Ltd. | Method for purifying ethylene carbonate through dynamic crystallization |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| AV01 | Patent right actively abandoned |
Granted publication date: 20110921 Effective date of abandoning: 20130227 |
|
| RGAV | Abandon patent right to avoid regrant |