CN201609594U - Normal-temperature return-flow vacuum spray concentrating tank - Google Patents
Normal-temperature return-flow vacuum spray concentrating tank Download PDFInfo
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- CN201609594U CN201609594U CN2010201206579U CN201020120657U CN201609594U CN 201609594 U CN201609594 U CN 201609594U CN 2010201206579 U CN2010201206579 U CN 2010201206579U CN 201020120657 U CN201020120657 U CN 201020120657U CN 201609594 U CN201609594 U CN 201609594U
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Abstract
The utility model discloses a normal-temperature return-flow vacuum spray concentrating tank which comprises a tank top, a tank body and a tank bottom, wherein the tank top is provided with a vacuum pumping hole for connecting a condenser with a vacuum pump, the upper part of the tank body is provided with a circulating sprayer communicated with a liquid inlet, the middle part of the tank body is provided with a tube type heat exchanger, the tank bottom is an interlayer material tank and is provided with a temperature adjusting device which is provided with a flange hole, the flange hole is used as a hot water, steam or refrigerating fluid inlet and communicated with an interlayer, and the tank bottom is provided with a material pumping hole sending feed liquid which is not gasified back to the sprayer. The normal-temperature return-flow vacuum spray concentrating tank can ensure materials to be condensed at normal temperature and intermediate temperature, can adapt to biological pharmacy and enzymatic preparation, peptide production, biotin production and biologically active substances production, and also is good equipment for purifying low-boiling chemical reagent; and compared with the prior art, the normal-temperature return-flow vacuum spray concentrating tank greatly improves production efficiency, reduces production cost and has a reliable grasp of product quality.
Description
Technical field
The utility model relates to a kind of concentration tank, particularly material is carried out low temperature or the concentrated concentration tank of normal temperature.
Background technology
Along with the biotechnology high speed development, in the production application of enzyme, biotin and activated protein peptide more and more widely, and these biologic products can only carry out concentrate drying at normal temperature or the middle temperature below 80 ℃.The concentrate drying method of using mainly contains frozen drying method, concentrate drying method, vacuum concentrate drying method, spraying concentrate drying method, boiling decompression concentrate drying method at present.Though these methods are each has something to recommend him, its common shortcoming is that production efficiency is low, as the most frequently used freeze-drying from this process of high concentration that reaches of low concentration time-consumingly take a lot of work, energy consumption is big, the cycle is long, cost is high.Vacuum concentration method and for example, temperature is low then can not to be concentrated, and also can cause the hydrolysis sex change of desired biologic product; The temperature height then causes desired biologic product because of the sex change of overtemperature inactivation.In prior art, also there is not normal temperature reverse-flow type vacuum spraying concentration tank.
The utility model content
The purpose of this utility model is to overcome the shortcoming of prior art, provides a kind of effect height, quality to have and reliably can be applied to bio-pharmaceuticals such as enzyme, biotin and activated protein peptide, also can be applied to the to purify normal temperature reverse-flow type vacuum spraying concentration tank of some low boiling chemical reagent.
The vacuum spraying concentration tank comprises tank deck, tank body, jar end, on tank deck, be provided with the vacuum pumping opening that connects condenser and vavuum pump, the circulation sprayer that is communicated with inlet is housed on tank body top, tubular heat exchanger is housed at the tank body middle part, the described jar of end is the interlayer batch can, on at the bottom of the jar, be provided with temperature-adjusting device, described temperature-adjusting device is to be provided with the flange hole that advances hot water or steam or freezing liquid that is communicated with interlayer, and what the feed liquid that not gasification is housed at the bottom of the jar sent back to sprayer takes out material mouthful.
The described jar end, be provided with the pressure reducing air inlet hole drain hole of holding concurrently.
1-20 shower nozzle is housed on the described sprayer.
Described tank body is provided with digital display type thermometer and peep hole.
Described tank body bottom is provided with delivery port or air inlet.
Described tank deck is or/and tank body is provided with access hole.
The lighting mouth is housed in the described tank body.
The utility model can guarantee that material concentrates under concentrated under normal temperature, the middle temperature even low temperature, can be adapted to the production of bio-pharmaceuticals and enzyme preparation production, protein peptides production, biotin production and bioactivator, the active ingredient that can prevent feed liquid destroyed and inactivation or hydrolysis sex change; Also be the good equipment of some low boiling chemical reagent of purification; Its effect can improve more than several times and even ten times compared with the prior art, has improved production efficiency greatly, has reduced production cost, and product quality is had reliable assurance.
Description of drawings
Fig. 1 is a structural representation of the present utility model.
The specific embodiment
Below in conjunction with the drawings and specific embodiments the utility model is described further.
Reverse-flow type vacuum spraying concentration tank is made up of tank deck I, tank body II, a jar end III, be provided with the vacuum pumping opening 1 that connects condenser and vavuum pump and access hole 2, vacuum meter interface 3 at tank deck, the tank body II is divided into upper, middle, and lower part, the sprayer of being made up of a plurality of shower nozzles 5 that is communicated with charging aperture 4 is housed on top, in two sides peep hole 15 is housed respectively, tubular heat exchanger 7 is housed at the middle part, carries out heat exchange by cold and hot exchange pipe 6 and 8; The heat-exchange tube of present embodiment is a steam, and cold exchange pipe is a freezing liquid, and the spray film contact heat exchanger that sprayer 5 is sprayed out produces the temperature difference, and operative liquid is become gaseous state, extracts out by vacuum pumping opening 1 vacuum.The tank body bottom is provided with delivery port or air inlet 10, other is provided with liquid level mouth and peep hole 15, so that observe liquid level and the concentrated situation of material, also one lighting mouth 16 is housed on peep hole 15 opposites, digital display type thermometer 14 is housed in the following side, can accurately grasp temperature of charge, other is provided with the manhole 9 of a diameter 400mm; Jar end III is an interlayer, and interlayer is heated to material temperature required by the flange hole 13 that advances hot water or steam or freezing liquid or cools to temperature requiredly, can guarantee that thing liquid reaches best temperature difference effect when being sprayed to exchanger surfaces.Be provided with the pressure reducing air inlet hole drain hole 12 of holding concurrently at the bottom of the jar.After vacuumizing, can open valve more slightly,, make aqueous vapor by the best extraction of vavuum pump even make depressed gas enter the feed liquid boiling.Other be equipped with connect delivery pump take out material hole 11, the liquid feed liquid that does not gasify can be transmitted back to charging aperture 4 and spray once more by sprayer 5 again, carry out once more concentrated, so repeatedly, very to reaching concentrated purpose.
Claims (7)
1. normal temperature reverse-flow type vacuum spraying concentration tank, comprise tank deck, tank body, jar end, on tank deck, be provided with the vacuum pumping opening that connects condenser and vavuum pump, the circulation sprayer that is communicated with inlet is housed on tank body top, tubular heat exchanger is housed at the tank body middle part, the described jar of end is the interlayer batch can, on at the bottom of the jar, be provided with temperature-adjusting device, described temperature-adjusting device is to be provided with the flange hole that advances hot water or steam or freezing liquid that is communicated with interlayer, and what the feed liquid that not gasification is housed at the bottom of the jar sent back to sprayer takes out material mouthful.
2. normal temperature reverse-flow type vacuum spraying concentration tank according to claim 1 is characterized in that, the described jar end is provided with the pressure reducing air inlet hole drain hole of holding concurrently.
3. normal temperature reverse-flow type vacuum spraying concentration tank according to claim 1 is characterized in that, 1-20 shower nozzle is housed on the described sprayer.
4. normal temperature reverse-flow type vacuum spraying concentration tank according to claim 1 is characterized in that described tank body is provided with digital display type thermometer and peep hole.
5. normal temperature reverse-flow type vacuum spraying concentration tank according to claim 1 is characterized in that described tank body bottom is provided with delivery port or air inlet.
6. normal temperature reverse-flow type vacuum spraying concentration tank according to claim 1 is characterized in that described tank deck is or/and tank body is provided with access hole.
7. the described normal temperature reverse-flow type of claim 1 vacuum spraying concentration tank is characterized in that, the lighting mouth is housed in the described tank body.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010201206579U CN201609594U (en) | 2010-03-01 | 2010-03-01 | Normal-temperature return-flow vacuum spray concentrating tank |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010201206579U CN201609594U (en) | 2010-03-01 | 2010-03-01 | Normal-temperature return-flow vacuum spray concentrating tank |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN201609594U true CN201609594U (en) | 2010-10-20 |
Family
ID=42960225
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2010201206579U Expired - Fee Related CN201609594U (en) | 2010-03-01 | 2010-03-01 | Normal-temperature return-flow vacuum spray concentrating tank |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN201609594U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106807101A (en) * | 2015-11-30 | 2017-06-09 | 衡阳春天医药化工设备有限公司 | A kind of deep red membrane concentrator |
| CN112023425A (en) * | 2020-08-07 | 2020-12-04 | 成都市三跃机械设备有限公司 | Honey enrichment facility |
-
2010
- 2010-03-01 CN CN2010201206579U patent/CN201609594U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106807101A (en) * | 2015-11-30 | 2017-06-09 | 衡阳春天医药化工设备有限公司 | A kind of deep red membrane concentrator |
| CN112023425A (en) * | 2020-08-07 | 2020-12-04 | 成都市三跃机械设备有限公司 | Honey enrichment facility |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| ASS | Succession or assignment of patent right |
Owner name: HUNAN HUINONG TECHNOLOGY CO., LTD. Free format text: FORMER OWNER: HUNAN BENZHI BIOTECHNOLOGY CO., LTD. Effective date: 20140617 |
|
| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20140617 Address after: 410005 No. 80 middle Huang Xing Road, Furong district, Hunan, Changsha Patentee after: HUNAN HUINONG TECHNOLOGY CO., LTD. Address before: 410005 No. 80 middle Huang Xing Road, Hunan, Changsha Patentee before: Hunan Benzhi Biotechnology Co., Ltd. |
|
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20101020 Termination date: 20190301 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |