CN201454559U - Distillation and purification device for solvents - Google Patents

Distillation and purification device for solvents Download PDF

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Publication number
CN201454559U
CN201454559U CN2009200877959U CN200920087795U CN201454559U CN 201454559 U CN201454559 U CN 201454559U CN 2009200877959 U CN2009200877959 U CN 2009200877959U CN 200920087795 U CN200920087795 U CN 200920087795U CN 201454559 U CN201454559 U CN 201454559U
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CN
China
Prior art keywords
distillation
outlet
steam
receiving flask
liquid receiving
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN2009200877959U
Other languages
Chinese (zh)
Inventor
何长华
钟贤贵
何先兵
何长云
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
JINGMEN YUKUI CHEMICAL CO Ltd
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JINGMEN YUKUI CHEMICAL CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by JINGMEN YUKUI CHEMICAL CO Ltd filed Critical JINGMEN YUKUI CHEMICAL CO Ltd
Priority to CN2009200877959U priority Critical patent/CN201454559U/en
Application granted granted Critical
Publication of CN201454559U publication Critical patent/CN201454559U/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

The utility model relates to a distillation and purification device for solvents. A distillation flask (2) is placed on an electric hot plate of an electric heater (1); the steam outlet of the distillation flask (2) is communicated with one end of a distillation tube (3); the other end of the distillation tube (3) extends into the middle part of a condensate collecting bottle (4); two to three steam outlets (3-1) are formed at the upper end of the distillation tube (3); the two to three steam outlets (3-1) of the distillation tube (3) are communicated with the condensate collecting bottle (4); the steam outlet of the condensate collecting bottle (4) is communicated with a condensation tube (5); a liquid outlet (6-1) with a valve is formed at the bottom of the condensate collecting bottle (4); and a water cooling tube (6) is sleeved outside the condensate collecting bottle (4). The distillation and purification device has the advantages of simple structure, low manufacturing cost, small equipment investment and good distillation and purification effects.

Description

A kind of solvent distillation purifying plant
Technical field
The utility model relates to the distilling apparatus field.
Background technology
The complex structure that existing solvent distillation purifying plant has, the manufacturing cost height, equipment investment is big, and the distillation refining effect that has is good inadequately.
The utility model content
The purpose of this utility model is exactly at the above-mentioned deficiency of existing solvent distillation purifying plant, and a kind of good solvent distillation purifying plant of refining effect that distills is provided.
The utility model is made up of electric heater, cucurbit, distillation cascade, condensate liquid receiving flask, condenser pipe and water composite cooling pipe; Cucurbit is placed on the electric hot plate of electric heater, the steam (vapor) outlet of cucurbit communicates with an end of distillation cascade, the other end of distillation cascade stretches to condensate liquid receiving flask middle part, be provided with 2-3 steam (vapor) outlet in the upper end of distillation cascade, the 2-3 of a distillation cascade steam (vapor) outlet communicates with the condensate liquid receiving flask, the steam (vapor) outlet of condensate liquid receiving flask communicates with condenser pipe, and the bottom of condensate liquid receiving flask is provided with the liquid outlet of band valve, and water composite cooling pipe is enclosed within outside the condensate liquid receiving flask.
The utility model has the advantages that: it is simple in structure, low cost of manufacture, and equipment investment is little, and the distillation refining effect is good.
Description of drawings
Accompanying drawing 1 is the utility model structural representation.
The specific embodiment
As shown in Figure 1, cucurbit 2 is placed on the electric hot plate of electric heater 1 (using temperature adjustable electrically heated device), the steam (vapor) outlet of cucurbit 2 communicates with an end of distillation cascade 3, the other end of distillation cascade 3 stretches to condensate liquid receiving flask 4 middle parts, be provided with 2-3 steam (vapor) outlet 3-1 in the upper end of distillation cascade 3, the 2-3 of distillation cascade 3 steam (vapor) outlet 3-1 communicates with condensate liquid receiving flask 4, the steam (vapor) outlet of condensate liquid receiving flask 4 communicates with condenser pipe 5, the bottom of condensate liquid receiving flask 4 is provided with the liquid outlet 6-1 of band valve, and water composite cooling pipe 6 is enclosed within outside the condensate liquid receiving flask 4.
Working method: open electric heater, regulate heating-up temperature extremely by the boiling point of purification solvent.By the vaporization of in distillation cascade 3, being heated of purification solvent, 2-3 steam (vapor) outlet 3-1 through distillation cascade enters condensate liquid receiving flask 4, become liquid after entering condenser pipe 5 cooling again, be back in the condensate liquid receiving flask 4, the band valve liquid outlet 6-1 through the bottom of condensate liquid receiving flask 4 flows out.

Claims (1)

1. solvent distillation purifying plant is characterized in that it is made up of electric heater (1), cucurbit (2), distillation cascade (3), condensate liquid receiving flask (4), condenser pipe (5) and water composite cooling pipe (6); Cucurbit (2) is placed on the electric hot plate of electric heater (1), the steam (vapor) outlet of cucurbit (2) communicates with an end of distillation cascade (3), the other end of distillation cascade (3) stretches to condensate liquid receiving flask (4) middle part, be provided with 2-3 steam (vapor) outlet (3-1) in the upper end of distillation cascade (3), 2-3 the steam (vapor) outlet (3-1) of distillation cascade (3) communicates with condensate liquid receiving flask (4), the steam (vapor) outlet of condensate liquid receiving flask (4) communicates with condenser pipe (5), the bottom of condensate liquid receiving flask (4) is provided with the liquid outlet (6-1) of band valve, and water composite cooling pipe (6) is enclosed within outside the condensate liquid receiving flask (4).
CN2009200877959U 2009-08-01 2009-08-01 Distillation and purification device for solvents Expired - Fee Related CN201454559U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2009200877959U CN201454559U (en) 2009-08-01 2009-08-01 Distillation and purification device for solvents

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2009200877959U CN201454559U (en) 2009-08-01 2009-08-01 Distillation and purification device for solvents

Publications (1)

Publication Number Publication Date
CN201454559U true CN201454559U (en) 2010-05-12

Family

ID=42381906

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2009200877959U Expired - Fee Related CN201454559U (en) 2009-08-01 2009-08-01 Distillation and purification device for solvents

Country Status (1)

Country Link
CN (1) CN201454559U (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102553293A (en) * 2012-01-20 2012-07-11 东北林业大学 Device for extracting betulinol
CN103331029A (en) * 2013-07-10 2013-10-02 湖州鑫鼎半导体材料有限公司 Distiller

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102553293A (en) * 2012-01-20 2012-07-11 东北林业大学 Device for extracting betulinol
CN103331029A (en) * 2013-07-10 2013-10-02 湖州鑫鼎半导体材料有限公司 Distiller
CN103331029B (en) * 2013-07-10 2015-06-17 湖州鑫鼎半导体材料有限公司 Distiller

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Legal Events

Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
C17 Cessation of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20100512

Termination date: 20120801