CN201357070Y - Spherical cobaltosic oxide reaction kettle - Google Patents
Spherical cobaltosic oxide reaction kettle Download PDFInfo
- Publication number
- CN201357070Y CN201357070Y CNU2009201135814U CN200920113581U CN201357070Y CN 201357070 Y CN201357070 Y CN 201357070Y CN U2009201135814 U CNU2009201135814 U CN U2009201135814U CN 200920113581 U CN200920113581 U CN 200920113581U CN 201357070 Y CN201357070 Y CN 201357070Y
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- kettle
- discharging opening
- cobaltosic oxide
- reaction kettle
- spherical cobaltosic
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Abstract
The utility model relates to a spherical cobaltosic oxide reaction kettle which comprises a driving device, a stirring shaft, an exhaust pipe, a kettle cover, a charging pipe, a discharging opening, an immersion type coiler heat exchanger, a temperature sensor, a pressure sensor, a stirring blade and a kettle body. The stirring shaft is connected with the stirring blade after stretching into the end part in the kettle body. The important points of the design are as follows: the discharging opening is arranged at the upper segment of the kettle body; the distance between the discharging opening and a kettle opening is within 20 to 40cm; and the discharging opening is connected with a pipeline so as to convey reacted liquid materials in the kettle body. The spherical cobaltosic oxide reaction kettle has the characteristics that the heating of the reacted mixed materials is uniform, the quality is stable, the temperature is easy to be controlled, and the production efficiency and product quality are greatly improved. The spherical cobaltosic oxide reaction kettle is particularly suitable for preparing spherical cobaltosic oxide, and is easy to be applied to the chemical reaction kettle of the same kind in a modified manner.
Description
Technical field
The utility model relates to a kind of spherical cobaltic-cobaltous oxide reactor.
Background technology
Reactor is one of container of chemical industry, medical production process, and material generally adopts carbon manganese steel, stainless steel, zirconium, nickel-base alloy and other composite.Inorganic chemical industry is produced and is adopted the reactor of synthesizing spherical cobaltosic oxide to comprise kettle, agitator, feed pipe, discharging opening usually, motor, heat exchanger, these reactor feed pipes are up, discharging opening is in bottom, and this phenomenon easily causes the reaction time longer, reacts abundant inadequately.Patent No. ZL200720125671.6 as the Chinese patent literature publication, Granted publication CN201117715Y, September 17 2008 Granted publication day, the utility model title " is used to prepare the stirring-type reactor that lithium ion battery coats negative material ", the motor of this reactor, device for discharging drive kettle cover, heating furnace moves up and down, make reacting furnace-e/or break away from heating furnace, and the rotation discharging.But its discharge way is comparatively complicated, and operating efficiency is lower.
Summary of the invention
For overcoming the deficiency of above-mentioned existence, the utility model purpose is a kind of spherical cobaltic-cobaltous oxide reactor that provides to this area, and it is long to make it can solve the existing like product reaction time, reacts abundant inadequately, and discharge method is the complicated technology problem comparatively.The purpose of this utility model is achieved by the following technical solution.
A kind of spherical cobaltic-cobaltous oxide reactor, this reactor comprises motor driver, shaft, blast pipe, kettle cover, feed pipe, paddle, kettle, discharge gate, kettle cover and kettle sealing, kettle cover is provided with shaft, blast pipe, feed pipe, submerged coil heat exchanger, thermometer boss, be provided with temperature sensor in the thermometer boss, autoclave body bottom is provided with discharge gate, and the outer end of the kettle cover of shaft is provided with motor driver, and the other end of shaft in kettle is provided with paddle.Its design main points are that the epimere of described kettle is provided with discharging opening, and the distance of this discharging opening and still mouth is 20～40cm; Discharging opening is connected with pipeline, carries the liquid material after reaction is finished in the kettle.
The import of described feed pipe places kettle cover, and the adjacent paddle of the outlet of feed pipe by the even stirring of paddle, reacts the raw material and the solution that enter kettle fully, improves the efficient of reactant reaction.
The adjacent paddle of temperature sensor in the described thermometer boss by the feedback of temperature sensor, is observed the temperature of kettle internal reaction process immediately, makes course of reaction relatively stable.
The utility model is in the preparation feedback process, and the heating of reaction batch mixing is comparatively even, quality is comparatively stable, and temperature is easy to control, and production efficiency and product quality all are greatly improved.Be particularly useful for producing of spherical cobaltic-cobaltous oxide, and be easy to use in similar chemical reaction still transformation.
Description of drawings
Fig. 1 is a structural representation of the present utility model.
Above figure number and title: 1, drive unit, 2, shaft, 3, blast pipe, 4, kettle cover, 5, feed pipe, 6, discharging opening, 7, submerged coil heat exchanger, 8, thermometer boss, 9, temperature sensor, 10, paddle, 11, discharge gate, 12, kettle, 13, baffle plate, 14, pressure sensor, 15, the pressure gauge sleeve pipe.
The specific embodiment
Embodiment is example to use.The spherical cobaltic-cobaltous oxide compound is sent into by feed pipe 5, drive unit 1 drives paddle 10 rotations of shaft 2, place the bottom of kettle 12 because of paddle, and stop by baffle plate 13, make the formation surfing of material in rotation of reaction, stir the spherical cobaltic-cobaltous oxide compound like this in the kettle and just stir relatively fully.The temperature sensor 9 of the thermometer boss 8 that inserts is adjacent to paddle, and the test reaction temperature is comparatively accurate.The blast pipe 3 that kettle cover 4 is provided with, plan is tested the higher gas that reactant produced by the pressure sensor in the pressure gauge sleeve pipe 15 14 and is discharged, heating or cool but medium are to regulate spherical cobaltic-cobaltous oxide compound in the kettle by submerged coil heat exchanger 7, and the discharging opening 6 of kettle will will react the spherical cobaltic-cobaltous oxide compound discharge of being finished by the compressed air that injects reactor.The discharge gate 11 of autoclave body bottom is to lay for the cleaning of kettle.
Therefore the utility model, has improved production efficiency by the mode charging and the discharging of " enterprising, upside goes out ", and quality is comparatively stable.
Claims (2)
1, a kind of spherical cobaltic-cobaltous oxide reactor, this reactor comprises drive unit (1), shaft (2), blast pipe (3), kettle cover (4), feed pipe (5), discharging opening (6), submerged coil heat exchanger (7), temperature sensor (9), paddle (10), discharge gate (11), kettle (12), pressure sensor (14), kettle cover and kettle sealing, kettle cover is provided with blast pipe, feed pipe, submerged coil heat exchanger, thermometer boss (8), be provided with temperature sensor in the thermometer boss, autoclave body bottom is provided with discharge gate, drive unit on the kettle cover connects shaft, and the end that shaft stretches in the kettle connects paddle; The epimere that it is characterized in that described kettle (12) is provided with discharging opening (6), and the distance of this discharging opening and still mouth is 20～40cm; The import of described feed pipe (5) places kettle cover (4), the adjacent paddle of the outlet of feed pipe (10).
2, spherical cobaltic-cobaltous oxide reactor as claimed in claim 1 is characterized in that the adjacent paddle of temperature sensor (9) (10) in the described thermometer boss (8).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNU2009201135814U CN201357070Y (en) | 2009-02-04 | 2009-02-04 | Spherical cobaltosic oxide reaction kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNU2009201135814U CN201357070Y (en) | 2009-02-04 | 2009-02-04 | Spherical cobaltosic oxide reaction kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN201357070Y true CN201357070Y (en) | 2009-12-09 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNU2009201135814U Expired - Lifetime CN201357070Y (en) | 2009-02-04 | 2009-02-04 | Spherical cobaltosic oxide reaction kettle |
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| CN (1) | CN201357070Y (en) |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103145200A (en) * | 2013-03-25 | 2013-06-12 | 安徽亚兰德新能源材料股份有限公司 | Method for synthesizing spherical cobaltosic oxide through mixing type oxidation |
| WO2015027841A1 (en) * | 2013-08-27 | 2015-03-05 | 江苏华东锂电技术研究院有限公司 | Method for preparing spherical cobalt oxyhydroxide |
| CN104998596A (en) * | 2015-07-13 | 2015-10-28 | 江苏凯力克钴业股份有限公司 | Production device for preparing pure-phase cobalt tetraoxide through liquid-phase synthesis |
| CN105312018A (en) * | 2014-07-31 | 2016-02-10 | 沣田宝农业科技有限公司 | Fully-intelligent variable-temperature chelating reactor |
| CN106149045A (en) * | 2016-08-25 | 2016-11-23 | 中国有色桂林矿产地质研究院有限公司 | A kind of spherical high-pressure reactor for hydrothermal method crystal growth |
| CN106524782A (en) * | 2016-12-30 | 2017-03-22 | 广东申菱环境***股份有限公司 | Immersive liquid-cooled module heat exchanger and manufacturing method thereof |
| CN106622074A (en) * | 2016-12-05 | 2017-05-10 | 安佐化学有限公司 | Weighing-supportive reaction kettle device for preparing acrylate adhesive |
| CN106622073A (en) * | 2016-12-05 | 2017-05-10 | 安佐化学有限公司 | Waste gas purifying and weighing integrated reaction kettle device |
| US11413594B1 (en) | 2021-12-13 | 2022-08-16 | King Abdulaziz University | Viscous fluid reaction apparatus |
-
2009
- 2009-02-04 CN CNU2009201135814U patent/CN201357070Y/en not_active Expired - Lifetime
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103145200A (en) * | 2013-03-25 | 2013-06-12 | 安徽亚兰德新能源材料股份有限公司 | Method for synthesizing spherical cobaltosic oxide through mixing type oxidation |
| CN103145200B (en) * | 2013-03-25 | 2015-08-05 | 安徽亚兰德新能源材料股份有限公司 | A kind of method of hybrid oxidative synthesis spherical cobaltic-cobaltous oxide |
| WO2015027841A1 (en) * | 2013-08-27 | 2015-03-05 | 江苏华东锂电技术研究院有限公司 | Method for preparing spherical cobalt oxyhydroxide |
| CN105312018A (en) * | 2014-07-31 | 2016-02-10 | 沣田宝农业科技有限公司 | Fully-intelligent variable-temperature chelating reactor |
| CN104998596A (en) * | 2015-07-13 | 2015-10-28 | 江苏凯力克钴业股份有限公司 | Production device for preparing pure-phase cobalt tetraoxide through liquid-phase synthesis |
| CN106149045A (en) * | 2016-08-25 | 2016-11-23 | 中国有色桂林矿产地质研究院有限公司 | A kind of spherical high-pressure reactor for hydrothermal method crystal growth |
| CN106622074A (en) * | 2016-12-05 | 2017-05-10 | 安佐化学有限公司 | Weighing-supportive reaction kettle device for preparing acrylate adhesive |
| CN106622073A (en) * | 2016-12-05 | 2017-05-10 | 安佐化学有限公司 | Waste gas purifying and weighing integrated reaction kettle device |
| CN106524782A (en) * | 2016-12-30 | 2017-03-22 | 广东申菱环境***股份有限公司 | Immersive liquid-cooled module heat exchanger and manufacturing method thereof |
| US11413594B1 (en) | 2021-12-13 | 2022-08-16 | King Abdulaziz University | Viscous fluid reaction apparatus |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| ASS | Succession or assignment of patent right |
Owner name: NINGBO JINHE LITHIUM BATTERY MATERIAL CO., LTD. Free format text: FORMER OWNER: NINGBO COBOTO COBALT + NICKEL CO., LTD. Effective date: 20141115 |
|
| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20141115 Address after: 315400 Zhejiang Province, Yuyao City Jia Ling Road No. 39 Patentee after: NINGBO JINHE LITHIUM BATTERY MATERIAL CO., LTD. Address before: 315400 Zhejiang Province, Yuyao City Jia Ling Road high tech Zone of Ningbo kebote cobalt and nickel Co. Ltd. Patentee before: Ningbo Coboto Cobalt & Nickel Co., Ltd. |
|
| CP03 | Change of name, title or address | ||
| CP03 | Change of name, title or address |
Address after: 315400 Cao E village, Xiao Cao E Town, Yuyao City, Ningbo, Zhejiang Patentee after: Ningbo new energy Polytron Technologies Inc Address before: No. 39, Tan Jialing East Road, Yuyao, Zhejiang Province Patentee before: NINGBO JINHE LITHIUM BATTERY MATERIAL CO., LTD. |
|
| CX01 | Expiry of patent term | ||
| CX01 | Expiry of patent term |
Granted publication date: 20091209 |