CN201080492Y - Titanium sponge reduced distillation U -type combined device - Google Patents
Titanium sponge reduced distillation U -type combined device Download PDFInfo
- Publication number
- CN201080492Y CN201080492Y CNU2007202010111U CN200720201011U CN201080492Y CN 201080492 Y CN201080492 Y CN 201080492Y CN U2007202010111 U CNU2007202010111 U CN U2007202010111U CN 200720201011 U CN200720201011 U CN 200720201011U CN 201080492 Y CN201080492 Y CN 201080492Y
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- reduction
- condenser
- reduction reactor
- distillation
- titanium sponge
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- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model discloses a U-shaped sponge titanium reduction-distillation combined apparatus, comprising a reduction reactor (1) and a condenser (2); wherein the reduction reactor (1) is arranged inside a reduction-distillation combined furnace (3) and the condenser (2) is arranged inside a cooler (4). A discharging pipe (5) and a feeding pipe (10) are arranged on the top of the reduction reactor (1); a connection tube (6) is arranged between the reduction reactor (1) and the condenser (2); and a high-temperature valve (7) is arranged on the connection tube (6). Compared with the prior art, the utility model can realize the instant communication between the reduction reactor (1) and the condenser (2) without the connection of the reduction reactor (1) with the condenser (2) through the connection tube by the worker under high temperature, thereby the utility model has the advantages of convenient operation, greatly improved work efficiency, safety and reliability, and high yield ratio.
Description
Technical field:
The utility model relates to a kind of reduction distillation reaction unit of titanium sponge, especially a kind of reduction distillation U type machinery of titanium sponge.
Background technology:
At present, the reaction unit that utilizes the reduction distillation of titanium sponge to react to produce metal titanium normally is made up of a reduction reactor, a reduction distillation associating stove and a condenser, reduction reactor is contained in the reduction distillation associating stove, condenser is contained in the water cooler, is provided with a discharge tube and two feeding tubes on reduction reactor.When reduction reaction, in the time of 550～600 ℃, add liquid Mg by a feeding tube, block this feeding tube with the magnesium plate then; In reduction reactor, add titanium sponge (TiCl by another root feeding tube
4), by the MgCl of discharge tube discharging reaction generation
2When reduction reaction closes to an end, need to remove the blind flange on the feeding tube that is used to add liquid Mg, with a pipe connecting reduction reactor is connected with condenser; After reduction reaction finished, stove had a power failure, and sealed discharge tube and that root feeding tube that is used to add titanium sponge on the reduction reactor then, entered still-process.
There are following problem in this technology and device: when reduction reaction closes to an end, the workman will remove the blind flange on that root feeding tube that is used to add liquid Mg under hot conditions, and electricity consumption removes to melt the magnesium dividing plate on this feeding tube, and connect reduction reactor and condenser with pipe connecting, not only efficient is low, and has certain potential safety hazard; In addition, when liquid magnesium adds the stove from feeding tube, because the discharge port of feeding tube is far away apart from furnace bottom, drop is bigger, and liquid magnesium can be splashed to the reduction reaction wall when reinforced, easily causes local reaction, influence the yield and the quality of product, and can cause production cost to increase.
The utility model content:
The purpose of this utility model is: provide a kind of easy to operate, safe and reliable, yield height of product, the reduction distillation U type machinery of the measured titanium sponge of matter, to solve the problem that prior art exists.
The utility model is to constitute like this: comprise reduction reactor 1 and condenser 2, reduction reactor 1 is contained in the reduction distillation associating stove 3, condenser 2 is contained in the water cooler 4, discharge tube 5 and filling tube 10 are housed at the top of reduction reactor 1, between reduction reactor 1 and condenser 2, be connected with pipe connecting 6, high-temperature valve 7 is housed on pipe connecting 6.
The two ends of pipe connecting 6 are connected on the top center of reduction reactor 1 and condenser 2.
Side and top at discharge tube 5 are respectively arranged with side branch pipe 8 and top manifold 9.
Compared with prior art, the utility model has been connected a pipe connecting between reduction reactor and condenser, and high-temperature valve (200610200512.8) is housed on pipe connecting, can be used for adding titanium tetrachloride, can close pipe connecting by Kei, like this when reduction reaction closes to an end, only need open high-temperature valve, can realize being communicated with between reduction reactor and the condenser, need not the workman and under hot conditions, connect reduction reactor and condenser with pipe connecting, not only improved working efficiency greatly, and safe and reliable.In addition, liquid magnesium is that disposable arm from discharge tube adds needed amount, because discharge tube is the bottom that is inserted in reduction reactor, therefore when adding liquid magnesium, liquid magnesium passes the part metals magnesium that melted and the condensation residue of magnesium chloride from the bottom of reduction reactor, not only can avoid splashing, and help the purification of magnesium, improve quality product.
Description of drawings:
Fig. 1 is a structural representation of the present utility model.
Embodiment:
Embodiment of the present utility model: as shown in Figure 1, comprise reduction reactor 1 and condenser 2, reduction reactor 1 is contained in the reduction distillation associating stove 3, condenser 2 is contained in the water cooler 4, discharge tube 5 and filling tube 10 are housed at the top of reduction reactor 1, are respectively arranged with side branch pipe 8 and top manifold 9 at the side and the top of discharge tube 5.Be connected with pipe connecting 6 between reduction reactor 1 and condenser 2, reduction reactor 1 is connected with condenser 2 by pipe connecting 6, and the two ends of pipe connecting 6 preferably are connected on the top center of reduction reactor 1 and condenser 2, help TiCl like this
4Be evenly distributed in the reduction reactor 1; High-temperature valve 7 is housed on pipe connecting 6.
Before reduction reaction begins, close the high-temperature valve 7 on the pipe connecting 6 earlier; When reduction reaction temperature reaches 550～600 ℃, by the filling tube 10 adding titanium chloride (TiCl at reduction reactor 1 top
4), by the top manifold 9 disposable adding liquid magnesium of discharge tube 5, add finish rear enclosed filling tube 10 and top manifold 9; Magnesium chloride (the Mgcl that reduction reaction produces
2Logical) discharge by the side branch pipe 8 of discharge tube 5; When reduction reaction closes to an end, open the high-temperature valve 7 on the pipe connecting 6, make between reduction reactor 1 and the condenser 2 to be interconnected, enter still-process, remain in magnesium and magnesium chloride (Mgcl in the reduction reactor 1
2) be condensed in condenser 2 by pipe connecting 6.
Claims (3)
1. the reduction distillation U type machinery of a titanium sponge, comprise reduction reactor (1) and condenser (2), reduction reactor (1) is contained in the reduction distillation associating stove (3), condenser (2) is contained in the water cooler (4), discharge tube (5) and filling tube (10) are housed at the top of reduction reactor (1), it is characterized in that: between reduction reactor (1) and condenser (2), be connected with pipe connecting (6), high-temperature valve (7) is housed on pipe connecting (6).
2. the reduction distillation U type machinery of titanium sponge according to claim 1 is characterized in that: the two ends of pipe connecting (6) are connected on the top center of reduction reactor (1) and condenser (2).
3. the reduction distillation U type machinery of titanium sponge according to claim 1, it is characterized in that: side and top at discharge tube (5) are respectively arranged with side branch pipe (8) and top manifold (9).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNU2007202010111U CN201080492Y (en) | 2007-09-13 | 2007-09-13 | Titanium sponge reduced distillation U -type combined device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNU2007202010111U CN201080492Y (en) | 2007-09-13 | 2007-09-13 | Titanium sponge reduced distillation U -type combined device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN201080492Y true CN201080492Y (en) | 2008-07-02 |
Family
ID=39614170
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNU2007202010111U Expired - Lifetime CN201080492Y (en) | 2007-09-13 | 2007-09-13 | Titanium sponge reduced distillation U -type combined device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN201080492Y (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101386920B (en) * | 2007-09-13 | 2010-10-20 | 贵阳铝镁设计研究院 | Reduction-distillation method of titanium sponge and U type complex unit |
| CN101724754B (en) * | 2008-10-30 | 2012-06-27 | 贵阳铝镁设计研究院有限公司 | Reduction and distillation furnace |
| CN102534261A (en) * | 2012-01-18 | 2012-07-04 | 深圳市新星轻合金材料股份有限公司 | Process method for preparing titanium sponge |
| CN102560152A (en) * | 2012-01-18 | 2012-07-11 | 深圳市新星轻合金材料股份有限公司 | Reaction device for producing titanium sponge |
| EP2618087A1 (en) * | 2012-01-18 | 2013-07-24 | Shenzhen Sunxing Light Alloys Materials Co., Ltd | Distillation equipment for producing sponge titanium |
| CN103215461A (en) * | 2013-05-22 | 2013-07-24 | 朝阳金达钛业股份有限公司 | 15-ton inverted-U-shaped combination device and production process for producing sponge titanium |
-
2007
- 2007-09-13 CN CNU2007202010111U patent/CN201080492Y/en not_active Expired - Lifetime
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101386920B (en) * | 2007-09-13 | 2010-10-20 | 贵阳铝镁设计研究院 | Reduction-distillation method of titanium sponge and U type complex unit |
| CN101724754B (en) * | 2008-10-30 | 2012-06-27 | 贵阳铝镁设计研究院有限公司 | Reduction and distillation furnace |
| CN102534261A (en) * | 2012-01-18 | 2012-07-04 | 深圳市新星轻合金材料股份有限公司 | Process method for preparing titanium sponge |
| CN102560152A (en) * | 2012-01-18 | 2012-07-11 | 深圳市新星轻合金材料股份有限公司 | Reaction device for producing titanium sponge |
| CN102534261B (en) * | 2012-01-18 | 2013-04-10 | 深圳市新星轻合金材料股份有限公司 | Process method for preparing titanium sponge |
| EP2618087A1 (en) * | 2012-01-18 | 2013-07-24 | Shenzhen Sunxing Light Alloys Materials Co., Ltd | Distillation equipment for producing sponge titanium |
| WO2013107109A1 (en) * | 2012-01-18 | 2013-07-25 | 深圳市新星轻合金材料股份有限公司 | Reaction apparatus for use in preparing titanium sponge |
| CN102560152B (en) * | 2012-01-18 | 2014-03-26 | 深圳市新星轻合金材料股份有限公司 | Reaction device for producing titanium sponge |
| CN103215461A (en) * | 2013-05-22 | 2013-07-24 | 朝阳金达钛业股份有限公司 | 15-ton inverted-U-shaped combination device and production process for producing sponge titanium |
| CN103215461B (en) * | 2013-05-22 | 2014-11-26 | 朝阳金达钛业股份有限公司 | 15-ton inverted-U-shaped combination device and production process for producing sponge titanium |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| ASS | Succession or assignment of patent right |
Owner name: GUIYANG ALUMINIUM AND MAGNESIUM DESIGN INSTITUTE C Free format text: FORMER OWNER: GUIYANG ALUMINIUM AND MAGNESIUM DESIGN INST. Effective date: 20110524 |
|
| C41 | Transfer of patent application or patent right or utility model | ||
| COR | Change of bibliographic data |
Free format text: CORRECT: ADDRESS; FROM: 550004 NO. 208, BEIJING ROAD, GUIYANG CITY, GUIZHOU PROVINCE TO: 550081 NO. 2, JINZHU ROAD, JINYANG NEW DISTRICT, GUIYANG CITY, GUIZHOU PROVINCE |
|
| TR01 | Transfer of patent right |
Effective date of registration: 20110524 Address after: 550081 Guiyang Province, Jinyang New District, Zhu Zhu Road, No. 2 Patentee after: Guiyang Aluminum & Magnesium Design Institute Co., Ltd. Address before: 550004 No. 208, Beijing Road, Guiyang, Guizhou Patentee before: Guiyang Aluminium and Magnesium Design Inst. |
|
| CX01 | Expiry of patent term |
Granted publication date: 20080702 |
|
| CX01 | Expiry of patent term |