CN1877309A - 铁***-鲁米诺化学发光体系定量甜叶菊糖苷的方法 - Google Patents
铁***-鲁米诺化学发光体系定量甜叶菊糖苷的方法 Download PDFInfo
- Publication number
- CN1877309A CN1877309A CN 200610010277 CN200610010277A CN1877309A CN 1877309 A CN1877309 A CN 1877309A CN 200610010277 CN200610010277 CN 200610010277 CN 200610010277 A CN200610010277 A CN 200610010277A CN 1877309 A CN1877309 A CN 1877309A
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- China
- Prior art keywords
- stevioside
- luminol
- solution
- potassium ferricyanide
- quantitative
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 229940013618 stevioside Drugs 0.000 title claims abstract description 61
- OHHNJQXIOPOJSC-UHFFFAOYSA-N stevioside Natural products CC1(CCCC2(C)C3(C)CCC4(CC3(CCC12C)CC4=C)OC5OC(CO)C(O)C(O)C5OC6OC(CO)C(O)C(O)C6O)C(=O)OC7OC(CO)C(O)C(O)C7O OHHNJQXIOPOJSC-UHFFFAOYSA-N 0.000 title claims abstract description 61
- 235000019202 steviosides Nutrition 0.000 title claims abstract description 61
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 title claims abstract description 5
- 229910052700 potassium Inorganic materials 0.000 title claims abstract description 5
- 239000011591 potassium Substances 0.000 title claims abstract description 5
- 238000000034 method Methods 0.000 claims abstract description 27
- 239000000243 solution Substances 0.000 claims abstract description 18
- HWYHZTIRURJOHG-UHFFFAOYSA-N luminol Chemical compound O=C1NNC(=O)C2=C1C(N)=CC=C2 HWYHZTIRURJOHG-UHFFFAOYSA-N 0.000 claims abstract description 17
- 239000012086 standard solution Substances 0.000 claims abstract description 10
- 230000002708 enhancing effect Effects 0.000 claims abstract description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 24
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 7
- OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 claims description 6
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- OWEGMIWEEQEYGQ-UHFFFAOYSA-N 100676-05-9 Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC2C(OC(O)C(O)C2O)CO)O1 OWEGMIWEEQEYGQ-UHFFFAOYSA-N 0.000 description 1
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- 235000014676 Phragmites communis Nutrition 0.000 description 1
- HELXLJCILKEWJH-SEAGSNCFSA-N Rebaudioside A Natural products O=C(O[C@H]1[C@@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1)[C@@]1(C)[C@@H]2[C@](C)([C@H]3[C@@]4(CC(=C)[C@@](O[C@H]5[C@H](O[C@H]6[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O6)[C@@H](O[C@H]6[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O6)[C@H](O)[C@@H](CO)O5)(C4)CC3)CC2)CCC1 HELXLJCILKEWJH-SEAGSNCFSA-N 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 241000544066 Stevia Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
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- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 1
- GUBGYTABKSRVRQ-QUYVBRFLSA-N beta-maltose Chemical compound OC[C@H]1O[C@H](O[C@H]2[C@H](O)[C@@H](O)[C@H](O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@@H]1O GUBGYTABKSRVRQ-QUYVBRFLSA-N 0.000 description 1
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- HELXLJCILKEWJH-UHFFFAOYSA-N entered according to Sigma 01432 Natural products C1CC2C3(C)CCCC(C)(C(=O)OC4C(C(O)C(O)C(CO)O4)O)C3CCC2(C2)CC(=C)C21OC(C1OC2C(C(O)C(O)C(CO)O2)O)OC(CO)C(O)C1OC1OC(CO)C(O)C(O)C1O HELXLJCILKEWJH-UHFFFAOYSA-N 0.000 description 1
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- 235000019203 rebaudioside A Nutrition 0.000 description 1
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- DAJSVUQLFFJUSX-UHFFFAOYSA-M sodium;dodecane-1-sulfonate Chemical compound [Na+].CCCCCCCCCCCCS([O-])(=O)=O DAJSVUQLFFJUSX-UHFFFAOYSA-M 0.000 description 1
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- ZRVXFJFFJZFRLQ-UHFFFAOYSA-M tetramethylazanium;iodate Chemical compound [O-]I(=O)=O.C[N+](C)(C)C ZRVXFJFFJZFRLQ-UHFFFAOYSA-M 0.000 description 1
- 238000004809 thin layer chromatography Methods 0.000 description 1
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- Investigating Or Analysing Materials By The Use Of Chemical Reactions (AREA)
Abstract
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CNB2006100102778A CN100476410C (zh) | 2006-07-12 | 2006-07-12 | 铁***-鲁米诺化学发光体系定量甜叶菊糖苷的方法 |
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CNB2006100102778A CN100476410C (zh) | 2006-07-12 | 2006-07-12 | 铁***-鲁米诺化学发光体系定量甜叶菊糖苷的方法 |
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CN1877309A true CN1877309A (zh) | 2006-12-13 |
CN100476410C CN100476410C (zh) | 2009-04-08 |
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CNB2006100102778A Expired - Fee Related CN100476410C (zh) | 2006-07-12 | 2006-07-12 | 铁***-鲁米诺化学发光体系定量甜叶菊糖苷的方法 |
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Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102253033A (zh) * | 2011-04-13 | 2011-11-23 | 桂林理工大学 | 一种在线快速检测甜叶菊糖苷的方法 |
CN102608106A (zh) * | 2012-03-31 | 2012-07-25 | 桂林理工大学 | 一种在线快速检测剑麻皂苷的方法 |
CN102692387A (zh) * | 2012-06-15 | 2012-09-26 | 南京农业大学 | 一种植物中硫代葡萄糖苷总量的测定方法 |
CN103091409A (zh) * | 2012-11-13 | 2013-05-08 | 江苏艾兰得营养品有限公司 | 一种低聚果糖菊粉纯度的鉴定方法 |
CN105891190A (zh) * | 2016-04-04 | 2016-08-24 | 广东工业大学 | 一种基于化学发光的结晶紫检测方法 |
CN105929010A (zh) * | 2016-04-14 | 2016-09-07 | 福建师范大学 | 一种基于曙红y的电致化学发光传感器 |
CN106383111A (zh) * | 2016-10-31 | 2017-02-08 | 内蒙古博奥现代蒙中药技术研究有限公司 | 一种扎冲十三味丸中没食子酸的检测方法 |
-
2006
- 2006-07-12 CN CNB2006100102778A patent/CN100476410C/zh not_active Expired - Fee Related
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102253033A (zh) * | 2011-04-13 | 2011-11-23 | 桂林理工大学 | 一种在线快速检测甜叶菊糖苷的方法 |
CN102608106A (zh) * | 2012-03-31 | 2012-07-25 | 桂林理工大学 | 一种在线快速检测剑麻皂苷的方法 |
CN102692387A (zh) * | 2012-06-15 | 2012-09-26 | 南京农业大学 | 一种植物中硫代葡萄糖苷总量的测定方法 |
CN103091409A (zh) * | 2012-11-13 | 2013-05-08 | 江苏艾兰得营养品有限公司 | 一种低聚果糖菊粉纯度的鉴定方法 |
CN105891190A (zh) * | 2016-04-04 | 2016-08-24 | 广东工业大学 | 一种基于化学发光的结晶紫检测方法 |
CN105929010A (zh) * | 2016-04-14 | 2016-09-07 | 福建师范大学 | 一种基于曙红y的电致化学发光传感器 |
CN106383111A (zh) * | 2016-10-31 | 2017-02-08 | 内蒙古博奥现代蒙中药技术研究有限公司 | 一种扎冲十三味丸中没食子酸的检测方法 |
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CN100476410C (zh) | 2009-04-08 |
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Effective date of registration: 20120209 Address after: 272000 Shandong province Jining Jinyu Road No. 135 Patentee after: Jining Aoxing Stevia Products Co., Ltd. Address before: 150030 School of life science, Northeast Agricultural University, 59 Wood Street, Xiangfang District, Heilongjiang, Harbin Patentee before: Hao Zaibin |
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