CN1865953A - Self-short-circuit type coaxial shock wave electric probe and method for manufacturing same - Google Patents
Self-short-circuit type coaxial shock wave electric probe and method for manufacturing same Download PDFInfo
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- CN1865953A CN1865953A CN 200610021177 CN200610021177A CN1865953A CN 1865953 A CN1865953 A CN 1865953A CN 200610021177 CN200610021177 CN 200610021177 CN 200610021177 A CN200610021177 A CN 200610021177A CN 1865953 A CN1865953 A CN 1865953A
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Abstract
The related self-short coaxial shock-wave electric probe comprises: an Al alloy bar with one end as semi-sphere and another end as plane. Wherein, the semi-sphere end covers 6-12um Al2O3 insulation film with 3-5um Ag-conductive film arranged a ring as the plane end and welt external electrode. The probe is prepared by mechanical polishing, chemical descaling and polishing, anodizing and chemical depositing film. This invention has well impact response, compatibility and repeatability.
Description
Technical field
The present invention relates to a kind of coaxial shock wave electric probe and method for making thereof, more particularly, relate to a kind of novel self-short-circuit type coaxial shock wave electric probe and method for making thereof that is applicable to shock velocity in the test liquid material.
Background technology
For simulation material is experiencing High Temperature High Pressure, the characteristic under the extreme conditions such as cryogenic high pressure and low-temp low-pressure, shock wave high velocity impact-measuring technique commonly used is carried out dynamic load to material, and the original state of material often is a liquid under these extreme conditions.Solid material can accurately calculate with crystal model, gas material can be used ideal gas model accurate description, but the structure of fluent material neither resembles solid material and does not resemble gas material again, thus be difficult to calculate with existing theoretical model, can only be with half classics or experimental formula approximate description.Based on this, so need the development coaxial shock wave electric probe, the ballistic motion speed that produces when being used for that fluent material carried out dynamic load is measured.This technology is particular importance in the research of manned spacecraft is used now, similarly uses to also have in torpedo, der Amphibien-Tank and naval vessel plate armour and resist the ability evaluation of missile impact and the assessment of practical function etc. in actual combat; Rocket ship is under extreme conditions resisted the ability of space trash bump in-flight; And the high velocity impact test carried out of the security of travelling for means of transports such as check automobile, train, naval vessels.Principal ingredient such as organization of human body is a water, the research fluent material just comprises the degree of human body damaged under thump in the performance change under the shock wave effect, tests and studies so all will implant the liquid measurand with this type of electric probe when determining the safety index of the Modern High-Speed vehicles.
Shock wave electric probe is to utilize detonation technology and impact compress technical research fluent material in High Temperature High Pressure, rerum natura under the extreme condition such as cryogenic high pressure and low-temp low-pressure, detonation is to utilize explosive strong shock wave compression sample material, impact compress is to utilize gas big gun technical modelling detonation wave, drive film flying collision specimen material, because speed is too fast, up to 7km/s, therefore, can't directly measure the rerum natura of fluent material by compression the time, can only measure indirectly in the velocity variations that causes by fluent material itself by measuring shock waves.According to the shock velocity in the fluent material that records, the time interval of promptly measuring the fixed length path on the path that shock wave passes through calculates shock velocity then, can obtain the high pressure property information of fluent material in conjunction with Hugoniot relation and the law of thermodynamics.The precision that needs nanosecond order during by measuring shock waves speed research fluent material characteristic, if deviation ± 1 nanosecond, material behavior estimate can deviation up to 10%.So big error is unallowable at conventional weapon such as tactical missile, rocket etc., obviously, the measuring accuracy of shock velocity has determined the correctness and the integrality of result of study, and shock wave electric probe is the principal element of decision shock velocity measuring accuracy.
At present, have only the coaxial shock wave electric probe that relies on home built " sandwich " formula sandwich structure fully to can be used for the detonation and the impact compress experiment of fluent material.Its sandwich structure is made of insullac coating-coating process: rely on the home built performance can satisfy the coaxial shock wave electric probe that " sandwich " formula sandwich structure is arranged of detonation and impact compress requirement of experiment fully, promptly its structure is insulation heart yearn-thin-walled nickel pipe-cup head-multilayer insulation enamelled coating-coat of metal-protective seam.Because the home built discreteness has determined the coaxial shock wave electric probe of " sandwich " formula sandwich structure that there is uncertain factor in consistance and the reliability of measuring.And with alumilite process-chemical settling membrane process, the coaxial shock wave electric probe that the anodization alumite is made on aluminum alloy material, though production environment is had certain requirement, but can significantly improve consistance, repeatability and the reliability of the coaxial shock wave electric probe parameter of " sandwich " formula sandwich structure, and can effectively enhance productivity.So, above described two kinds of shock wave electric probes each has something to recommend him technically.But consider that from aspects such as technology content, working (machining) efficiency and experimental precisions the exploitation that the electric probe that alumilite process-chemical settling membrane process is made obviously has better wide use prospect and Geng Gao is worth.
Summary of the invention
The objective of the invention is in order to overcome the existing existing defective of coaxial shock wave electric probe, provide a kind of and the pellumina thickness of extremely strong adhesion is arranged in 6-12 micron continuous controllable, statistic bias is not more than 2 microns, the electrical isolation proof strength is good under the 77K temperature, inspection parameter consistance repeatability is good, be particularly suitable for high temperature, low temperature, and the novel self-short-circuit type coaxial shock wave electric probe of the impact compression test of fluent material under the vertiginous big thermal shock environment of this temperature range environment; And the preparation method that a kind of this electric probe is provided.The self-short-circuit type coaxial shock wave electric probe of this method preparation is to Condensed Matter Physics, and the development of front subjects such as shock wave physics and weapon physics is to the research of fluent material rerum natura under the extreme condition with measure all significant.
The technical scheme that purpose of the present invention is made of following measure realizes.
Self-short-circuit type coaxial shock wave electric probe of the present invention; comprise that mainly aluminum-alloy wire is processed into the aluminium quarter butt; according to the present invention; the end grinding that also comprises the aluminium quarter butt is the aluminium cup head, and the other end is the aluminium butt end, generates the pellumina insulation course at the first end of aluminium semicircle; deposit silver conductive film on this insulation course; be mounted with garter spring respectively on the silver conductive film He on the aluminium butt end, weld outer electrode on the garter spring, on silver conductive film, be coated with organic insulating protective film wheat and receive film.
In the such scheme, on described silver conductive film, install and fix first garter spring, welding first outer electrode on first garter spring.
In the such scheme, on described aluminium butt end, install and fix second garter spring, welding second outer electrode on second garter spring.
In the such scheme, the pellumina insulation course of described aluminium semicircle head end is the pellumina insulation course on aluminium cup head end distance aluminium butt end 2/3 length.
In the such scheme, described pellumina insulation course is the pellumina thickness 6~12 microns continuous controllable that extremely strong adhesion is arranged.
Self-short-circuit type coaxial shock wave electric probe of the present invention, in use, two electrodes are inserted the high voltage network power supply respectively, when its aluminium semicircle head end is breakdown, form short circuit, the rapid discharge loop of network electric power charging capacitor is provided, to obtain the burst pulse of nanosecond, be used for the high precision that the fluent material shock velocity is measured to reach electric probe.
The method for making of the self-short-circuit type coaxial shock wave electric probe of above-mentioned arbitrary described scheme adopts aluminium anodeization-chemical deposition technique to make, and mainly comprises following processing step:
(1) mechanical buffing, deoil: aluminium quarter butt one terminal tool is ground to form the aluminium cup head, and the other end was the aluminium butt end, removes aluminium quarter butt surface dirt, with tap water flushing 1 minute;
(2) chemical cleaning-alkali cleaning: under 50~60 ℃ isoperibol, be 1: 1 NaOH and Na with volume ratio
2CO
3Saturated mixing electrolysis assisted solution stirs down and handled aluminium semicircle head end 2 minutes,, with tap water flushing 1 minute;
(3) chemical cleaning-pickling: under 50~60 ℃ isoperibol, with 1: 3 CrO
3And H
2SO
4Saturated mixing electrolysis assisted solution stirs down and handled aluminium semicircle head end 2 minutes, with tap water flushing 1 minute, soaks 1 minute with deionized water again;
(4) chemical polishing: under above-mentioned constant temperature stirring condition, the special electrolysis liquid for preparing is placed container, turn to solenoid with platinum filament and make negative electrode, platinum filament negative electrode and aluminium semicircle head end are put into the auxiliary liquid of electrolysis carried out electrolytic treatments 3 minutes, with tap water flushing 3 minutes, soaked 1 minute with deionized water more then;
(5) anodized aluminum semicircle head end: anodization electrolysis working solution, to be mixed with concentration be 3% lean solution with analyzing pure oxalic acid, lean solution is placed container, make electrolysis working fluid temperature constant simultaneously about 10 ℃, concentration of electrolyte is 3%, and the pH value of electrolytic solution is under 3~4 conditions, the first end of aluminium semicircle is put into the lean solution anodization, in 20~30 seconds of processing time, electrolysis generates the alumina insulating film of 6~12 microns continuous controllable, uses the tap water cleaning down again 5 minutes;
(6) the heavy film of chemistry: on alumina insulating film, generate 3~5 microns silver conductive film with conventional silver mirror deposition art;
(7) garter spring is installed: on silver conductive film, install and fix first garter spring, weld first outer electrode, on the aluminium butt end, install and fix second garter spring, weld second outer electrode;
(8) sealing of hole: with gauze parcel aluminium semicircle head end, put into the deionized water of 100ml, kept 10 minutes under fluidized state, constant temperature is 30 minutes under 70 ℃ of environment of usefulness electric dry oven;
(9) the aluminium quarter butt of above-mentioned processing is scribbled organizational security and protect the dielectric film wheat and receive film, promptly make the finished product self-short-circuit type coaxial shock wave electric probe.
The present invention compared with prior art has following characteristics:
1, self-short-circuit type coaxial shock wave electric probe of the present invention both had good electrical insulating property and thermal insulation, and volume is little, be easy to be placed in the fluent material, research and measure the shock velocity of fluent material, according to the Hugoniot relation, from so obtain the rerum natura of fluent material.
2, the first end of self-short-circuit type coaxial shock wave electric probe aluminium semicircle of the present invention has the pellumina thickness of continuous controllable in 6~12 micrometer ranges of extremely strong adhesion, and statistic bias is not more than 2 microns.
3, the electrical isolation proof strength of self-short-circuit type coaxial shock wave electric probe of the present invention under temperature 77K is not less than 200 volts, 5 minutes, inspection parameter consistance repeatability is good, be specially adapted to 200 ℃ of high temperature, low temperature-200 ℃, and the impact compression test of fluent material under the vertiginous big thermal shock environment of this temperature range environment.
4, the self-short-circuit type coaxial shock wave electric probe that makes of the inventive method is to Condensed Matter Physics, and the development of front subjects such as shock wave physics and weapon physics is to the research of fluent material rerum natura under the extreme condition with measure all significant.
Description of drawings
Fig. 1 self-short-circuit type coaxial shock wave electric probe structural profile of the present invention synoptic diagram
Fig. 2 electric probe aluminium of the present invention semicircle head end polarization curve
Fig. 3 electric probe anodization of the present invention device synoptic diagram
The used pulsation rectification circuit of Fig. 4 electric probe anodization of the present invention synoptic diagram
Among the figure, 1 aluminium cup head, 2 aluminium flush ends, 3 pellumina insulation courses, 4 silver conductive films, 5 first garter springs, 6 second garter springs, 7 first outer electrodes, 8 second outer electrodes, 9 platinum filament negative electrodes.
Embodiment
Below in conjunction with accompanying drawing, make principle and the present invention is further illustrated with embodiment.
Among Fig. 1 of the present invention, aluminum-alloy wire is processed into the aluminium quarter butt, aluminium quarter butt one end is an aluminium cup head 1, the other end is an aluminium butt end 2, the pellumina insulation course 3 that on the length of aluminium cup head 1 one end distance aluminium butt ends about 2/3, generates for alumite, on pellumina insulation course 3, deposit silver conductive film 4, install and fix first garter spring 5 on the silver conductive film 4, welding first outer electrode 7 on first garter spring 5, there is not to install and fix second garter spring 6 on another aluminium butt end 2 of pellumina insulation course welding second outer electrode 8 on second garter spring 6 at the aluminium quarter butt.
Among Fig. 2, will place container, and platinum filament be turned to solenoid make negative electrode, and platinum filament negative electrode 9 and the aluminium cup head utmost point in 1 Dragon Boat Festival be put into electrolytic solution carry out electrolytic treatments with the electrolysis working fluid for preparing.
Among Fig. 3, the polarization curve of aluminium semicircle head end is to be horizontal ordinate with the voltage parameter that records, and current parameters is the polarization curve that ordinate is done.
Embodiment
Self-short-circuit type coaxial shock wave electric probe of the present invention is made of aluminium anodeization-chemical settling membrane process, and the aluminum-alloy wire of 1 millimeter of φ is concentrated harness, is processed into 35 millimeters aluminium quarter butts with electric spark again, operates by following processing step:
(1) mechanical buffing, deoils: clamp the aluminium quarter butt with the minitype vertical type drill jig, be converted into 60 ° with 800 order fine sandpapers, aluminium quarter butt one end is carefully ground to form aluminium cup head 1, this end strives reaching 11 smooth finish 0.3, the other end is an aluminium butt end 2, remove aluminium quarter butt surface dirt with neutral cleanser, with tap water flushing 1 minute;
(2) chemical cleaning-alkali cleaning: be heated by resistive cover, temperature controller and mini-sized blender are controlled at temperature under 50~60 ℃ the isoperibol, are 1: 1 NaOH and Na with volume ratio
2CO
3Saturated mixing electrolysis assisted solution stirred down and handled aluminium semicircle head end 2 minutes, with tap water flushing 1 minute;
(3) chemical cleaning-pickling: under the same constant temperature stirring condition of step (2), with 1: 3 CrO
3And H
2SO
4Saturated mixing electrolysis assisted solution was handled aluminium semicircle head end 2 minutes, with tap water flushing 1 minute, soaked 1 minute with deionized water again;
(4) chemical polishing: under above-mentioned constant temperature stirring condition, the special electrolysis liquid for preparing is placed container, use diameter phi 0.2mm, the platinum filament of length L 1500mm turns to solenoid and makes negative electrode, platinum filament negative electrode 9 and aluminium cup head 1 end are put into electrolytic solution carried out electrolytic treatments 3 minutes, with tap water flushing 3 minutes, soaked 1 minute with deionized water more then;
(5) measure polarization curve: the polarization curve that records aluminium semicircle head end with HDV-7 transistor npn npn potentiostat;
(6) anodized aluminum semicircle head end: anodization electrolysis working solution, to be mixed with concentration be 3% lean solution with analyzing pure oxalic acid, lean solution is placed container, simultaneously according to polarization curve control Faradaic current and electrolysis time, situation according to production environment temperature and processing electric probe quantity, regulate the temperature of electrolysis working fluid, with electrolytic tank autogamy thermometer monitoring electrolyte temperature, make temperature constant about 10 ℃, electrolysis working fluid concentration is 3%, the pH value of electrolysis working fluid is under 3~4 conditions, aluminium cup head end distance aluminium butt end 2/3 length aluminium quarter butt is put into lean solution carry out anodic oxidation, the first end of aluminium semicircle then adheres to the pellumina insulation course 3 of one deck 6-12 micron continuous controllable, uses tap water cleaning down 5 minutes;
(7) the heavy film of chemistry: the silver conductive film 4 that on alumina insulating film, generates 3~5 microns of one decks with conventional silver mirror deposition art;
(8) garter spring is installed: on silver conductive film 4, install and fix first garter spring 5, weld first outer electrode 7, on aluminium butt end 2, install and fix second garter spring 6, weld second outer electrode 8;
(9) sealing of hole: avoiding the damaged in collision oxide film,, put into the deionized water of 100ml, under fluidized state, kept 10 minutes, used under 70 ℃ of environment of electric dry oven constant temperature again 30 minutes with the semicircle head end 1 of gauze parcel aluminium quarter butt;
(10) the aluminium quarter butt of above-mentioned processing is scribbled organizational security cuticula wheat and receive film, promptly obtain the finished product self-short-circuit type coaxial shock wave electric probe.
The prescription of electrolysis working solution of the present invention is made up of the chemical reagent of different component: H
2SO
4, volume parts is 2%, H
3PO
4, volume parts is 5%, C
3H
8O
3, volume parts is 2%, C
2H
6O, volume parts is 2% and C
12H
22O
11, volume parts is 0.01%, the initial electrolysis current density is 0.2I/A/cm
2
Electric probe of the present invention carries out aluminium quarter butt anodization batch processing simultaneously by above-mentioned steps and the given auxiliary liquid of electrolysis, electrolysis working fluid and running parameter, after the anodization electrolytic process finishes, by different electrolysis times sample number into spectrum is got final product.The electric probe that the present invention makes, can carry out painted as required: with the sodium alizarinsulfonate of 0.1 grams per liter, 0.04 the alizarin yellow of grams per liter and deionized water are mixed with 100 milliliters mixed liquor, temperature constant is carried out electrolytic coloring at 50~60 ℃, handled 5 minutes, and formed back, golden yellow surface and take out, cleaned 5 minutes, at last test specimen is put into 100 ℃ constant temperature oven, toasted and got final product in 4 hours.
Electric probe of the present invention is with the device electrolysis pretreatment aluminium quarter butt of similar Fig. 2, for fear of the ablation on pure DC current antianode surface in electrolytic process with the anode barrier potential that increases gradually, designed half-wave rectifying circuit as shown in Figure 4, regulate electric current and voltage, utilize the level and smooth flip-flop equivalence combined electrolysis pulsafeeder of big pulsating waveform and capacitor.Commutation diode is selected IN4002 for use in the circuit, or other reverse maximum breakdown voltage is not less than 200V, and maximum forward current value is not less than the semiconductor rectifier tube of 1A, and the capacity of pressure regulator is 500VA.
The thickness of the alumina insulating film of aluminium semicircle head end of the present invention has reflected the dynamic response and the electrical insulating property of electric probe, and its thickness increases, and electric probe impact force-responsive slows down, but electrical insulating property improves; Otherwise it is then opposite.Therefore, the present invention had both had and had well hit force-responsive from the thickness 6-12 of short circuit coaxial shock wave electric probe alumina insulating film micron, and excellent electric insulating is arranged again, had improved consistance and the reliability of existing electric probe to the fluent material parameter measurement.
The thickness 6-12 micron of electric probe alumina insulating film of the present invention, be concentration 3% at the self-control Working electrolyte, its temperature constant is about 10 ℃, the pH value of Working electrolyte is under 3~4 conditions, the alumina insulation film thickness that generates is in 6-12 micron continuous controllable, and statistic bias is not more than 2 microns.
The making of self-short-circuit type coaxial shock wave electric probe of the present invention is according to the alumilite process electrochemical principle, utilizes the dc electrolysis film-forming process to realize.According to the electrochemical filming principle, the aluminium blank is being carried out on the meticulous pre-treatment bases such as mechanical lapping, electrochemical treatment, utilize independently developed miniature aluminum alloy workpiece anode oxidation process flow process, technological parameter and electrolysis special formula of liquid directly go out hard uniformly densely pellumina in the superficial growth of precision machined cup head section bar.Then by ripe aftertreatment technology, make and meet the novel of detonation and impact compress requirement of experiment from the short circuit coaxial shock wave electric probe.Of the present invention have the pellumina thickness of extremely strong adhesion 6~12 microns continuous controllable from the short circuit coaxial shock wave electric probe, statistic bias is not more than 2 microns, electrical isolation proof strength under the 77K temperature is not less than 100 volts, 30 minutes, it is good that inspection parameter repeats consistance, is particularly suitable for 200 ℃ of high temperature, low temperature-200 ℃ and the impact compression test of fluid sample under the vertiginous big thermal shock environment of this temperature range environment.Self-short-circuit type coaxial shock wave electric probe shock wave physics of the present invention, astrophysics, geophysics, the development of front subjects such as Condensed Matter Physics and weapon physics, all significant to the research of material property under the extreme condition.
Claims (6)
1. self-short-circuit type coaxial shock wave electric probe; comprise that aluminum-alloy wire is processed into the aluminium quarter butt; it is characterized in that also comprising that an end of aluminium quarter butt is aluminium cup head (1); the other end is aluminium butt end (2); on aluminium cup head (1) one end, generate pellumina insulation course (3) is arranged; deposit silver conductive film (4) on this insulation course; silver conductive film (4) upward and on the aluminium butt end (2) installs and fixes garter spring respectively; weld outer electrode on the garter spring, also on silver conductive film (4), scribble organizational security cuticula wheat and receive film.
2. electric probe according to claim 1 is characterized in that installing and fixing first garter spring (5) on the described silver conductive film (4), welding first outer electrode (7) on first garter spring.
3. electric probe according to claim 1 is characterized in that installing and fixing second garter spring (6) on the described aluminium butt end (2), welding second outer electrode (8) on second garter spring.
4. electric probe according to claim 1, the pellumina insulation course (3) that it is characterized in that described aluminium cup head (1) one end are the alumina insulating layers that generates on aluminium cup head end distance aluminium butt end 2/3 length.
5. according to claim 1 or 4 described electric probes, it is characterized in that described pellumina insulation course (3) for have extremely strong adhesion at 6~12 microns pellumina thickness.
6. the method for making of arbitrary described electric probe among the claim 1-5 adopts the heavy membrane technology of aluminium anodeization-chemistry to make, and it is characterized in that comprising following processing step:
(1) mechanical buffing, deoil: aluminium quarter butt one terminal tool is ground to form aluminium cup head (1), and the other end was aluminium butt end (2), removes aluminium quarter butt surface dirt, with tap water flushing 1 minute;
(2) chemical cleaning-alkali cleaning: under 50~60 ℃ isoperibol, be 1: 1 NaOH and Na with volume ratio
2CO
3Saturated mixing electrolysis assisted solution stirred down and handled aluminium semicircle head end 2 minutes, with tap water flushing 1 minute;
(3) chemical cleaning-pickling: under 50~60 ℃ isoperibol, with 1: 3 CrO
3And H
2SO
4Saturated mixing electrolysis assisted solution was handled aluminium semicircle head end 2 minutes, with tap water flushing 1 minute, soaked 1 minute with deionized water again;
(4) chemical polishing: under above-mentioned constant temperature stirring condition, the special electrolysis liquid for preparing is placed container, use diameter phi 0.2mm, the platinum filament of length L 1500mm turns to solenoid and makes negative electrode, platinum filament negative electrode (9) and aluminium quarter butt anode (10) aluminium cup head (1) end is put into electrolytic solution carried out electrolytic treatments 3 minutes, with tap water flushing 3 minutes, soaked 1 minute with deionized water more then;
(5) anodized aluminum semicircle head end: anodization electrolysis working solution, to be mixed with concentration be 3% lean solution with analyzing pure oxalic acid, lean solution is placed container, the first end of aluminium semicircle is put into lean solution carry out anodized 20-30 second, promptly generating thickness is the pellumina insulation course (3) of 6-12 micron continuous controllable, uses tap water cleaning down 5 minutes;
(6) the heavy film of chemistry: the silver conductive film (4) that on alumina insulating film, generates 3~5 microns of one decks with conventional silver mirror deposition art;
(7) garter spring is installed: on silver conductive film (4), install and fix first garter spring (5), weld first outer electrode (7), on aluminium butt end (2), install and fix second garter spring (6), weld second outer electrode (8);
(8) sealing of hole: avoiding the damaged in collision oxide film,, put into the deionized water of 100ml, under fluidized state, kept 10 minutes, used under 70 ℃ of environment of electric dry oven constant temperature again 30 minutes with the semicircle head end (1) of gauze parcel aluminium quarter butt;
(9) the aluminium quarter butt of above-mentioned processing is scribbled organizational security cuticula wheat and receive film, promptly obtain the finished product self-short-circuit type coaxial shock wave electric probe.
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CN103608493A (en) * | 2011-06-24 | 2014-02-26 | 苹果公司 | Cosmetic defect reduction in anodized parts |
CN103811901A (en) * | 2014-02-26 | 2014-05-21 | 陆腾蛟 | Electric spark eliminating plug and chemical treatment production process |
CN103811902A (en) * | 2014-02-26 | 2014-05-21 | 陆腾蛟 | Electric spark eliminating socket and chemical treatment production process |
CN103900622A (en) * | 2014-04-04 | 2014-07-02 | 中国工程物理研究院流体物理研究所 | Photoelectric integrated probe |
CN105350052A (en) * | 2015-11-28 | 2016-02-24 | 贵州航天林泉电机有限公司 | Preparation method for golden aluminum alloy conductive oxidation film |
CN108490228A (en) * | 2018-03-16 | 2018-09-04 | 武汉理工大学 | A kind of electric probe and preparation method thereof for impact wave measurement |
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Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
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CN103608493A (en) * | 2011-06-24 | 2014-02-26 | 苹果公司 | Cosmetic defect reduction in anodized parts |
CN103608493B (en) * | 2011-06-24 | 2016-06-08 | 苹果公司 | Reduce the appearance defect of anodization parts |
CN103811901A (en) * | 2014-02-26 | 2014-05-21 | 陆腾蛟 | Electric spark eliminating plug and chemical treatment production process |
CN103811902A (en) * | 2014-02-26 | 2014-05-21 | 陆腾蛟 | Electric spark eliminating socket and chemical treatment production process |
CN103811902B (en) * | 2014-02-26 | 2016-06-15 | 陆腾蛟 | A kind of chemical treatment production technology of the socket eliminating electric spark |
CN103900622A (en) * | 2014-04-04 | 2014-07-02 | 中国工程物理研究院流体物理研究所 | Photoelectric integrated probe |
CN105350052A (en) * | 2015-11-28 | 2016-02-24 | 贵州航天林泉电机有限公司 | Preparation method for golden aluminum alloy conductive oxidation film |
CN108490228A (en) * | 2018-03-16 | 2018-09-04 | 武汉理工大学 | A kind of electric probe and preparation method thereof for impact wave measurement |
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