CN1839784B - Bathing agent possessing skin-moisturizing, skin-whitening function and its preparation method - Google Patents
Bathing agent possessing skin-moisturizing, skin-whitening function and its preparation method Download PDFInfo
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Abstract
The invention relates to a bath lotion for moistening and whitening skin, which comprises the following constituents: sodium hydrogen carbonate 2.0-40.0%, metaboric acid 2.5-8.0%, strontium chloride 5.0-10.0%, metasillicio acid 26-30%, sodium chloride 10.0-17.0%, sulfur flour 13.0-20.0%, borax 1.5-3.0%, keratin agent 1.0-5.0%, cutin degradation agent 1.0-5.0%, sodium sulfate powder 5.0-48.0%, sodium bromide 5.0-10.0%, magnesium chloride 2.5-5.0%, potassium chloride 5.0-10.0%, sodium fluoride 0.5-5.0%, sodium carbonate 15.0-20.0%, aloe 20.0-30.0%, hyaluronic acid 1.0-2.5%, SOD 0.5-2.0%, lecithine 0.5-3.0%, kojic acid 0.5-2.5%, and anti-oxidant 1.5-5.0%, the ratio being weight percent.
Description
Technical field
The present invention relates to a kind of bathing agent agent and preparation method thereof with skin-moisturizing, skin-whitening function.
Background technology
Because people's living standard improves constantly, especially the modern metropolitan cities people works heavyly, and health is tired out, After Hours can not eliminate the fatigue of health fully by traditional mode of having a shower.Most of urbanites bathe bathing in hot spring and show special preference to, and its reason is that natural thermal water is rich in several mineral materials, all contain the mineral element of useful healths such as metasilicic acid, bromine, copper, strontium, selenium in the general thermal water.And thermal water has medical function to following disease: obesity, locomotor disease, nervous system disease, early stage slight cardiovascular system, digestive system disease, metabolism, to rheumatism, arthritis, nerve osteodynia, gout, multiple disease such as dermatosis has special efficacy, can play relaxing muscles and tendons and activating QI and blood in the collateral, building body, skin moistening skin care, calm the nerves compose oneself, the anti-ageing health-care effect of waiting for a long time.But enjoy natural spa, people must arrive countryside far away, to the place that hot spring is arranged, just can enjoy the pleasant of natural hot spring bath, and cost are bigger, and this has but brought great inconvenience to the ordinary people.For these reasons, occur hot spring bathing agent on the market, its dosage form is based on powder.Only need during use the hot spring powder is placed on 25～40 ℃ warm water, the hot spring powder is dissolved in rapidly in the water, reach the effect of natural hot spring water.
But the defective of hot spring powder existence on the market is now, can not effectively control the preserve moisture moisturizing and the skin moistening of skin, and can not reach beautiful gloss and the effect of whitening to skin.If life-time service makes skin dehydration and the drying that seems, owing to xerosis cutis causes pruritus.So hot spring bathing agent is not on the market now also accepted by masses fully.As Chinese patent CN99114795.2 number, its name is called " hot spring bathing tablet and preparation method thereof ", discloses the technology with components such as Cosan and alkali-metal oxyhydroxides, owing to do not contain the composition of preserving moisture such as glycerol, so the effect that skin is not preserved moisture.As Chinese patent application CN200310110426.4, it is called the patent of " hot spring champignon bathing agent and preparation method thereof ", disclosing a kind of hot spring bathing agent raw material components is the technology of sodium hydroxide, sodium silicate, potassium hydroxide, sodium bicarbonate, Sublimed Sulfur and quintessence oil, owing to do not contain the compositions of preserving moisture such as Aloe, equally skin do not had the effect of skin-moisturizing, skin.For example No. 02152153.0, the Chinese patent patent application, and its name is called " Aloe skin-care cleaning dew ", and its effect is to wash one's hands not hinder hands, and the effect of skin protection is arranged, and does not have the practical value of health-care effect but be added in to bath in the warm water.No. 02135953.9, Chinese patent application for example again, its name is called " a kind of agent for hot spring bath and preparation method thereof ", disclose and contained sodium sesquicarbonate, refining rock salt, salicylic acid and components such as derivant, malic acid, Polyethylene Glycol, citric acid, Sublimed Sulfur, Borneolum Syntheticum, Borax and quintessence oil and medicine soup thereof, its Chinese medicine soup discloses and has included aloetic composition, and skin is not had moisture-keeping function.Its reason be Aloe through add ethanol and other Chinese medicine decocted 2 hours extracting solution; The oxidation because the Aloe decocting time is oversize, aloetic surface activity effect has lost, so the Aloe composition in this patented technology does not have moistening effect to skin.
Technological deficiency based on above-mentioned hot spring bathing agent, the present invention proposes a kind of health-care effect of existing natural hot spring water, the metabolism that can reach skin prevents skin aging again, thereby skin is had the moisturizing of preserving moisture, and makes skin reach the technical scheme of beautiful gloss and whitening effect.
Summary of the invention
The object of the present invention is to provide a kind of bathing agent and preparation method thereof with skin-moisturizing, skin-whitening function, this bathing agent can be processed into powder, tablet, Emulsion and unguentum, health-care effect with bathing natural hot spring water, and the metabolism of scalable skin, prevent skin aging, to the skin moisture-keeping moisturizing, make beautiful gloss of skin and whitening effect thereby reach.
For achieving the above object, the invention provides a kind of bathing agent with skin-moisturizing, skin-whitening function, it necessary component and percentage by weight that comprises is as follows:
Sodium bicarbonate 2.0～40.0%
Metaboric acid 2.5～8.0%
Strontium chloride 5.0～10.0%
Metasilicic acid 26.0～30.0%
Sodium chloride 10.0～17.0%
Cosan 13.0～20.0%
Borax 1.5～3.0%
Molten keratoprotein agent 1.0～5.0%
Malic acid 1.0～5.0%
Molten keratoprotein agent among the present invention is salicylic acid and salt thereof, and the salt of these different chemical compounds is enough to reach and makes skin become younger.
And the cutin cracking-off agent among the present invention is a kind of in malic acid or Fructus Citri Limoniae juice extract, Alpha-hydroxy acetic acid and the derivant thereof; Its effect is the cutin cracking-off agent, and the forming process of melanosome was divided into for five phases: the first phase, cheese nitronic acid enzyme is synthetic in the endoplasmic reticulum of endochylema, and the Golgi body cavity increases synthetic protein simultaneously.The second phase claims the preceding melanin granule phase.The third phase claims the melanin granule period of maturation, and melanocyte is mainly synthetic at this first phase.The fourth phase, sophisticated melanin granule is deposited in the endochylema, transports to the angle myocyte by the dendritic processes of cell.The fifth phase, the release of melanin granule.Transfer to the keratin cell. melanin granule along with epidermis cell goes upward to horny layer, and come off and drain with horny layer. therefore, add the cutin cracking-off agent in the component of the whitening thing, can promote the metabolism of keratin cell, quicken disappearing of mottle;
And the antioxidant among the present invention comprises vitamin E and derivant thereof, vitamin C and derivant thereof, at least a or more than one; Effect is to whiten to add certain antioxidant in the component thing, has to suppress the facilitation that the radical pair melanocyte forms and keep the active dual-use function of tyrosinase inhibitor, and to the auxiliary effect of having whitened.
The present invention also provides a kind of above-mentioned preparation method with bathing agent of skin-moisturizing, skin-whitening function, and it may further comprise the steps:
Step 1: solid each component is ground to form 120～200 order fine powders respectively;
Step 2: the solution Organic substance is poured in the clean container, in container, added the fine powder of getting ready then and stir;
Step 3: after stirring, dewater;
Step 4: the fine powder after the dehydration is sent in the drying machine dried then;
Step 5: the fine powder after will drying fill according to quantity promptly gets the powder goods of bathing agent.
In the above-mentioned preparation method,, promptly can be made into tablet, Emulsion and unguentum stirring in the adjuvant of the adding of the fine powder after the dehydration after dissolving is got ready.
The present invention has following beneficial effect: contain at least among the present invention more than one natural surfactant, at least contain more than one natural moisture preserving composition, contain more than one natural whiting composition at least, therefore the health-care effect that not only has the bathing natural hot spring water, and the metabolism of scalable skin, prevent skin aging, to the skin moisture-keeping moisturizing, make beautiful gloss of skin and whitening effect.
The specific embodiment
The present invention has the bathing agent of skin-moisturizing, skin-whitening function, and it comprises that the component of following necessity and weight ratio are as follows: sodium bicarbonate 2.0～40.0%; Metaboric acid 2.5～8.0%; Strontium chloride 5.0～10.0%; Metasilicic acid 26.0～30.0%; Sodium chloride 10.0～17.0%; Cosan 13.0～20.0%; Borax 1.5～3.0%; Keratolytic 1.0～5.0%; Cutin cracking-off agent 1.0～5.0%, above percent all is weight percentage.
The bathing agent that the present invention has skin-moisturizing, skin-whitening function can also comprise following component and percentage by weight: sodium bromide 5.0～10.0%; Magnesium chloride 2.5～5.0%; Potassium chloride 5.0～10.0%; Sodium fluoride 0.5～5.0%; Sodium carbonate 15.0～20.0%; Aloe 20.0～30.0%; Hyaluronic acid 0.5～2.0%; Lecithin 0.5～3.0%; Kojic acid 0.5～2.5%; Antioxidant 1.5～5.0%, above percent all is weight percentage.
Natural surfactant includes: lanoline, tea saponin, protein, saponins, saccharide and sodium lauryl sulphate, hydroxyethyl-cellulose, hydroxy sulfo lycine, sodium lauroyl sarcosine, cocos nucifera oil diethyl alcohol amide, alkyl polyglucoside.
The natural moisture preserving composition includes: glycerol, hyaluronic acid, pyrrolidone sodium carboxylate, lactic acid, nature moisturizing factor, ceramide, collagen protein, carbamide, carapace procreation biology, Aloe, Sargassum extract, aminoacid, fatty acid, aliphatic alcohol, wax ester, linolenic acid, arachidonic acid, various vitamin.
The natural whiting composition includes: kojic acid, arbutin, Aloe vulgaris, Radix Glycyrrhizae and mulberry extract, endothelin antagonist.
The present invention has the bathing agent of skin-moisturizing, skin-whitening function, can make powder, Emulsion, unguentum.
Component and percentage by weight that first kind of optimization formula comprises are as follows:
Sodium bicarbonate 5.0～29.0%
Metaboric acid 5.0～8.0%
Metasilicic acid 26.0～28.0%
Strontium chloride 5.0～8.0%
Sodium chloride 10.0～12.0%
Salicylic acid 1.0～4.5%
Malic acid 1.0～5.0%
Aloe vulgaris 20.0～22.0%
Hyaluronic acid 1.0～1.5%
Lecithin 0.5～3.0%
Vitamin E 1.5～4.0%
The powder that this prescription can be made bathing uses.And this prescription has been furnished with Aloe vulgaris, hyaluronic acid, cholesterol, vitamin E, and its effect is respectively the moisturizing of whitening, preserve moisture, and the matching surface activating agent makes the moisturizing nutritional labeling infiltration skin of whitening and preserve moisture, and reaches ideal effect.In use, can pour in the warm water that fills 100～150 liters, after dissolving, get final product bathing.
Component and percentage by weight that second kind of optimization formula comprises are as follows:
Sodium bicarbonate 2.0～28.0%
Strontium chloride 5.0～6.0%
Metasilicic acid 26.0～28.0%
Sodium fluoride 0.5～5.0%
Sodium chloride 10.0～12.0%
Sodium bromide 8.0～10.0%
Cosan 15.0～16.0%
Salicylic acid 2.0～4.0%
Malic acid 2.0～3.0%
Hydroxyethyl-cellulose 0.5～4.0%
Nature moisturizing factor 0.5～1.5%
Arbutin 0～1.5%
Superoxide dismutase 0.5～2.0%
Vitamin C 2.0～5.0%
The emulsifying agent that this prescription can be made bathing uses.Wherein, hydroxyethyl-cellulose is a surfactant; Nature moisturizing factor is the best composition of moisturizing of preserving moisture; Arbutin is the Pear Power skin both, has again to suppress the effect that melanin generates; Superoxide dismutase is the active factors of deep and thorough skin; Vitamin is an antioxidant, can play again to prevent that other has the oxidation in high temperature of functional nutrient component; In use, can pour in the warm water that fills 100～150 liters, after dissolving, get final product bathing.
Component and percentage by weight that the third optimization formula comprises are as follows:
Sodium bicarbonate 2.0～31.5%
Metasilicic acid 26.0～27.0%
Sodium chloride 10.0～11.0%
Borax 1.5～3.0%
Salicylic acid 1.0～3.5%
Fruit acid 1.0～3.0%
Matrii Sulfas Exsiccatus 5.0～10.0%
Magnesium chloride 2.5～3.5%
Potassium chloride 5.0～10.0%
Sodium carbonate 15.0～16.0%
Cholesterol 0.5～3.0%
Fatty acid 0.5～4.0%
Endothelin antagonist 0.5～4.0%
The unguentum that this prescription can be made bathing uses.Wherein, cholesterol is a surfactant component; Fatty acid is the composition of preserving moisture; The Endothelin antagonist is the component of whitening.In use, can pour in the warm water that fills 100～150 liters, after dissolving, get final product bathing.
Embodiment one
Get sodium bicarbonate 29.0%, metaboric acid 5.0%, strontium chloride 5.0%, metasilicic acid 26.0%, sodium chloride 10.0%, salicylic acid 1.0%, malic acid 1.0%, Aloe 20.0%, hyaluronic acid 1.0%, lecithin 0.5%, vitamin E 1.5% is made powder, pours in 150 kilograms the warm water, its water temperature is 38 ℃, gets final product bathing after the dissolving that stirs.After 20 minutes bathing test, dry health with bath towel, after 1 hour, observe its skin moisturizing exquisiteness, and high resilience.
Embodiment two
Get sodium bicarbonate 5.0%, metaboric acid 8.0%, strontium chloride 8.0%, metasilicic acid 28.0%, sodium chloride 12.0%, salicylic acid 4.5%, malic acid 5.0%, Aloe 22.0%, hyaluronic acid 1.5%, lecithin 3.0%, vitamin E 4.0% grade is made Emulsion, pour in 150 kilograms the warm water, its water temperature is 35 ℃, gets final product bathing after the dissolving that stirs.After 20 minutes bathing test, dry health with bath towel, after 1 hour, to observe, its skin moistens fine and smooth equally, and high resilience.
Embodiment three
Get sodium bicarbonate 28.0%, strontium chloride 5.0%, metasilicic acid 26.0%, sodium fluoride 0.5%, sodium chloride 10.0%, sodium bromide 8.0%, Cosan 15.0, salicylic acid 2.0%, malic acid 2.0%, hydroxyethyl-cellulose 0.5%, nature moisturizing factor 0.5%, arbutin 0.5%, superoxide dismutase 0.5%, vitamin C 2.0% grade is made emulsifying agent, pours in 150 kilograms the warm water, its water temperature is 35 ℃, gets final product bathing after the dissolving that stirs.After 20 minutes bathing test, dry health with bath towel, after 1 hour, observe, remove skin and have the exquisiteness of moistening, and outside the high resilience, sensation skin returns to high resilience, the moisturizing effect of preserving moisture is remarkable, the effect of life-time service Pear Power.
According to the above embodiments,, remarkable result of the present invention is described with the experiment mode of comparing.Experiment one is dry powder bathing agent.The setting of bathing time is that general each bathing does not surpass 20 minutes according to the bubble natural hot spring, and preferably bathing is 15 minutes, and the time of bathing must be no more than secondary weekly at interval.Its reason is that the mineral composition that contains of natural hot spring water is a lot, and is very strong to the stimulation of skin, the bathing overlong time, and the moisture of skin the inside will be got rid of, and the moisture of excessive eliminating skin because defat is too serious, will make skin seem dry.Judge whether exsiccant standard is skin, belongs to dry skin between the measurement range 45-50, and scope belongs to the neutral skin at 50-56, and scope belongs to oily skin at 56-66.Experimental situation is indoor the carrying out at 25 ℃, and its experimental facilities is the intelligent control of a constant temperature bathtub, and the equipment of test skin is NAUMP specialty skin detection analytical system, can obtain the percent water value of test place skin.
Table one
According to the interpretation in the table, 35 ℃ of the water temperatures of bathing for the first time, bathing 15 minutes does not see that with an eye direct observation skin has dry-out phenomenon when just going out to bathe, and dries behind the moisture on one's body after tested, its skin index is 51 to be neutrality.Bathing for the second time is at interval after two days, the 3rd heaven-made bathing experiment second time, the water temperature of current experiment bathing is higher a little, water temperature is 38 ℃, bathing time lengthening 5 minutes does not see that with an eye direct observation skin has dry-out phenomenon when going out to bathe, but dries behind on one's body the moisture after tested, its skin index is 48 to be dryness, shows that skin defat dehydration seems dry.Shi Yan time is after testing a week for the second time for the third time, the bathing water temperature of this experiment is adjusted to 40 ℃, but the bathing time ratio lacks 5 minutes for the second time, do not see that with the eye direct observation skin has dry-out phenomenon when going out to bathe yet, but dry behind the moisture on one's body after tested, its skin index is 43.5 to be dryness, shows that skin defat dehydration is serious, and xerosis cutis is obvious.Crossed three heaven-made the 4th experiments, the bathing time still is 15 minutes, 35 ℃ of water temperatures, may be seen indistinctly and have skin that dry sensation is arranged with an eye direct observation when going out to bathe, dry behind the moisture on one's body after tested, its skin index is 41 to be dryness, show that skin defat dehydration is serious, xerosis cutis is very obvious.
Conclusion does not add the bathing agent of the component of preserving moisture, no matter bathing and the length of blanking time, and the height that water temperature is regulated during bathing all can make skin dehydration, can not lightheartedly use at any time.
Experiment table two
According to the interpretation in the table, 35 ℃ of the water temperatures of bathing for the first time, bathing 15 minutes does not see that with an eye direct observation skin has dry-out phenomenon when just going out to bathe, and dries behind the moisture on one's body after tested, its skin index is 51 to be neutrality.Bathing for the second time is at interval after two days, the 3rd heaven-made bathing experiment second time, the water temperature of current experiment bathing is higher a little, water temperature is 40 ℃, and bathing time lengthening 3 minutes does not see that with the eye direct observation skin has dry-out phenomenon when going out to bathe, but dry behind the moisture on one's body after tested, its skin index is 52 to be neutral, shows that skin moisture-keeping moisture increases index, illustrates that this bathing agent has certain effect to skin moisture-keeping.Shi Yan time is after testing two days for the second time for the third time, the bathing water temperature of this experiment is adjusted to 36 ℃, but bathing time ratio many 2 minutes for the second time, do not see that with the eye direct observation skin has dry-out phenomenon when going out to bathe yet, but dry behind the moisture on one's body after tested, its skin index is 52.5 to be neutral, shows that skin dehydration divides not only not influence, makes the skin moisture-keeping effect more obvious on the contrary.Continued experiment in second day, the 4th experiment, the bathing time still is 25 minutes, 36 ℃ of water temperatures have moisture feeling with eye direct observation skin when going out to bathe, and dry behind the moisture on one's body after tested, its skin index is 53.1 to be neutral, show that skin moisture-keeping is not only stable, and the skin index increases constantly, effect is still remarkable.After having spent a week, 40 ℃ of the water temperatures of the 5th experiment, the bathing time prolongs 5 minutes on the 4th time basis, on one's body globule nature landing when going out to bathe has moist soapy feeling with a direct observation skin, dries behind the moisture on one's body after tested, its skin index is 53 to be neutral, show that skin moisture-keeping is stable, and the beautiful gloss of skin, effect is very good.
Conclusion is added with the bathing agent component of skin-moisturizing, skin and antioxidant, no matter bathing and the length of blanking time, the height that water temperature is regulated during bathing, all to skin without any influence, can lightheartedly use at any time.
The present invention has the preparation method of the bathing agent of skin-moisturizing, skin-whitening function, also comprises the steps:
Step 1: solid each component is ground to form 120～200 order fine powders respectively;
Step 2: the solution Organic substance is poured in the clean container, in container, added the fine powder of getting ready then and stir;
Step 3: after stirring, dewater;
Step 4: the fine powder after the dehydration is sent in the drying machine dried then;
Step 5: the fine powder after will drying fill according to quantity promptly gets the powder goods of bathing agent.
In the above-mentioned preparation method,, promptly can be made into tablet, Emulsion and unguentum stirring in the adjuvant of the adding of the fine powder after the dehydration after dissolving is got ready.During the preparation tablet, send into and strike out definite shape in the mould, the direct fill of Emulsion or unguentum gets final product.
At least contain among the present invention more than one natural surfactant, at least contain more than one natural moisture preserving composition, contain more than one natural whiting composition at least, therefore the health-care effect that not only has the bathing natural hot spring water, and can regulate the metabolism of skin, prevent skin aging, to the skin moisture-keeping moisturizing, make the beautiful gloss of skin and whitening effect.
Claims (5)
1. bathing agent with skin-moisturizing, skin-whitening function is characterized in that the component and the percentage by weight that comprise are as follows:
Sodium bicarbonate 2.0～40.0%
Metaboric acid 2.5～8.0%
Strontium chloride 5.0～10.0%
Metasilicic acid 26.0～30.0%
Sodium chloride 10.0～17.0%
Cosan 13.0～20.0%
Borax 1.5～3.0%
Molten keratoprotein agent 1.0～5.0%
Malic acid 1.0～5.0%.
2. the preparation method with bathing agent of skin-moisturizing, skin-whitening function according to claim 1 is characterized in that it may further comprise the steps:
Step 1: solid each component is ground to form 120～200 order fine powders respectively;
Step 2: the solution Organic substance is poured in the clean container, in container, added the fine powder of getting ready then and stir;
Step 3: after stirring, dewater;
Step 4: the fine powder after the dehydration is sent in the drying machine dried then;
Step 5: the fine powder after will drying fill according to quantity promptly gets the powder goods of bathing agent;
Step 6: as required, also can promptly can be made into tablet, Emulsion and unguentum stirring in the adjuvant of the adding of the fine powder after the dehydration after dissolving is got ready.
3. the preparation method with bathing agent of skin-moisturizing, skin-whitening function according to claim 2 is characterized in that: during the preparation tablet, send into and strike out definite shape in the mould.
4. the bathing agent with skin-moisturizing, skin-whitening function according to claim 1 is characterized in that described molten keratoprotein agent is salicylic acid and salt thereof.
5. bathing agent with skin-moisturizing, skin-whitening function is characterized in that the weight percentages of components of this prescription is as follows:
Sodium bicarbonate 5.0～29.0%
Metaboric acid 5.0～8.0%
Metasilicic acid 26.0～28.0%
Strontium chloride 5.0～8.0%
Sodium chloride 10.0～12.0%
Salicylic acid 1.0～4.5%
Malic acid 1.0～5.0%
Aloe 20.0～22.0%
Hyaluronic acid 1.0～1.5%
Lecithin 0.5～3.0%
Vitamin E 1.5～4.0%.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102634419B (en) * | 2012-04-01 | 2013-10-16 | 亚森·克力木 | Method for preparing washing product with health care function |
| CN104042462A (en) * | 2013-03-16 | 2014-09-17 | 李江水 | Preparation and production of sulfurous spring powdery bath salt |
| CN104288028A (en) * | 2014-09-28 | 2015-01-21 | 青岛康和食品有限公司 | Moisturizing bath foam |
| CN106726790B (en) * | 2016-08-31 | 2020-06-05 | 广州市巧美化妆品有限公司 | Hot spring mineral humectant and preparation method thereof |
| EP3706675B1 (en) * | 2017-11-08 | 2023-07-12 | Coloplast A/S | An adhesive wafer with a neutralizer matrix |
| CN109010120A (en) * | 2018-08-28 | 2018-12-18 | 上海优康化妆品有限公司 | Aqueous Victoria C bilayer Essence, preparation method and application method |
| CN115590798B (en) * | 2022-06-14 | 2023-06-16 | 中国科学院过程工程研究所 | Double-component bath lotion with anti-allergy and skin tendering effects and preparation method thereof |
| CN115414265A (en) * | 2022-08-29 | 2022-12-02 | 中国科学院过程工程研究所 | Composition and face cream with effects of color correction, skin tendering and moisturizing and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1270805A (en) * | 1999-04-15 | 2000-10-25 | 殷季侠 | Hot spring bathing tablet and its production process |
| CN1504181A (en) * | 2002-11-28 | 2004-06-16 | 漳州艾妮沐浴用品有限公司 | Agent for hot spring bath and its preparation method |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1270805A (en) * | 1999-04-15 | 2000-10-25 | 殷季侠 | Hot spring bathing tablet and its production process |
| CN1504181A (en) * | 2002-11-28 | 2004-06-16 | 漳州艾妮沐浴用品有限公司 | Agent for hot spring bath and its preparation method |
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