CN1768761A - Method for producing turkey bone collagen powder - Google Patents
Method for producing turkey bone collagen powder Download PDFInfo
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- CN1768761A CN1768761A CNA2005100104618A CN200510010461A CN1768761A CN 1768761 A CN1768761 A CN 1768761A CN A2005100104618 A CNA2005100104618 A CN A2005100104618A CN 200510010461 A CN200510010461 A CN 200510010461A CN 1768761 A CN1768761 A CN 1768761A
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Abstract
The invention relates to a method for producing turkey bone collagen powder, which can solve the problem of former method which can not supply in large amount. The producing processes comprises: (1) washing and freezing fresh turkey bone; (2) disintegrating; (3) dipping; (4) cooling and filtering; (5) vacuum concentration; (6) adding nutrients to be mixed uniformly at high pressure; (7) spraying and drying. The invention uses the turkey bone as raw material which has lower cost, and the turkey has fast growth speed, and short breeding cycle, which can be cultured in large scale to meet the large demand of industry.
Description
Technical field
The present invention relates to a kind of production method of bone collagen powder.
Background technology
Along with the raising of people's living standard, expanding economy, people's nourishing healthy, the requirement kept fit of replenishing the calcium are made bone collagen powder more and more strongly and in the past and are adopted the bone of cattle, pig, deer, yak or large-scale domestic animal as raw material more.But large-scale domestic animal poor growth such as cattle, pig, the breeding cycle is long, has influenced the long-term a large amount of supplies of raw material.
Summary of the invention
The objective of the invention is to make the problem that the bone collagen powder raw material can't be supplied for a long time in a large number in order to solve in the past, and the production method of a kind of turkey bone collagen powder that provides.Technological process of the present invention is undertaken by following step: (one) cleans with clear water through the fresh turkey bone of health quarantine, is being lower than quick freezing under-25 ℃ the condition; (2) refrigerated turkey bone is ground into osseous granules, and flush away dirt, blood and slime, bone slag; (3) add the acetic acid that concentration is 9-10% after the osseous granules of cleaning being put into 100 ℃ clear water, lixiviate 4h-6h under 90-100 ℃, the condition of 0.1MPa; (4) lixiviating solution is cooled to 40 ℃ of-50 ℃ of after-filtration; (5) filtrate vacuum concentration 2-4h in 45 ℃-50 ℃, solid concentration reaches 5-8%; (6) nutrient substance is dissolved in the concentrated solution, mix homogeneously, the reuse high pressure homogenizer carries out homogenizing; (7) concentrated solution behind the homogenizing carries out spray drying again, and cooling is finished product.The present invention adopts turkey bone to make not only low price of raw material, and the turkey fast growth, and the breeding cycle is short, and extensive raising of being more convenient for can be satisfied the demand of the long-term mass production bone collagen powder of industry.
The finished product turkey bone collagen powder that the present invention produces is nutritious, and calcium content is 120mg/g-250mg/g; Phosphorus content is 90mg/g-200mg/g; Hydroxyproline is 2mg/g-10mg/g; Phosphopeptide caseinate is 1mg/g-4mg/g.Technology of the present invention is simple, and is with short production cycle, and the turkey bone collagen powder of producing can also carry out deep processing as raw material production ossein electuary and bone collagenous soft capsule.
The specific embodiment
The specific embodiment one: present embodiment is undertaken by following step: (one) will clean with clear water through the fresh turkey bone of health quarantine, be lower than quick freezing under-25 ℃ the condition; (2) turkey bone after freezing is ground into the osseous granules that granularity is 1cm-2cm, and flush away dirt, blood and slime, bone slag; (3) add the acetic acid that concentration is 9-10% after the osseous granules of cleaning being put into 100 ℃ clear water, lixiviate 4h-6h under 90-100 ℃, the condition of 0.1MPa; (4) lixiviating solution is cooled to 40 ℃ of-50 ℃ of after-filtration; (5) filtrate vacuum concentration 2-4h in 45 ℃-50 ℃, solid concentration reaches 5-8%; (6) nutrient substance phosphopeptide caseinate, vitamin E, dextrin, soybean protein isolate, glucose and whey powder are dissolved in the concentrated solution, mix homogeneously, the reuse high pressure homogenizer carries out double-stage homogenization, homogenizing temperature is 55-60 ℃, one-level homogenization pressure 10-15MPa, double-stage homogenization pressure 25-30MPa; (7) concentrated solution behind the homogenizing carries out spray drying again, and cooling is finished product.Fresh turkey bone is being lower than quick freezing under-25 ℃ the condition in the present embodiment, is convenient to the pulverizing of bone.
The specific embodiment two: the difference of the present embodiment and the specific embodiment one is: the nutrient substance that adds in the step (six) accounts for the concentrated solution percentage by weight and is respectively phosphopeptide caseinate 0.2%-0.4%, vitamin E 0.1%-0.2%, dextrin 5.0%-7.0%, soybean protein isolate 1.0%-2.0%, glucose 3.0%-5.0%, whey powder 6.0%-8.0%.
The specific embodiment three: the difference of the present embodiment and the specific embodiment one, two is: the nutrient substance that adds in the step (six) accounts for the concentrated solution percentage by weight and is respectively phosphopeptide caseinate 0.3%, vitamin E 0.15%, dextrin 6%, soybean protein isolate 1.5%, glucose 4%, whey powder 7%.
The specific embodiment four: the difference of the present embodiment and the specific embodiment three is: the acetic acid that the middle concentration of step (three) is 9-10% adds in the ratio of putting 1mL-3mL in every 100g bone and the water mixed liquid.
The specific embodiment five: the difference of the present embodiment and the specific embodiment four is: the weight ratio of osseous granules and clear water is 1 in the step (three): 1-1: 4.
The specific embodiment six: the difference of the present embodiment and the specific embodiment two is: filtrate vacuum concentration under 49 ℃ condition in the step (five).
The specific embodiment seven: the difference of the present embodiment and the specific embodiment one is: turkey bone collagen powder is carried out deep processing, make bone collagenous soft capsule.The processing technology of its bone collagenous soft capsule is as follows:
The distilled water that a, gelatin add 0.8 times of own vol makes it to expand;
B, weighing account for the glycerol of gelatin and distilled water total weight percent 0.5-1%;
In c, placing of the water glue jar, be heated to 70-80 ℃, add expansible gelatin again, stir, insulation 1h-2h 0.5 times of glycerol and gelatin volume;
D, evacuation are got rid of the air in the glue, by making adhesive tape in the automatic rotation system capsule machine;
The composition of e, bone collagenous soft capsule is formed by following weight ratio: 1 part of turkey bone collagen powder, soybean oil 1-5 part;
F, the raw material stirring in the component is even makes the soft capsule first product by automatic rotation system capsule machine, and room temperature is 20 ℃-24 ℃ in the production process, relative air humidity 35%;
G, soft capsule first product enter dry in the drying machine, typing, 30 ℃-35 ℃ of baking temperatures, and relative air humidity 20%, dry 4h make the moisture of soft capsule shell reduce to 6%-8%;
H, be that 5: 1 ethanol and acetone mixed liquor inject and wash pill wiping machine with volume ratio, the oil reservoir of flush away capsule surface, dry up washing liquid again, dry 30h in the hothouse of 21 ℃-24 ℃ of temperature of immigration, relative humidity 30%-40% promptly obtains the bone collagenous soft capsule finished product.
The turkey bone collagen powder that adopts the present invention to produce is nutritious as the bone collagenous soft capsule that raw material produces, and is rich in collagen protein, can promote the metabolism of cell, bone density improving.
Claims (7)
1, a kind of production method of turkey bone collagen powder is characterized in that its technological process is undertaken by following step: (one) cleans with clear water through the fresh turkey bone of health quarantine, is being lower than quick freezing under-25 ℃ the condition; (2) refrigerated turkey bone is ground into osseous granules, and flush away dirt, blood and slime, bone slag; (3) add the acetic acid that concentration is 9-10% after the osseous granules of cleaning being put into 100 ℃ clear water, lixiviate 4h-6h under 90-100 ℃, the condition of 0.1MPa; (4) lixiviating solution is cooled to 40 ℃ of-50 ℃ of after-filtration; (5) filtrate vacuum concentration 2-4h in 45 ℃-50 ℃, solid concentration reaches 5-8%; (6) nutrient substance is dissolved in the concentrated solution, mix homogeneously, the reuse high pressure homogenizer carries out homogenizing; (7) concentrated solution behind the homogenizing carries out spray drying again, and cooling is finished product.
2, the production method of turkey bone collagen powder according to claim 1 is characterized in that the osseous granules granularity is 1cm-2cm in the step ().
3, the production method of turkey bone collagen powder according to claim 1 is characterized in that the weight ratio of middle osseous granules of step (three) and clear water is 1: 1-1: 4.
4, the production method of turkey bone collagen powder according to claim 1 is characterized in that adding concentration in the ratio of putting 1mL-3mL in every 100g bone and the water mixed liquid in the step (three) is the acetic acid of 9-10%.
5, the production method of turkey bone collagen powder according to claim 1 is characterized in that the nutrient substance that is added in the step (six) mainly is made up of phosphopeptide caseinate, vitamin E, dextrin, soybean protein isolate, glucose and whey powder.
6, the production method of turkey bone collagen powder according to claim 1 or 5 is characterized in that the nutrient substance that adds in the step (six) accounts for the concentrated solution percentage by weight and is respectively phosphopeptide caseinate 0.2%-0.4%, vitamin E 0.1%-0.2%, dextrin 5.0%-7.0%, soybean protein isolate 1.0%-2.0%, glucose 3.0%-5.0%, whey powder 6.0%-8.0%.
7, the production method of turkey bone collagen powder according to claim 1 is characterized in that step (six) mesohigh homogenizing adopts double-stage homogenization, and homogenizing temperature is 55-60 ℃, one-level homogenization pressure 10-15MPa, double-stage homogenization pressure 25-30MPa.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2005100104618A CN1327850C (en) | 2005-10-21 | 2005-10-21 | Method for producing turkey bone collagen powder |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2005100104618A CN1327850C (en) | 2005-10-21 | 2005-10-21 | Method for producing turkey bone collagen powder |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1768761A true CN1768761A (en) | 2006-05-10 |
| CN1327850C CN1327850C (en) | 2007-07-25 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2005100104618A Expired - Fee Related CN1327850C (en) | 2005-10-21 | 2005-10-21 | Method for producing turkey bone collagen powder |
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| CN (1) | CN1327850C (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104336190A (en) * | 2013-08-07 | 2015-02-11 | 青岛博研达工业技术研究所(普通合伙) | Method for making collagen protein film coproduction organic compounds |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1151222C (en) * | 2001-04-08 | 2004-05-26 | 内蒙古草原兴发股份有限公司 | Process for preparing bone collagen |
-
2005
- 2005-10-21 CN CNB2005100104618A patent/CN1327850C/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104336190A (en) * | 2013-08-07 | 2015-02-11 | 青岛博研达工业技术研究所(普通合伙) | Method for making collagen protein film coproduction organic compounds |
| CN104336190B (en) * | 2013-08-07 | 2018-07-17 | 青岛博研达工业技术研究所(普通合伙) | A kind of method of glue collagen film coproduction organic matter |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1327850C (en) | 2007-07-25 |
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