CN1626728A - Method for preparing environmental protective wool easy of health and easy of nurse - Google Patents
Method for preparing environmental protective wool easy of health and easy of nurse Download PDFInfo
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- CN1626728A CN1626728A CN 200310109259 CN200310109259A CN1626728A CN 1626728 A CN1626728 A CN 1626728A CN 200310109259 CN200310109259 CN 200310109259 CN 200310109259 A CN200310109259 A CN 200310109259A CN 1626728 A CN1626728 A CN 1626728A
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Abstract
The invention relates to a method for preparing wool which is beneficial to health of human body, easy to maintain and favourable to environmental protection. Said method includes the following steps: twisting, prewashing, metal treatment, oxidation treatment, alkali treatment, alkali reduction, reduction treatment, washing with hot water, acid treatment, washing with hot water, softening treatment and drying treatment.
Description
Technical field
The present invention relates to a kind of preparation method of wool, relate in particular to the preparation method of a kind of E-WOOL (easily healthy, easily nursing, environmental protection) wool.
Background technology
Because the wool surface exists keratin protein layer (scale) structure, so, shortcomings such as bad, the easy balling-up of the performance that contracts, hygroscopicity difference washed.In order to overcome these shortcomings, people have adopted chemically treated method to process at present.But the most universal shrink-resistant finish method is to adopt salt element (as: liquid chlorine, hypochlorous acid etc.) now, and the salt element is the reason material that causes dioxin to take place, and earth environment, source mill's workers'health are all had harm.
International community shows that to the care of earth environment the consciousness to keeping human health improves rapidly, and especially various countries use the laws and regulations of harmful substance to be gradually improved to restriction and be strict, positive anxious the treating in correction of some ideas in the past.
Because the salt element uses in a large number as the bleaching agent of paper, paper pulp, and water quality is had adverse effect, all there is certain regulation restriction countries in the world to its use.Use European Community's eco-label (Eco-label) etc. as European Union about authorizing textile product.
Summary of the invention
The technical issues that need to address of the present invention have provided a kind of preparation method of E-WOOL wool, are intended to solve at present in the process of preparation wool, adopt the oxidation of chlorine class medicament and cause the defective of contaminated environment.
In order to solve the problems of the technologies described above, the present invention realizes by following steps:
Twist thread;
Prewashing;
Metal is handled;
Oxidation processes;
Alkali treatment;
The alkali reduction;
Reduction is handled;
Hot wash;
Acid treatment;
Hot wash;
Soft treatment;
Oven dry is handled.
Compared with prior art, the invention has the beneficial effects as follows: owing to be effect by physically, and do not adopt chlorine class medicament in the oxidation process, accomplished easy health truly, easily nursing and environmental protection.
The specific embodiment
Embodiment 1
Twist thread 1;
Prewashing 2;
Metal handles 3;
Oxidation processes 4;
Alkali treatment 5;
Alkali reduction 6;
Reduction handles 7;
Hot wash 8;
Acid treatment 9;
Hot wash 10;
Soft treatment 11;
Oven dry handles 12.
In step 1, realize by following steps:
Bar heavily handles 101;
Twisting handles 102;
In step 101, according to the fibrousness of raw material, the weight of the strip that processing is put is done following adjustment:
Raw fiber degree 17.5-22.0, the heavy 28g/m of bar;
In step 102, revolution is 8.5 rev/mins;
In step 2, adopt surfactant, concentration is 0.09%sol; Lotion, concentration are 0.09%sol; Defoamer, concentration are 0.03%sol; Temperature is 35 °, and required time is 1.3 minutes;
In step 3, adopt copper sulphate, concentration is 0.03%sol; Zinc sulfate, concentration are 0.020%sol; Defoamer, concentration are 0.03%sol; Adopt surfactant, concentration is 0.13%sol; Temperature is 20 °, and required time is 3 minutes;
In step 4, adopt hydrogen peroxide, concentration is 15%sol; Single potassium hydrogen persulfate, concentration are 1.5%sol; Surfactant, concentration are 0.08%sol; Defoamer, concentration are 0.03%sol; Temperature is 15 °, and required time is 0.8 minute;
In step 5, adopt sodium carbonate, concentration is 1.5%sol; Defoamer, concentration are 0.03%sol; Temperature is 65 °, and required time is 3 minutes;
In step 6, adopt sodium carbonate, concentration is 0.4%sol; Sodium sulfite, concentration are 0.15%sol; Surfactant, concentration are 0.008%sol; Temperature is 25 °, and required time is 3 minutes;
In step 7, adopt sodium sulfite, concentration is 0.4%sol; Sodium hydrogensulfite, concentration are 0.4%sol; Wool protective agent, concentration are 0.04%sol; Temperature is 30 °, and required time is 3 minutes;
In step 8, the hot water temperature is 30 °, and required time is 0.8 minute;
In step 9, adopt formic acid, concentration is 0.4%sol; Temperature is 30 °, and required time is 0.8 minute:
In step 10, the hot water temperature is 30 °, and required time is 4 minutes;
In step 11, adopt softener, concentration is 1.0%sol; Temperature is 30 °, and required time is 0.8 minute.
Embodiment 2
Step is with embodiment 1, wherein:
In step 102, revolution is 9.0 rev/mins.
Embodiment 3
Step is with embodiment 1, wherein:
In step 102, revolution is 9.5 rev/mins.
Embodiment 4
Step is with embodiment 1, wherein:
In step 101, raw fiber degree 22.1-25.0, the heavy 30g/m of bar;
In step 102, revolution is 9.0 rev/mins.
Embodiment 5
Step is with embodiment 4, wherein:
In step 102, revolution is 9.5 rev/mins.
Embodiment 6
Step is with embodiment 4, wherein:
In step 102, revolution is 10.0 rev/mins.
Embodiment 7
Step is with embodiment 1, wherein:
In step 101, the raw fiber degree is more than 25.1, and bar weighs 32g/m;
In step 102, revolution is 9.5 rev/mins.
Embodiment 8
Step is with embodiment 7, wherein:
In step 102, revolution is 10.0 rev/mins.
Embodiment 9
Step is with embodiment 7, wherein:
In step 102, revolution is 11.0 rev/mins.
Embodiment 10
Step is with embodiment 1, wherein:
In step 2, adopt surfactant, concentration is 1.0%sol; Lotion, concentration are 1.0%sol; Defoamer, concentration are 0.05%sol; Temperature is 40 °, and required time is 1.5 minutes;
In step 3, adopt copper sulphate, concentration is 0.04%sol; Zinc sulfate, concentration are 0.025%sol; Defoamer, concentration are 0.05%sol; Adopt surfactant, concentration is 0.15%sol; Temperature is 25 °, and required time is 3.5 minutes;
In step 4, adopt hydrogen peroxide, concentration is 20%sol; Single potassium hydrogen persulfate, concentration are 2.0%sol; Surfactant, concentration are 0.1%sol; Defoamer, concentration are 0.05%sol; Temperature is 20 °, and required time is 1.0 minutes;
In step 5, adopt sodium carbonate, concentration is 2.0%sol; Defoamer, concentration are 0.05%sol; Temperature is 70 °, and required time is 4 minutes;
In step 6, adopt sodium carbonate, concentration is 0.5%sol; Sodium sulfite, concentration are 0.2%sol; Surfactant, concentration are 0.01%sol; Temperature is 30 °, and required time is 4 minutes;
In step 7, adopt sodium sulfite, concentration is 0.5%sol; Sodium hydrogensulfite, concentration are 0.5%sol; Wool protective agent, concentration are 0.05%sol; Temperature is 40 °, and required time is 4 minutes;
In step 8, the hot water temperature is 40 °, and required time is 1 minute;
In step 9, adopt formic acid, concentration is 0.5%sol; Temperature is 40 °, and required time is 1 minute;
In step 10, the hot water temperature is 40 °, and required time is 5 minutes;
In step 11, adopt softener, concentration is 1.5%sol; Temperature is 40 °, and required time is 1 minute.
Embodiment 11
Step is with embodiment 1, wherein:
In step 2, adopt surfactant, concentration is 1.1%sol; Lotion, concentration are 1.1%sol; Defoamer, concentration are 0.07%sol; Temperature is 45 °, and required time is 1.7 minutes;
In step 3, adopt copper sulphate, concentration is 0.05%sol; Zinc sulfate, concentration are 0.030%sol; Defoamer, concentration are 0.07%sol; Adopt surfactant, concentration is 0.17%sol; Temperature is 30 °, and required time is 4 minutes;
In step 4, adopt hydrogen peroxide, concentration is 25%sol; Single potassium hydrogen persulfate, concentration are 2.5%sol; Surfactant, concentration are 0.12%sol; Defoamer, concentration are 0.07%sol; Temperature is 25 °, and required time is 1.2 minutes;
In step 5, adopt sodium carbonate, concentration is 2.5%sol; Defoamer, concentration are 0.07%sol; Temperature is 75 °, and required time is 5 minutes;
In step 6, adopt sodium carbonate, concentration is 0.6%sol; Sodium sulfite, concentration are 0.25%sol; Surfactant, concentration are 0.012%sol; Temperature is 35 °, and required time is 5 minutes;
In step 7, adopt sodium sulfite, concentration is 0.6%sol; Sodium hydrogensulfite, concentration are 0.6%sol; Wool protective agent, concentration are 0.06%sol; Temperature is 50 °, and required time is 5 minutes;
In step 8, the hot water temperature is 50 °, and required time is 1.2 minutes;
In step 9, adopt formic acid, concentration is 0.6%sol; Temperature is 50 °, and required time is 1.2 minutes;
In step 10, the hot water temperature is 50 °, and required time is 6 minutes;
In step 11, adopt softener, concentration is 2.0%sol; Temperature is 50 °, and required time is 1.2 minutes.
Embodiment 12
Step is with embodiment 2, wherein:
Adopt surfactant, concentration is 1.0%sol; Lotion, concentration are 1.0%sol; Defoamer, concentration are 0.05%sol; Temperature is 40 °, and required time is 1.5 minutes;
In step 3, adopt copper sulphate, concentration is 0.04%sol; Zinc sulfate, concentration are 0.025%sol; Defoamer, concentration are 0.05%sol; Adopt surfactant, concentration is 0.15%sol; Temperature is 25 °, and required time is 3.5 minutes;
In step 4, adopt hydrogen peroxide, concentration is 20%sol; Single potassium hydrogen persulfate, concentration are 2.0%sol; Surfactant, concentration are 0.1%sol; Defoamer, concentration are 0.05%sol; Temperature is 20 °, and required time is 1.0 minutes;
In step 5, adopt sodium carbonate, concentration is 2.0%sol; Defoamer, concentration are 0.05%sol; Temperature is 70 °, and required time is 4 minutes;
In step 6, adopt sodium carbonate, concentration is 0.5%sol; Sodium sulfite, concentration are 0.2%sol; Surfactant, concentration are 0.01%sol; Temperature is 30 °, and required time is 4 minutes;
In step 7, adopt sodium sulfite, concentration is 0.5%sol; Sodium hydrogensulfite, concentration are 0.5%sol; Wool protective agent, concentration are 0.05%sol; Temperature is 40 °, and required time is 4 minutes;
In step 8, the hot water temperature is 40 °, and required time is 1 minute;
In step 9, adopt formic acid, concentration is 0.5%sol; Temperature is 40 °, and required time is 1 minute;
In step 10, the hot water temperature is 40 °, and required time is 5 minutes;
In step 11, adopt softener, concentration is 1.5%sol; Temperature is 40 °, and required time is 1 minute.
Embodiment 13
Step is with embodiment 3, wherein:
In step 2, adopt surfactant, concentration is 1.1%sol; Lotion, concentration are 1.1%sol; Defoamer, concentration are 0.07%sol; Temperature is 45 °, and required time is 1.7 minutes;
In step 3, adopt copper sulphate, concentration is 0.05%sol; Zinc sulfate, concentration are 0.030%sol; Defoamer, concentration are 0.07%sol; Adopt surfactant, concentration is 0.17%sol; Temperature is 30 °, and required time is 4 minutes;
In step 4, adopt hydrogen peroxide, concentration is 25%sol; Single potassium hydrogen persulfate, concentration are 2.5%sol; Surfactant, concentration are 0.12%sol; Defoamer, concentration are 0.07%sol; Temperature is 25 °, and required time is 1.2 minutes;
In step 5, adopt sodium carbonate, concentration is 2.5%sol; Defoamer, concentration are 0.07%sol; Temperature is 75 °, and required time is 5 minutes;
In step 6, adopt sodium carbonate, concentration is 0.6%sol; Sodium sulfite, concentration are 0.25%sol; Surfactant, concentration are 0.012%sol; Temperature is 35 °, and required time is 5 minutes;
In step 7, adopt sodium sulfite, concentration is 0.6%sol; Sodium hydrogensulfite, concentration are 0.6%sol; Wool protective agent, concentration are 0.06%sol; Temperature is 50 °, and required time is 5 minutes;
In step 8, the hot water temperature is 50 °, and required time is 1.2 minutes;
In step 9, adopt formic acid, concentration is 0.6%sol; Temperature is 50 °, and required time is 1.2 minutes;
In step 10, the hot water temperature is 50 °, and required time is 6 minutes;
In step 11, adopt softener, concentration is 2.0%sol; Temperature is 50 °, and required time is 1.2 minutes.
Below principle of the present invention is described as follows:
Wool is dipped in the water, and firecoat is holded up, and adds the effect physically that is caused by the gear shape cylinder, makes the firecoat of holding up bigger, promotes the absorption of various chemical reagent, and reaching by the drawing-off filament simultaneously increases the purpose that firecoat is peeled off;
The present invention is the raw material that firecoat is holded up, with the metal is that catalyst is adsorbed in fiber surface, makes oxidant such as hydrogen peroxide carry out instantaneous oxidation reaction then in alkaline bath, by the expansive force and the heat generation of the oxygen that produces this moment, apply the effect of physical property simultaneously, peel off firecoat.
Claims (10)
1. easily healthy, easy preparation method of the wool of nursing, environmental protection is characterized in that may further comprise the steps:
Twist thread (1);
Prewashing (2);
Metal is handled (3);
Oxidation processes (4);
Alkali treatment (5);
Alkali reduction (6);
(7) are handled in reduction;
Hot wash (8);
Acid treatment (9);
Hot wash (10);
Soft treatment (11);
(12) are handled in oven dry.
2. the preparation method of the wool of easy health according to claim 1, easy nursing, environmental protection is characterized in that: described in step (1), realize by following steps:
Bar is heavily handled (101);
(102) are handled in twisting.
3. the preparation method of the wool of easy health according to claim 2, easy nursing, environmental protection is characterized in that:
In step (101), raw fiber degree 17.5-22.0, the heavy 28g/m of bar;
In step (102), revolution is 8.5-9.5 rev/min.
4. the preparation method of the wool of easy health according to claim 3, easy nursing, environmental protection, it is characterized in that: described revolution is 9.0 rev/mins.
5. the preparation method of the wool of easy health according to claim 2, easy nursing, environmental protection is characterized in that:
In step (101), raw fiber degree 22.1-25.0, the heavy 30g/m of bar;
In step (102), revolution is 9.0-10.0 rev/min.
6. the preparation method of the wool of easy health according to claim 5, easy nursing, environmental protection, it is characterized in that: described revolution is 9.5 rev/mins.
7. the preparation method of the wool of easy health according to claim 2, easy nursing, environmental protection is characterized in that:
In step (101), the raw fiber degree is more than 25.1, and bar weighs 32g/m;
In step (102), revolution is 9.5-11.0 rev/min.
8. the preparation method of the wool of easy health according to claim 7, easy nursing, environmental protection, it is characterized in that: described revolution is 10.0 rev/mins.
9. according to the described easy health of each claim in the claim 3 to 8, the easy preparation method of the wool of nursing, environmental protection, it is characterized in that:
In step (2), adopt surfactant, concentration is 0.09-1.1%sol; Lotion, concentration are 0.09-1.1%sol; Defoamer, concentration are 0.03-0.07%sol; Temperature is 35 °-45 °, and required time is 1.3-1.7 minute;
In step (3), adopt copper sulphate, concentration is 0.03-0.05%sol; Zinc sulfate, concentration are 0.020-0.030%sol; Defoamer, concentration are 0.03-0.07%sol; Adopt surfactant, concentration is 0.13-0.17%sol; Temperature is 20 °-30 °, and required time is 3-4 minute;
In step (4), adopt hydrogen peroxide, concentration is 15-25%sol; Single potassium hydrogen persulfate, concentration are 1.5-2.5%sol; Surfactant, concentration are 0.08-0.12%sol; Defoamer, concentration are 0.03-0.07%sol; Temperature is 15 °-25 °, and required time is 0.8-1.2 minute;
In step (5), adopt sodium carbonate, concentration is 1.5-2.5%sol; Defoamer, concentration are 0.03-0.07%sol; Temperature is 65 °-75 °, and required time is 3 minutes;
In step (6), adopt sodium carbonate, concentration is 0.4-0.6%sol; Sodium sulfite, concentration are 0.15-0.25%sol; Surfactant, concentration are 0.008-0.012%sol; Temperature is 25 °-35 °, and required time is 3-5 minute;
In step (7), adopt sodium sulfite, concentration is 0.4-0.6%sol; Sodium hydrogensulfite, concentration are 0.4-0.6%sol; Wool protective agent, concentration are 0.04-0.06%sol; Temperature is 30 °-50 °, and required time is 3-5 minute;
In step (8), the hot water temperature is 30 °-50 °, and required time is 0.8-1.2 minute;
In step (9), adopt formic acid, concentration is 0.4-0.6%sol; Temperature is 30 °-50 °, and required time is 0.8-1.2 minute;
In step (10), the hot water temperature is 30 °-50 °, and required time is 4-6 minute;
In step (11), adopt softener, concentration is 1.0-2.0%sol; Temperature is 30 °-50 °, and required time is 0.8-1.2 minute.
10. the preparation method of the wool of easy health according to claim 9, easy nursing, environmental protection is characterized in that:
In step (2), adopt surfactant, concentration is 1.0%sol; Lotion, concentration are 1.0%sol; Defoamer, concentration are 0.05%sol; Temperature is 40 °, and required time is 1.5 minutes;
In step (3), adopt copper sulphate, concentration is 0.04%sol; Zinc sulfate, concentration are 0.025%sol; Defoamer, concentration are 0.05%sol; Adopt surfactant, concentration is 0.15%sol; Temperature is 25 °, and required time is 3.5 minutes;
In step (4), adopt hydrogen peroxide, concentration is 20%sol; Single potassium hydrogen persulfate, concentration are 2.0%sol; Surfactant, concentration are 0.1%sol; Defoamer, concentration are 0.05%sol; Temperature is 20 °, and required time is 1.0 minutes;
In step (5), adopt sodium carbonate, concentration is 2.0%sol; Defoamer, concentration are 0.05%sol; Temperature is 70 °, and required time is 4 minutes;
In step (6), adopt sodium carbonate, concentration is 0.5%sol; Sodium sulfite, concentration are 0.2%sol; Surfactant, concentration are 0.01%sol; Temperature is 30 °, and required time is 4 minutes;
In step (7), adopt sodium sulfite, concentration is 0.5%sol; Sodium hydrogensulfite, concentration are 0.5%sol; Wool protective agent, concentration are 0.05%sol; Temperature is 40 °, and required time is 4 minutes;
In step (8), the hot water temperature is 40 °, and required time is 1 minute;
In step (9), adopt formic acid, concentration is 0.5%sol; Temperature is 40 °, and required time is 1 minute;
In step (10), the hot water temperature is 40 °, and required time is 5 minutes;
In step (11), adopt softener, concentration is 1.5%sol; Temperature is 40 °, and required time is 1 minute.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2003101092591A CN100352997C (en) | 2003-12-10 | 2003-12-10 | Method for preparing environmental protective wool easy of health and easy of nurse |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2003101092591A CN100352997C (en) | 2003-12-10 | 2003-12-10 | Method for preparing environmental protective wool easy of health and easy of nurse |
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| CN1626728A true CN1626728A (en) | 2005-06-15 |
| CN100352997C CN100352997C (en) | 2007-12-05 |
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| CNB2003101092591A Expired - Fee Related CN100352997C (en) | 2003-12-10 | 2003-12-10 | Method for preparing environmental protective wool easy of health and easy of nurse |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101424040B (en) * | 2008-10-28 | 2011-05-04 | 苏州大学 | Wool fiber modification treatment method |
| CN102936833A (en) * | 2012-11-15 | 2013-02-20 | 湖州铁佛耐火材料有限公司 | Method for preparing total easy caring wool tops and product of wool tops |
| CN103820991A (en) * | 2014-01-23 | 2014-05-28 | 浙江神州毛纺织有限公司 | Wool surface catalytic oxidation and modification method |
| CN105926274A (en) * | 2016-05-23 | 2016-09-07 | 浙江新中和羊毛有限公司 | Non-chlorine treatment method of ecological, environmentally friendly, healthy and anti-pilling non-shrinkable wool tops |
| CN109023950A (en) * | 2018-07-10 | 2018-12-18 | 江苏阳光股份有限公司 | A kind of conformal method for sorting of wool fabric |
| CN112647288A (en) * | 2020-12-08 | 2021-04-13 | 常熟市新光毛条处理有限公司 | Environment-friendly wool top mercerizing and shrink-proof treatment process |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1071475A (en) * | 1991-10-17 | 1993-04-28 | 东台市毛线厂 | The manufacture method of shrinkproof, mothproof, anti-balling-up knitting wool |
| JP3338975B2 (en) * | 1994-06-07 | 2002-10-28 | 博史 北條 | Keratin fiber modification method |
| JP2002146671A (en) * | 2000-08-31 | 2002-05-22 | Osaka Prefecture | Method for preventing shrinkage of animal hair fiber |
| CN1415796A (en) * | 2002-12-05 | 2003-05-07 | 北京思达信科技开发有限公司 | Method for easy to attend on wool |
-
2003
- 2003-12-10 CN CNB2003101092591A patent/CN100352997C/en not_active Expired - Fee Related
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101424040B (en) * | 2008-10-28 | 2011-05-04 | 苏州大学 | Wool fiber modification treatment method |
| CN102936833A (en) * | 2012-11-15 | 2013-02-20 | 湖州铁佛耐火材料有限公司 | Method for preparing total easy caring wool tops and product of wool tops |
| CN103820991A (en) * | 2014-01-23 | 2014-05-28 | 浙江神州毛纺织有限公司 | Wool surface catalytic oxidation and modification method |
| CN105926274A (en) * | 2016-05-23 | 2016-09-07 | 浙江新中和羊毛有限公司 | Non-chlorine treatment method of ecological, environmentally friendly, healthy and anti-pilling non-shrinkable wool tops |
| CN109023950A (en) * | 2018-07-10 | 2018-12-18 | 江苏阳光股份有限公司 | A kind of conformal method for sorting of wool fabric |
| CN109023950B (en) * | 2018-07-10 | 2021-07-09 | 江苏阳光股份有限公司 | Shape-preserving finishing method for wool fabric |
| CN112647288A (en) * | 2020-12-08 | 2021-04-13 | 常熟市新光毛条处理有限公司 | Environment-friendly wool top mercerizing and shrink-proof treatment process |
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| Publication number | Publication date |
|---|---|
| CN100352997C (en) | 2007-12-05 |
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