CN1611498A - Grosvenor momordical flavone and its preparing prcess - Google Patents
Grosvenor momordical flavone and its preparing prcess Download PDFInfo
- Publication number
- CN1611498A CN1611498A CNA200310110827XA CN200310110827A CN1611498A CN 1611498 A CN1611498 A CN 1611498A CN A200310110827X A CNA200310110827X A CN A200310110827XA CN 200310110827 A CN200310110827 A CN 200310110827A CN 1611498 A CN1611498 A CN 1611498A
- Authority
- CN
- China
- Prior art keywords
- grosvenor momordica
- flavonoid
- ethanol
- concentrated
- crude product
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229930003944 flavone Natural products 0.000 title abstract description 15
- 235000011949 flavones Nutrition 0.000 title abstract description 15
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 title abstract description 10
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 title abstract description 10
- 150000002212 flavone derivatives Chemical class 0.000 title abstract 6
- 235000009815 Momordica Nutrition 0.000 claims abstract description 37
- 241000218984 Momordica Species 0.000 claims abstract description 37
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 32
- -1 and elute Substances 0.000 claims abstract description 13
- 241000345998 Calamus manan Species 0.000 claims abstract description 10
- 235000012950 rattan cane Nutrition 0.000 claims abstract description 10
- 229920005989 resin Polymers 0.000 claims abstract description 10
- 239000011347 resin Substances 0.000 claims abstract description 10
- 238000005516 engineering process Methods 0.000 claims abstract description 7
- 238000000605 extraction Methods 0.000 claims abstract description 7
- 238000010992 reflux Methods 0.000 claims abstract description 7
- 239000000284 extract Substances 0.000 claims abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 5
- 239000002994 raw material Substances 0.000 claims abstract description 4
- 238000000034 method Methods 0.000 claims abstract description 3
- 239000002904 solvent Substances 0.000 claims abstract description 3
- 229930003935 flavonoid Natural products 0.000 claims description 28
- 235000017173 flavonoids Nutrition 0.000 claims description 28
- 150000002215 flavonoids Chemical class 0.000 claims description 20
- 239000012043 crude product Substances 0.000 claims description 10
- 238000001035 drying Methods 0.000 claims description 8
- 238000010521 absorption reaction Methods 0.000 claims description 7
- 239000007788 liquid Substances 0.000 claims description 7
- 239000000243 solution Substances 0.000 claims description 7
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 claims description 6
- 239000012530 fluid Substances 0.000 claims description 5
- 238000002360 preparation method Methods 0.000 claims description 5
- 238000009835 boiling Methods 0.000 claims description 4
- 239000003463 adsorbent Substances 0.000 claims description 3
- 238000001914 filtration Methods 0.000 claims description 3
- 238000012545 processing Methods 0.000 claims description 3
- 238000007598 dipping method Methods 0.000 claims description 2
- 238000010438 heat treatment Methods 0.000 claims description 2
- 239000011259 mixed solution Substances 0.000 claims description 2
- 229920006122 polyamide resin Polymers 0.000 claims description 2
- 238000011084 recovery Methods 0.000 claims description 2
- 239000007787 solid Substances 0.000 claims description 2
- 238000005406 washing Methods 0.000 claims description 2
- 238000010828 elution Methods 0.000 claims 1
- 239000012141 concentrate Substances 0.000 abstract description 4
- 239000000047 product Substances 0.000 abstract description 4
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 239000000706 filtrate Substances 0.000 abstract 1
- 238000001179 sorption measurement Methods 0.000 abstract 1
- 150000002213 flavones Chemical class 0.000 description 5
- 229930182470 glycoside Natural products 0.000 description 4
- REFJWTPEDVJJIY-UHFFFAOYSA-N Quercetin Chemical compound C=1C(O)=CC(O)=C(C(C=2O)=O)C=1OC=2C1=CC=C(O)C(O)=C1 REFJWTPEDVJJIY-UHFFFAOYSA-N 0.000 description 2
- 235000013399 edible fruits Nutrition 0.000 description 2
- 238000004128 high performance liquid chromatography Methods 0.000 description 2
- IYRMWMYZSQPJKC-UHFFFAOYSA-N kaempferol Chemical compound C1=CC(O)=CC=C1C1=C(O)C(=O)C2=C(O)C=C(O)C=C2O1 IYRMWMYZSQPJKC-UHFFFAOYSA-N 0.000 description 2
- MWDZOUNAPSSOEL-UHFFFAOYSA-N kaempferol Natural products OC1=C(C(=O)c2cc(O)cc(O)c2O1)c3ccc(O)cc3 MWDZOUNAPSSOEL-UHFFFAOYSA-N 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- UBSCDKPKWHYZNX-UHFFFAOYSA-N Demethoxycapillarisin Natural products C1=CC(O)=CC=C1OC1=CC(=O)C2=C(O)C=C(O)C=C2O1 UBSCDKPKWHYZNX-UHFFFAOYSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 235000019082 Osmanthus Nutrition 0.000 description 1
- 241000333181 Osmanthus Species 0.000 description 1
- ZVOLCUVKHLEPEV-UHFFFAOYSA-N Quercetagetin Natural products C1=C(O)C(O)=CC=C1C1=C(O)C(=O)C2=C(O)C(O)=C(O)C=C2O1 ZVOLCUVKHLEPEV-UHFFFAOYSA-N 0.000 description 1
- HWTZYBCRDDUBJY-UHFFFAOYSA-N Rhynchosin Natural products C1=C(O)C(O)=CC=C1C1=C(O)C(=O)C2=CC(O)=C(O)C=C2O1 HWTZYBCRDDUBJY-UHFFFAOYSA-N 0.000 description 1
- 230000001093 anti-cancer Effects 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- 230000003115 biocidal effect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 229930182486 flavonoid glycoside Natural products 0.000 description 1
- 150000007955 flavonoid glycosides Chemical class 0.000 description 1
- 235000020688 green tea extract Nutrition 0.000 description 1
- 229940094952 green tea extract Drugs 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 235000008777 kaempferol Nutrition 0.000 description 1
- UXOUKMQIEVGVLY-UHFFFAOYSA-N morin Natural products OC1=CC(O)=CC(C2=C(C(=O)C3=C(O)C=C(O)C=C3O2)O)=C1 UXOUKMQIEVGVLY-UHFFFAOYSA-N 0.000 description 1
- 230000000144 pharmacologic effect Effects 0.000 description 1
- 230000008092 positive effect Effects 0.000 description 1
- 235000005875 quercetin Nutrition 0.000 description 1
- 229960001285 quercetin Drugs 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
Landscapes
- Medicines Containing Plant Substances (AREA)
Abstract
Description
Claims (2)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CNB200310110827XA CN1313457C (en) | 2003-10-28 | 2003-10-28 | Grosvenor momordical flavone and its preparing prcess |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CNB200310110827XA CN1313457C (en) | 2003-10-28 | 2003-10-28 | Grosvenor momordical flavone and its preparing prcess |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1611498A true CN1611498A (en) | 2005-05-04 |
CN1313457C CN1313457C (en) | 2007-05-02 |
Family
ID=34759242
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CNB200310110827XA Expired - Lifetime CN1313457C (en) | 2003-10-28 | 2003-10-28 | Grosvenor momordical flavone and its preparing prcess |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN1313457C (en) |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1324043C (en) * | 2005-05-26 | 2007-07-04 | 广西中医学院 | Prepn and use of high-purity momordica glycoside V |
CN102138958A (en) * | 2011-04-06 | 2011-08-03 | 湖北汇特生物医药技术有限公司 | Process for extracting and purifying flavonoids in grosvener siraitia plants |
CN102977165A (en) * | 2012-12-07 | 2013-03-20 | 上海交通大学 | Optimized purification preparation method for momordica grosvenori flavine |
CN106860503A (en) * | 2017-03-29 | 2017-06-20 | 桂林实力科技有限公司 | The method that flavones is extracted from Luohanguo's residue |
CN106866759A (en) * | 2017-03-28 | 2017-06-20 | 广西甙元植物制品有限公司 | The technique that grosvenor momordica flavonoid is produced from the waste liquid of Momordica-Glycosides decolorizing resin post discharge |
CN111764194A (en) * | 2020-07-02 | 2020-10-13 | 广西中烟工业有限责任公司 | Preparation method of cigarette tipping paper containing momordica grosvenori flavone |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1375499A (en) * | 2002-03-28 | 2002-10-23 | 何伟平 | Method of extracting and separating several components from mangsteen |
-
2003
- 2003-10-28 CN CNB200310110827XA patent/CN1313457C/en not_active Expired - Lifetime
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1324043C (en) * | 2005-05-26 | 2007-07-04 | 广西中医学院 | Prepn and use of high-purity momordica glycoside V |
CN102138958A (en) * | 2011-04-06 | 2011-08-03 | 湖北汇特生物医药技术有限公司 | Process for extracting and purifying flavonoids in grosvener siraitia plants |
CN102977165A (en) * | 2012-12-07 | 2013-03-20 | 上海交通大学 | Optimized purification preparation method for momordica grosvenori flavine |
CN102977165B (en) * | 2012-12-07 | 2015-05-27 | 上海交通大学 | Optimized purification preparation method for momordica grosvenori flavine |
CN106866759A (en) * | 2017-03-28 | 2017-06-20 | 广西甙元植物制品有限公司 | The technique that grosvenor momordica flavonoid is produced from the waste liquid of Momordica-Glycosides decolorizing resin post discharge |
CN106866759B (en) * | 2017-03-28 | 2019-09-10 | 湖南华诚生物资源股份有限公司 | The technique of grosvenor momordica flavonoid is produced from the waste liquid that Momordica-Glycosides decolorizing resin column is discharged |
CN106860503A (en) * | 2017-03-29 | 2017-06-20 | 桂林实力科技有限公司 | The method that flavones is extracted from Luohanguo's residue |
CN111764194A (en) * | 2020-07-02 | 2020-10-13 | 广西中烟工业有限责任公司 | Preparation method of cigarette tipping paper containing momordica grosvenori flavone |
Also Published As
Publication number | Publication date |
---|---|
CN1313457C (en) | 2007-05-02 |
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Legal Events
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C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
ASS | Succession or assignment of patent right |
Owner name: ZHONGZHU CHINESE MEDICINES CO., LTD., GUILIN Free format text: FORMER OWNER: GUANGXI NORMAL UNIVERSITY Effective date: 20120110 |
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C41 | Transfer of patent application or patent right or utility model | ||
COR | Change of bibliographic data |
Free format text: CORRECT: ADDRESS; FROM: 541004 GUILIN, GUANGXI ZHUANG AUTONOMOUS REGION TO: 541800 GUILIN, GUANGXI ZHUANG AUTONOMOUS REGION |
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TR01 | Transfer of patent right |
Effective date of registration: 20120110 Address after: 541800 No. 40 Xiangyang Road, Yongfu County, Guilin, the Guangxi Zhuang Autonomous Region Patentee after: GUILIN ZHONGZU TRADITIONAL CHINESE MEDICINE CO.,LTD. Address before: 541004 Guangxi Normal University, 15 Yucai Road, Guilin, the Guangxi Zhuang Autonomous Region Patentee before: Guangxi Normal University |
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CX01 | Expiry of patent term |
Granted publication date: 20070502 |
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CX01 | Expiry of patent term |