CN1553947A - 改进的抗氧化添加剂组合物和含有此添加剂组合物的润滑剂组合物 - Google Patents
改进的抗氧化添加剂组合物和含有此添加剂组合物的润滑剂组合物 Download PDFInfo
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- CN1553947A CN1553947A CNA028177002A CN02817700A CN1553947A CN 1553947 A CN1553947 A CN 1553947A CN A028177002 A CNA028177002 A CN A028177002A CN 02817700 A CN02817700 A CN 02817700A CN 1553947 A CN1553947 A CN 1553947A
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- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
- C10M2215/06—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to carbon atoms of six-membered aromatic rings
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- C10M2219/06—Thio-acids; Thiocyanates; Derivatives thereof
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- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/10—Heterocyclic compounds containing sulfur, selenium or tellurium compounds in the ring
- C10M2219/104—Heterocyclic compounds containing sulfur, selenium or tellurium compounds in the ring containing sulfur and carbon with nitrogen or oxygen in the ring
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- C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
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- C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
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- C10M2223/047—Thioderivatives not containing metallic elements
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- Chemical Kinetics & Catalysis (AREA)
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- Materials Engineering (AREA)
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Abstract
Description
组分 | 实施方案1(%) | 实施方案2(%) | 实施方案3(%) |
总组合物:(1)+(2)+(3) | 0.15-12.0 | 0.40-8.5 | 0.75-3.5 |
(1)有机钼化合物 | 0.05-3.0 | 0.10-2.0 | 0.15-1.0 |
(2)ADPA | 0.05-5.0 | 0.1-2.0 | 0.20-1.5 |
(3)含硫化合物* | 0.05-4.0 | 0.20-2.5 | 0.40-1.0 |
(a)噻二唑 | 0-4.0 | 0-2.5 | 0-1.0 |
(b)二硫代氨基甲酸酯 | 0-4.0 | 0-2.5 | 0-1.0 |
1 | 2 | 3 | 4 | 5 | 6 | |
有机钼(Molyvan855) | 0.16 | 0.16 | 0.16 | 0.40 | 0.40 | 0.40 |
烷基化二苯胺(Vanlube81) | 0.20 | 0.20 | 0.20 | 0.20 | 0.20 | 0.20 |
硫化异丁烯(VanlubeSB) | 0.40 | - | - | 0.40 | - | - |
噻二唑(Vanlube871) | - | 0.40 | 0.93 | - | 0.40 | 0.93 |
分散剂TC 9596A 91-4284 | 5.00 | 5.00 | 5.00 | 5.00 | 5.00 | 5.00 |
基础油(II类油) | 94.24 | 94.24 | 93.71 | 94.00 | 94.00 | 93.47 |
TEOST沉积试验 | 74.4 | 61.5 | ||||
铜腐蚀,24h@121℃-(ASTM D-130) | 4a | 3b | ||||
润滑剂油的氧化诱导时间(分钟),加压差示扫描量热法(PDSC),500psi@210℃-(ASTM D6186) | ||||||
试验1 | 11.6 | 15.9 | 13.9 | |||
试验2 | 14.3 | 12.5 | 12.4 | |||
试验3 | 17.1 | 13.9 | 9.8 | |||
试验4 | 14.8 | 12.8 | 13.8 | |||
试验5 | 15.6 | - | - | |||
试验6 | 12.2 | - | - | |||
平均值(分钟) | 14.3 | 13.8 | 12.5 | |||
按分钟计的T-1000薄膜氧气吸收-TFOUT-(ASTM D4742) | ||||||
160 | 117 | 470 | ||||
172 | 230 | 530 | ||||
- | 185 | - | ||||
平均值,分钟 | 166 | 177 | 500 | |||
T-900 Falex No.1低压@201b,90分钟 | ||||||
摩擦系数:@90分钟 | 0.02200.0160 | 0.0150 | 0.0075 |
7 | 8 | 9 | 10 | 11 | |
有机钼(Molyvan855) | 0.16 | 0.16 | 0.40 | 0.40 | 0.40 |
烷基化二苯胺(Vanlube81) | 0.20 | 0.20 | 0.20 | 0.20 | 0.20 |
硫化异丁烯(VanlubeSB) | 0.40 | - | 0.40 | - | - |
亚甲基双二硫代氨基甲酸二丁酯(Vanlube7723) | - | 0.40 | - | 0.40 | 0.93 |
分散剂TC 9596A 91-4284 | 5.00 | 5.00 | 5.00 | 5.00 | 5.00 |
基础油(II类油) | 94.24 | 94.24 | 94.00 | 94.00 | 93.27 |
铜腐蚀,24h@121℃-(ASTM D-130) | 4a | 3b | |||
按分钟计的T-1000薄膜氧气吸收-TFOUT-(ASTM D4742) | |||||
160 | 190 | ||||
172 | 186 | ||||
平均值,分钟 | 166 | 188 | |||
T-900 Falex No.1低压@201b,90分钟 | |||||
摩擦系数:@90分钟 | 0.0220/0.0160 | 0.0065 | 0.0006 |
化合物 | 13 | 14 | 15 | 16 | 17 | 18 | 19 | 20 | 21 | 22 | 23 |
基础油(GF-45W-20) | 100 | 99.10 | 99.0 | 98.5 | 97.61 | 98.11 | 97.5 | 97.34 | 97.05 | 96.61 | 96.61 |
Molyvan855 | 0.90 | 0.89 | 0.89 | 0.16 | 0.45 | 0.89 | |||||
VanlubeAZ(50%的活性成分) | 1.0 | 1.0 | 1.0 | 1.0 | 1.0 | 1.0 | |||||
Vanlube SL | 1.5 | 1.5 | 1.5 | 1.5 | 1.5 | 1.5 | |||||
Molyvan855(26.3mol.%)、VanlubeAZ(29.5mol.%)、VanlubeSL(44.2mol.%)的预混合物 | 3.39 | ||||||||||
Mo ppm | 0 | 702 | 0 | 0 | 703 | 703 | 0 | 126 | 355 | 703 | 703 |
TEOST MHT-4 | |||||||||||
棒上沉积物,mg | 66.9 | 58.2 | 94.0 | ||||||||
总沉积物,mg | 105.5 | 99.7 | 81.3 | 37.4 | 31.6 | 29.5 | 25.1 | 28.8 |
Claims (18)
Applications Claiming Priority (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US32415801P | 2001-09-21 | 2001-09-21 | |
US60/324,158 | 2001-09-21 | ||
US33587701P | 2001-11-15 | 2001-11-15 | |
US60/335,877 | 2001-11-15 |
Publications (2)
Publication Number | Publication Date |
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CN1553947A true CN1553947A (zh) | 2004-12-08 |
CN100575467C CN100575467C (zh) | 2009-12-30 |
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Application Number | Title | Priority Date | Filing Date |
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CN02817700A Expired - Lifetime CN100575467C (zh) | 2001-09-21 | 2002-09-19 | 改进的抗氧化添加剂组合物和含有此添加剂组合物的润滑剂组合物 |
Country Status (6)
Country | Link |
---|---|
US (1) | US6806241B2 (zh) |
EP (1) | EP1468063B1 (zh) |
JP (1) | JP4005559B2 (zh) |
CN (1) | CN100575467C (zh) |
ES (1) | ES2656777T3 (zh) |
WO (1) | WO2003027215A2 (zh) |
Cited By (6)
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CN101787322A (zh) * | 2010-03-18 | 2010-07-28 | 上海交通大学 | 含酯基噻二唑衍生物极压抗磨剂及其制备方法 |
CN102812111A (zh) * | 2010-03-25 | 2012-12-05 | R.T.范德比尔特公司 | 超低磷润滑剂组合物 |
CN102959061A (zh) * | 2010-06-25 | 2013-03-06 | 道达尔炼油与销售部 | 用于机动车辆传动装置的润滑剂组合物 |
CN103103007A (zh) * | 2011-11-09 | 2013-05-15 | 中国石油化工股份有限公司 | 一种自动变速箱油组合物 |
CN107849479A (zh) * | 2015-07-07 | 2018-03-27 | Ab纳米技术公司 | 有机金属盐组合物、其制备方法和润滑剂添加剂组合物 |
CN115362243A (zh) * | 2020-04-01 | 2022-11-18 | 道达尔能源一技术公司 | 包含2,5-二巯基-1,3,4-噻二唑烷基聚羧酸酯化合物的润滑剂组合物 |
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US8123982B2 (en) | 2004-03-26 | 2012-02-28 | Akzo Nobel N.V. | Sulfur based corrosion inhibitors |
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US20080139425A1 (en) * | 2006-12-11 | 2008-06-12 | Hutchison David A | Lubricating composition |
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PL2132082T3 (pl) | 2007-03-06 | 2013-01-31 | Vanderbilt Chemicals Llc | Związki molibdenu i kompozycje smarowe je zawierające |
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CN101830865B (zh) * | 2010-03-19 | 2012-05-02 | 华东交通大学 | 一种含羟基的噻二唑衍生物及其制备方法和应用 |
US9150812B2 (en) * | 2012-03-22 | 2015-10-06 | Exxonmobil Research And Engineering Company | Antioxidant combination and synthetic base oils containing the same |
US9623350B2 (en) | 2013-03-01 | 2017-04-18 | Fram Group Ip Llc | Extended-life oil management system and method of using same |
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FR3014898B1 (fr) * | 2013-12-17 | 2016-01-29 | Total Marketing Services | Composition lubrifiante a base de triamines grasses |
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BR112018076938A2 (pt) | 2016-06-24 | 2019-08-06 | Dow Global Technologies Llc | composições de embalagem antioxidante e de lubrificante, e, processos para preparar uma composição de embalagem antioxidante e de lubrificante. |
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- 2002-09-19 EP EP02768869.6A patent/EP1468063B1/en not_active Expired - Lifetime
- 2002-09-19 CN CN02817700A patent/CN100575467C/zh not_active Expired - Lifetime
- 2002-09-19 WO PCT/US2002/029712 patent/WO2003027215A2/en active Application Filing
- 2002-09-19 JP JP2003530788A patent/JP4005559B2/ja not_active Expired - Lifetime
- 2002-09-19 US US10/247,012 patent/US6806241B2/en not_active Expired - Lifetime
- 2002-09-19 ES ES02768869.6T patent/ES2656777T3/es not_active Expired - Lifetime
Cited By (11)
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CN101787322A (zh) * | 2010-03-18 | 2010-07-28 | 上海交通大学 | 含酯基噻二唑衍生物极压抗磨剂及其制备方法 |
CN102812111A (zh) * | 2010-03-25 | 2012-12-05 | R.T.范德比尔特公司 | 超低磷润滑剂组合物 |
CN102812111B (zh) * | 2010-03-25 | 2014-06-04 | 范德比尔特化学品有限责任公司 | 超低磷润滑剂组合物 |
CN102959061A (zh) * | 2010-06-25 | 2013-03-06 | 道达尔炼油与销售部 | 用于机动车辆传动装置的润滑剂组合物 |
CN102959061B (zh) * | 2010-06-25 | 2016-02-10 | 道达尔销售服务公司 | 用于机动车辆传动装置的润滑剂组合物 |
CN103103007A (zh) * | 2011-11-09 | 2013-05-15 | 中国石油化工股份有限公司 | 一种自动变速箱油组合物 |
CN103103007B (zh) * | 2011-11-09 | 2014-09-17 | 中国石油化工股份有限公司 | 一种自动变速箱油组合物 |
CN107849479A (zh) * | 2015-07-07 | 2018-03-27 | Ab纳米技术公司 | 有机金属盐组合物、其制备方法和润滑剂添加剂组合物 |
CN107849479B (zh) * | 2015-07-07 | 2021-02-02 | Ab纳米技术公司 | 有机金属盐组合物、其制备方法和润滑剂添加剂组合物 |
CN115362243A (zh) * | 2020-04-01 | 2022-11-18 | 道达尔能源一技术公司 | 包含2,5-二巯基-1,3,4-噻二唑烷基聚羧酸酯化合物的润滑剂组合物 |
CN115362243B (zh) * | 2020-04-01 | 2023-08-25 | 道达尔能源一技术公司 | 包含2,5-二巯基-1,3,4-噻二唑烷基聚羧酸酯化合物的润滑剂组合物 |
Also Published As
Publication number | Publication date |
---|---|
US6806241B2 (en) | 2004-10-19 |
ES2656777T3 (es) | 2018-02-28 |
EP1468063A2 (en) | 2004-10-20 |
WO2003027215A3 (en) | 2003-07-10 |
WO2003027215A2 (en) | 2003-04-03 |
JP4005559B2 (ja) | 2007-11-07 |
CN100575467C (zh) | 2009-12-30 |
EP1468063B1 (en) | 2017-12-13 |
US20030158051A1 (en) | 2003-08-21 |
JP2005504142A (ja) | 2005-02-10 |
EP1468063A4 (en) | 2010-07-21 |
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