CN1524427A - Celery oil preparation for prevention and cure of bees and acarids and the use thereof - Google Patents
Celery oil preparation for prevention and cure of bees and acarids and the use thereof Download PDFInfo
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- CN1524427A CN1524427A CNA031110460A CN03111046A CN1524427A CN 1524427 A CN1524427 A CN 1524427A CN A031110460 A CNA031110460 A CN A031110460A CN 03111046 A CN03111046 A CN 03111046A CN 1524427 A CN1524427 A CN 1524427A
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Abstract
The invention relates to a celery seed oil preparation for prevention and cure of honeybee acarid and use thereof, wherein the preparation comprises water, 40-70 weight parts of celery oil, 7-15 parts by weight of perfume compound, 950-1100 weight parts of water. The celery seed oil according to the invention poses no contamination and nuisance to honeybee product.
Description
Technical field: the present invention relates to a kind of preparation that contains celery seed fat of preventing and treating varoa mite and chalcid fly mite, and the application of said preparation aspect control honeybee mite.
Background technology: the honeybee mite is the most general, the main parasitic insect pest that harm is the most serious during current bee-keeping is produced.Present honeybee acarid control agent generally has the shortcoming of polluting bee product, has had a strong impact on the quality of bee product.The useful broken celery of bee keeper reduces the influence of honeybee mite for many years, still, is which material in the celery has inhibitory action to the honeybee mite, can't confirm.And, because honeybee do not eat celery, therefore, use broken celery after, bee colony is also had certain influence, honeybee has for celery significantly walks quickly and keeps away reaction.
Summary of the invention: the purpose of this invention is to provide and a kind of bee product is not polluted, there is no celery oil preparation and application thereof repellent action, that can prevent and treat the honeybee mite efficiently to honeybee is harmless.
Above-mentioned purpose realizes by following technical scheme:
The celery oil preparation of control honeybee mite, its composition comprises: water, the parts by weight that contain the celery oil of 40-70 weight portion, the essence of 7-15 weight portion, wherein said water in the described water are 950-1100.
The celery oil preparation of above-mentioned control honeybee mite, three kinds of predominant quantity portion rates that contain in the described celery oil are that the obedient vinyl compound of benzinum wash-out is 2-6, the higher unsaturated fatty acid 30-50 of ether wash-out, the high boiling point composition 4-12 of ethanol elution.
The celery oil preparation of above-mentioned control honeybee mite, described essence is for adopting flavoring essence, for example grape essence or flavoring banana essence or honey peach essence or Hami melon essence or pear essence or citrus essence or kiwi flavor.
The preparation method of above-mentioned celery oil, for example adopt the petroleum ether extraction method:
Celery seed was pulverized 40 mesh sieves, in the Nylon Bag of packing into, in extractor extracting to flow out liquid colourless till, residue is placed distillation flask, discard steam the benzinum of residue absorption with water-bath after, extractor can continued operation, and the celery oil in flask is about at 1/2 o'clock to be stopped, a spot of celery oil in the celery oil is steamed, obtain the refining celery oil that the present invention uses, its proportion 0.92 (20 ℃), refraction index 1.4779 (20 ℃), saponification number 181.1, allusion quotation value 89.7.The absworption peak of its infrared spectrum is: 3010 (MS), 2930 (S), 2830 (S), 1750 (VS), 1715 (MS), 1460 (MS), 1380 (M), 1150 (S), 720 (M).
The separating method of celery oil kind active ingredient:
Can adopt silica gel column chromatography to measure the key component of celery oil, for example adopt the silica gel column chromatography of 800mm, benzinum is a solvent, after adding above-mentioned refining celery oil 30 grams, when the band pasta is reduced to the chromatography face, begin to add benzinum and carry out wash-out, coloured from flowing out liquid, to flow out liquid colourless till, this leacheate is steamed solvent, and weak yellow liquid---described obedient vinyl compound is eluted to chromatographic column colourless again with ether to obtain about 3 grams, leacheate steams solvent, get about about 20 grams of yellow green thick liquid, this liquid is described higher unsaturated fatty acid, and chromatographic column is extremely colourless with ethanol elution more then, leacheate steams solvent and obtains about about 5 grams of blackish green paste, and this paste is described high boiling point composition.
A kind of above-mentioned application of celery oil preparation on control honeybee mite.
This technical scheme has following beneficial effect:
1. the present invention adopts natural harmless fat control honeybee mite, and have and do not pollute bee product, to honeybee safety, non-harmful distinguishing feature.Through the test of group honeybee surplus 300, use this product can reduce the honeybee loss more than 20%, improve bee colony and produce honey about 20%.Each bee colony control three times, cost 0.18-0.3 unit can increase economic efficiency more than 50 yuan.Guaranteed the advantage of pollution-free honey outlet.
2. miticidal effect is good, adopt this product of 1.0,1.5,2.0,2.5,3.0,3.5,4.0 milliliters in beehive, to kill the mite test respectively, every dosetest all repeats to spray twice, and corresponding acaricidal rate is 90.59%, 90.50%, 90.67%, 95.05%, 94.53%, 98.00%, 99.67%.
3. the lethality of honeybee is low, adopt this product under the mite equal conditions honeybee being sprayed extremely for 3.0,3.5,4.0,4.5,5.0,5.5 milliliters, the bee death rate is successively: 0%, 0%, 1.7%, 0%, 1.7%, 0%, 3.3%, and the mortality of honeybee and dosage it doesn't matter.
4. the celery oil unsaturated fatty acid that contains in this product is the main body of killing mite, and this material content in this product, contains these two kinds of components the mite extremely of unsaturated fatty acid is had the obvious synergistic facilitation though other two components content are little than higher.The simple miticidal effect that adopts unsaturated fatty acid is lower than the miticidal effect of the celery oil that contains other two kinds of compositions, and the miticidal effect of simple unsaturated fatty acid is 95% of the celery oil effect that contains above-mentioned three class materials.
5. overcome behind the adding essence honeybee to celery oil do not accept promptly produce the problem of walking quickly and keeping away reaction.Honeybee has for simple use celery oil goods significantly walks quickly and keeps away reaction, light level is for restlessness and send slight chimes of doom, middle rank sends bigger chimes of doom for bee colony, heavy duty is that the bee colony order is affected, and send very loud noise, even the part honeybee leaves the honeycomb of spray formulation, and this to walk quickly and keep away problem on the rise with increasing of temperature, with bee colony institute gathering honey kind certain relation is arranged, increase essence after, obtained effect preferably.Wherein, adopt the product of kiwi flavor 1% or Hami melon essence 1% and the celery oil preparation of 4%-6% generally to accept for honeybee experimental field, effect is best, bee colony for light level avoidance effect can be eliminated the effects of the act fully, can eliminate to light level or eliminate fully for the bee colony of intermediate avoidance effect, can alleviate to light level the bee colony of heavy duty avoidance effect.The present invention is under the receptible prerequisite of honeybee, celery oil is applied to kill removes the honeybee mite, protects bee colony and bee product production.
The specific embodiment of the present invention:
Embodiment 1:
The celery oil preparation of control honeybee mite, its composition comprises: water 1000 grams wherein contain the celery oil of 40 grams, 50 grams, 60 grams, 70 grams, again in this content range can, this celery oil can adopt the above-mentioned described method of summary of the invention part to make, and also can adopt other method to produce.The essence that is added can be according to the kind difference that adds, the adaptive capacity of the different and different bee colonies in area, select to add the essence of 7-15 gram, even areal, different bee colonies is also different to the adaptive capacity of essence, generally about 10 grams, the weight of wherein said water can restrain for 950-1100.And can make spray or emulsifier with this ratio.
Difference according to the place of production, the difference of acquisition mode method, in the active ingredient of described celery oil, the weight content ratio of three kinds of main active ingredients is: the obedient vinyl compound that contains the benzinum wash-out is 2-6, generally account between the 5-15% of weight, the higher unsaturated fatty acid 30-50 of ether wash-out, generally account for the 50-85% of total amount, the high boiling point composition 4-10 of ethanol elution, generally account between the 8-17% of weight, three kinds of compositions are the celery oil of this ratio of weight and number, and the composition that can be used as this product adds.
Embodiment 2:
Essence in the celery oil preparation of control honeybee mite in the foregoing description is flavoring essence, can be that grape essence also can be a flavoring banana essence, perhaps honey peach essence, perhaps Hami melon essence, perhaps pear essence, perhaps citrus essence, perhaps kiwi flavor.Can attempt selecting according to the situation of the hobby of honeybee.
Embodiment 3:
The application of above-mentioned celery oil preparation on control honeybee mite.
Get the celery oil preparation, contain the celery oil of 5-6%, contain Hami melon essence 1%, be sprayed onto at dusk every day in the beehive, every frame 0.3-0.5 milliliter is general just passable, and next day, early honeybee went out the mite number that falls at the bottom of the inspection box before the nest, continuous 3-4 days.The control efficiency 100% of each case has miticidal effect 100%, acaricidal rate 96.44%.Bee colony does not produce and walks quickly and keeps away phenomenon.
Claims (4)
1. celery oil preparation of preventing and treating the honeybee mite, its composition comprises: water is characterized in that: the parts by weight that contain the celery oil of 40-70 weight portion, the essence of 7-15 weight portion, wherein said water in the described water are 950-1100.
2. the celery oil preparation of control honeybee mite according to claim 1, it is characterized in that: three kinds of predominant quantity portion rates that contain in the described celery oil are that the obedient vinyl compound of benzinum wash-out is 2-6, the higher unsaturated fatty acid 30-50 of ether wash-out, the high boiling point composition 4-10 of ethanol elution.
3. the celery oil preparation of control honeybee mite according to claim 1 and 2, it is characterized in that: described essence is flavoring essence, comprising: grape essence or flavoring banana essence or honey peach essence or Hami melon essence or pear essence or citrus essence or kiwi flavor.
4. claim 1 or the 2 described celery oil preparations application on control honeybee mite.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA031110460A CN1524427A (en) | 2003-02-24 | 2003-02-24 | Celery oil preparation for prevention and cure of bees and acarids and the use thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA031110460A CN1524427A (en) | 2003-02-24 | 2003-02-24 | Celery oil preparation for prevention and cure of bees and acarids and the use thereof |
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| Publication Number | Publication Date |
|---|---|
| CN1524427A true CN1524427A (en) | 2004-09-01 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNA031110460A Pending CN1524427A (en) | 2003-02-24 | 2003-02-24 | Celery oil preparation for prevention and cure of bees and acarids and the use thereof |
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| CN (1) | CN1524427A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101278681B (en) * | 2008-05-14 | 2012-06-13 | 陈盛禄 | Prescription for preventing and controlling bee mite |
| CN106561726A (en) * | 2016-10-28 | 2017-04-19 | 华南农业大学 | Shielding protection insecticide capable of repelling natural enemy insects and bees |
| CN106577804A (en) * | 2016-10-28 | 2017-04-26 | 华南农业大学 | Shield protective type insecticide for repelling natural enemy insects and honeybees |
-
2003
- 2003-02-24 CN CNA031110460A patent/CN1524427A/en active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101278681B (en) * | 2008-05-14 | 2012-06-13 | 陈盛禄 | Prescription for preventing and controlling bee mite |
| CN106561726A (en) * | 2016-10-28 | 2017-04-19 | 华南农业大学 | Shielding protection insecticide capable of repelling natural enemy insects and bees |
| CN106577804A (en) * | 2016-10-28 | 2017-04-26 | 华南农业大学 | Shield protective type insecticide for repelling natural enemy insects and honeybees |
| CN106577804B (en) * | 2016-10-28 | 2019-09-20 | 华南农业大学 | A kind of shielding protection type insecticide of repellent natural enemy insect and honeybee |
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