CN1488330A - Cosmestic composite additive containing dandelion and bletilla striata extract and preparing process and use in csomestics thereof - Google Patents
Cosmestic composite additive containing dandelion and bletilla striata extract and preparing process and use in csomestics thereof Download PDFInfo
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- CN1488330A CN1488330A CNA03132343XA CN03132343A CN1488330A CN 1488330 A CN1488330 A CN 1488330A CN A03132343X A CNA03132343X A CN A03132343XA CN 03132343 A CN03132343 A CN 03132343A CN 1488330 A CN1488330 A CN 1488330A
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Abstract
The invention discloses a makeup compound additive containing the extracts of dandelion and bletilla striata, making technique and application in the makeup. The making technique: purify the dandelion, wash, cut up, extract by ultrasonic immersion method, filter, flocculate, centrifuge, ultrafilter, absorb by large aperture resin, wash by alcohol, and condense to get the standard extract; take the bletilla striata, add in alcohol, crush and make plasm, filter, grind by colloid mill, place still to centrifuge, add edible alcohol in the top clear liquid to blend, place still under normal temperature, draw-filter and wash by anhydrous alcohol or acetone, add in water to dissolve and dilute, and adjust pH value to get the standard extract; mix two extracts in proportion for homogenizing to make it.
Description
Technical field
The present invention relates to a kind of cosmetics additive, particularly relate to a kind of cosmetics compound additive and preparation technology and application in cosmetics that contains Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract.
Background technology
Natural plants is long at the applicating history of beauty treatment aspect the skin and complexion improving, promptly occur period as far back as Qin Han, to the Tang Dynasty very in vogue.Material such as contained organic acid, oils and fats, alkaloid, the matter of trampling on, glycoside, quintessence oil, phlegmatic temperament, protein, aminoacid, vitamins, mineral, trace element, phytohormone all can be to the generation different effect and the influence of human body skin in the plant.As the effect of the matter Bearberry Extract skin of trampling on, Saponin tool decontamination contaminant releasing effect, acid have anti-inflammation and sterilization effect, mucopolysaccharide to have the moisture-keeping function, aminoacid can skin nutrition, reduce wrinkle, and protein is also helpful to strengthening skin elasticity.Along with progress of science and technology, numerous and diverse chemical constitution of natural plants is revealed gradually, and numerous active component also can be extracted and separate, and this has created condition for such plant in the application of natural household chemicals field.
At present, cosmetics industry in people life in occupation of considerable status, the daily use chemicals industry development of China is very fast, new product makes rapid progress, market presents unprecedented prosperity scene, wherein functional component come from that the cosmetics of plant are safe in utilization because of it, action temperature and, significantly extremely consumer's favor of effect.A lot of medicinal plants are applied to functional cosmetics production successively, have produced good social and economic benefit.
Therefore, use the compound cosmetics additive of various plants extracting solution more and more higher being paid much attention in the day chemical industry of Chinese medicine scientific principle opinion and modern science and technology preparation.
The skin protection mechanism of Herba Taraxaci extract: Herba Taraxaci (Taraxacum mongolicum) has another name called Herba crotalariae albidae, grandmother's fourth, for the Dandelion feverfew, extensively distributes in China.Because of its rich in proteins and multivitamin, and abnormal smells from the patient delicate fragrance, among the people edible as wild herbs.Herba Taraxaci also is the Chinese crude drug of heat-clearing and toxic substances removing, and the traditional Chinese medical science is used for the diuresis eliminating stagnation, treats the poison detumescence.Modern scientific research has disclosed Herba Taraxaci and has contained the various active material, as taraxol, taraxerol, chlorogenic acid, mannitol, choline, Saponin etc., pharmacological evaluation has proved that Herba Taraxaci extract has stronger inhibitory action to staphylococcus aureus, common pathogenic dermatophytes is also had inhibitory action, and the Herba Taraxaci preserved material has great choleretic effect.At field of medicaments, at present the analysis of Herba Taraxaci extraction of active ingredients, pharmacology medicineization, the mechanism of action and clinical application research are deepened continuously, at field of food, because the dietotherapeutic plant resources that the Dandelion health ministry is assert, thereby also be developed to plurality kinds of health care food and beverage.
Studies show that, plurality of active ingredients such as the taraxasterol that the Herba Taraxaci herb contains, Flavonoids, chlorogenic acid, has broad-spectrum antibacterial action, its extract has stronger bactericidal action to staphylococcus aureus, Hemolytic streptococcus, Diplococcus pneumoniae, bacillus pyocyaneus, Bacillus proteus, dysentery bacterium, Bacillus typhi etc. are also had certain kill and suppress the growth effect, Herba Taraxaci has curative effect preferably to dermatosiss such as multiple folliculitis, infectiousness eczema, furuncle, red and swollen pyretic toxicity and skin infections clinically.Be applied in the daily chemical products, can play the cleaning skin effect preferably, avoid pathogen infecting human body.
Herba Taraxaci has wrinkle resistant and function of anti-skin aging: antioxidant comprises materials such as superoxide dismutase (SOD), peroxidase (POD), catalase (CAT), glutathione peroxidase (GSH-Px) and sterol, flavone, chlorogenic acid in the Herba Taraxaci, and content is higher in the wild plant.Adopt suitable extracting method can keep in the herb antioxidant, as chlorogenic acid, Flavonoids and part SOD or quasi-SOD material, be used for skin care product, its contained active component has the effect of quasi-SOD sample, can improve endogenous SOD activity, augment the deficiency of exogenous sod.These have very the active material of high anti-oxidation can remove free radical rapidly subcutaneous, blocks the damaging action of radical pair skin effectively, thereby plays good wrinkle resistant effect, the aging of delaying skin.
Herba Taraxaci has the dispelling speckles and whitening face effect to skin: studies show that Herba Taraxaci extract has the active effect of stronger restraint of tyrosinase, reduce the formation of intradermal melanin and secondary melanocyte.In addition, the senile lipofuscin deposition that causes because of lipid oxidation, the generation of chloasma also there is certain inhibitory action.
Herba Taraxaci has the effect of the acne of inhibition: use Herba Taraxaci extract, chlorogenic acid wherein is antibiotic to wait material effectively to kill and suppress the acne pathogenic microorganism, slow down acne symptom, accelerate its healing, simultaneously, antioxidation class material can act on the free radical material that acne produces in the Herba Taraxaci, alleviates stimulation and inflammation damnification to skin histology, acne symptom is obviously alleviated, and accelerate the reparation of skin lesion position and focus.
The skin protection mechanism of Pseudobulbus Bletillae (Rhizoma Bletillae) extract: the Pseudobulbus Bletillae (Rhizoma Bletillae) (Bletilla striata Reichb.L.) belongs to the orchid family; the Pseudobulbus Bletillae (Rhizoma Bletillae) belongs to; claim again the little Pseudobulbus Bletillae (Rhizoma Bletillae), lotus and grass, sweet, Bletilla striata (Thunb.ex A.Murray)Rchb.f., bamboo foxtail millet glue, snow as not, the Rhizoma Bletillae Pseudobulbus Bletillae (Rhizoma Bletillae) uses as Chinese medicine over the past thousands of years always; its major function is to hold back skin ulcer hemostasis, tonifying the lung, detumescence and promoting granulation; can treat haematemesis, pneumonopathy, hemoptysis, chronic gastric ulcer etc.; being applied in has protection skin, the effect of delaying decrepitude of skin in the cosmetics.Bletilla striata polyoses glue is formed by mannose and glucose polymerisation, and the ratio of two kinds of glycosyls is approximately 4: 1.The mean molecule quantity 2800000 of glue, its filming performance is better than sodium carboxymethyl cellulose and polyvinyl alcohol, is a kind of good natural thickener, is applied to various cosmetics, can substitute various chemical thickening agents, reduces the zest harm to skin.Pseudobulbus Bletillae (Rhizoma Bletillae) rubber powder and Pseudobulbus Bletillae (Rhizoma Bletillae) glucomannoglycan glue are the pharmaceutic adjuvant and the quite promising biomedical materials of medical material, performance brilliance safely and efficiently.
Summary of the invention
The purpose of this invention is to provide a kind of emulsifiability good, be uniformly dispersed, bioactive substance is stablized, can be used for developing the cosmetics compound additive that contains Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract of the cosmetics that have bactericidal antiphlogistic, freckle removing and whitening, anti-Zou's health care concurrently.
Another object of the present invention provides the above-mentioned preparation technology who contains the cosmetics compound additive of Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract.
A further object of the present invention provides the above-mentioned application of cosmetics compound additive in cosmetics that contains Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract.
The present invention develops a kind of compound additive that is applied to cosmetics, according to Chinese materia medica " mutual reinforcement between " compatibility principle, and with drug effect close Herba Taraxaci and Pseudobulbus Bletillae (Rhizoma Bletillae) compatibility, the anti-inflammation of collection Herba Taraxaci and the removing the necrotic tissue and promoting granulation of the Pseudobulbus Bletillae (Rhizoma Bletillae), antipruritic skin moistening is an one, produces synergism.To spot dispelling whitening, delaying decrepitude of skin, cleaning skin, anti-inflammation etc. all have remarkable effect behind the relevant cosmetic product of adding.
Purpose of the present invention can realize by following measures:
A kind of cosmetics compound additive that contains Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract comprises following components in weight percentage:
Herba Taraxaci standard extract: 6%-12% Pseudobulbus Bletillae (Rhizoma Bletillae) standard extract: 88%-94%
Wherein the compound additive canonical parameter is: the Herba Taraxaci general flavone content is 1.08%-2.64%, and Pseudobulbus Bletillae (Rhizoma Bletillae) glue mannan content is 7.04%-11.28%;
Wherein Herba Taraxaci standard extract canonical parameter is in the compound additive: the percentage by weight of Herba Taraxaci general flavone content in the Herba Taraxaci standard extract is 18%-22%;
Wherein Pseudobulbus Bletillae (Rhizoma Bletillae) standard extract canonical parameter is in the compound additive: the percentage by weight of Pseudobulbus Bletillae (Rhizoma Bletillae) glue mannan content in Pseudobulbus Bletillae (Rhizoma Bletillae) standard extract is 8%-12%.
The described cosmetics compound additive that contains Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract, wherein the preparation method of Herba Taraxaci standard extract is as follows:
A. Herba Taraxaci roguing, clean, be chopped into 1～3cm size;
B. use the ultrasonic water immersion method to extract, total amount of water is 10～15Kg water/every Kg dry weight raw material, extracts 40～45 ℃ of temperature, lixiviate 30-60 minute, continues to extract twice as stated above, merging filtrate with coarse filtration equipment filtered filtration residue;
C. after adding flocculating agent in the filtrate and stirring, leave standstill flocculation 7～10 hours, the centrifugal removal precipitation of 5000rpm;
D. supernatant with the aperture be 0.3～1.0nm ceramic super-filtering film under pressure 0.1 5～0.30MPa, 30～40 ℃ of temperature, cocnentration factor 1: 8～10 conditions or molecular cut off under pressure 0.25～0.35MPa, 35～45 ℃ of temperature, cocnentration factor 1: 10～12 conditions, carry out hyperfiltration treatment greater than 5000 doughnut polysulfones filter membranes, ultrafiltrate;
E. macroporous resin adsorption on the ultrafiltrate, be eluted to colourless with distilled water, 25%-95% ethanol gradient elution, eluent detects collection active component reduced vacuum and concentrates, get the Herba Taraxaci standard extract, mainly contain Flavonoids in the finished product extract, the percentage by weight of Herba Taraxaci general flavone content in the Herba Taraxaci standard extract is 18%-22%;
The described cosmetics compound additive that contains Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract, wherein the preparation method of Pseudobulbus Bletillae (Rhizoma Bletillae) standard extract is as follows:
A. after fresh Pseudobulbus Bletillae (Rhizoma Bletillae) pseudobulb being cleaned, add 3 times of 40% ethanol, after the pulverizer fragmentation, pull an oar with beater, 40 mesh filter screens filter, and after grinding with colloid mill, leave standstill 3000rpm centrifugalize after 4-6 hour, get its supernatant, it is a small amount of that filtering residue adds 40% ethanol once more, with method extraction secondary;
B. slowly stir in the edible ethanol of supernatant adding 70%-95%, leave standstill under the room temperature, separate out white floccule, sucking filtration and with anhydrous alcohol or washing with acetone adds the deionized water of 4 times of volumes again, progressively be warming up to 50 ℃ after dissolved dilution, regulate pH to 3.5-4, obtain Pseudobulbus Bletillae (Rhizoma Bletillae) standard extract; Finished product Pseudobulbus Bletillae (Rhizoma Bletillae) standard extract mainly contains Pseudobulbus Bletillae (Rhizoma Bletillae) glue mannan, and the percentage by weight of Pseudobulbus Bletillae (Rhizoma Bletillae) glue mannan content in Pseudobulbus Bletillae (Rhizoma Bletillae) standard extract is 8%-12%.
A kind of preparation technology who contains the cosmetics compound additive of Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract comprises following step:
A. prepare the Herba Taraxaci standard extract:
1. Herba Taraxaci roguing, clean, be chopped into 1～3cm size;
2. use the ultrasonic water immersion method to extract, total amount of water is 10～15Kg water/every Kg dry weight raw material, extracts 40～45 ℃ of temperature, lixiviate 30-60 minute, continues to extract twice as stated above, merging filtrate with coarse filtration equipment filtered filtration residue;
3. after adding flocculating agent in the filtrate and stirring, leave standstill flocculation 7～10 hours, the centrifugal removal precipitation of 5000rpm;
4. supernatant with the aperture be 0.3～1.0nm the ceramic super-filtering film ultrafiltration under pressure 0.15～0.30MPa, 30～40 ℃ of temperature, cocnentration factor 1: 8～10 conditions or molecular cut off under pressure 0.25～0.35MPa, 35～45 ℃ of temperature, cocnentration factor 1: 10～12 conditions, carry out hyperfiltration treatment greater than 5000 doughnut polysulfones filter membrane ultrafiltration, ultrafiltrate;
5. macroporous resin adsorption on the ultrafiltrate, be eluted to colourless with distilled water, 25%-95% ethanol gradient elution, eluent detects collection active component reduced vacuum and concentrates, get the Herba Taraxaci standard extract, mainly contain Flavonoids in the finished product extract, the percentage by weight of Herba Taraxaci general flavone content in the Herba Taraxaci standard extract is 18%-22%;
B. prepare Pseudobulbus Bletillae (Rhizoma Bletillae) standard extract:
1. after fresh Pseudobulbus Bletillae (Rhizoma Bletillae) pseudobulb being cleaned, add 3 times of 40% ethanol, after the pulverizer fragmentation, pull an oar with beater, 40 mesh filter screens filter, and after grinding with colloid mill, leave standstill 3000rpm centrifugalize after 4-6 hour, get its supernatant, it is a small amount of that filtering residue adds 40% ethanol once more, with method extraction secondary;
2. slowly stir in the edible ethanol of supernatant adding 70%-95%, leave standstill under the room temperature, separate out white floccule, sucking filtration and with anhydrous alcohol or washing with acetone adds the deionized water of 4 times of volumes again, progressively be warming up to 50 ℃ after dissolved dilution, regulate pH to 3.5-4, obtain Pseudobulbus Bletillae (Rhizoma Bletillae) standard extract; Finished product Pseudobulbus Bletillae (Rhizoma Bletillae) standard extract mainly contains Pseudobulbus Bletillae (Rhizoma Bletillae) glue mannan, and the percentage by weight of Pseudobulbus Bletillae (Rhizoma Bletillae) glue mannan content in Pseudobulbus Bletillae (Rhizoma Bletillae) standard extract is 8%-12%;
C. Herba Taraxaci extract and Pseudobulbus Bletillae (Rhizoma Bletillae) extract is even by the proportioning mixed.
Purpose of the present invention can also realize by following measures:
The raw material that the production of Herba Taraxaci standard extract is used among the preparation technology of the described cosmetics compound additive that contains Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract, it can be new fresh Herba Taraxaci plant, also can be the Herba Taraxaci herb through natural drying, inventory be all calculated with dry weight.
Herba Taraxaci roguing cleaning step among the preparation technology of the described cosmetics compound additive that contains Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract can use the vibration separation screen roguing, and fresh herb needs water to clean, and cleans 15～30 ℃ of water temperatures, cleaning process 20-30 minute.
Used macroporous resin is the D101 type among the preparation technology of the described cosmetics compound additive that contains Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract.
Used flocculating agent is a polyacrylamide among the preparation technology of the described cosmetics compound additive that contains Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract, and consumption is 0.1～0.3% of a filtrate weight.
The described application of cosmetics compound additive in skin type cream cream cosmetic that contains Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract.
The described percentage by weight of cosmetics compound additive in skin type cream cream cosmetic that contains Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract is 0.5%-5%.
The described application of cosmetics compound additive in washing class cosmetics that contains Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract.
The described percentage by weight of cosmetics compound additive in washing class cosmetics that contains Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract is 1%-10%.
Advantage of the present invention is:
The progress that is applied as natural daily use chemicals and the development of this compound additive provide more choices.In general, the compound additive that is applied to cosmetics of the present invention has following characteristics:
1. Herba Taraxaci extract has kept multiple functional activity material in the Herba Taraxaci herb morely in this compound additive, as taraxasterol, chlorogenic acid, flavone, quasi-SOD and other small-molecule substances etc.
2. the Pseudobulbus Bletillae (Rhizoma Bletillae) takes gentle low temperature cold extraction method to obtain the Pseudobulbus Bletillae (Rhizoma Bletillae) vegetable polysaccharides glue of high concentration in this compound additive, has kept integrity and its activity of its polysaccharide chain preferably, has played finely dispersed effect in this compound additive effectively.
3. adopt extractive techniques such as low-temperature ultrasonic extraction, membrane separating, macroporous resin adsorption, the leaching process gentleness, the extract dispersive property is good, microbial contamination is few, does not contain organic solvent.
4. this compound additive emulsifiability is good, be uniformly dispersed, bioactive substance is stable, can standardized production and application, function is remarkable, can be used for developing multiple cosmetic products such as effect cosmetics such as having bactericidal antiphlogistic, freckle removing and whitening, anti-Zou's health care concurrently and washing class.
The specific embodiment
The invention will be further described by the following example.
Embodiment 1:
Preparation Herba Taraxaci standard extract: the Herba Taraxaci medical material 200Kg (dry weight) with vibration separation screen roguing purification of the natural drying of learning from else's experience is ground into the 3cm segment.2M packs into
3The ultrasonic extraction jar adds water 1500L, is heated to 43 ℃, ultrasonic lixiviate 60 minutes, and drop goes out lixiviating solution.Add entry 1000L again, in 45 ℃ of ultrasonic lixiviates 40 minutes twice, drop went out lixiviating solution, and vacuum filtration merges lixiviating solution 3200L altogether.Add polyacrylamide 6Kg, stirred 10 minutes, leave standstill flocculation 10 hours.Tube bank centrifuge centrifugal (5000rpm) is removed post precipitation and is got supernatant, the use molecular cut off carries out ultrafiltration greater than 5000 doughnut polysulfones filter membrane under ultrafiltration pressure 0.35MPa, 45 ℃ of conditions of temperature, filtrate is gone up the D101 macroporous resin adsorption again, behind the distilled water eluting, adopt 95% edible ethanol as the eluant gradient elution, collect and with the multiple-effect concentrator in the concentrated effective active component of 45 reduced vacuum to the 50Kg concentrated solution.
Preparation Pseudobulbus Bletillae (Rhizoma Bletillae) extract: the fresh tuber 200Kg of the Pseudobulbus Bletillae (Rhizoma Bletillae), clean the back and add 500L 40% ethanol, after pulverizing with pulverizer, the making beating of reuse beater, 40 mesh filter screens filter, last colloid barreling mill left standstill the 3000rpm centrifugalize 4 hours, get its supernatant, it is a small amount of that residue adds ethanol once more, with method extraction secondary, merge lixiviating solution 1000L.Slowly stir in the edible ethanol of concentrated solution adding 95%, leave standstill under the room temperature, separate out white floccule, adding with anhydrous alcohol or washing with acetone after sucking filtration, add the deionized water of 4 times of volumes again, progressively be warming up to 50 ℃ after dissolved dilution, regulate pH to 4, obtain Pseudobulbus Bletillae (Rhizoma Bletillae) standard extract 100Kg.Mannan content: 10%.
Getting Herba Taraxaci extract 6% and Pseudobulbus Bletillae (Rhizoma Bletillae) extract 94% by weight percentage mixes the back and is uniformly dispersed with homogenizer and promptly gets this cosmetics compound additive.
Embodiment 2:
Preparation Herba Taraxaci standard extract: get new fresh Herba Taraxaci herb and clean the Herba Taraxaci medical material 200Kg (being equivalent to dry weight) that purified in 30 minutes, be ground into the 1cm segment with 30 ℃ of water.2M packs into
3The ultrasonic extraction jar adds water 1500L, is heated to 43 ℃, ultrasonic lixiviate 40 minutes, and drop goes out lixiviating solution.Add entry 1000L again, in 40 ℃ of ultrasonic lixiviates 30 minutes twice, drop went out lixiviating solution, and vacuum filtration merges lixiviating solution 3200L altogether.Add polyacrylamide 6Kg, stirred 10 minutes, leave standstill flocculation 10 hours.Tube bank centrifuge centrifugal (5000rpm) is removed post precipitation and is got supernatant, use under the 40 ℃ of conditions of ceramic super-filtering film ultrafiltration pressure 0.30MPa, temperature of aperture and carry out ultrafiltration as 1.0nm, filtrate is gone up the D101 macroporous resin adsorption again, behind the distilled water eluting, adopt 95% edible ethanol as the eluant gradient elution, collect and with the multiple-effect concentrator in the concentrated effective active component of 45 ℃ of reduced vacuum to the 50Kg concentrated solution.
Preparation Pseudobulbus Bletillae (Rhizoma Bletillae) standard extract: the fresh tuber 200Kg of the Pseudobulbus Bletillae (Rhizoma Bletillae), clean the back and add 500L40% ethanol, after pulverizing with pulverizer, the making beating of reuse beater, 40 mesh filter screens filter, last colloid barreling mill left standstill the 3000rpm centrifugalize 6 hours, get its supernatant, it is a small amount of that residue adds ethanol once more, with method extraction secondary, merge lixiviating solution 1000L.Slowly stir in the edible ethanol of concentrated solution adding 70%, leave standstill under the room temperature, separate out white floccule, adding with anhydrous alcohol or washing with acetone after sucking filtration, add the deionized water of 4 times of volumes again, progressively be warming up to 50 ℃ after dissolved dilution, regulate pH to 3.5, obtain Pseudobulbus Bletillae (Rhizoma Bletillae) standard extract 100Kg.Mannan content: 10%;
Getting Herba Taraxaci standard extract 12% and Pseudobulbus Bletillae (Rhizoma Bletillae) standard extract 88% by weight percentage mixes the back and is uniformly dispersed with homogenizer and promptly gets this cosmetics compound additive.
Embodiment 3: using method and the ratio of cosmetics compound additive in skin type cream cream cosmetic that contains Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract
Skin cream prescription and production technology:
Material title addition (g) composition classification and function
A phase: octadecanol 40 high fatty alcohols
Monoglyceride 15 high fatty alcohols
Squalane 30 hydrocarbons
White oil 20 hydrocarbons
Isopropyl palmitate 10 Esters
Brij72 24 surfactants
Brij721 16 surfactants
BHT 1 antioxidant
Nipalgin the third 0.5 antiseptic
Dimethicone 10
Isopropyl stearate 10 Esters
B phase: propylene glycol 25 wetting agents
Glycerol 50 wetting agents
Cosmetics compound additive 5 active component
Metagin 1.5 antiseptic
C phase: essence 1
TEA 1 pH regulator agent
Deionized water adds to 1000g
A is heated with stirring to 85 ℃ mutually, is incubated 20 minutes.B is heated with stirring to 45 ℃ mutually, and A, B merge mutually, and emulsifying is 30 minutes in emulsifying device, is cooled to 45 ℃, adds C phase material, after stirring, and is chilled to 40 ℃, discharging.Chemically examine after testing qualified after, pack.
Embodiment 4: using method and the ratio of cosmetics compound additive in skin type cream cream cosmetic that contains Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract
Skin cream prescription and production technology:
Material title addition (g) composition classification and function
A phase: octadecanol 40 high fatty alcohols
Monoglyceride 15 high fatty alcohols
Squalane 30 hydrocarbons
White oil 20 hydrocarbons
Isopropyl palmitate 10 Esters
Brij72 24 surfactants
Brij721 16 surfactants
BHT 1 antioxidant
Nipalgin the third 0.5 antiseptic
Dimethicone 10
Isopropyl stearate 10 Esters
B phase: propylene glycol 25 wetting agents
Glycerol 50 wetting agents
Cosmetics compound additive 50 active component
Metagin 1.5 antiseptic
C phase: essence 1
TEA 1 pH regulator agent
Deionized water adds to 1000g
A is heated with stirring to 90 ℃ mutually, is incubated 10 minutes.B is heated with stirring to 50 ℃ mutually, and A, B merge mutually, and emulsifying is 30 minutes in emulsifying device, is cooled to 60 ℃, adds C phase material, after stirring, and is chilled to 40 ℃, discharging.Chemically examine after testing qualified after, pack.
Embodiment 5: using method and the ratio of cosmetics compound additive in washing class cosmetics that contains Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract
The prescription of child's cleaning product and production technology:
Cosmetics compound additive: 100g natural surfactant: 150g
Ester: 30g wetting agent: 30g
Antiseptic: 0.5g essence: 0.5g
Deionized water: 689g
Production technology:
Formula components 50 ℃ of dissolvings evenly outgases, and slowly cools to 30 ℃, discharging.Chemically examine after testing qualified after, pack.
Embodiment 6: using method and the ratio of cosmetics compound additive in washing class cosmetics that contains Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract
The prescription of child's cleaning product and production technology:
Cosmetics compound additive: 10g natural surfactant: 300g
Ester: 15g wetting agent: 15g
Antiseptic: 0.5g essence: 0.5g
Deionized water: 659g
Production technology:
Formula components 50 ℃ of dissolvings evenly outgases, and slowly cools to 30 ℃, discharging.Chemically examine after testing qualified after, pack.
Claims (12)
1, a kind of cosmetics compound additive that contains Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract is characterized in that it being to comprise following components in weight percentage:
Herba Taraxaci standard extract: 6%-12% Pseudobulbus Bletillae (Rhizoma Bletillae) standard extract: 88%-94%
Wherein the compound additive canonical parameter is: the Herba Taraxaci general flavone content is 1.08%-2.64%, and Pseudobulbus Bletillae (Rhizoma Bletillae) glue mannan content is 7.04%-11.28%;
Wherein Herba Taraxaci standard extract canonical parameter is in the compound additive: the percentage by weight of Herba Taraxaci general flavone content in the Herba Taraxaci standard extract is 18%-22%;
Wherein Pseudobulbus Bletillae (Rhizoma Bletillae) standard extract canonical parameter is in the compound additive: the percentage by weight of Pseudobulbus Bletillae (Rhizoma Bletillae) glue mannan content in Pseudobulbus Bletillae (Rhizoma Bletillae) standard extract is 8%-12%.
2, the cosmetics compound additive that contains Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract according to claim 1, wherein the preparation method of Herba Taraxaci standard extract is as follows:
A. Herba Taraxaci roguing, clean, be chopped into 1～3cm size;
B. use the ultrasonic water immersion method to extract, total amount of water is 10～15Kg water/every Kg dry weight raw material, extracts 40～45 ℃ of temperature, lixiviate 30-60 minute, continues to extract twice as stated above, merging filtrate with coarse filtration equipment filtered filtration residue;
C. after adding flocculating agent in the filtrate and stirring, leave standstill flocculation 7～10 hours, the centrifugal removal precipitation of 5000rpm;
D. supernatant with the aperture be 0.3～1.0nm ceramic super-filtering film under pressure 0.15～0.30MPa, 30～40 ℃ of temperature, cocnentration factor 1: 8～10 conditions or molecular cut off under pressure 0.25～0.35MPa, 35～45 ℃ of temperature, cocnentration factor 1: 10～12 conditions, carry out hyperfiltration treatment greater than 5000 doughnut polysulfones filter membranes, ultrafiltrate;
E. macroporous resin adsorption on the ultrafiltrate, be eluted to colourless with distilled water, 25%-95% ethanol gradient elution, eluent detects collection active component reduced vacuum and concentrates, get the Herba Taraxaci standard extract, mainly contain Flavonoids in the finished product extract, the percentage by weight of Herba Taraxaci general flavone content in the Herba Taraxaci standard extract is 18%-22%;
3, the cosmetics compound additive that contains Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract according to claim 1, wherein the preparation method of Pseudobulbus Bletillae (Rhizoma Bletillae) standard extract is as follows:
A. after fresh Pseudobulbus Bletillae (Rhizoma Bletillae) pseudobulb being cleaned, add 3 times of 40% ethanol, after the pulverizer fragmentation, pull an oar with beater, 40 mesh filter screens filter, and after grinding with colloid mill, leave standstill 3000rpm centrifugalize after 4-6 hour, get its supernatant, it is a small amount of that filtering residue adds 40% ethanol once more, with method extraction secondary;
B. slowly stir in the edible ethanol of supernatant adding 70%-95%, leave standstill under the room temperature, separate out white floccule, sucking filtration and with anhydrous alcohol or washing with acetone, the deionized water that adds 4 times of volumes again, dissolved dilution after progressively being warming up to 50 ℃ is regulated pH to 3.5-4, obtains Pseudobulbus Bletillae (Rhizoma Bletillae) glue standard extract; Finished product Pseudobulbus Bletillae (Rhizoma Bletillae) standard extract mainly contains Pseudobulbus Bletillae (Rhizoma Bletillae) glue mannan, and the percentage by weight of Pseudobulbus Bletillae (Rhizoma Bletillae) glue mannan content in Pseudobulbus Bletillae (Rhizoma Bletillae) standard extract is 8%-12%.
4, a kind of preparation technology who contains the cosmetics compound additive of Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract is characterized in that comprising following step:
A. prepare Herba Taraxaci extract:
1. Herba Taraxaci roguing, clean, be chopped into 1～3cm size;
2. use the ultrasonic water immersion method to extract, total amount of water is 10～15Kg water/every Kg dry weight raw material, extracts 40～45 ℃ of temperature, lixiviate 30-60 minute, continues to extract twice as stated above, merging filtrate with coarse filtration equipment filtered filtration residue;
3. after adding flocculating agent in the filtrate and stirring, leave standstill flocculation 7～10 hours, the centrifugal removal precipitation of 5000rpm;
4. supernatant with the aperture be 0.3～1.0nm ceramic super-filtering film under pressure 0.15～0.30MPa, 30～40 ℃ of temperature, cocnentration factor 1: 8～10 conditions or molecular cut off under pressure 0.25～0.35MPa, 35～45 ℃ of temperature, cocnentration factor 1: 10～12 conditions, carry out hyperfiltration treatment greater than 5000 doughnut polysulfones filter membranes, ultrafiltrate;
5. macroporous resin adsorption on the ultrafiltrate, be eluted to colourless with distilled water, 25%-95% ethanol gradient elution, eluent detects collection active component reduced vacuum and concentrates, get the Herba Taraxaci standard extract, mainly contain Flavonoids in the finished product extract, the percentage by weight of Herba Taraxaci general flavone content in the Herba Taraxaci standard extract is 18%-22%;
B. prepare Pseudobulbus Bletillae (Rhizoma Bletillae) extract:
1. after fresh Pseudobulbus Bletillae (Rhizoma Bletillae) pseudobulb being cleaned, add 3 times of 40% ethanol, after the pulverizer fragmentation, pull an oar with beater, 40 mesh filter screens filter, and after grinding with colloid mill, leave standstill 3000rpm centrifugalize after 4-6 hour, get its supernatant, it is a small amount of that filtering residue adds 40% ethanol once more, with method extraction secondary;
2. slowly stir in the edible ethanol of supernatant adding 70%-95%, leave standstill under the room temperature, separate out white floccule, sucking filtration and with anhydrous alcohol or washing with acetone adds the deionized water of 4 times of volumes again, progressively be warming up to 50 ℃ after dissolved dilution, regulate pH to 3.5-4, obtain Pseudobulbus Bletillae (Rhizoma Bletillae) standard extract; Finished product Pseudobulbus Bletillae (Rhizoma Bletillae) standard extract mainly contains Pseudobulbus Bletillae (Rhizoma Bletillae) glue mannan, and the percentage by weight of Pseudobulbus Bletillae (Rhizoma Bletillae) glue mannan content in Pseudobulbus Bletillae (Rhizoma Bletillae) standard extract is 8%-12%;
C. Herba Taraxaci extract and Pseudobulbus Bletillae (Rhizoma Bletillae) extract is even by the proportioning mixed.
5, according to claim 2 or the 4 described preparation technologies that contain the cosmetics compound additive of Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract, it is characterized in that the raw material that Herba Taraxaci extract production is used, it can be new fresh Herba Taraxaci plant, also can be the Herba Taraxaci herb through natural drying, inventory be all calculated with dry weight.
6, according to claim 2 or the 4 described preparation technologies that contain the cosmetics compound additive of Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract, it is characterized in that Herba Taraxaci roguing cleaning step, can use the vibration separation screen roguing, fresh herb needs water to clean, clean 15～30 ℃ of water temperatures, cleaning process 20-30 minute.
7, according to claim 2 or the 4 described preparation technologies that contain the cosmetics compound additive of Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract, it is characterized in that used macroporous resin is the D101 type.
8, according to claim 2 or the 4 described preparation technologies that contain the cosmetics compound additive of Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract, it is characterized in that used flocculating agent is a polyacrylamide, consumption is 0.1～0.3% of a filtrate weight.
9, the described application of cosmetics compound additive in skin type cream cream cosmetic that contains the cosmetics compound additive of Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract of claim 1.
10. the percentage by weight in skin type cream cream cosmetic that contains the cosmetics compound additive of Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract according to claim 9 is 0.5%-5%.
11, the described application of cosmetics compound additive in washing class cosmetics that contains the cosmetics compound additive of Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract of claim 1.
12. the percentage by weight in washing class cosmetics that contains the cosmetics compound additive of Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract according to claim 11 is 1%-10%.
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| CN1927230B (en) * | 2006-09-06 | 2010-05-12 | 成都信息工程学院 | Process for extracting and purifying resin from traditional Chinese medicine by ultrasonic |
| CN101129786B (en) * | 2006-08-25 | 2010-07-07 | 山东轩竹医药科技有限公司 | Pharmaceutical composition used for ulcer of upper digestive tract |
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| CN103536462A (en) * | 2012-07-12 | 2014-01-29 | 上海家化联合股份有限公司 | Preparation method and application of bletilla striata extract |
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| CN107041864A (en) * | 2017-05-04 | 2017-08-15 | 中国林业科学研究院林产化学工业研究所 | A kind of application of dandelion extract in whitening sun protection cosmetics |
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| CN101129786B (en) * | 2006-08-25 | 2010-07-07 | 山东轩竹医药科技有限公司 | Pharmaceutical composition used for ulcer of upper digestive tract |
| CN1927230B (en) * | 2006-09-06 | 2010-05-12 | 成都信息工程学院 | Process for extracting and purifying resin from traditional Chinese medicine by ultrasonic |
| CN102958500A (en) * | 2010-06-30 | 2013-03-06 | 雀巢产品技术援助有限公司 | Use of caftaric acid and derivatives in food or beverages for regulating skin pigmentation |
| CN103536462A (en) * | 2012-07-12 | 2014-01-29 | 上海家化联合股份有限公司 | Preparation method and application of bletilla striata extract |
| CN105287282A (en) * | 2015-10-22 | 2016-02-03 | 上海应用技术学院 | Chocolate paste nutrition mask and preparation method thereof |
| CN105287282B (en) * | 2015-10-22 | 2019-04-19 | 上海应用技术学院 | A kind of chocolate lees nutritional mask and preparation method thereof |
| CN106924143A (en) * | 2017-04-11 | 2017-07-07 | 贵州盛茂白芨开发有限公司 | A kind of preparation method of bletilla shin moisturizer |
| CN106866835B (en) * | 2017-04-14 | 2019-03-01 | 张仕英 | A kind of ultrasonic technology extracts the preparation method of bletilla striata extract |
| CN106866835A (en) * | 2017-04-14 | 2017-06-20 | 张仕英 | A kind of ultrasonic technology extracts the preparation method of bletilla striata extract |
| CN107041864A (en) * | 2017-05-04 | 2017-08-15 | 中国林业科学研究院林产化学工业研究所 | A kind of application of dandelion extract in whitening sun protection cosmetics |
| CN107157838A (en) * | 2017-06-05 | 2017-09-15 | 云南摩尔农庄生物科技开发有限公司 | A kind of antioxidant composition containing walnut peel extract |
| CN107157838B (en) * | 2017-06-05 | 2020-12-08 | 云南摩尔农庄生物科技开发有限公司 | Antioxidant composition containing walnut green husk extract |
| CN112656734A (en) * | 2021-01-14 | 2021-04-16 | 科丝美诗(中国)化妆品有限公司 | Preparation method of dandelion extract, extract and application thereof |
| CN114272176A (en) * | 2021-12-29 | 2022-04-05 | 重庆佰东生物科技有限公司 | Plant extract and its extraction process and application |
| CN115177982A (en) * | 2022-06-21 | 2022-10-14 | 广东海洋大学 | Application of flocculant polyacrylamide |
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Assignee: Shantou Youqing Fine Chemical Co., Ltd. Assignor: Nanjing Institute for Comprehensive Utilization of Wild Plant, China CO-OP Contract fulfillment period: 2008.1.15 to 2018.1.14 Contract record no.: 2009440000277 Denomination of invention: Cosmestic composite additive containing dandelion and bletilla striata extract and preparing process and use in csomestics thereof Granted publication date: 20050706 License type: Exclusive license Record date: 20090422 |
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