CN1432422A - Mixing, washing, filtering and drying machine - Google Patents
Mixing, washing, filtering and drying machine Download PDFInfo
- Publication number
- CN1432422A CN1432422A CN 02112541 CN02112541A CN1432422A CN 1432422 A CN1432422 A CN 1432422A CN 02112541 CN02112541 CN 02112541 CN 02112541 A CN02112541 A CN 02112541A CN 1432422 A CN1432422 A CN 1432422A
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- washing
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- mixing
- drying machine
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Abstract
The present invention discloses a mixing, washing, filtering and drying machine comprising container, stirring shaft, man hole, transmission system and hydraulic system. The filtering bed in the middle part of the container separates the container into upper cavity and lower cavity, which is provided with vacuum pumping port to vacuate the lower cavity and thus produces diefference between the upper cavity and the lower cavity for filtering the produced matter. The hollow stirring shaft and blades are penetrated, so that hot water or hot air can be led in to heat reactant or dry product; and the stirring shaft has casing for cooling water to be led in and with spraying container-washing pipes.
Description
The present invention relates to a kind of reaction vessel, especially a kind of reaction vessel that mixing, washing, filtration, functions/drying are integrated.
At present, the reactor that uses in the chemical products production process all only has stirring, function that hybrid reaction is single, and the filtration of reaction product and dryly should adopt other special filtering machine and drying machine causes whole process flow long, and efficient is low.
The purpose of this invention is to provide a kind of mixing, washing, filtering and drying machine, it can be effectively with mix function and washing and filtering, functions/drying is combined in same reactor and finishes.
The object of the present invention is achieved like this: laterally make a filter bed in the reaction vessel of jacket type or coiled, reactor is divided into two compartments up and down, add reactant in the top compartment and mix chemically reactive, following compartment has a mouth that vacuumizes, following compartment is evacuated, make to form a pressure differential between the upper and lower chamber, with the rate of filtration of accelerated reaction product; Shaft is designed to hollow shaft, agitator design is a multi-disc scraper-type hollow blade, two rotatable joints are housed on shaft top, be connected to hot water (gas) inlet pipe respectively and go out pipe, hot water or hot vapour flow in the hollow stirrer paddle that is contained in the hollow shaft lower end by water inlet pipe and add thermal response or play the heat drying effect, the installation of blade has certain angle, and stirrer paddle is rotated counterclockwise and stirs, emit filter cake or the level and smooth filter cake and close the crack of turning clockwise; Also be hinged with two hydraulic cylinders on shaft top, can have made agitator hollow shaft, motor, reductor do vertical up-or-down movement; A flange port is arranged at the compartment bottom in the above, and connects stopple formula baiting valve, and product is finished press filtration, discharge from drain hole dry back.
Owing to adopt technique scheme, reactant is finished reaction in container after, product on filter bed by elimination moisture, and be dried, final this container of discharging, this mixing, washing, filtering and drying machine integrates mixing, washing, filtration, functions/drying, has shortened technological process greatly, has improved production efficiency.
Below in conjunction with drawings and Examples the present invention is done further explanation.
Accompanying drawing is the structure chart of mixing, washing, filtering and drying machine of the present invention.
Mixing, washing, filtering and drying machine as shown in drawings, be the jacket type reactor, manhole 4 and chuck charging aperture are arranged on it, safety valve, temperature-measuring port, visor hole etc., at container 11 bosom horizontally sets one by orifice plate, silk screen, the filter bed 3 that filter cloth is superimposed and forms, filter bed is divided into epicoele 8 and cavity of resorption 10 with container 11, shaft 7 is arranged in the epicoele 8, stirrer paddle 12, be mechanical seal between shaft 7 and the container 11, shaft 7 is a hollow shaft, stirrer paddle 12 is a hollow blade, stirrer paddle 12 is connected the lower end of shaft 7 and connects with shaft 7, two rotatable joints 15 are equipped with on shaft 7 tops, and be connected to hot water (gas) inlet pipe respectively and go out pipe, hot water or hot gas form circulation by water inlet pipe material are heated in hollow shaft 7 flows to hollow stirrer paddle 12.Hollow shaft 7 adds a sleeve pipe 16, be used for cooling off between shaft and the mechanical seal, two rotatable joints 17 are equipped with in sleeve pipe 16 upper ends, and be connected to cooling water inlet pipe and outlet pipe respectively, also be connected with spray washing pipe 18 on the sleeve pipe 16, the spray of spray washing pipe 18 relies on hydraulic pressure control in the pipe, when the outlet pipe valve open, the spray inner pipe water pressure slows down little, mouth spray is closed automatically, and this moment is only by 16 cooling effects of sleeve pipe, when closing the outlet pipe valve, hydraulic pressure increases in the pipe, and mouth spray has been opened the effect of spray washing container automatically.Stirrer paddle 12 in shaft 7 lower ends is equipped with certain angle, blade 12 can reaction stirred or is emitted filter cake when being rotated counterclockwise, when turning clockwise, blade 12 is level and smooth filter cake surface and close the crack again, and right handed blade can also slightly squeeze filter cake when reducing blade 12.
On the top of the appearance of container 11, the upper end of the shaft 7 that propelling container 11 is outer is connected with the transmission system 5 that motor, reductor form and can makes shaft 7 and hydraulic system 6 that stirrer paddle 12, motor, reductor move vertically.
One flange port 13 is set in the bottom of epicoele 8, be connected with the stopple formula baiting valve 9 that has bigger flange port with flange port through particular design, the profile of stopple formula baiting valve 9 merges mutually with the flexibility of the shell side of container 11, and the packing ring on this baiting valve 9 and the big flange can bear the identical pressure of maximum operating pressure in the container 11.In cavity of resorption 10, be provided with well cabinet frame 14, pumping equipment 2 and leakage fluid dram 1, pumping equipment 2 is fixedly connected with filter bed 3, well cabinet frame 14, also offer vacuum orifice on the cavity of resorption 10, the state that cavity of resorption 10 can be evacuated makes and forms the speed of filter pressing of a pressure differential with the accelerated reaction product between cavity of resorption 10 and the epicoele 8.
Claims (5)
1, a kind of mixing, washing, filtering and drying machine is made up of transmission device (5), shaft (7), stirrer paddle (12) that container (11), manhole (4), charging aperture, Pressure gauge, lamp mirror, safety valve, temperature-measuring port, visor hole, motor and reductor are formed; It is characterized in that at container (11) bosom horizontally set one filter bed (3), filter bed (3) is separated into epicoele (8) and cavity of resorption (10) with container (11), the stirrer paddle (12) that shaft (7) is arranged in the epicoele (8) and be connected with shaft (7), sleeve pipe (16) is arranged on the shaft (7), the bottom of epicoele (8) is provided with a flange port (13), be connected with the stopple formula baiting valve (9) that has bigger flange port with flange port (13), in cavity of resorption (10), be provided with well cabinet frame (14), pumping equipment (2), pumping equipment (2) and well cabinet frame (14), filter bed (3) is fixedly connected, and cavity of resorption also offers vacuum orifice on (10).
2, mixing, washing, filtering and drying machine according to claim 1 is characterized in that filter bed (3) is fixed together and is formed by orifice plate, silk screen, filter cloth stack.
3, mixing, washing, filtering and drying machine according to claim 2 is characterized in that sleeve pipe (16) upper end is connected to two cooling water swivel joints (17), connects water inlet pipe and outlet pipe respectively, also is connected to spray washing pipe (18) on the sleeve pipe (16).
4, mixing, washing, filtering and drying machine according to claim 3 is characterized in that shaft (7), stirrer paddle (12) are hollow and connect, and two rotatable joints (15) also are housed on the shaft (7), connects hot water (gas) inlet pipe respectively and goes out pipe.
5, mixing, washing, filtering and drying machine according to claim 4 is characterized in that the stirrer paddle (12) of shaft (7) lower end is equipped with certain angle.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 02112541 CN1432422A (en) | 2002-01-14 | 2002-01-14 | Mixing, washing, filtering and drying machine |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 02112541 CN1432422A (en) | 2002-01-14 | 2002-01-14 | Mixing, washing, filtering and drying machine |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1432422A true CN1432422A (en) | 2003-07-30 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 02112541 Pending CN1432422A (en) | 2002-01-14 | 2002-01-14 | Mixing, washing, filtering and drying machine |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1432422A (en) |
Cited By (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102274648A (en) * | 2011-08-08 | 2011-12-14 | 瓮福（集团）有限责任公司 | Vacuum separation method for electronic chemicals |
| CN101716848B (en) * | 2009-12-03 | 2011-12-28 | 浚鑫科技股份有限公司 | Device and method for treating aluminum paste |
| CN102671606A (en) * | 2012-05-21 | 2012-09-19 | 苏州市金翔钛设备有限公司 | Reaction kettle easy to clean |
| CN103819579A (en) * | 2013-12-10 | 2014-05-28 | 上海景峰制药股份有限公司 | Drying method of sodium hyaluronate |
| CN103962080A (en) * | 2014-04-29 | 2014-08-06 | 苏州市金翔钛设备有限公司 | Reaction kettle easy to clean |
| CN104922957A (en) * | 2015-06-30 | 2015-09-23 | 浙江诚信医化设备有限公司 | Filtering device of multi-functional filtering and drying machine |
| CN105435502A (en) * | 2016-01-12 | 2016-03-30 | 密友集团有限公司 | Three-in-one kettle structure |
| CN105457380A (en) * | 2016-01-12 | 2016-04-06 | 密友集团有限公司 | Security linkage protection structure for three-in-one kettle |
| CN106040124A (en) * | 2016-07-15 | 2016-10-26 | 山东国丰君达化工科技股份有限公司 | Integrated reaction kettle for uniform pressure filtration, washing and drying of solid cationic etherifying agent |
| CN106091649A (en) * | 2016-07-27 | 2016-11-09 | 湖北富邦科技股份有限公司 | A kind of dehydrate integrated device of superfine slurry |
| CN113262738A (en) * | 2021-04-12 | 2021-08-17 | 合肥通用机械研究院有限公司 | Hydraulic extrusion type integrated machine integrating reaction crystallization, slurry washing, filtering and drying functions |
| CN113262739A (en) * | 2021-04-12 | 2021-08-17 | 合肥通用机械研究院有限公司 | Hydraulic extrusion method integrating reaction crystallization, slurry washing, filtering and drying functions |
| CN113262550A (en) * | 2021-04-12 | 2021-08-17 | 合肥通用机械研究院有限公司 | Press cover for filter |
| WO2021237778A1 (en) * | 2020-05-29 | 2021-12-02 | 国家能源集团宁夏煤业有限责任公司 | Reaction kettle |
| CN114917676A (en) * | 2022-05-17 | 2022-08-19 | 恒丰泰精密机械股份有限公司 | A two unification agitated vessel of filtration washing for preparing lithium cell cathode material |
-
2002
- 2002-01-14 CN CN 02112541 patent/CN1432422A/en active Pending
Cited By (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101716848B (en) * | 2009-12-03 | 2011-12-28 | 浚鑫科技股份有限公司 | Device and method for treating aluminum paste |
| CN102274648A (en) * | 2011-08-08 | 2011-12-14 | 瓮福（集团）有限责任公司 | Vacuum separation method for electronic chemicals |
| CN102671606A (en) * | 2012-05-21 | 2012-09-19 | 苏州市金翔钛设备有限公司 | Reaction kettle easy to clean |
| CN103819579B (en) * | 2013-12-10 | 2017-01-04 | 上海景峰制药股份有限公司 | A kind of drying means of hyaluronic acid sodium |
| CN103819579A (en) * | 2013-12-10 | 2014-05-28 | 上海景峰制药股份有限公司 | Drying method of sodium hyaluronate |
| CN103962080A (en) * | 2014-04-29 | 2014-08-06 | 苏州市金翔钛设备有限公司 | Reaction kettle easy to clean |
| CN104922957A (en) * | 2015-06-30 | 2015-09-23 | 浙江诚信医化设备有限公司 | Filtering device of multi-functional filtering and drying machine |
| CN105457380A (en) * | 2016-01-12 | 2016-04-06 | 密友集团有限公司 | Security linkage protection structure for three-in-one kettle |
| CN105435502A (en) * | 2016-01-12 | 2016-03-30 | 密友集团有限公司 | Three-in-one kettle structure |
| CN105457380B (en) * | 2016-01-12 | 2017-07-04 | 密友集团有限公司 | A kind of safety interaction safeguard structure of three-in-one kettle |
| CN106040124A (en) * | 2016-07-15 | 2016-10-26 | 山东国丰君达化工科技股份有限公司 | Integrated reaction kettle for uniform pressure filtration, washing and drying of solid cationic etherifying agent |
| CN106091649A (en) * | 2016-07-27 | 2016-11-09 | 湖北富邦科技股份有限公司 | A kind of dehydrate integrated device of superfine slurry |
| WO2021237778A1 (en) * | 2020-05-29 | 2021-12-02 | 国家能源集团宁夏煤业有限责任公司 | Reaction kettle |
| CN113262739A (en) * | 2021-04-12 | 2021-08-17 | 合肥通用机械研究院有限公司 | Hydraulic extrusion method integrating reaction crystallization, slurry washing, filtering and drying functions |
| CN113262550A (en) * | 2021-04-12 | 2021-08-17 | 合肥通用机械研究院有限公司 | Press cover for filter |
| CN113262738A (en) * | 2021-04-12 | 2021-08-17 | 合肥通用机械研究院有限公司 | Hydraulic extrusion type integrated machine integrating reaction crystallization, slurry washing, filtering and drying functions |
| CN113262739B (en) * | 2021-04-12 | 2022-09-27 | 合肥通用机械研究院有限公司 | Hydraulic extrusion method integrating reaction crystallization, slurry washing, filtering and drying functions |
| CN113262738B (en) * | 2021-04-12 | 2023-02-28 | 合肥通用机械研究院有限公司 | Hydraulic extrusion type integrated machine integrating reaction crystallization, slurry washing, filtering and drying functions |
| CN114917676A (en) * | 2022-05-17 | 2022-08-19 | 恒丰泰精密机械股份有限公司 | A two unification agitated vessel of filtration washing for preparing lithium cell cathode material |
| CN114917676B (en) * | 2022-05-17 | 2024-06-07 | 恒丰泰精密机械股份有限公司 | Filtering and washing two-in-one stirring device for preparing lithium battery anode material |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |