CN1292671C - Method for producing tu-chung instant tea and its water drinking product - Google Patents
Method for producing tu-chung instant tea and its water drinking product Download PDFInfo
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- CN1292671C CN1292671C CNB2005100188219A CN200510018821A CN1292671C CN 1292671 C CN1292671 C CN 1292671C CN B2005100188219 A CNB2005100188219 A CN B2005100188219A CN 200510018821 A CN200510018821 A CN 200510018821A CN 1292671 C CN1292671 C CN 1292671C
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Abstract
The present invention applies a modern traditional Chinese medicine production method and uses eucommia bark or twigs and leaves, siberian solomonseal rhizome, haw, black plum and green tea as raw materials to prepare instant eucommia tea with the functions of treating constipation, promoting urination, reducing blood fat, regulating blood pressure, resisting senility, protecting the liver, nourishing the kidney, losing weight and beautifying and a water beverage thereof by means of a supercritical carbon dioxide extraction technology. The production method has the advantages of high extraction efficiency, short extraction time and strong selectivity. The whole operation process does not exceed 50 DEG C. The present invention can prevent effective ingredients from being damaged. The method adopts a high efficiency spray granulation technology. Three process steps including mixing, drying and fine grain preparation are completed in the same device. The present invention has the characteristics of compact equipment, short technological process, high production efficiency, etc.
Description
Technical field
The invention belongs to a kind of method for preparing drink, be specifically related to a kind of bark of eucommia instant tea and water drink preparation method.
Background technology
Main component in the folium cortex eucommiae is the canopy skin element of chlorogenic acid, aucubin, Geniposidic acid and flavonoids and Kaempferol etc.Wherein chlorogenic acid has antibiotic, antivirus action, and has remarkable increase enterogastric peristalsis and promote gastric secretion and choleretic effect; Flavones has reducing blood lipid, effect such as hypotensive; Aucubin and Geniposidic acid not only have discharge function, and can reduce neutral fat, promote the synthetic of human collagen albumen, have the reducing weight and beautifying features effect." angle medicinal herbs warp " record: sealwort has the effect of " beneficial gas in wide is transferred very the five internal organs, and flesh falls more living ".Modern study proves that sealwort can bring high blood pressure down, and reduces blood sugar, prevents artery sclerosis, strengthens the immunologic function of human body.But the hawthorn reducing blood lipid, norcholesterol helps hemangiectasis, stimulates circulation, and pain relieves the pain." world commerce comment " report, hawthorn are the strongest a kind of of anti-aging effects in the fruit.Be rich in citric acid, oleanolic acid, malic acid and carbohydrate, it has unique anti-allergic effects and choleretic effect.The article report is arranged, and the dark plum activity of fighting against senium is strong, makes body tissue's trend rejuvenation.Some is " fragile muscle and skin of having rosy cheeks " after seventy-year-old person eats dark plum.STEVIA REBAUDIANA: call sugared chrysanthemum, the composite family herbaceos perennial.Be a kind of sweet taste crop, leaf portion is the main distribution place of sweet part, and flower and stem are less, and this sweet ingredient is referred to as STEVIA REBAUDIANA.The STEVIA REBAUDIANA pharmacological action: relieve sore throat quenches the thirst, and is anti-infective, hypotensive.Now used toxin-expelling and face nourishing rheum officinale, the fleece-flower root, cassia seed, aloe and folium sennae on the market contain the anthraquinone glycoside medicine.Bark of eucommia tea on the market all adopts fried green, rubs, technical process such as oven dry, and is dark brown and the soup look bad, and pained flavour of a drug are dense, the mouthfeel extreme difference, and market sale is not smooth.Enterprise is arranged in order to improve mouthfeel, in bark of eucommia tea, add tealeaves or fragrant flower,, reduced the deal and the active ingredient of folium cortex eucommiae accordingly, reduced the health care of bark of eucommia tea though can improve mouthfeel.
Therefore, seek a kind of active ingredient that neither influences the bark of eucommia and health care and the bark of eucommia instant tea that can conveniently drink and water drink and preparation method and become the industry problem demanding prompt solution.
Summary of the invention
The objective of the invention is to use the modern Chinese herbal medicine production method, with bark of eucommia skin or branch and leaf, sealwort, hawthorn, dark plum and green tea is raw material, the utilization supercritical carbon dioxide extraction method produce have defaecation, diuresis, reducing blood lipid, adjusting blood pressure, anti-ageing, the bark of eucommia instant tea and the water drink that protect the liver kidney tonifying and reducing weight and beautifying features effect.
Realize that technical scheme of the present invention is:
A kind of bark of eucommia instant tea with anti-aging effects of the present invention, this instant tea are to be the supercritical CO of 40～200 parts of bark of eucommia skin or branch and 1000 parts on leaf, 20～100 parts of sealworts, 40～200 parts of hawthorn, 20～100 parts of dark plums and green tea by parts by weight
2The medicinal extract of extraction, the spray-dried particulate of making.This bark of eucommia instant tea is packed the heavy 2g of every bag.
A kind of bark of eucommia tea drink with anti-aging effects of the present invention, this bark of eucommia tea drink are that parts by weight are the supercritical CO of 20～100 parts of bark of eucommia skin or branch and 1000 parts on leaf, 20～100 parts of sealworts, 40～200 parts of hawthorn and dark plums
2The medicinal extract of extraction, spray-dried goods to 20～200 portions of green tea.The heavy 2g of the every bag of this bark of eucommia tea drink packing.
The preparation method of bark of eucommia instant tea of the present invention, its preparation process is:
1st, with bark of eucommia skin or branch and leaf, sealwort, hawthorn, dark plum and green tea classification, require to concoct according to Chinese Pharmacopoeia:
2nd, each medicinal material that step 1 concocted of learning from else's experience is pulverized respectively, crosses 40 orders with top sieve, takes by weighing by the proportioning metering and pulverizes material and mix;
3rd, get step 2 mixed powder particle and place supercritical extraction unit step extraction as follows:
A, control extracting pressure 35MPa, 50 ℃ of temperature are used CO
2Extracted 1 hour, controlled pressure 8MPa then, 40 ℃ of temperature are emitted the extraction medicinal extract 1 of separation, controlled pressure 5MPa again, 35 ℃ of temperature are emitted the extraction medicinal extract 2 of separation;
B, the extraction of adding volumetric concentration 95% ethanolic solution, its ethanolic solution addition is a 4ml/5g mixed powder particle, control extracting pressure 35MPa, 50 ℃ of temperature are used CO
2Extracted 1 hour, controlled pressure 8MPa then, 40 ℃ of temperature are emitted separating alcohol liquid 1, and decompression recycling ethanol gets medicinal extract 3, controlled pressure 4MPa then, 35 ℃ of temperature are emitted separating alcohol liquid 2, and decompression recycling ethanol gets medicinal extract 4;
4th, a of step 3 step gained medicinal extract 1 and the b of medicinal extract 2 and step 3 are gone on foot gained medicinal extract 3 and mix with medicinal extract 4 and mix well, spray-drying promptly gets bark of eucommia instant tea particulate, and metering packing gets product.
The preparation method of bark of eucommia tea drink of the present invention, its preparation process is:
1st, with bark of eucommia skin or skin or branch and leaf, sealwort, hawthorn and dark plum classification, require to concoct according to Chinese Pharmacopoeia;
2nd, each medicinal material that step 1 concocted of learning from else's experience is pulverized respectively, crosses 40 orders with top sieve, takes by weighing by the proportioning metering and pulverizes material and mix;
3rd, get step 2 mixed powder particle and place the step extraction as follows of supercritical extract dress:
A, control extracting pressure 35MPa, 50 ℃ of temperature are used CO
2Extracted 1 hour, controlled pressure 8MPa then, 40 ℃ of temperature are emitted the extraction medicinal extract 1 of separation, controlled pressure 5MPa again, 35 ℃ of temperature are emitted the extraction medicinal extract 2 of separation;
B, the extraction of adding volumetric concentration 95% ethanolic solution, its ethanolic solution addition is a 4ml/5g mixed powder particle, control extracting pressure 35MPa, 50 ℃ of temperature are used CO
2Extracted 1 hour, controlled pressure 8MPa then, 40 ℃ of temperature are emitted separating alcohol liquid 1, and decompression recycling ethanol gets medicinal extract 3, controlled pressure 5MPa again, 35 ℃ of temperature are emitted separating alcohol liquid 2, and decompression recycling ethanol gets medicinal extract 4;
4th, a of step 3 step gained medicinal extract 1 is mixed with medicinal extract 4 with the b step gained medicinal extract 3 of medicinal extract 2 and step 3 mix well, promptly get bark of eucommia tea drink on the green tea that spray-drying to proportioning is measured, metering packing gets product.
Used supercritical extraction unit model among the present invention: its loading capacity of HA-22-40-11C is 1L (can hold sample 260g) and 10L (can hold sample 3000g).
Bark of eucommia instant tea of the present invention and water drink add boiled water, and drinking pure water is promptly drinkable, one time one bag, the heavy 2g of every bag.
Advantage of the present invention:
1, because the good characteristic of supercritical carbon dioxide fluid, make it have the extraction efficiency height, extraction time is short, advantages such as selectivity is strong, change the polarity of fluid by the temperature, pressure that adds 95% ethanol entrainer and regulation system, optionally extract all kinds of compositions, collection extracts and separates a step and finish, simultaneous temperature is lower, and this operating process is no more than 50 ℃ of (CO
2Supercritical temperature is 33.1 ℃), can guarantee that effective ingredient is not destroyed.
2, owing to adopt the efficient spray granulation technique that three operations of combination drying system particulate are finished in same device, has facility compact, flow process is short, characteristics such as production efficiency height, easily charing and high temperature easily cause the effective ingredient loss in drying course to have avoided the Chinese medicine thick paste, so not only can make drug quality more guaranteed, and increase substantially labor productivity, reduce labour intensity.
3, bark of eucommia instant tea of the present invention and bark of eucommia tea drink have defaecation, diuresis, reducing blood lipid, adjusting blood pressure, anti-ageing, protect the liver kidney tonifying and reducing weight and beautifying features effect.
The specific embodiment
Embodiment 1
The preparation of bark of eucommia instant tea, its preparation process is:
1, with bark of eucommia skin or branch and leaf, sealwort, hawthorn, dark plum and green tea classification, requires to concoct according to Chinese Pharmacopoeia;
2, each medicinal material that step 1 concocted of learning from else's experience is pulverized respectively, crosses 40 mesh sieves, takes by weighing meal and mixes by bark of eucommia skin or branch and leaf 500g, sealwort 50g, hawthorn 100g, dark plum 50g, green tea 100g amount;
3, get step 2 mixing meal and place supercritical extraction unit (its loading capacity of model: HA-22-40-11C is that 10L can hold sample 3000g) step extraction as follows:
A, control extracting pressure 35MPa, 50 ℃ of temperature are used CO
2Extracted 1 hour, controlled pressure 8MPa then, 40 ℃ of temperature are emitted the extraction medicinal extract 1 and the controlled pressure 5MPa of separation, and 35 ℃ of temperature are emitted the extraction medicinal extract 2 of separation
B, the extraction of adding volumetric concentration 95% ethanolic solution, its ethanolic solution addition is a 4ml/5g mixing meal, control extracting pressure 35MPa, 50 ℃ of temperature are used CO
2Extracted 1 hour, controlled pressure 8MPa then, 40 ℃ of temperature are emitted separating alcohol liquid 1, and decompression recycling ethanol gets medicinal extract 3, controlled pressure 5MPa, 35 ℃ of temperature are emitted separating alcohol liquid 2, and decompression recycling ethanol gets medicinal extract 4;
4, b in a step gained medicinal extract 1 in the step 3 and medicinal extract 2 and the step 3 is gone on foot gained medicinal extract 3 and mix with medicinal extract 4 and mix well, spray-drying gets bark of eucommia instant tea particulate.And be packaged into the pouch of 2g/ bag, the bark of eucommia that gets product instant tea.
Embodiment 2
The preparation of bark of eucommia tea drink, its preparation process is:
1, with bark of eucommia skin or branch and leaf, sealwort, hawthorn and dark plum classification, requires to concoct according to Chinese Pharmacopoeia;
2, get each medicinal material and pulverize respectively, cross 40 mesh sieves, take by weighing meal and mix by bark of eucommia skin or branch and leaf 500g, sealwort 10g, hawthorn 20g, dark plum 10g, green tea 20g amount;
3, get the mixing meal and place supercritical extraction unit (its loading capacity of model: HA-22-40-11C is that 10L can hold sample 3000g) step extraction as follows:
A, control extracting pressure 35MPa, 50 ℃ of temperature are used CO
2Extracted 1 hour, controlled pressure 8MPa then, 40 ℃ of temperature are emitted the extraction medicinal extract 1 and the controlled pressure 5MPa of separation, and 35 ℃ of temperature are emitted the extraction medicinal extract 2 of separation
B, the extraction of adding 95% (volume) ethanolic solution, its ethanolic solution addition is a 4ml/5g mixing meal, control extracting pressure 35MPa, 50 ℃ of temperature are used CO
2Extracted 1 hour, controlled pressure 8MPa then, 40 ℃ of temperature are emitted separating alcohol liquid 1, and decompression recycling ethanol gets medicinal extract 3, controlled pressure 5MPa, 35 ℃ of temperature are emitted separating alcohol liquid 2, and decompression recycling ethanol gets medicinal extract 4;
4, b step gained medicinal extract 3 in a step gained medicinal extract 1 in the step 3 and medicinal extract 2 and the step 3 is mixed with medicinal extract 4 mix well, spray-drying must bark of eucommia tea drink to the green tea, and is packaged into the pouch that 2g/ wraps, the bark of eucommia that gets product tea drink.
Claims (2)
1, a kind of bark of eucommia tea with anti-aging effects is characterized in that instant tea, and this instant tea is to be the supercritical CO of 40～200 parts of bark of eucommia skin or branch and 1000 parts on leaf, 20～100 parts of sealworts, 40～200 parts of hawthorn, 20～100 parts of dark plums and green tea by parts by weight
2The medicinal extract of extraction, the spray-dried particulate of making; Its preparation process is:
1st, with bark of eucommia skin or branch and leaf, sealwort, hawthorn, dark plum and green tea classification, require to concoct according to Chinese Pharmacopoeia;
2nd, each medicinal material that step 1 concocted of learning from else's experience is pulverized respectively, crosses 40 orders with top sieve, takes by weighing by the proportioning metering and pulverizes material and mix;
3rd, get step 2 mixed powder particle and place supercritical extraction unit step extraction as follows:
A, control extracting pressure 35MPa, 50 ℃ of temperature are used CO
2Extracted 1 hour, controlled pressure 8MPa then, 40 ℃ of temperature are emitted the extraction medicinal extract 1 of separation, controlled pressure 5MPa again, 35 ℃ of temperature are emitted the extraction medicinal extract 2 of separation;
B, the extraction of adding volumetric concentration 95% ethanolic solution, its ethanolic solution addition is a 4ml/5g mixed powder particle, control extracting pressure 35MPa, 50 ℃ of temperature are used CO
2Extracted 1 hour, controlled pressure 8MPa then, 40 ℃ of temperature are emitted separating alcohol liquid 1, and decompression recycling ethanol gets medicinal extract 3, controlled pressure 5MPa then, 35 ℃ of temperature are emitted separating alcohol liquid 2, and decompression recycling ethanol gets medicinal extract 4;
4th, a of step 3 step gained medicinal extract 1 and the b of medicinal extract 2 and step 3 are gone on foot gained medicinal extract 3 and mix with medicinal extract 4 and mix well, spray-drying promptly gets bark of eucommia instant tea particulate, and metering packing gets product.
2, a kind of bark of eucommia tea with anti-aging effects is characterized in that, it is the supercritical CO of bark of eucommia skin or branch and 1000 parts on leaf, 20～100 parts of sealworts, 40～200 parts of hawthorn, 20～100 parts of dark plums by parts by weight
2The medicinal extract of extraction, the spray-dried product of making to 20～200 portions of green tea; Its preparation process is:
1st, with bark of eucommia skin or branch and leaf, sealwort, hawthorn and dark plum classification, require to concoct according to Chinese Pharmacopoeia;
2nd, each medicinal material that step 1 concocted of learning from else's experience is pulverized respectively, crosses 40 orders with top sieve, takes by weighing by the proportioning metering and pulverizes material and mix;
3rd, get step 2 mixed powder particle and place supercritical extraction unit step extraction as follows:
A, control extracting pressure 35MPa, 50 ℃ of temperature are used CO
2Extracted 1 hour, controlled pressure 8MPa then, 40 ℃ of temperature are emitted the extraction medicinal extract 1 of separation, controlled pressure 5MPa again, 35 ℃ of temperature are emitted the extraction medicinal extract 2 of separation;
B, the extraction of adding volumetric concentration 95% ethanolic solution, its ethanolic solution addition is a 4ml/5g mixed powder particle, control extracting pressure 35MPa, 50 ℃ of temperature are used CO
2Extracted 1 hour, controlled pressure 8MPa then, 40 ℃ of temperature are emitted separating alcohol liquid 1, and decompression recycling ethanol gets medicinal extract 3, controlled pressure 5MPa again, 35 ℃ of temperature are emitted separating alcohol liquid 2, and decompression recycling ethanol gets medicinal extract 4;
4th, a of step 3 step gained medicinal extract 1 is mixed with medicinal extract 4 with the b step gained medicinal extract 3 of medicinal extract 2 and step 3 mix well, spray-drying to proportioning is measured on the green tea promptly, and metering packing gets product.
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| CNB2005100188219A CN1292671C (en) | 2005-05-31 | 2005-05-31 | Method for producing tu-chung instant tea and its water drinking product |
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| CNB2005100188219A CN1292671C (en) | 2005-05-31 | 2005-05-31 | Method for producing tu-chung instant tea and its water drinking product |
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| CN1292671C true CN1292671C (en) | 2007-01-03 |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| WO2009135353A1 (en) * | 2008-05-05 | 2009-11-12 | 杭州尤美特科技有限公司 | Use of prunus mume extracts |
| CN104305450B (en) * | 2014-10-21 | 2016-08-31 | 浙江科技学院 | A kind of siberian solomonseal beverage and new process for producing thereof |
| CN104397245A (en) * | 2014-12-03 | 2015-03-11 | 巫溪县兴农茶叶专业合作社 | Traditional Chinese medicine health-care instant tea |
| CN104605057B (en) * | 2015-02-12 | 2017-09-22 | 华祥苑茶业股份有限公司 | Tea perfume gaseous beverages and its manufacture craft |
| CN104686760A (en) * | 2015-03-31 | 2015-06-10 | 刘爱民 | Liver protecting and kidney tonifying tea |
| CN105920556A (en) * | 2016-05-27 | 2016-09-07 | 惠州同富康生物科技有限公司 | Application of plum extract containing composition to preparation of blood sugar reducing health product |
| CN108308313A (en) * | 2018-04-12 | 2018-07-24 | 广西中医药大学 | A kind of blue or green money willow Hypoylycemic health tea and preparation method thereof |
| CN108740176A (en) * | 2018-06-08 | 2018-11-06 | 贵州合力茶业有限公司 | A kind of production method of tea cream |
| CN110226651A (en) * | 2019-05-31 | 2019-09-13 | 熊发翠 | Health protection tea composition |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1112426A (en) * | 1994-05-21 | 1995-11-29 | 中国科学院化学研究所 | Eucommia ulmoides extract and its preparing method and application |
| CN1381253A (en) * | 2002-05-09 | 2002-11-27 | 大连理工大学 | Supercritical CO2 fluid process for extracting and purifying medicinal component from eucommia bark |
| CN1568833A (en) * | 2003-07-25 | 2005-01-26 | 符星辉 | Eucommia instant tea |
-
2005
- 2005-05-31 CN CNB2005100188219A patent/CN1292671C/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1112426A (en) * | 1994-05-21 | 1995-11-29 | 中国科学院化学研究所 | Eucommia ulmoides extract and its preparing method and application |
| CN1381253A (en) * | 2002-05-09 | 2002-11-27 | 大连理工大学 | Supercritical CO2 fluid process for extracting and purifying medicinal component from eucommia bark |
| CN1568833A (en) * | 2003-07-25 | 2005-01-26 | 符星辉 | Eucommia instant tea |
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| CN1692787A (en) | 2005-11-09 |
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