CN1245157A - Production method of biological active compound phosphate fertilizer - Google Patents
Production method of biological active compound phosphate fertilizer Download PDFInfo
- Publication number
- CN1245157A CN1245157A CN99115104A CN99115104A CN1245157A CN 1245157 A CN1245157 A CN 1245157A CN 99115104 A CN99115104 A CN 99115104A CN 99115104 A CN99115104 A CN 99115104A CN 1245157 A CN1245157 A CN 1245157A
- Authority
- CN
- China
- Prior art keywords
- excrement
- waste
- fertilizer
- absorption chamber
- production method
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 150000001875 compounds Chemical class 0.000 title claims abstract description 18
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 15
- 239000002686 phosphate fertilizer Substances 0.000 title description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 31
- 239000003337 fertilizer Substances 0.000 claims abstract description 27
- 241001465754 Metazoa Species 0.000 claims abstract description 20
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims abstract description 20
- 239000002002 slurry Substances 0.000 claims abstract description 15
- 238000006243 chemical reaction Methods 0.000 claims abstract description 13
- 238000002156 mixing Methods 0.000 claims abstract description 12
- 239000002699 waste material Substances 0.000 claims abstract description 11
- 230000000975 bioactive effect Effects 0.000 claims abstract description 9
- 210000000988 bone and bone Anatomy 0.000 claims abstract description 7
- 239000000843 powder Substances 0.000 claims abstract description 7
- 239000010902 straw Substances 0.000 claims abstract description 7
- 239000007795 chemical reaction product Substances 0.000 claims abstract description 6
- 210000003608 fece Anatomy 0.000 claims abstract description 6
- 235000012343 cottonseed oil Nutrition 0.000 claims abstract description 4
- 238000010521 absorption reaction Methods 0.000 claims description 26
- 239000000047 product Substances 0.000 claims description 17
- 241000196324 Embryophyta Species 0.000 claims description 16
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 14
- 239000007789 gas Substances 0.000 claims description 14
- 239000000463 material Substances 0.000 claims description 13
- 239000010791 domestic waste Substances 0.000 claims description 10
- 229910052761 rare earth metal Inorganic materials 0.000 claims description 9
- 150000002910 rare earth metals Chemical class 0.000 claims description 9
- 235000000340 Solanum pseudocapsicum Nutrition 0.000 claims description 8
- 235000001978 Withania somnifera Nutrition 0.000 claims description 8
- 240000004482 Withania somnifera Species 0.000 claims description 8
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 7
- 229910052500 inorganic mineral Inorganic materials 0.000 claims description 7
- 239000004571 lime Substances 0.000 claims description 7
- 239000011707 mineral Substances 0.000 claims description 7
- 239000000203 mixture Substances 0.000 claims description 7
- 235000008733 Citrus aurantifolia Nutrition 0.000 claims description 6
- 235000011941 Tilia x europaea Nutrition 0.000 claims description 6
- 238000000855 fermentation Methods 0.000 claims description 6
- 230000004151 fermentation Effects 0.000 claims description 6
- 244000144972 livestock Species 0.000 claims description 6
- 244000144977 poultry Species 0.000 claims description 6
- 238000003860 storage Methods 0.000 claims description 5
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 4
- 239000005864 Sulphur Substances 0.000 claims description 4
- 239000002374 bone meal Substances 0.000 claims description 4
- 229940036811 bone meal Drugs 0.000 claims description 4
- 239000002367 phosphate rock Substances 0.000 claims description 4
- 239000010822 slaughterhouse waste Substances 0.000 claims description 4
- 235000019779 Rapeseed Meal Nutrition 0.000 claims description 3
- 238000000498 ball milling Methods 0.000 claims description 3
- 235000012054 meals Nutrition 0.000 claims description 3
- 238000000465 moulding Methods 0.000 claims description 3
- 239000004033 plastic Substances 0.000 claims description 3
- 229920003023 plastic Polymers 0.000 claims description 3
- 239000004456 rapeseed meal Substances 0.000 claims description 3
- 238000000926 separation method Methods 0.000 claims description 3
- 238000007873 sieving Methods 0.000 claims description 3
- 230000002269 spontaneous effect Effects 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- 239000004575 stone Substances 0.000 claims description 3
- 239000002912 waste gas Substances 0.000 claims description 3
- 239000011541 reaction mixture Substances 0.000 claims description 2
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 abstract description 11
- 239000011574 phosphorus Substances 0.000 abstract description 11
- 229910052698 phosphorus Inorganic materials 0.000 abstract description 11
- 244000188595 Brassica sinapistrum Species 0.000 abstract 1
- 235000004977 Brassica sinapistrum Nutrition 0.000 abstract 1
- 238000007689 inspection Methods 0.000 abstract 1
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
- 239000002689 soil Substances 0.000 description 7
- 238000000034 method Methods 0.000 description 5
- 229910052757 nitrogen Inorganic materials 0.000 description 4
- 239000005416 organic matter Substances 0.000 description 4
- 241000894006 Bacteria Species 0.000 description 3
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 3
- 239000011591 potassium Substances 0.000 description 3
- 229910052700 potassium Inorganic materials 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 208000034189 Sclerosis Diseases 0.000 description 2
- YYRMJZQKEFZXMX-UHFFFAOYSA-L calcium bis(dihydrogenphosphate) Chemical compound [Ca+2].OP(O)([O-])=O.OP(O)([O-])=O YYRMJZQKEFZXMX-UHFFFAOYSA-L 0.000 description 2
- 229910000389 calcium phosphate Inorganic materials 0.000 description 2
- 230000015556 catabolic process Effects 0.000 description 2
- 238000006731 degradation reaction Methods 0.000 description 2
- 244000005700 microbiome Species 0.000 description 2
- 235000019691 monocalcium phosphate Nutrition 0.000 description 2
- -1 refuse Substances 0.000 description 2
- YGSDEFSMJLZEOE-UHFFFAOYSA-N salicylic acid Chemical compound OC(=O)C1=CC=CC=C1O YGSDEFSMJLZEOE-UHFFFAOYSA-N 0.000 description 2
- 241000272525 Anas platyrhynchos Species 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 241001478240 Coccus Species 0.000 description 1
- 102000002322 Egg Proteins Human genes 0.000 description 1
- 108010000912 Egg Proteins Proteins 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 241000283073 Equus caballus Species 0.000 description 1
- 241000287828 Gallus gallus Species 0.000 description 1
- 241000238631 Hexapoda Species 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 241000283973 Oryctolagus cuniculus Species 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 241001494479 Pecora Species 0.000 description 1
- 241000282898 Sus scrofa Species 0.000 description 1
- 241000209140 Triticum Species 0.000 description 1
- 235000021307 Triticum Nutrition 0.000 description 1
- IUNLYRFGCQIVIB-UHFFFAOYSA-N [Na].[B].C1=CC=CC=C1 Chemical compound [Na].[B].C1=CC=CC=C1 IUNLYRFGCQIVIB-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 239000004411 aluminium Substances 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 230000033558 biomineral tissue development Effects 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 210000004027 cell Anatomy 0.000 description 1
- 230000006735 deficit Effects 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 230000035558 fertility Effects 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000004459 forage Substances 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 238000012009 microbiological test Methods 0.000 description 1
- 239000003895 organic fertilizer Substances 0.000 description 1
- 210000004681 ovum Anatomy 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- FJKROLUGYXJWQN-UHFFFAOYSA-N papa-hydroxy-benzoic acid Natural products OC(=O)C1=CC=C(O)C=C1 FJKROLUGYXJWQN-UHFFFAOYSA-N 0.000 description 1
- KMUONIBRACKNSN-UHFFFAOYSA-N potassium dichromate Chemical compound [K+].[K+].[O-][Cr](=O)(=O)O[Cr]([O-])(=O)=O KMUONIBRACKNSN-UHFFFAOYSA-N 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 229960004889 salicylic acid Drugs 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 230000032258 transport Effects 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G1/00—Mixtures of fertilisers belonging individually to different subclasses of C05
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F3/00—Fertilisers from human or animal excrements, e.g. manure
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/10—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
- Y02A40/20—Fertilizers of biological origin, e.g. guano or fertilizers made from animal corpses
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/141—Feedstock
- Y02P20/145—Feedstock the feedstock being materials of biological origin
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/40—Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Fertilizers (AREA)
- Processing Of Solid Wastes (AREA)
Abstract
A process for preparing bioactive compound P fertilizer includes such steps as mixing human and animal dung, rapeseed or cottonseed dregs, waste from slaughterhouse, straw and garbage to obtain a dung slurry containing water (60-80%), adding 28-30% phosphorus ore, ball grinding, adding 23-27% sulfuric acid, mixing, reaction, (4) adding bone powder (4-6 portions) per 100 portions of reaction product, fermenting, and inspection.
Description
The invention belongs to a kind of production method of compound phosphatic fertilizer, relate to a kind of production method by raw material production bio-active compound phosphatic fertilizers such as people's animal dung or rubbish, refuse, Rock Phosphate (72Min BPL), sulfuric acid.
Have phosphate fertilizer, especially calcium superphosphate now, fertilizer efficiency is single, has water absorbability, hardening property in addition, the moisture absorption caking very easily takes place in storage, transportation and application and cause fertilizer efficiency degradation failure; Use since the available phosphorus in the calcium superphosphate very easily with soil in active iron, aluminium, calcium, magnesium plasma fix, plant is difficult to be absorbed, available phosphorus reduces, so its availability is lower, generally only is about effective 10%-25%.In order to address the above problem, people adopt the method that will use again behind phosphate fertilizer and fertilizer the mixings stack retting, though the utilization ratio of this measure phosphate fertilizer increase, phosphate fertilizer sclerosis caking have still existence now.
The present invention's purpose is intended to overcome above-mentioned weak point of the prior art, a kind of storage is provided, transports and uses do not lump sclerosis, utilization ratio height, fertilizer efficiency diversification, contain the production method of the bio-active compound phosphatic fertilizer of plurality of active ingredients (beneficial microorganism, organism).
Content of the present invention is: one and the production method of bio-active compound phosphatic fertilizer, it is characterized in that comprising the following steps:
A, system excrement slurry: get (weight %, plant straw after afterwards together) 10～40% people's animal dung, 1～3% rapeseed meal or cottonseed meal, 0～30% livestock and poultry slaughterhouse waste, 0～15% are pulverized, animals and plants waste, the excess water in 0～20% domestic waste, mixing and stirring is made the excrement slurry, and to make the water content in the excrement slurry be 60～80%;
B, system excrement ore pulp material: by excrement slurry 34～48%, contain P
2O
5The ratio amount of getting of 28～30% Rock Phosphate (72Min BPL) 52～66% is made excrement ore pulp material through the ball mill mixing and ball milling;
C, wintercherry hybrid reaction: in the ratio amount of getting of excrement ore pulp material 73～77%, sulfuric acid 23～27%, sulfuric acid and excrement ore pulp material are sent into thorough mixing reaction in the agitator simultaneously, send into the curing room moulding again, the waste gas that produces in the reaction is sent into the off gas treatment chamber;
D, add bone meal: add the ratio of 4～6 parts of animal bone powders in per 100 parts of wintercherry reaction product, get animal bone powder and add in the reaction product and mix, make compound;
E, fermentation: compound is sent into indoor stacking, stack 1.5～2.5 meters of height, put scarifying after 3～7 days, 28～35 ℃ of following spontaneous fermentations 15～25 days, promptly make product again;
F, product are packed after checking, are put in storage.
In the content of the present invention: can also be added with rare earth fertilizer, add the ratio of 0.04～0.07 rare earth fertilizer in per 100 parts of products, get rare earth fertilizer and add in the described excrement ore pulp of step (b) and mix.
The sorting of the animals and plants waste described in the described step of content of the present invention (a) in the domestic waste comprises the following steps:
(1) primary election: select vial in the domestic waste, plastics, stone etc. and can not utilize thing, discard;
(2) rubbish is sent in the tank, stirred, make adhesion thing separation in the rubbish;
(3) with high pressure water with rubbish and water mixture dash through shaking-sieving from, sieve goes silt, other parts to send in the settling bowl;
(4) from settling bowl, take out the animals and plants waste.
Off gas treatment chamber described in the described step of content of the present invention (c) is by absorption chamber (8) that exhaust gas entrance (1) and water port (12) are arranged, the pipe connecting (5) that head end directly is equipped with blower fan (6) is communicated with absorption chamber (8), tail end has the absorption chamber (9) of exhaust passage (2) and water port (13), be arranged in the absorption chamber (8), be equipped with 1～4 strainer (10) of calcium carbonate mineral, be arranged in the absorption chamber (9), be equipped with 3～16 strainers arranged side by side (11) of calcium carbonate mineral and sulphur, be arranged at absorption chamber (8) and absorption chamber (9) top, the hydraulic pipe (3) of one group of sprinkler head (4) is installed, be communicated with water port (12) and water port (13) settling tank (16), the lime pond (14) that is communicated with settling tank, the circulatory pool (15) that is communicated with lime pond (14), and the pump (7) that is communicated with circulatory pool (15) and hydraulic pipe (3) is formed.
Compared with prior art, the present invention has the row characteristics:
(1) overcome the caking degradation phenomena that existing phosphate fertilizer takes place fully in storage, transportation and application, improve the utilization ratio of available phosphorus, use year after year, can protect soil organism mineralising and available phosphorus, product structure improves, keep water, fertilizer, gas, the heat of soil to coordinate, thereby guarantee crop growth and increasing both production and income;
(2) raw material is easy to get, make be difficult to handle and cause the people of environmental pollution or livestock and poultry (chicken, duck, pig, ox, sheep, horse, rabbit etc.) ight soil, livestock and poultry slaughterhouse waste (for example: livestock and poultry offal etc.), plant stalk (for example: the useless forage on straw, wheat straw, beautiful material bar, rape straw, grassland, paper mill or the like), and domestic waste obtains utilizing, turn waste into wealth, and be beneficial to environment protection;
(3) fertilizer efficiency diversification; Product of the present invention not only contains available phosphorus, also has multiple elements such as abundant organic matter, beneficial microorganism, nitrogen, potassium, integrates fertilizer and inorganic fertilizer;
(4) product of the present invention proves through being applied to various farm crop, has easily by plant absorbing, makes the obvious drought resisting of farm crop, resistant to lodging, disease and insect resistance, strong seed volume increase;
(5) product is used for soil and has and keep organic corruption to plant the mineralization rate of matter, keeps soil to continue fertility and characteristics such as loose, and inexpensive, practical.
Accompanying drawing is an off gas treatment cell structure principle schematic in the invention.
Among the figure: 1-exhaust gas entrance, 2-exhaust passage, 3-hydraulic pipe, 4-sprinkler head, 5-pipe connecting, 6-blower fan, 7-pump, 8-absorption chamber, 9-absorption chamber, 10-strainer, 11-strainer, 12-water port, 13-water port, 14-lime pond, 15-circulatory pool, 16-settling tank.
The invention will be further described passing through embodiment down:
A kind of production method of bio-active compound phosphatic fertilizer, comprise the following steps:
A, system excrement slurry: get (weight %, plant straw after afterwards together) 10～40% people's animal dung, 1～3% rapeseed meal or cottonseed meal, 0～30% livestock and poultry slaughterhouse waste, 0～15% are pulverized, animals and plants waste, the excess water in 0～20% domestic waste, mixing and stirring is made the excrement slurry, and to make water content in the excrement slurry be that 60～80% (water content in the excrement slurry can be learnt by mensuration, moisture deficit can be added water, moisturely excessively transfers to standard by adding the dry raw material;
The sorting of the animals and plants waste in the described domestic waste can be chosen through the following steps:
(1) primary election: select vial in the domestic waste, plastics, stone etc. and can not utilize thing, discard;
(2) rubbish is sent in the tank, stirred, make adhesion thing separation in the rubbish;
(3) with high pressure water with rubbish and water mixture dash through shaking-sieving from, sieve goes silt, other parts to send in the settling bowl;
(4) from settling bowl, take out the animals and plants waste.
B, system excrement ore pulp material: by excrement slurry 34～48%, contain P
2O
5The ratio of 28～30% Rock Phosphate (72Min BPL) 52～66% is the amount of getting respectively, through ball mill both mixing and ball milling is made excrement ore pulp material;
C, wintercherry hybrid reaction: in the ratio of excrement ore pulp material 73～77%, sulfuric acid 23～27% amount of getting respectively, sulfuric acid and excrement ore pulp material are sent into thorough mixing reaction in the agitator simultaneously, and (physical strength and the time of control wintercherry hybrid reaction is: linear speed 12-20 p.s. rice, time 3-4 minute; Sulfuric acid makes the indissoluble phosphorus in the phosphorus ore slurry be replaced into soluble available phosphorus, and the heat that produces in acid and the reaction kills harmful worm's ovum and harmful bacteria, and making thick organic matter transformation is active organic matter.), product is sent into the curing room moulding, and the waste gas that produces in the reaction is sent into the off gas treatment chamber;
D, add bone meal: add the ratio of 4～6 parts of animal bone powders (the bone meal fineness is 100 orders) in per 100 parts of wintercherry reaction product, get animal bone powder and add in the product and mix, make compound (pH value is 3.5～5.5);
E, fermentation: compound is sent into indoor stacking, stack 1.5～2.5 meters of height, put scarifying after 3～7 days, again 28～35 ℃ of following spontaneous fermentations 15～25 days, surperficial adularescent or grey enzyme bacterium (for vinelandii, coccus etc.) promptly make product;
F, the examination and test of products.1. available phosphorus is pressed the ZBG21003-87 standard test; 2. the organic soil organism potassium bichromate titrimetric method mensuration of pressing; 3. bacterium is pressed the microbiology observation or presses the GB13093-91 standard, also can measure with reference to microbiological Test method in ISO4833-1987 international food and the animal-feed; 4. nitrogen disappears by the full nitrogen of organic fertilizer, sulfuric acid, salicylic acid and boils distillation method mensuration; 5. potassium is pressed back benzene boron sodium method mensuration;
Standard: available phosphorus is (with P
2O
5Meter) 8～12%, organic matter 2～10%, total plate count 1 * 10
8～5 * 10
8Individual/gram, moisture content＜18%, total nitrogen＞0.005%, effectively potassium is (with K
2The O meter)＞0.1%, pH value＜6.5.
G, packing.In mould and outer compile every bag of net weight 50kg ± 0.5kg.Warehouse-in etc. is sold.
In addition, can also add rare earth fertilizer in the embodiment product: add the ratio of 0.04～0.07 rare earth in per 100 parts of finished products, get rare earth fertilizer and add in the described excrement ore pulp of step (b) and mix.
Off gas treatment chamber described in the step (c) is by the absorption chamber 8 that exhaust gas entrance 1 and water port 12 are arranged, the pipe connecting 5 that head end directly is equipped with blower fan 6 is communicated with absorption chamber 8, tail end has the absorption chamber 9 of exhaust passage 2 and water port 13, be arranged in the absorption chamber 8, be equipped with 1～4 strainer 10 of calcium carbonate mineral (Φ 8～Φ 10cm), be arranged in the absorption chamber 9, be equipped with 3～16 strainers arranged side by side 11 of calcium carbonate mineral (Φ 0.3～Φ 0.5cm) and sulphur, be arranged at absorption chamber 8 and absorption chamber 9 tops, the hydraulic pipe 3 of one group of sprinkler head 4 is installed, be communicated with water port 12 and water port 13 settling tank 16, the lime pond 14 that is communicated with settling tank, the circulatory pool 15 that is communicated with lime pond 14, and the pump 7 that is communicated with circulatory pool 15 and hydraulic pipe 3 is formed (referring to accompanying drawing).After the absorption of the fluoro-gas that produces in the wintercherry hybrid reaction calcium carbonate mineral and sulphur in this chamber and the absorption of circulation liming, through exhaust passage 2 dischargings gas promptly reach state specified standards.
Adopt embodiment 1～7 each component consumption of aforementioned production method to see table, product all can reach described standard.
The invention is not restricted to the foregoing description, content of the present invention is described all can implement and have good result, slightly.
Claims (4)
1, a kind of production method of bio-active compound phosphatic fertilizer is characterized in that comprising the following steps:
A, system excrement slurry: get (weight %, plant straw after afterwards together) 10～40% people's animal dung, 1～3% rapeseed meal or cottonseed meal, 0～30% livestock and poultry slaughterhouse waste, 0～15% are pulverized, animals and plants waste, the excess water in 0～20% domestic waste, mixing and stirring is made the excrement slurry, and to make the water content in the excrement slurry be 60～80%;
B, system excrement ore pulp material: by excrement slurry 34～48%, contain P
2O
5The ratio amount of getting of 28～30% Rock Phosphate (72Min BPL) 52～66% is made excrement ore pulp material through the ball mill mixing and ball milling;
C, wintercherry hybrid reaction: in the ratio amount of getting of excrement ore pulp material 73～77%, sulfuric acid 23～27%, sulfuric acid and excrement ore pulp material are sent into thorough mixing reaction in the agitator simultaneously, send into the curing room moulding again, the waste gas that produces in the reaction is sent into the off gas treatment chamber;
D, add bone meal: add the ratio of 4～6 parts of animal bone powders in per 100 parts of wintercherry reaction product, get animal bone powder and add in the reaction product and mix, make compound;
E, fermentation: compound is sent into indoor stacking, stack 1.5～2.5 meters of height, put scarifying after 3～7 days, 28～35 ℃ of following spontaneous fermentations 15～25 days, promptly make product again;
F, product are packed after checking, are put in storage.
2, press the production method of the described bio-active compound phosphatic fertilizer of claim 1, it is characterized in that: also be added with rare earth fertilizer, the ratio that promptly adds 0.04～0.07 rare earth fertilizer in per 100 parts of products is got rare earth fertilizer and is added in the described excrement ore pulp of step (b) and mix.
3, by the production method of the described bio-active compound phosphatic fertilizer of claim 1, it is characterized in that: the sorting of the animals and plants waste described in the step (a) in the domestic waste comprises the following steps:
(1) primary election: select vial in the domestic waste, plastics, stone etc. and can not utilize thing, discard;
(2) rubbish is sent in the tank, stirred, make adhesion thing separation in the rubbish;
(3) with high pressure water with rubbish and water mixture dash through shaking-sieving from, sieve goes silt, other parts to send in the settling bowl;
(4) from settling bowl, take out the animals and plants waste.
4, production method by the described biological compound phosphatic fertilizer of claim 1, it is characterized in that: off gas treatment chamber described in the step (c) is by absorption chamber (8) that exhaust gas entrance (1) and water port (12) are arranged, the pipe connecting (5) that head end directly is equipped with blower fan (6) is communicated with absorption chamber (8), tail end has the absorption chamber (9) of exhaust passage (2) and water port (13), be arranged in the absorption chamber (8), be equipped with 1～4 strainer (10) of calcium carbonate mineral, be arranged in the absorption chamber (9), be equipped with 3～16 strainers arranged side by side (11) of calcium carbonate mineral and sulphur, be arranged at absorption chamber (8) and absorption chamber (9) top, the hydraulic pipe (3) of one group of sprinkler head (4) is installed, be communicated with water port (12) and water port (13) settling tank (16), the lime pond (14) that is communicated with settling tank, the circulatory pool (15) that is communicated with lime pond (14), and the pump (7) that is communicated with circulatory pool (15) and hydraulic pipe (3) is formed.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB991151046A CN1139557C (en) | 1999-08-25 | 1999-08-25 | Production method of biological active compound phosphate fertilizer |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB991151046A CN1139557C (en) | 1999-08-25 | 1999-08-25 | Production method of biological active compound phosphate fertilizer |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1245157A true CN1245157A (en) | 2000-02-23 |
| CN1139557C CN1139557C (en) | 2004-02-25 |
Family
ID=5278119
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB991151046A Expired - Fee Related CN1139557C (en) | 1999-08-25 | 1999-08-25 | Production method of biological active compound phosphate fertilizer |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1139557C (en) |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2003014043A1 (en) * | 2001-07-31 | 2003-02-20 | Guoliang Zhao | High efficiency active bioorganic fertilizer and its production method |
| CN100387555C (en) * | 2005-02-25 | 2008-05-14 | 邹鸿祥 | Production process of active organic fertilizer |
| CN100408519C (en) * | 2006-11-27 | 2008-08-06 | 邱云生 | Quick decomposition process for dungs and droppings |
| CN101195545B (en) * | 2007-12-12 | 2010-06-16 | 任峰果 | Biological fertilizer |
| CN102424612A (en) * | 2011-09-08 | 2012-04-25 | 河南省洁苑环保科技有限公司 | Rapid degradation and fertilizer making technology for degradable organic matter in household garbage |
| CN102430557A (en) * | 2011-09-08 | 2012-05-02 | 河南省洁苑环保科技有限公司 | Household waste hydraulic separation technology |
| WO2016107560A1 (en) * | 2014-12-30 | 2016-07-07 | 成都新柯力化工科技有限公司 | Ecological functional phosphorus fertilizer and preparation method therefor |
| CN105766593A (en) * | 2016-04-28 | 2016-07-20 | 开县安德农业科技开发有限公司 | Nutrient Soil and method for cultivation of Caulis Dendrobii |
| CN107586156A (en) * | 2017-09-09 | 2018-01-16 | 安徽瑞虎肥业有限公司 | A kind of organic fertilizer production equipment |
-
1999
- 1999-08-25 CN CNB991151046A patent/CN1139557C/en not_active Expired - Fee Related
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2003014043A1 (en) * | 2001-07-31 | 2003-02-20 | Guoliang Zhao | High efficiency active bioorganic fertilizer and its production method |
| CN100387555C (en) * | 2005-02-25 | 2008-05-14 | 邹鸿祥 | Production process of active organic fertilizer |
| CN100408519C (en) * | 2006-11-27 | 2008-08-06 | 邱云生 | Quick decomposition process for dungs and droppings |
| CN101195545B (en) * | 2007-12-12 | 2010-06-16 | 任峰果 | Biological fertilizer |
| CN102424612A (en) * | 2011-09-08 | 2012-04-25 | 河南省洁苑环保科技有限公司 | Rapid degradation and fertilizer making technology for degradable organic matter in household garbage |
| CN102430557A (en) * | 2011-09-08 | 2012-05-02 | 河南省洁苑环保科技有限公司 | Household waste hydraulic separation technology |
| WO2016107560A1 (en) * | 2014-12-30 | 2016-07-07 | 成都新柯力化工科技有限公司 | Ecological functional phosphorus fertilizer and preparation method therefor |
| CN105766593A (en) * | 2016-04-28 | 2016-07-20 | 开县安德农业科技开发有限公司 | Nutrient Soil and method for cultivation of Caulis Dendrobii |
| CN107586156A (en) * | 2017-09-09 | 2018-01-16 | 安徽瑞虎肥业有限公司 | A kind of organic fertilizer production equipment |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1139557C (en) | 2004-02-25 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN1280239C (en) | Organic fertilizer composed of waste liquid and waste residue and decomposing leaven from sugar refinery and method for preparing the same | |
| CN101200387B (en) | Preparation of microorganium fertilizer by using bacilluslaterosporus and bacillus subtilis | |
| CN102351589B (en) | Bio-organic fertilizer produced by use of municipal sludge and production method thereof | |
| CN103449911B (en) | Medium soil produced from active sludge building waste residue and production method of medium soil | |
| CN103694004B (en) | A kind of preparation method of seaweed bio organic fertilizer | |
| CN101503315A (en) | Humic acid biological organic composite bacterial manure and production process | |
| CN102584371A (en) | Method for making biological organic fertilizer by using rice straws as main raw material | |
| CN106754461A (en) | A kind of biological flocculation and its preparation method and application | |
| CN104016748A (en) | Organic compound fertilizer and manufacturing method thereof | |
| CN101759452A (en) | Preparation method for bio-organic fertilizer | |
| CN104030751A (en) | Bioorganic compound fertilizer and preparation method thereof | |
| CN101284742A (en) | Preparation process for worm cast organic fertilizer based on water hyacinth | |
| CN101538177A (en) | Production and use method of organic bio-fertilizer | |
| CN106946630A (en) | A kind of organic fungi-manure using sludge as raw material and preparation method thereof | |
| CN103613447A (en) | Polyelement slow release granular fertilizer with high fertilizer efficiency and preparation method thereof | |
| CN104003773A (en) | Biological organic fertilizer and preparation method thereof | |
| CN102344319A (en) | Microbial organic fertilizer produced by papermaking sludge and producing method thereof | |
| CN1408683A (en) | Biological organic composite fertilizer and its producing method | |
| CN102173887A (en) | Production method of biological organic fertilizer containing Avermectins | |
| CN1139557C (en) | Production method of biological active compound phosphate fertilizer | |
| CN1315757C (en) | Biological organic full-ingradient-fertilizer | |
| CN103641593A (en) | Method for preparing garden media from biogas slurry | |
| CN103265354A (en) | Bio-organic fertilizer prepared from modeling clay slag as main material and preparation method thereof | |
| CN102557808A (en) | Method for preparing organic-inorganic potassium-calcium-silicon compound fertilizer | |
| CN103044099A (en) | Method for making special novel fertilizer for strawberries |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C06 | Publication | ||
| PB01 | Publication | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C19 | Lapse of patent right due to non-payment of the annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |