CN1240815C - Powder or granule formed fat/oil and its production method - Google Patents
Powder or granule formed fat/oil and its production method Download PDFInfo
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- CN1240815C CN1240815C CNB031330274A CN03133027A CN1240815C CN 1240815 C CN1240815 C CN 1240815C CN B031330274 A CNB031330274 A CN B031330274A CN 03133027 A CN03133027 A CN 03133027A CN 1240815 C CN1240815 C CN 1240815C
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
- A23D9/04—Working-up
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/06—Production of fats or fatty oils from raw materials by pressing
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- Life Sciences & Earth Sciences (AREA)
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- Chemical Kinetics & Catalysis (AREA)
- Polymers & Plastics (AREA)
- Food Science & Technology (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
- Seasonings (AREA)
- Edible Oils And Fats (AREA)
- Seeds, Soups, And Other Foods (AREA)
Abstract
Provided is powdery or granular oils and fats, starting from various oils and fats, which contain a relatively large amount of oils and fats without emulsifying them, give out flavor satisfactorily and exhibit high flowability and high solubility. The powdery or granular oils and fats are manufactured using oils and fats together with a substrate for including the oils and fats and a polyol. In the manufacture, the water content, the maximum particle size, the average particle size and the angle of repose are adjusted to at most 15 wt%, at most 10 mm, at most 5 mm and at most 70[deg.], respectively.
Description
Technical field
The present invention relates to a kind of fats/oils that contains the powdery or the granular form of polyvalent alcohol, the invention still further relates to its production method.
Background technology
Recently find that the requirement of originating as fats/oils in bread, cake, biscuit, Deep-fried doughnut, pancake and ice-creams and other the various ready-to-eat Preblendes for the fats/oils of powder-form increases day by day.
The method of the fats/oils of at present used production powder-form comprises (1) freezing and pulverizing method, wherein will have dystectic solid fat pulverizes at low temperatures, produce powder, (2) spray cooling, wherein fused edible-fat/oil is sprayed to be used for the refrigerated freezer compartment (referring to, the JP patent application is not examined and is disclosed clear 54-126207), (3) absorption process, wherein fats/oils is absorbed in lipotropy base-material such as starch producing or the Mierocrystalline cellulose, and (4) spray-drying process, wherein by using synthetic emulsifier such as sugar ester, protein such as casein or gelatin, starch or the like is produced emulsion oil-in-water, and with emulsion spraying drying (examine disclose clear 55-150845 referring to, JP patent application).
A kind of fats/oils composition of the powder-form that is suitable for cooking is disclosed among the JP patent publication No. 61-13774.Containing fusing point in this composition is 35 ℃ or lower edible-fat/oil, zymolytic starch, glycerine-polyunsaturated fatty acid ester and/or sorbitan-unsaturated fatty acid ester.
Yet the freezing and pulverizing method of above-mentioned (1), its defective are that the fats/oils of the powder-form of gained is not easy to melt in mouth, because this method is only applicable to winterized stearin, the fusing point of winterized stearin is high at least 60 ℃.The product of Sheng Chaning also has following shortcoming by this method: products obtained therefrom has winterized stearin institute inherent peculiar smell, and this product is not suitable for using in product such as cake compound in every day.
The spray cooling of above-mentioned (2) also has following defective: promptly this method only is applicable to solid fat, and this method only just can be used when the fat of gained powder-form need be stored under the refrigeration condition and transport.
The fats/oils of the powder-form that the absorption process by above-mentioned (3) is produced, its defective is when flowability when forfeiture that need avoid oozing out because of fats/oils the gained powdery fats/oils that causes, the content of its fats/oils also is reduced, and when increasing the content of fats/oils, the flowability of gained powdery fats/oils is lowered because of oozing out of fats/oils.
The spray-drying process of above-mentioned (4), its defective be only when water content increases to the 70-90% high-content this method could implement, this is because have high viscosity through emulsive solution, thereby just must will evaporate a large amount of moisture, thereby causes the significantly increase of cost of energy.Another defective is by the fats/oils of the powder-form of this method production, only can be used for limited application, because the fats/oils of this powder-form becomes emulsified and opacification when dissolving.
For example, fats/oils is mixed with the soup stock that is used for Chinese style noodles soup stock or Chinese style soup stock (soup stock) compound or with the powdery seasoning matter, expectation is in case add hot water or cold water in the powder to and will disengage fats/oils rapidly.Yet, the emulsified and opacification that after adding water, can become of the fats/oils in spray dried prod, and the fats/oils powder-product major part in market all is this spray dried prod.When used fats/oils is that its local flavor will almost be lost if fats/oils is emulsified when increasing flavor oil.
Except that than, being used to described in the above-mentioned patent publication us cooked the fats/oils composition of the powder-form of purpose, its defective is to use zymolytic starch (Pine Flow, Matsutani chemical industry company limited) just can produce the fats/oils composition of this powder-form, and this zymolytic starch has extremely big surface-area.
Under these situations, for soup stock that contains fats/oils and food flavouring, for example, the powdery soup stock that is used for fast food Chinese style noodles soup stock, the soup stock that is used for Chinese style or Western-style soup stock, powdery cream flour paste base-material, the Chinese style food flavouring, seasoning matter, mayonnaise or the like, fats/oils is with the independent packaged form of fats/oils (promptly, the form of separating with other component) provides, the realization of this mode is by producing the product of liquid or pasty state form, perhaps by very small amount of fats/oils is infiltrated in flavouring base material, so that reach the degree that fats/oils is not oozed out from powder.
Summary of the invention
An object of the present invention is to provide the fats/oils of a kind of powdery or granular form, it can keep containing a large amount of relatively fats/oils emulsifying effect not take place simultaneously, the fats/oils of this powdery or granular form has the solvability of height and the flowability of height, and has wherein kept the original flavor and the fragrance of fats/oils.Another object of the present invention provides the production method of the fats/oils of this powdery or granular form.
For realizing these purposes, the invention provides the fats/oils of a kind of powdery or granular form, it contains fats/oils, is used to keep the base-material and the polyvalent alcohol of fats/oils, the fats/oils of powdery or granular form wherein, the as many as 15wt% of its water content, maximum particle size for as many as 10mm and average grain granularity maximum to 5mm, and the slope of repose that shows for maximum to 70 degree.
In the fats/oils of producing powdery or granular form, by except that fats/oils, also be used to keep the base-material and the polyvalent alcohol of fats/oils, and by water content being reduced to as many as 15wt%, can produce its inside and have the relative significant quantities of fat/powdery of oil or the fats/oils of granular form, but avoid or reduced fats/oils from product, oozing out, and irrelevant with the type of fats/oils.Simultaneously, can easily produce have the slope of repose for maximum to the powderies of 70 degree or the fats/oils of granular form.In addition, keep by used being used to of suitable selection fats/oils base-material type and maximum particle size is adjusted to maximum to 10mm with the average grain granularity is adjusted to maximum to 5mm, can easily improve the solvability of the fats/oils of powdery or granular form.
In the fats/oils of this powdery or granular form, apparent filling tap density is preferably 0.55-0.85g/cm
3, because in this scope, can increase the fats/oils content of per unit volume in the fatty oil of powdery or granular form when apparent filling tap density.
For realizing these purposes, the present invention also provides a kind of method that is used to produce the fats/oils of powdery or granular form, may further comprise the steps: will contain fats/oils, be used to keep the base-material of fats/oils and the starting material of liquid polyol to stir, till material evenly.The preparation starting material makes the ratio of fats/oils, in 100 weight part fats/oils be used to keep the gross weight of the base-material of fats/oils, is the 1-70 weight part, and the ratio of liquid polyol, in the said gross weight of 100 weight parts, is the 0.1-10 weight part.
The fats/oils of powdery of the present invention or granular form can be by using fats/oils, be used to keep the base-material and the liquid polyol of fats/oils in aforesaid ratio, and these materials are carried out even stir process produce.
In this production method, by will can easily producing the fats/oils that per unit volume contains the powdery or the granular form of higher amount fats/oils through the further compacting under the pressure of 0.01-1000MPa of material of even stir process.
Embodiment
Next, will the fats/oils and the production method thereof of powdery of the present invention or granular form be described in detail thoroughly.
The fats/oils of A, powdery or granular form
As mentioned above, contain fats/oils in the fats/oils of powdery of the present invention or granular form, be used to keep the base-material of fats/oils and polyvalent alcohol as its main component.These key components are described below.
(1) fats/oils
The used fats/oils of the present invention has no particular limits, and used fats/oils can be solid, semisolid or liquid aliphatic/oil or its mixture that derives from plant or animal.Fats/oils among the present invention also can be by with physics mode such as hot extracting, from spice, herbaceous plant, animal meat, the flesh of fish, shell or have extracting flavour substances other material of plant, animal or other fats/oils and the flavor oil (increasing flavor oil) that produces; Perhaps by dissolving in the material of low boiling point solvent such as vinylchlorid, hexane, acetone, ether etc., use this solvent and distill solvent and extract the oleoresin of acquisition from plant or animal material, essential oil, dyestuff, fats/oils, resin, perfume composition etc.
Fats/oils used among the present invention has proportion 0.75-1.00g/cm usually
3
(2) be used to keep the base-material of fats/oils
Term used herein " is used to keep the base-material of fats/oils " and is meant be used to comprise or the fats/oils base-material of portion within it that infiltrates.This base-material that is used to keep fats/oils is hydrophilic materials preferably.
Being used to keep the used hydrophilic materials of base-material of fats/oils can be any material that comprises that the following stated material is at least a: (i) hydrophilic protein matter, as gelatin, casein, sodium-caseinate, whey-protein, albumin etc.; (2) starch and the treated starch (starch powder of acid dilution; Sumstar 190; Pre-gelatinized starch; Cross-linking starch is wherein introduced polyfunctional group with two or more hydroxyls of bonding; The starch of wet heat treatment; Graft starch; Have wherein carboxymethyl of introducing, hydroxyalkyl etc. etherification starch and with the esterification starch of reactions such as acetate, phosphoric acid); (iii) wetting ability polysaccharide, for example Lalgine, Sudan Gum-arabic, guar gum, xanthan gum, pectin, carboxymethyl cellulose, agarose or the like; The (iv) protein of partial hydrolysis is as hydrolyzed animal protein (HAP) and hydrolyzing plant animal (HVP) or the like; (the v) starch of partial hydrolysis is as dextrin and oligose or the like; (the vi hydrophilic amino acid is as L-glutamic acid and Methionin and their salt; (vii) sugared, as lactose; (viii) organic acid is as acetate, citric acid, succsinic acid and hexanodioic acid and their salt; (ix) nucleosides hydrochlorate and Nucleotide, as 5 '-Sodium Inosinate and 5 '-sodium guanylate; And the salt of (x) using in the bread and cheese, as sodium-chlor, Repone K or the like; Not necessarily use other material.
Containing at least a edible composition of above-mentioned hydrophilic materials also can be with acting on the base-material that keeps fats/oils.The example of this edible composition comprises the foodstuff that (i) produces by processing animals meat, the flesh of fish, shell, egg, milk, cereal, vegetables, fruit, marine alga etc.; The (ii) powder of producing by above-mentioned foodstuff is dry and efflorescence or extraction, for example egg white powder, milk powder, powdery whey, soyflour, pre-gelatinization flour, bake brown roux, starch hydrolysis powder, carry powder, powdered juice or the like; And the (iii) powder of natural flavouring (HAP, HVP etc.), soy sauce, vinegar, sugar, miso, tomato ketchup or the like.
The base-material that is used to keep fats/oils that the present invention is used, its apparent filling tap density is generally 0.30-1.10g/cm
3, preferred 0.35-0.90g/cm
3, first-selected 0.40-0.80g/cm
3, but apparent filling tap density is not limited to this scope especially.
The base-material that is used to keep fats/oils that the present invention is used, its shape without limits.Yet base-material preferably is the powdery that comprises spheroidal particle or granular, and the grain graininess of base-material is preferably maximum to passing 50 orders, more preferably, maximum to passing 100 orders.
The preferably as many as 15wt% of water content, more preferably as many as 10wt%.The used base-material that is used to keep fats/oils does not preferably contain the emulsification base-material, as Yelkin TTS.
(3) polyvalent alcohol
Used polyvalent alcohol can be non-toxicity dibasic alcohol, as glycerine or propylene glycol, sugar or sugar alcohol.
The example of this sugar comprises the listed sugar in following (1)-(3):
(1) liquid sugar: thick solution, Nulomoline, glucose, isomerized sugar or its mixture of sugar, solid content is about 60-80%.
(2) starch hydrolyzates: by starch is decomposed the thick liquid that obtains with acid or amylase, solid content is about 80-90%.The mixture of glucose, maltose, dextrin etc.
(3) hydrogenated starch hydrolysate: the mixture of Sorbitol Powder, maltose alcohol, maltose triol, oligose, alcohol etc. (solid content, 60-80%).
The used polyvalent alcohol of the present invention preferably at room temperature is liquid (liquid polyol), and glycerine preferably.
Fats/oils, be used to keep the base-material of fats/oils and polyvalent alcohol to use by suitable amount, the purposes that said suitable amount is desired according to the fats/oils of the type of used fats/oils and powdery or granular form decides.Yet, the usage quantity of fats/oils keeps the gross weight of the base-material of fats/oils in 100 weight part fats/oils and being used to, preferably 1-70 weight part and more preferably 20-50 weight part, and the usage quantity of polyvalent alcohol is in the said gross weight of 100 weight parts, preferably 0.1-10 weight part and more preferably 2-5 weight part.
Portion introduces the powdery of fats/oils or the fats/oils of granular form within it, can produce by these three kinds of components are stirred.Prerequisite is, in the fats/oils of this powdery or granular form, the particle of base-material that is used to keep fats/oils is because polyvalent alcohol and crosslinked mutually, forms three-dimensional powdery or granular texture and fats/oils is contained in this structure.
Yet when water content was too high, fats/oils can be oozed out from the fats/oils of powdery or granular form, and this seepage it is believed that owing to aforesaid three-dimensional structure is partly subsided and taken place.When this fats/oils oozing out from the fats/oils of powdery or granular form taken place, the fats/oils of powdery or granular form can become gatherings and mobile decline.In addition, the fats/oils of powdery or granular form also can be showed the reduction of fats/oils content.
For preventing oozing out of fats/oils, preferably water content is adjusted to maximum 15wt%, preferably as many as 10wt%.Notice that among the present invention, water content is to measure by the heated drying method under standard pressure.
When the fats/oils with powdery or granular form was dissolved in the predetermined liquid, the interior fats/oils of fats/oils that remains on powdery or granular form was discharged in the liquid.For reaching the solvability of practical level, the maximum particle size of the fats/oils of powdery or granular form can be maximum to 10mm, preferred maximum to 5mm and average grain granularity be maximum to 5mm, preferred maximum to 2mm.Notice that the average grain granularity among the present invention is to measure by the screening of using the standard screen cloth.
For producing the fats/oils that per unit volume has the powdery or the granular form of high-content fats/oils, the apparent filling tap density of the fats/oils of preferred powdery or granular form is 0.55-0.85g/cm
3, preferred 0.70-0.85g/cm
3, and first-selected 0.70-0.80g/cm
3
Term used herein " apparent filling tap density " is also referred to as fills tap density or PBD (filling tap density), and in the present invention, apparent filling tap density is measured by E-type PowderTester (trade name that Hosokawa Micromeritics Laboratory manufactures a product).Say that more specifically " apparent filling tap density " used herein is meant the density of measuring under condition as described below.
At first, the preparation sampling receptacle is 100cm by an additional cylinder is connected internal volume
3The top of cylindrical metal container.In will this sampling receptacle of fats/oils impouring above the powdery of the amount of this cylindrical metal vessel volume or granular form.This sampling receptacle was made 180 times freely falling body from the 2cm eminence in 3 minutes.Remove additional cylinder then, and will be deposited in the fats/oils leveling of the powdery or the granular form of cylindrical metal container top with a sheet glass.Then, measure the total mass of the fats/oils of powdery in metal vessel and the container or granular form, and calculate poor between the quality W2 of this quality W1 and cylindrical metal container.With the internal volume of this difference, obtain apparent filling tap density thus divided by the cylindrical metal container.
As long as composition is that by the method and the condition of suitable its production of selection, the apparent filling tap density of the fats/oils of powdery or granular form is adjustable uniformly.The details of this adjustment will be described later.
When the water content of the fats/oils of powdery or granular form and grain graininess are in above-mentioned concrete scope, can Powder Tester (trade name will be passed through, Hosokawa Micron Corporation manufacturing) slope of repose of measuring is adjusted to maximum to 70 degree, and it is in some cases, extremely maximum to 60 degree.Powder Tester is a kind of instrument that can measure the slope of repose by the angle of measuring remaining taper (remaining cone).
When the fats/oils of powdery or granular form has aforesaid composition and characteristic, can include a large amount of relatively fats/oils in the product, even not with fatty oil/emulsification.The local flavor that this product also has outstanding lysotype and courant and can not lose the uniqueness of fats/oils.
For example, when using the hydrophilic materials conduct to be used to keep the base-material of fats/oils, be maintained at and thisly be used for keeping the fats/oils of the base-material of fats/oils from the product that obtains, to discharge very soon, and the fats/oils of powdery of being produced or granular form can emulsification or make oil phase or the water muddiness by hydrolysis.The fats/oils of this powdery or granular form suits to use in producing food flavouring, soup stock compound etc. especially, even because when using when increasing distinguish the flavor of oil or flavor oil and being used as fats/oils, its local flavor can not ruined yet.
In addition, because being used for keeping the base-material of fats/oils can select from a lot of various materials, thereby by utilizing component contained usually in food flavouring, the cake cake compound etc. as the base-material that is used to keep fat/oil, the fats/oils that just can easily produce powdery or granular form.So the powdery of gained or the fats/oils of granular form unlikely can have a negative impact to the taste that uses its food of producing, local flavor, quality or the like.
In addition, the fats/oils of powdery of the present invention or granular form can easily be adjusted to has high fluidity, and therefore can easily produce maneuverable product when using this product when this product being filled into its packing or in the cooking.
The production method of the fats/oils of B, powdery or granular form
In the production method of the fats/oils of powdery of the present invention or granular form, to contain fats/oils, be used to keep the base-material of fats/oils and the starting material of liquid polyol to stir, till material evenly, and the preparation starting material makes the ratio of fats/oils, in 100 weight part fats/oils be used to keep the gross weight of the base-material of fats/oils, it is the 1-70 weight part, and the ratio of liquid polyol in the said gross weight of 100 weight parts, is the 0.1-10 weight part.
Fats/oils and be used to keep the base-material front of fats/oils to describe.So no longer these components are described.
Term used herein " liquid polyol " comprises it itself being liquid polyvalent alcohol, also comprises the aqueous solution of polyvalent alcohol.More specifically saying, is liquid polyol such as the dibasic alcohol of glycerine or propylene glycol, as long as hold it under the temperature that is higher than its fusing point, and sugar and sugar alcohol can become liquid polyol, when they during with the form of for example aqueous solution.
The fats/oils of aforesaid powdery of the present invention or granular form can be produced by starting material (it has been prepared to the component that contains above-mentioned defined ratio) is stirred till material evenly.
Next, describe the even stirring of starting material in detail.
(1) even stirring method
The even stirring of starting material can realize by using any machine that uses in the bread and cheese production technique such as blender, kneader, nodulizer, and the type of used machine has no particular limits.Used exemplary machine comprises vane-type blender, screw mixing machine, dough mixing machine, pulverizer, dissimilar kneader, blender/nodulizer, fluidised bed granulator and extrusion-type nodulizer.
(2) process that evenly stirs
For realizing even stirring; general preferred water content is adjusted to as many as 15wt%; and more preferably extremely as many as 10wt% because in having the system of higher moisture, is used to keep the base-material efflorescence of fats/oils and/or granulation to become difficult by polyvalent alcohol is feasible.Yet, also can be by starting material being dispersed in the water and, making water content be reduced to maximum 15wt% and finish efflorescence and/or granulation with the dispersion liquid spraying drying, this method also belongs to scope of the present invention.
Fats/oils, be used to keep the even stirring of the base-material and the liquid polyol of fats/oils, perhaps can by with two kinds of blend in advance in three kinds of components, add remaining ingredient and stirring the mixture afterwards and finish, perhaps finish by stirring with all three kinds of disposable mixing of component and with mixture.
In this process, preferably, use this fats/oils with the form of liquid by fats/oils being increased to the temperature that is higher than its fusing point.Term used herein " fusing point " be the melt temperature that in the temperature elevation process, records (referring to, " the fats/oils chemistry handbook " that Japan fats/oils chemistry association (Japanese Association of Fat/Oil Chemistry) compiles, Maruzen, 1958, the 907-908 pages or leaves).
In the fats/oils of producing powdery or granular form, the homodisperse of liquid polyol is important.When the desire homodisperse has the sugar alcohol aqueous solution of full-bodied polyvalent alcohol such as glycerine or high density, be very effective with liquid polyol heating and spraying.
The time that starting material stirs, depend on that material is formed and industrial scale is done to select aptly.
By using above-mentioned instrument and condition that starting material is carried out even stir process, perhaps further select the powder or the particle of desirable grain graininess by screening, can produce the powdery with desirable grain graininess or the fats/oils of granular form.The material that evenly stirs further can be extruded granulation, perhaps after extruding granulation, further sieve processing, select particle thus with desirable grain graininess scope.
For example, by using high-speed stirring type nodulizer or being equipped with the fluidized bed type nodulizer of agitating vane, can produce the average grain granularity and be the powdery of about 200-1000 μ m or the fats/oils of granular form with consistent relatively grain graininess.Have the particle of consistent relatively grain graininess when will further extruding granulation through the material of even stir process, and also can producing for the consistent shape of about 1-5mm.
Producing apparent filling tap density when desire is about 0.55-0.85g/cm
3Powdery or during the fats/oils of granular form, powder or the particle of being produced by even stir process starting material further can be carried out compaction treatment under the pressure of 0.01-1000MPa, preferred 0.1-100MPa, first-selected 0.5-50MPa.
The used method of compaction treatment has no particular limits, and exemplary method comprises that tableted, roller press type briquetting and roller press type press.
In tableted, with powder or particles filled in mould and compacting.In the roller press type briquetting, use pair of rolls, the model of predetermined shape is carved with on the surface of each roller, provides powder or particle to push in the slit between these two rotation rollers.In roller press type presses, use a pair of roller that does not have die sinking, and provide powder or particle to push in the slit between these two rotation rollers.
In roller press type presses, to carry out the additional processing of particle size reduction to the material that compresses usually, so that produce powder or particle thus.This particle size reduction can be by so-called grinding mill, shredder, grind or instrument with vibrator of mechanical effect is finished, wherein material is shifted onto on semicylindrical screen cloth (weaving wire) or the perforated metal (it is installed with the metal sheet in the hole of predetermined shape) from its inside by the rotation spatula, produced particle thus with predetermined particle size.Exemplary this instrument comprises Randel mill (manufacturing of Tokuju company limited), Oscillator (manufacturing of Kikusui Seisakusho company limited) and Flake Crusher (manufacturing of HosokawaMicron company).
Production method of producing the fats/oils of powdery or granular form as mentioned above of the present invention is effective especially to liquid oils or semi-solid fatty efflorescence or granulation.
It should be noted that the invention is not restricted to aforesaid with the way of example embodiments shown.Have any technology of substantially the same formation and similar work characteristics with the defined technological concept of claims of the present invention, all belong to technical scope of the present invention.
Embodiment
Next, the present invention will describe in further detail by the mode of reference example, and these embodiment are any implication of the scope of the invention without limits.
Embodiment 1
With 30 weight parts in 45 ℃ of heating baths fused theobroma oil and 70 weight part dextrine powders (dextrose equivalent value (DE, the directly per-cent of reducing sugar) is 3.5, water content 5.3%, apparent filling tap density 0.56g/cm
3, grain graininess is for passing 50 orders and particle shape spherical in shape) thoroughly mediate.In the mixture of gained, add 4.5 weight part glycerine, and mixture was stirred 10 minutes at 45 ℃, until mixture evenly and efflorescence, obtain the fat of powder-form.
The fat of the powder-form of gained, its water content are 6.5%, maximum particle size 2.0mm, and average grain granularity 700 μ m, and the slope of repose is 44 degree.Do not observed fat and oozed out, and this powder-like product shows outstanding flowability from the inside.
Embodiment 2
With 35 weight part soybean oil and 65 weight part dextrine powders (DE value 7.5, water content 5.5%, apparent filling tap density 0.63g/cm
3, grain graininess is for passing 50 orders and particle shape spherical in shape) thoroughly mediate, and in mixture, add 3 weight part propylene glycol.Mixture was stirred 15 minutes at 15 ℃, until mixture evenly and efflorescence, obtain the oil of powder-form.
The oil of the powder-form of gained, its water content are 7.4%, maximum particle size 6.0mm, and average grain granularity 1200 μ m, and the slope of repose is 43 degree.Do not observe oil and ooze out, and this powder-like product shows outstanding flowability from the inside.
When the oil with this powder-form adds in the hot water, the dispersion that becomes immediately of the oil in the oil of powder-form, water keeps transparent simultaneously.
Embodiment 3
With 30 weight parts in 45 ℃ of heating baths fused theobroma oil and 70 weight part dextrine powders (the DE value is 3.5, water content 5.3%, apparent filling tap density 0.56g/cm
3, grain graininess is for passing 50 orders and particle shape spherical in shape) thoroughly mediate.In the mixture of gained, add 5 weight part propylene glycol, and mixture was stirred 20 minutes at 40 ℃, until mixture evenly and efflorescence, obtain the fat of powder-form.
The fat of the powder-form of gained, its water content are 6.6%, maximum particle size 1.5mm, and average grain granularity 470 μ m, and the slope of repose is 53 degree.Do not observed oil and oozed out, and this powder-like product shows outstanding flowability from the inside.
Embodiment 4
With 30 weight part soybean oil and 70 weight part sweet-whey powder (water content 7.0%, apparent filling tap density 0.59g/cm
3, grain graininess is for passing 50 orders and particle shape spherical in shape) thoroughly mediate, and in mixture, add 4 weight part glycerine.Mixture was stirred 5 minutes at 25 ℃, until mixture evenly and efflorescence, obtain the oil of powder-form.
The oil of the powder-form of gained, its water content are 9.9%, maximum particle size 4.0mm, and average grain granularity 930 μ m, and the slope of repose is 39 degree.Almost do not observed oil and oozed out, and this powder-like product shows outstanding flowability from the inside.
The oil of this powder-form can be used as the oil in the Preblend of cake, biscuit etc.
Embodiment 5
With 40 weight parts fused plam oil and 60 weight part skim-milks (water content 3.8% apparent filling tap density 0.79g/cm in 50 ℃ of heating baths
3, grain graininess is for passing 50 orders and particle shape spherical in shape is thoroughly mediated.In the mixture of gained, add 5 weight part glycerine, and mixture was stirred 5 minutes at 50 ℃, until mixture evenly and efflorescence, obtain the oil of powder-form.
The oil of the powder-form of gained, its water content are 11.5%, maximum particle size 6.5mm, and average grain granularity 1050 μ m, and the slope of repose is 46 degree.Almost do not observed oil and oozed out, and this powder-like product shows outstanding flowability from the inside.
With blend such as the oil of this powder-form and flour, sugar, obtain the cake compound.Because the base-material that is used for keeping fats/oils (skim-milk) that constitutes in the oil of this powder-form is the component that the cake compound comprises usually, thereby provides this oil ingredient can not have a negative impact to taste, local flavor, quality etc.
Embodiment 6
With the 45 weight part Semen Maydis oils and the 55 weight part egg-white powder water yields 6.5%, apparent filling tap density 0.55g/cm
3, grain graininess is for passing 50 orders and particle shape spherical in shape) thoroughly mediate.In the mixture of gained, add 2.5 weight part glycerine, and mixture was stirred 15 minutes at 15 ℃, until mixture evenly and efflorescence, obtain the oil of powder-form.
The oil of the powder-form of gained, its water content are 6.8%, maximum particle size 6.5mm, and average grain granularity 1200 μ m, and the slope of repose is 34 degree.Almost do not observed oil and oozed out, and this powder-like product shows outstanding flowability from the inside.
With oil and flour, sugar, the skimmed milk of this powder-form, bake blend such as powder, obtain the steamed bun premix, this premix is adapted at using in the microwave oven.Because the base-material that is used for keeping fats/oils (egg-white powder) that constitutes in the oil of this powder-form is the component that the steamed bun premix comprises usually, thereby provides this oil ingredient can not have a negative impact to taste, local flavor, quality etc.
Embodiment 7
(the DE value is 9.0, water content 5.5%, apparent filling tap density 0.62g/cm with 32.5 weight part Oleum Gossypii semens and 67.5 weight part dextrin
3, grain graininess is for passing 50 orders and particle shape spherical in shape) thoroughly mediate.In the mixture of gained, add 3.5 weight part glycerine, and mixture was stirred 5 minutes at 30 ℃, until mixture evenly and efflorescence, obtain the oil of powder-form.
The oil of the powder-form of gained, its water content are 6.4%, maximum particle size 6.0mm, and average grain granularity 860 μ m, and the slope of repose is 49 degree.Observe and have only some oil to ooze out, and this powder-like product shows outstanding flowability from the inside.
With blend such as the oil of this powder-form and powdery fermented vinegar, salt, Sodium Glutamate, HVP, sugar, spices, obtain the seasoning matter of powder-form thus.
When with the seasoning matter of this powder-form all over the wet vegetable surface that is sprinkling upon band water, the very fast dissolving of the oil of powder-form, and the oil in the seasoning matter (Oleum Gossypii semen) dispersion that becomes.
Embodiment 8
With 35 weight parts fused dairy fats and 65 weight part dextrine powders (DE value 13.0, water content 3.9%, apparent filling tap density 0.62g/cm in 45 ℃ of heating baths
3, grain graininess is for passing 50 orders and particle shape spherical in shape) thoroughly mediate.In the mixture of gained, add 3 weight part glycerine, and mixture was stirred 10 minutes at 40 ℃, until mixture evenly and efflorescence, obtain the oil of powder-form.
The oil of the powder-form of gained, its water content are 5.7%, maximum particle size 3.5mm, and average grain granularity 930 μ m, and the slope of repose is 42 degree.Do not observed oil and oozed out, and this powder-like product shows outstanding flowability from the inside.
The oil of this powder-form is molded as cubes with tabletting machine, and this cubes is used as the cream square (the band creamy taste) that the instant noodle soup stock is used.This cream square is very fast decomposition in hot water, and disengages dairy fats from square.The dairy fats that disengages swims in the surface of soup, and emulsifying effect does not take place.
Embodiment 9
(the DE value is 3.5, water content 5.3%, apparent filling tap density 0.56g/cm with 35 weight part sesame oil and 65 weight part dextrine powders
3, grain graininess is for passing 50 orders and particle shape spherical in shape) in vertical dough mixing tank, thoroughly mediate.In the mixture of gained, add 3 weight part glycerine, and mixture was stirred 20 minutes at 20 ℃, until mixture evenly and efflorescence, obtain the oil of powder-form.
The oil of the powder-form of gained, its water content are 5.7%, maximum particle size 9.0mm, and average grain granularity 1800 μ m, and the slope of repose is 50 degree.Almost do not observed oil and oozed out, and this granulated product shows outstanding flowability from the inside.
With blend such as the oil of this granular form and salt, Sodium Glutamate, meat extract powder, soy sauce powder, spices, obtain Chinese style soup stock compound thus.
When impouring hot water in this soup stock compound, the very fast dissolving of the oil of granular form, and at the surface flotation sesame oil of soup.Because oil (sesame oil) does not have emulsification, thereby oil has kept its delicious sesame local flavor and soup keeps transparent, and the soup that is produced is very welcome.
Embodiment 10
(the DE value is 3.5, water content 5.3%, apparent filling tap density 0.56g/cm with 32.5 weight part soybean oil and 67.5 weight part dextrine powders
3, grain graininess is for passing 50 orders and particle shape spherical in shape) in Vertical Granulator (trade name of high-speed mixing type nodulizer, Fuji Sangyo K.K. makes), thoroughly mediate.The driving screw speed of rotation of this Vertical Granulator is set at 400rpm and cross screw rod speed of rotation to be set at 3000rpm and to use.
Continue along with mediating, 3 weight part glycerine are sprayed onto (flow velocity on the mixture, 23g/min), and the driving screw speed of rotation is set at 300rpm and cross screw rod speed of rotation is set at 3000rpm, continue to mediate other 10 minutes at 45 ℃, until mixture evenly and efflorescence, obtain the oil of powder-form.
The oil of the powder-form of gained, its water content are 6.8%, maximum particle size 2.0mm, and average grain granularity 300 μ m, and the slope of repose is 52 degree.Observe and have only some oil to ooze out, and this powder-like product shows outstanding flowability from the inside.
Embodiment 11
By with 32.5 weight part soybean oil and 3 weight part glycerine emulsifications in the family expenses blender, prepare emulsion.This emulsion is sprayed onto with the flow velocity of 63g/min (the DE value is 3.5, water content 5.3%, apparent filling tap density 0.56g/cm on the 67.5 weight part dextrine powders
3, the diameter of powder is for can passing 50 orders and particle shape spherical in shape), simultaneously with this dextrin in New Marumerizer (trade name with fluidised bed granulator of agitating vane, Fuji Paudal company limited makes) in 40 ℃ of following fluidisations.This New Marumetizer is speed of rotation and the 2m of 300rpm with the agitating vane
3The air upper reaches speed operation of/min.
The sprinkling for the treatment of emulsion is proceeded other 10 minutes with fluidisation after finishing under 40 ℃, obtain the oil of powder-form thus.The product that obtains like this, its water content is 5.7%, maximum particle size 2.0mm, average grain granularity 400 μ m, and the slope of repose is 48 degree.Almost do not observed oil and oozed out, and this powder-like product shows outstanding flowability from the inside.
Embodiment 12
The glycerine of 3 weight parts is sprayed onto with the flow velocity of 1.5g/min (the DE value is 3.5, water content 5.3%, apparent filling tap density 0.56g/cm on the 67.5 weight part dextrine powders
3, the diameter of powder is for can passing 50 orders and particle shape spherical in shape), simultaneously with this dextrin fluidisation under the condition identical with embodiment 11.Wait to spray finish after 5 minutes, the soybean oil of spraying 32.5 weight parts with the flow velocity of 4.5g/min, and under identical condition, continue fluidisation simultaneously.
After the sprinkling for the treatment of soybean oil is finished, continued fluidisation about 5 minutes in addition, obtain the oil of powder-form thus, its water content is 5.5%, maximum particle size 1.5mm, and average grain granularity 400 μ m, and the slope of repose is 50 degree.Almost do not observed oil and oozed out, and this powder-like product shows outstanding flowability from the inside.
Embodiment 13
With 37.5 weight parts in 55 ℃ of heating baths fused lard and 62.5 weight part jelly powders (molecular weight is 3000-5000, water content 7.2%, apparent filling tap density 0.48g/cm
3, grain graininess is for passing 50 orders and particle shape spherical in shape) in vertical dough mixing tank, thoroughly mediate.In the mixture of gained, add 3.5 weight part glycerine, and mixture was stirred 1 minute at 55 ℃, even until mixture.With the uniform mixture that so obtains with Soft Ryuzer (trade name of extrusion type nodulizer, FujiPaudal company limited makes) by 14 eye mesh screens (width of mesh: 1180 μ m) extrude, obtain the fat of granular form.
The fat of the granular form of gained, its water content are 7.4%, maximum particle size 3.5mm, and the slope of repose is 45 degree.Do not observed oil and oozed out, and this granulated product shows outstanding flowability from the inside.
Fat and salt, soy sauce powder, Sodium Glutamate, extract powder, sugar and spice blend with this granular form obtain the soup stock powder that Chinese style noodles soup stock is used thus.When impouring hot water in this soup stock powder, the very fast dispersion of the fat of granular form (lard), and lard swims in the surface of soup.Because the fat of this granular-form does not have emulsification, thereby soup is clarified very much and lard has good local flavor.
Embodiment 14
With 50 weight parts fused dairy fats and 50 weight part soy sauce powders (water content 11.0%, apparent filling tap density 0.70g/cm in 45 ℃ of heating baths
3, grain graininess is for passing 50 orders and particle shape spherical in shape) in vertical dough mixing tank, thoroughly mediate.In the mixture of gained, add 2 weight part glycerine, and mixture was stirred 1 minute at 45 ℃, even until mixture.Use Soft Ryuzer with the used same model of embodiment 13 by 20 eye mesh screens (width of mesh: 850 μ m) extrude, obtain the fat of granular form the uniform mixture that so obtains.
The fat of the granular form of gained, its water content are 12.0%, maximum particle size 3.5mm, and the slope of repose is 51 degree.Observe and have only some oil to ooze out, and this granulated product shows outstanding flowability from the inside.
The fat of this granular form can be used for various soup stocks, comprises Chinese style noodles soup stock, also can be used for the beefsteak flavouring paste.
Embodiment 15
With 33 weight part soybean oil, 67 weight part HVP powder (water content 8.3%, apparent filling tap density 0.75g/cm
3, grain graininess is for can passing 100 orders and particle shape spherical in shape), 3 weight part glycerine and the physical property emulsification in the high speed blender of 260 weight parts waters, spraying drying is carried out efflorescence then, obtains the oil of powder-form.
The oil of the powder-form of gained, its water content are 10.6%, maximum particle size 0.5mm, and average grain granularity 100 μ m, and the slope of repose is 55 degree.Do not observed oil and oozed out, and this powder-like product shows outstanding flowability from the inside.
Embodiment 16
With solid curry cream flour paste (oleaginousness 37% and water content 3.2%) fusion in 55 ℃ of heating baths of the commercially available acquisition of 100 weight parts, and add 2 weight part glycerine.Mixture was stirred 1 minute at 55 ℃, even until mixture.With the uniform mixture that so obtains with Soft Ryuzer (trade name of extrusion type nodulizer, Fuji Paudal company limited makes) by 14 eye mesh screens (width of mesh: 1180 μ m) extrude, obtain the fat of granular form.
The curry cream flour paste particle of gained, its water content is 3.5%, maximum particle size 3.5mm, and the slope of repose is 52 degree.Do not observed oil and oozed out, and this granulated product shows outstanding flowability from the inside.
Embodiment 17
(the DE value is 9.0, water content 5.5%, apparent filling tap density 0.62g/cm for flavor oil that 35 weight parts are produced by the garlic that at high temperature extracts with vegetables oil and 65 weight part dextrine powders
3, the powder diameter is for passing 50 orders and particle shape spherical in shape) thoroughly mediate.In the mixture of gained, add 3 weight part glycerine, and mixture was stirred 5 minutes at 20 ℃, until mixture evenly and efflorescence, obtain the oil of powder-form.
The oil of the powder-form of gained, its water content are 6.0%, maximum particle size 6.5mm, and average grain granularity 1200 μ m, and the slope of repose is 50 degree.Almost do not observed oil and oozed out, and this powder-like product shows outstanding flowability from the inside.
Fat, salt, soy sauce powder, Sodium Glutamate, extract powder, sugar and the spice blend of the granular form that the fat of this powder-form and embodiment 13 are produced obtain the soup stock powder that Chinese style noodles soup stock is used thus.When impouring hot water in this soup stock powder, the very fast dispersion of the oil in the oil of powder-form (flavor oil), and oil float is on the surface of soup gives out welcome especially garlicky.
Embodiment 18
(the DE value is 8.5, water content 5.0%, apparent filling tap density 0.58g/cm with 32 weight part sesame oil (Kadoya K.K. manufacturing), 57.7 weight part dextrine powders
3, the powder diameter is for can passing 50 orders and shape spherical in shape), 10.3 weight part lactose (water content 0.2%, apparent filling tap density 1.02g/cm
3The powder diameter is for can passing 50 orders and shape spherical in shape) and 3 weight part glycerine (manufacturing of Kaneka company) in a 5L twin screw kneader (Irie Shokai company limited), mediate; even until mixture; and is to extrude the basket granulation test machine (Hata Tekkousho K.K. manufacturing) of 1.2mm granulation with mould the mixture of gained from having diameter, obtains the oil of granular form thus.Notice that lactose is used from the effect of the base-material that keeps fats/oils.
The oil of the granular form of gained, its water content are 6.2%, maximum particle size 3.6mm, and average grain granularity 2.5mm, the slope of repose is 35 degree, and apparent filling tap density 0.49g/cm
3Almost do not observed oil and oozed out, and this granulated product shows outstanding flowability from the inside.
Embodiment 19
(the DE value is 8.5, water content 5.0%, apparent filling tap density 0.58g/cm with oil (manufacturing of Hasegawa Koryo company limited), the 56.7 weight part dextrine powders of 33 weight part bands Japan beef flavour
3, the powder diameter is for can passing 50 orders and shape spherical in shape), 10.3 weight part Sodium Glutamates (water content 0.1%, apparent filling tap density 0.91g/cm
3The powder diameter for can pass 120 orders and shape amorphous) and 3 weight part glycerine (manufacturing of Kaneka company) in a 500L twin screw kneader (manufacturing of Fuji Paudal company limited), mediate; even until mixture; and is to extrude the basket granulation test machine (Hata Tekkousho K.K. manufacturing) of 2.5mm granulation with mould the mixture of gained from having diameter, obtains the oil of granular form.Notice that Sodium Glutamate is used from the effect of the base-material that keeps fats/oils.
The oil of the granular form of gained, its water content are 6.1%, maximum particle size 3.6mm, and average grain granularity 2.4mm, the slope of repose is 34 degree, and apparent filling tap density 0.51g/cm
3Almost do not observed oil and oozed out, and this granulated product shows outstanding flowability from the inside.
Embodiment 20
(the DE value is 8.5, water content 5.0%, apparent filling tap density 0.58g/cm with 32 weight part sesame oil (Kadoya K.K. manufacturing), 57.7 weight part dextrine powders
3, the powder diameter is for can passing 50 orders and shape spherical in shape), 10.3 weight part lactose (water content 0.2%, apparent filling tap density 1.02g/cm
3The powder diameter is for passing 50 orders and shape spherical in shape) and 3 weight part glycerine (Kanegafuchi chemistry company limited makes) kneading in a 5L twin screw kneader (Irie Shokai company limited); even until mixture; and mixture compacting in roll-type compressor TF-mini (trade(brand)name of the dry granulation machine that Freund Industrial Co., Ltd makes) with gained; and pulverization obtains the oil of granular form thus.
By the dry granulation machine mixture compacted is carried out under the pressure of 15.3MPa, and pulverization undertakies by using grinding mill, it is 2.4mm * 2.4mm that said grinding mill is provided with woven wire cloth of SUS and width of mesh.
The oil of the granular form of gained, its water content are 6.2%, maximum particle size 3.0mm, and average grain granularity 2.5mm, the slope of repose is 40 degree, and apparent filling tap density 0.77g/cm
3Almost do not observed oil and oozed out, and this granulated product shows outstanding flowability from the inside.
Embodiment 21
With the imitated dairy fats (manufacturing of Hasegawa Koryo company limited) of 34 weight parts, (the DE value is 8.5 to 55.7 weight part dextrine powders, water content 5.0%, apparent filling tap density 0.58g/cm
3, the powder diameter is for can passing 50 orders and shape spherical in shape), 10.3 weight part Sodium Glutamates (water content 0.1%, apparent filling tap density 0.91g/cm
3The powder diameter for can pass 120 orders and shape amorphous) and 3 weight part glycerine (Kanegafuchi chemistry company limited make) kneading in a 5L twin screw kneader (Irie Shokai company limited); even until mixture; and mixture compacting in roll-type compressor TF-mini (trade(brand)name of the dry granulation machine that Freund Industrial Co., Ltd makes) with gained; and pulverization obtains the oil of granular form thus.
By the dry granulation machine mixture compacted is carried out under the pressure of 10.2MPa, and pulverization undertakies by using grinding mill, it is 2.4mm * 2.4mm that said grinding mill is provided with woven wire cloth of SUS and width of mesh.
The oil of the granular form of gained, its water content are 6.0%, maximum particle size 2.9mm, and average grain granularity 2.4mm, the slope of repose is 41 degree, and apparent filling tap density 0.77g/cm
3Almost do not observed oil and oozed out, and this granulated product shows outstanding flowability from the inside.
Embodiment 22
(the DE value is 3.5, water content 5.3%, apparent filling tap density 0.51g/cm with 34 weight part lards (manufacturing of Maruzen Foods company), 45.4 weight part dextrine powders
3, the powder diameter is for can passing 50 orders and shape spherical in shape), 10.3 weight part lactose (water content 0.2%, apparent filling tap density 1.02g/cm
3, the powder diameter is for can passing 50 orders and shape spherical in shape), 10.3 weight part powder of amino acids (water content 8.3%, apparent filling tap density 0.75g/cm
3The powder diameter is for can passing 100 orders and shape spherical in shape) and 3 weight part glycerine (manufacturing of Kanegafuchi chemical company) in a 500L twin screw kneader (manufacturing of FujiPaudal company limited), mediate; even until mixture; and mixture compacting in roller type press RC-3012 (trade(brand)name of the dry granulation machine that Freund Industrial Co., Ltd makes) with gained; and pulverization obtains the oil of granular form thus.
By the dry granulation machine mixture compacted is carried out under the pressure of 2.0MPa, and pulverization undertakies by using grinding mill, it is 2.4mm * 2.4mm that said grinding mill is provided with woven wire cloth of SUS and width of mesh.
The oil of the granular form of gained, its water content are 7.3%, maximum particle size 3.1mm, and average grain granularity 2.5mm, the slope of repose is 45 degree, and apparent filling tap density 0.59g/cm
3Almost do not observed oil and oozed out, and this granulated product shows outstanding flowability from the inside.
The invention effect
When base-material and the polyalcohol production powdery or granular by using fats/oils and being used for keeping fats/oils The fats/oils of form, and the water content of product is during for as many as 15wt%, in the product of gained can Including relatively a large amount of fats/oils in the product does not have the emulsification of fats/oils simultaneously, and product still is rich in Local flavor with the height flowable. In addition, by product being adjusted to maximum particle size for maximum Be maximum to 5mm to 10mm and average grain granularity, can easily produce and have outstanding dissolubility Powdery or the fats/oils of granular form.
Claims (4)
1, the fat of a kind of powdery or granular form or oily, it contains fat or oil, is used to comprise or infiltrate fat or oily the wetting ability base-material and the polyvalent alcohol of portion within it, wherein the fat of powdery or granular form or oily water content are as many as 15wt%, maximum particle size be maximum to 10mm and average grain granularity for maximum to 5mm, and show maximum slope of repose to 70 degree.
2, the fat of the powdery of claim 1 or granular form or oily, its apparent filling tap density is 0.55-0.85g/cm
3
3, a kind of fat or oily method that is used for the powdery or the granular form of production claim 1, may further comprise the steps: will contain fat or oil, be used to comprise or the wetting ability base-material of infiltrate fat or oily portion within it and the starting material stirring of liquid polyol, till material evenly; Prepare said starting material, feasible fat or oily ratio, in 100 weight parts fat or oil be used to comprise or infiltrate fat or the oily gross weight of the wetting ability base-material of portion within it, it is the 1-70 weight part, and the ratio of described liquid polyol, in the said gross weight of 100 weight parts, be the 0.1-10 weight part.
4, the fat or the oily method of the production powdery of claim 3 or granular form, wherein after said starting material being stirred to evenly, the pressure by applying 0.01-1000MPa is with the material compacting.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2002193953A JP2004035700A (en) | 2002-07-02 | 2002-07-02 | Powdery or granular oil and fat, and its manufacturing method |
| JP193953/2002 | 2002-07-02 | ||
| JP193953/02 | 2002-07-02 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1478874A CN1478874A (en) | 2004-03-03 |
| CN1240815C true CN1240815C (en) | 2006-02-08 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB031330274A Expired - Lifetime CN1240815C (en) | 2002-07-02 | 2003-07-02 | Powder or granule formed fat/oil and its production method |
Country Status (4)
| Country | Link |
|---|---|
| JP (1) | JP2004035700A (en) |
| KR (1) | KR20040004085A (en) |
| CN (1) | CN1240815C (en) |
| HK (1) | HK1061867A1 (en) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4648916B2 (en) * | 2007-03-26 | 2011-03-09 | 理研ビタミン株式会社 | Liquid seasoning composition for cooking |
| JP5016405B2 (en) * | 2007-07-06 | 2012-09-05 | 日本たばこ産業株式会社 | Control method for exudation of fats and oils from oil-containing granules |
| JP5301924B2 (en) * | 2007-09-28 | 2013-09-25 | 理研ビタミン株式会社 | Method for producing powdered emulsified oil |
| JP5400365B2 (en) * | 2008-12-01 | 2014-01-29 | テーブルマーク株式会社 | Butter flavor seasoning composition and method for enhancing butter flavor of food and drink |
| JP5783649B2 (en) * | 2011-03-22 | 2015-09-24 | キッコーマン株式会社 | Method for producing granular soy sauce and granular soy sauce |
| CN102860557B (en) * | 2011-07-07 | 2015-12-02 | 雀巢公司 | Instant granular solid beverage |
| JP5877718B2 (en) * | 2012-01-11 | 2016-03-08 | キッコーマン株式会社 | Liquid seasoning containing ingredients and cooking oil |
| JP6397169B2 (en) * | 2013-07-16 | 2018-09-26 | テーブルマーク株式会社 | Oil-containing solid seasoning |
| JP6238454B2 (en) * | 2014-09-09 | 2017-11-29 | 長谷川香料株式会社 | Powdered fat composition for imparting milk flavor, and method for imparting milk flavor to food and drink |
| JP7316718B2 (en) * | 2019-07-31 | 2023-07-28 | 株式会社ニップン | Seasoning mix and snack food using the same |
| CN112237220A (en) * | 2019-11-12 | 2021-01-19 | 上海南侨食品有限公司 | Baking grease suitable for pastry and preparation method thereof |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS56104998A (en) * | 1980-01-28 | 1981-08-21 | House Food Industrial Co | Manufacture of powdery grease |
| JP2601300B2 (en) * | 1987-04-06 | 1997-04-16 | 旭化成工業株式会社 | Powdery or granular fats and oils and their production |
| KR910003309A (en) * | 1989-07-31 | 1991-02-27 | 김유중 | Pipes or valves that generate a specified sound during transport of gas or fluid |
| KR920009248B1 (en) * | 1989-08-25 | 1992-10-15 | 가부시기가이샤 도요다지도우 쇽기세이사꾸쇼 | Weft detecting device in jet loom |
| JP3509109B2 (en) * | 1991-08-06 | 2004-03-22 | 日本たばこ産業株式会社 | Oil and fat-containing molded products |
| JP3930140B2 (en) * | 1998-03-20 | 2007-06-13 | 長谷川香料株式会社 | Powdered fat composition |
-
2002
- 2002-07-02 JP JP2002193953A patent/JP2004035700A/en active Pending
-
2003
- 2003-06-30 KR KR1020030043486A patent/KR20040004085A/en not_active Application Discontinuation
- 2003-07-02 CN CNB031330274A patent/CN1240815C/en not_active Expired - Lifetime
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2004
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| Publication number | Publication date |
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| KR20040004085A (en) | 2004-01-13 |
| CN1478874A (en) | 2004-03-03 |
| HK1061867A1 (en) | 2004-10-08 |
| JP2004035700A (en) | 2004-02-05 |
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