CN1236314A - Biocidal compositions - Google Patents

Biocidal compositions Download PDF

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Publication number
CN1236314A
CN1236314A CN97198985A CN97198985A CN1236314A CN 1236314 A CN1236314 A CN 1236314A CN 97198985 A CN97198985 A CN 97198985A CN 97198985 A CN97198985 A CN 97198985A CN 1236314 A CN1236314 A CN 1236314A
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Prior art keywords
benzoic acid
animal
compositions
pig
derivatives
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CN97198985A
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Chinese (zh)
Inventor
J·A·C·范奥延
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Koninklijke DSM NV
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DSM NV
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00—Medicinal preparations containing organic active ingredients
    • A61K31/185—Acids; Anhydrides, halides or salts thereof, e.g. sulfur acids, imidic, hydrazonic or hydroximic acids
    • A61K31/19—Carboxylic acids, e.g. valproic acid
    • A61K31/192—Carboxylic acids, e.g. valproic acid having aromatic groups, e.g. sulindac, 2-aryl-propionic acids, ethacrynic acid 
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23K—FODDER
    • A23K20/00—Accessory food factors for animal feeding-stuffs
    • A23K20/10—Organic substances
    • A23K20/111—Aromatic compounds
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23K—FODDER
    • A23K50/00—Feeding-stuffs specially adapted for particular animals
    • A23K50/30—Feeding-stuffs specially adapted for particular animals for swines

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Polymers & Plastics (AREA)
  • Health & Medical Sciences (AREA)
  • Animal Husbandry (AREA)
  • Zoology (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Medicinal Chemistry (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Fodder In General (AREA)
  • Feed For Specific Animals (AREA)

Abstract

This invention relates to a composition comprising benzoic acid or a derivative of benzoic acid capable of giving rise to free benzoic acid in vivo for use as a medicament for animals, wherein said acid/derivative functions as an antibiotic, promotes growth, decreases feed conversion and improves digestibility of amino acids administered in animal feeds. The benzoic acid or its derivative can be administered to the animal either in its feed composition or in its drinking water. It is particularly effective in pigs.

Description

The compositions of Biocidal
The present invention relates to contain the purposes of benzoic compositions, promote the growth of animal simultaneously and improve the amino acid whose digestibility of feeding animal as veterinary drug (especially for pig).
Known from we own previous disclosed EP-A-0683985, the animal that feeding contains the compositions of benzoic acid or its salt can make debirs, and especially the stink ammonia that distributes of Excreta of animal and muck minimizes.
Have now found that except that the above-mentioned functions effect benzoic acid can also be used for replacing the high antibiotic of relative costs in animal, in addition, such acid/salt also helps and promotes growth, reduces food conversion and improves amino acid whose digestibility in the animal feed.
Therefore, the present invention is the compositions that contains benzoic acid or benzoic acid derivative, can be as veterinary drug in order to produce free benzoic acid in vivo.
The benzoic acid or derivatives thereof gives animal as the component of the compositions of conventional feeding animals can produce benzoic acid in vivo.Like this, benzoic acid and derivant thereof the component that can be suitable as in animal feed or its drinking-water gives animal.The particular example that can produce benzoic benzoic acid derivative in vivo comprises benzoic salt such as benzoic alkali metal salt, alkali salt and ammonium salt.
The benzoic acid or derivatives thereof is during as insecticide, its consumption that gives animal for enough to prevent/treat the suitable consumption of any infection of animal.Such consumption is suitably for based on the scope of feeding to the 0.001-5% of each feedstuff gross weight of animal.If yet the effect of benzoic acid or derivatives thereof be not only as insecticide, thereby and the control pH value of feeding the animal excrements of this kind feedstuff when suppressing the stink of the ammonia that from Excreta, distributes, consumption at this moment can be higher.Such consumption can suitably be limited in the maximum consumption based on animal feed composition total amount about 10%.
Particularly benzoic acid/salt can be used as antibiotic, has the growth of promotion, reduces food conversion and improve the amino acid digestibility that gives in animal feed.
List the general prescription of animal feed composition among the following table l, all consumptions shown in it all are weight percentage and feed to pig:
Table 1
Compositions The contrast II Embodiment 2
Meat powder (58% thick protein) ?????3.20 ????3.20
Molasses ?????5.00 ????5.00
Semen Tritici aestivi ?????5.90 ????5.90
Semen sojae atricolor powder (45% thick protein) ????15.1 ????15.1
Tapioca starch (66% starch) ????36.5 ????35.5
Alcomeal ?????15 ?????15
Animal fat ?????3.3 ?????3.3
Limestone ?????0.74 ?????0.74
Lysine hydrochloride (98%) ?????0.06 ?????0.06
The premix vitamin ?????0.5 ?????0.5
Trace mineral ?????0.5 ?????0.5
The Helianthi powder ????12.2 ????12.2
Ammonium chloride ?????2 ?????2
Ammonium benzoate ?????- ?????1
Like this, benzoic acid or derivatives thereof and the composition commonly used such as calcium carbonate, electrolyte such as ammonium chloride, protein such as Semen sojae atricolor powder, Semen Tritici aestivi, starch, Helianthi powder, corn, meat and bone meal, aminoacid, Animal fat, vitamin and the trace mineral that are present in the animal feed composition (food) are used in combination.
In such compositions, the ratio of electrolyte para Toluic Acid or derivatives thereof is adapted at the scope of 0.5: 1 to 5: 1 (w/w), preferred 1.5: 1 to 3: 1 (w/w).
To animal such as poultry, pig or cattle,, be effective especially as medicine with the benzoic acid or derivatives thereof especially for pig.
To further specify the present invention: embodiment 1 with reference to following embodiment:
Be fodder compound prescription (shown in the following table 2) below, wherein all consumptions are all represented with percentage by weight and are fed to pig.
Table 2
Compositions The contrast I The contrast II Embodiment 1
Meat powder (58% thick protein) ?????3.20 ????3.20 ????3.20
Molasses ?????5.00 ????5.00 ????5.00
Semen Tritici aestivi ?????5.90 ????5.90 ????5.90
Semen sojae atricolor powder (45% crude protein) ?????15.1 ????15.1 ????15.1
Tapioca starch (66% starch) ?????38.5 ????36.5 ????35.5
Alcomeal ?????15 ?????15 ?????15
Animal fat ?????3.3 ?????3.3 ?????3.3
Limestone ?????0.74 ?????0.74 ????0.74
Lysine hydrochloride (98%) ?????0.06 ?????0.06 ????0.06
The premix vitamin ?????0.5 ?????0.5 ?????0.5
Trace mineral ?????0.5 ?????0.5 ?????0.5
The Helianthi powder ????12.2 ?????12.2 ?????12.5
Ammonium chloride ?????- ??????2 ??????2
Ammonium benzoate ?????- ??????- ??????1
Fed pigs two days with these feedstuffs, in the pH of different time supervision pig urine, result's following (face table 3 as follows): table 3
Time Contrast I-pH Contrast II-pH Embodiment 2-pH
After 0 day * ????8.15 ????5.22 ????4.68
After 7 days ????8.30 ????8.57 ????5.01
After 10 days ????8.30 ????8.60 ????6.92
*Feed two days later the Excreta first time of pig
Most clearly see from these results, use additive of the present invention can cause excremental peracidity and stable p H-number, therefore, almost or not produce distributing of ammonia flavor.Embodiment 2
In further contrast test, feed a collection of pig with the standard feed shown in the following table 4.Except replace repeating embodiment 2 0.7% weight of alcomeal in the standard feed with formic acid.The result is listed as in the following table 5:
Table 4
Compositions Weight %
Fructus Hordei Vulgaris ????36.15
Semen Tritici aestivi ????30
Semen Pisi sativi ????3.5
The young powder of Brassica campestris L ?????3
Semen sojae atricolor oil meal (Brazilian) ????17
Alcomeal ????2.5 *
Animal fat ????1.9
Limestone ????0.61
Lysine hydrochloride (98%) ????0.18
The premix vitamin ?????1
Molasses ????3.4
Methionine ????0.11
One-lime phosphate ????0.4
Salt ????0.25
Table 5
Variable Embodiment 2 * Comparative test
Feed pig quantity ?????33 ????33
Every pig starting weight (kg) ?????23.8 ????23.0
Every pig final weight (kg) ?????40 ????40.3
Every pig increment every day (g) ????577 ????588
Food conversion ????1.91 ????2.11
Feedstuff intake (kg) ????1.104 ????1.239
*Benzoic acid replaces 0.7% weight of alcomeal in the standard feed
The above results shows with the pig that contains the benzoic acid forage feed has much lower food conversion (based on feedstuff intake and every pig growth ratio calculating every day) than the pig with no benzoic acid forage feed.This shows that the described feedstuff of use feeds pigs more effective.Embodiment 3:
To contain the effect of benzoic acid experiment forage feed pig and not contain any benzoic control feed and compare.Present embodiment uses the pig house that six pigsties are arranged in 3 cycles.The pig of 3 pigsties is wherein fed control feed and the pig of other 3 pigsties is fed the experiment feedstuff.Below the as shown in table 6 and result of implementation of the fodder compound row in the table 7.The pig that feeds the experiment feedstuff as seen from Table 7 has low-down feed conversion rate.This may be owing to reduced the pH of intestinal, thereby has perhaps improved the result of digestibility.
The designing chemical composition (g/Kg) of table 6 raw material (10%) and feedstuff
Component Initial feedstuff Final feed
Experiment Contrast Experiment Contrast
Rye (Secale cereale L.) ????5.0 ????5.0 ???15.0 ????15.0
Fructus Hordei Vulgaris ???30.0 ???30.0 ???15.0 ????15.0
Semen Tritici aestivi ???27.8 ???27.2 ???25.0 ????24.0
Semen Pisi sativi ???3.5 ????3.5 ????14.5 ???13.0
The corn gluten feedstuff ????- ?????- ?????7.1 ????6.5
The young powder of Brassica campestris L ???3.0 ????3.0 ?????2.3 ????2.5
Semen sojae atricolor powder ??15.2 ???14.0 ?????6.5 ????7.3
Alcomeal ???2.8 ????4.4 ?????5.0 ????5.0
Cane molasses ???5.0 ????5.0 ?????3.2 ????6.0
Animal powder ???1.3 ????2.0 ??????- ?????-
Animal fat ???1.90 ????1.83 ?????2.20 ????2.21
Methionine and cystine mixture (Mervit ) ???0.55 ????0.56 ?????0.35 ????0.36
Threonine (Mervit ) ???0.26 ????0.29 ?????0.29 ????0.30
Liquid lysine ???0.76 ????0.78 ?????0.56 ????0.57
Calprona?P * ???1.0 ????0.70 ?????0.6 ?????-
One-lime phosphate ???0.33 ????0.22 ??????- ????0.02
Sodium chloride ???0.22 ????0.21 ?????0.25 ????0.24
Vitamin/mineral pre-composition (Mervit ) for initial feedstuff ???0.50 ????0.50 ??????- ?????-
Vitamin/mineral pre-composition (Mervit ) for final feed ????- ?????- ?????0.50 ????0.5
Phytase (Mervit ) ???0.20 ????0.24 ?????0.21 ????0.20
Limestone ????- ????0.55 ??????- ????1.13
Benzoic acid ???2.7 ?????- ?????1.4 ?????-
*This is the mixture of Ca (25%) and carboxylic acid (75%) mixture (wherein sour and sour consumption is formic acid 30%, acetic acid 30%, the mixture of propanoic acid 30% and citric acid 10%).The compositions of design chemical analysis
Component Initial feedstuff Final feed
Experiment Contrast Experiment Contrast
Energy value # ????1.08 ??1.08 ????1.07 ????1.07
Water ????131 ??132 ????130 ????134
Easy digestible lysine ????8.4 ??8.4 ????7.0 ????7.0
Easily digest methionine and cysteine ????5.2 ??5.2 ????4.5 ????4.5
Starch ????380 ??380 ????400 ????388
Calcium ????7.3 ??7.3 ????6.3 ????6.3
Phosphorus ????4.8 ??4.8 ????4.1 ????4.1
Easily digest phosphorus ????2.9 ??2.9 ????2.1 ????2.1
Sodium ????1.2 ??1.2 ????1.3 ????1.4
Potassium ????9.0 ??9.0 ????8.3 ????9.1
Chlorine ????3.2 ??3.2 ????3.0 ????3.4
Per kilogram content
Crude protein ???169 ????170 ????150 ????150
Crude fat ????39 ????40 ????41 ?????41
Crude fibre ????39 ????40 ????40 ?????39
Ash ????50 ????53 ????44 ?????53
# unit energy value=8.8MJ (pig produces and keep clean acquisition energy)
Table 7
The control feed group Experiment feedstuff group
The quantity of pig ????99 ????99
Initial live-weight (kg) ????26.2 ???26.29
Final live-weight (kg) ????107.4 ???108.2
Rate of growth (g/ days) ????723 ????738
Feedstuff intake (1cg/ days) ????1.97 ????1.95
Feed conversion rate ????2.72 ???2.64
Go out the meat percentage rate ????56.1 ???56.3
Pick out pig ?????5 ????2

Claims (12)

1. as the compositions that contains benzoic acid or benzoic acid derivative of veterinary drug, can produce free benzoic acid in vivo.
2. the compositions of claim 1, wherein the benzoic acid or derivatives thereof gives animal capable as the component of animal feed composition and produces free benzoic acid in vivo.
3. the compositions of claim 1, wherein benzoic acid and its derivant give animal as the component of animal drinking-water.
4. the compositions of any one in the aforementioned claim, wherein can produce benzoic benzoic acid derivative in vivo is the benzoic salt that is selected from alkali metal benzoate, alkaline-earth metal benzoate and ammonium benzoate.
5. the compositions of any one in the aforementioned claim, the amount that wherein gives the benzoic acid or derivatives thereof of animal is enough to play the amount of insecticide effect.
6. the compositions of any one in the aforementioned claim, wherein the maximum consumption of benzoic acid or derivatives thereof is limited in based on about 10% of animal feed composition total amount.
7. the compositions of any one in the aforementioned claim, the amount that wherein gives the benzoic acid or derivatives thereof of animal is based on each 0.001-5% that feeds to the animal feed gross weight.
8. the compositions of any one in the aforementioned claim, wherein said benzoic acid or derivatives thereof gives animal with one or more following ingredients combinations that are present in the animal feed composition (food): calcium carbonate; Electrolyte, particularly ammonium chloride; Protein especially comprises Semen sojae atricolor powder, Semen Tritici aestivi, starch, Helianthi powder, corn, meat and bone meal; Aminoacid; Animal fat; Vitamin and trace mineral.
9. the compositions of claim 8, wherein the ratio of electrolyte para Toluic Acid or derivatives thereof is 0.5 in animal feed composition: 1-5: 1 (w/w).
10. list the prescription of animal feed composition in tabulating down, wherein all consumptions are all represented with percentage by weight: Compositions Consumption Meat powder (58% crude protein) ?????3.20 Molasses ?????5.00 Semen Tritici aestivi ?????5.9 Semen sojae atricolor powder (45% crude protein) ????15.1 Maninot esculenta crantz. (66% starch) ????35.5 Alcomeal ????15 Animal fat ????3.3 Limestone ????0.74 Lysine hydrochloride (98%) ????0.06 The premix vitamin ????0.5 Trace mineral ????0.5 The Helianthi powder ???12.2 Ammonium chloride ????2 Ammonium benzoate ????1
11. contain the animal feed composition of benzoic acid or derivatives thereof, can be selected from poultry as medicine at any time, the animal of pig and cattle.
12. the compositions of any one in the aforementioned claim, wherein benzoic acid is used for containing the formula for pig forage of component shown in the tabulation 4 and 8 down:
Table 4 Compositions Weight % Fructus Hordei Vulgaris ????36.15 Semen Tritici aestivi ????30 Semen Pisi sativi ?????3.5 The young powder of Brassica campestris L ?????3 Semen sojae atricolor oil meal (Brazilian) ????17
Alcomeal ????2.5 Animal fat ????1.9 Limestone ????0.61 Lysine hydrochloride (98%) ????0.18 The little element of giving birth to of premix ?????1 Molasses ????3.4 Methionine ????0.11 One-lime phosphate ????0.4 Salt ????0.25
Table 8 Variable Consumption * Feed pig quantity ?????33 Every pig starting weight (kg) ????23.8 Every pig final weight (kg) ?????40 Every pig increment every day (g) ????577 Food conversion ????1.91 Feedstuff intake (kg) ????1.104
*Benzoic acid replaces 0.7% weight of alcomeal in the standard feed.
CN97198985A 1996-08-27 1997-08-19 Biocidal compositions Pending CN1236314A (en)

Applications Claiming Priority (2)

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GBGB9618008.8A GB9618008D0 (en) 1996-08-27 1996-08-27 Biocidal compositions
GB9618008.8 1996-08-27

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CN1236314A true CN1236314A (en) 1999-11-24

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EP (1) EP0921792A1 (en)
KR (1) KR100505971B1 (en)
CN (1) CN1236314A (en)
AU (1) AU4027797A (en)
BR (1) BR9711977A (en)
CA (1) CA2265046C (en)
GB (1) GB9618008D0 (en)
PL (1) PL191241B1 (en)
WO (1) WO1998008499A1 (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101331915A (en) * 2007-06-29 2008-12-31 帝斯曼知识产权资产管理有限公司 Animal feed composition
CN101360426B (en) * 2006-01-13 2012-10-03 帝斯曼知识产权资产管理有限公司 Novel use of a nutraceutical composition in animal feed
CN105661046A (en) * 2016-02-23 2016-06-15 广州英赛特生物技术有限公司 Application of calcium benzoate to preparing of animal feed additive
WO2016131205A1 (en) * 2015-02-16 2016-08-25 广州英赛特生物技术有限公司 Application of p-methyl benzoic acid or salt thereof as animal feed additive
CN108617856A (en) * 2018-03-14 2018-10-09 广州英赛特生物技术有限公司 Application of the zinc benzoate in preparing animal feed additive

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NL1016974C2 (en) * 2000-12-22 2002-06-25 Dsm Nv Benzoic acid particles.
DE102006021392B4 (en) * 2006-05-08 2013-06-27 Ligrana Gmbh composition
JP2009029789A (en) * 2007-06-26 2009-02-12 Marubeni Nisshin Feed Co Ltd Composition for preventing and treating domestic animal urinary tract infection
DE102016101603B3 (en) 2016-01-29 2017-05-11 Hanon Systems Fastening element and method for fastening fluid pipe ends
DE102016203477A1 (en) 2016-03-03 2017-09-07 Addcon Europe Gmbh Preparation and use of alkali metal diformates with medium-chain fatty acid derivatives
WO2020002595A1 (en) 2018-06-29 2020-01-02 Dsm Ip Assets B.V. Fast release benzoic acid in feed

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Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101360426B (en) * 2006-01-13 2012-10-03 帝斯曼知识产权资产管理有限公司 Novel use of a nutraceutical composition in animal feed
CN101331915A (en) * 2007-06-29 2008-12-31 帝斯曼知识产权资产管理有限公司 Animal feed composition
CN101331915B (en) * 2007-06-29 2013-04-03 帝斯曼知识产权资产管理有限公司 Animal feed composition
CN102239962B (en) * 2007-06-29 2014-07-02 帝斯曼知识产权资产管理有限公司 Animal feed composition
WO2016131205A1 (en) * 2015-02-16 2016-08-25 广州英赛特生物技术有限公司 Application of p-methyl benzoic acid or salt thereof as animal feed additive
CN105661046A (en) * 2016-02-23 2016-06-15 广州英赛特生物技术有限公司 Application of calcium benzoate to preparing of animal feed additive
CN105661046B (en) * 2016-02-23 2020-12-18 广州英赛特生物技术有限公司 Application of calcium benzoate in preparation of animal feed additive
CN108617856A (en) * 2018-03-14 2018-10-09 广州英赛特生物技术有限公司 Application of the zinc benzoate in preparing animal feed additive

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PL331763A1 (en) 1999-08-02
PL191241B1 (en) 2006-04-28
EP0921792A1 (en) 1999-06-16
BR9711977A (en) 1999-08-24
WO1998008499A1 (en) 1998-03-05
CA2265046C (en) 2010-05-25
CA2265046A1 (en) 1998-03-05
KR100505971B1 (en) 2005-08-05
KR20000035832A (en) 2000-06-26
AU4027797A (en) 1998-03-19
GB9618008D0 (en) 1996-10-09

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