CN1201662C - Preparation technique of biopesticide stellerin emulsion - Google Patents
Preparation technique of biopesticide stellerin emulsion Download PDFInfo
- Publication number
- CN1201662C CN1201662C CN 02133769 CN02133769A CN1201662C CN 1201662 C CN1201662 C CN 1201662C CN 02133769 CN02133769 CN 02133769 CN 02133769 A CN02133769 A CN 02133769A CN 1201662 C CN1201662 C CN 1201662C
- Authority
- CN
- China
- Prior art keywords
- chamaejasmine
- aqueous emulsion
- biological pesticide
- chinese stellera
- stellera root
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000000839 emulsion Substances 0.000 title claims abstract description 19
- 238000002360 preparation method Methods 0.000 title claims description 8
- 238000000034 method Methods 0.000 title abstract 4
- 230000000853 biopesticidal effect Effects 0.000 title description 3
- 239000000575 pesticide Substances 0.000 claims abstract description 21
- RNQBLQALVMHBKH-HHGOQMMWSA-N (2r,3s)-3-[(2r,3s)-5,7-dihydroxy-2-(4-hydroxyphenyl)-4-oxo-2,3-dihydrochromen-3-yl]-5,7-dihydroxy-2-(4-hydroxyphenyl)-2,3-dihydrochromen-4-one Chemical compound C1=CC(O)=CC=C1[C@H]1[C@H]([C@@H]2C(C3=C(O)C=C(O)C=C3O[C@H]2C=2C=CC(O)=CC=2)=O)C(=O)C2=C(O)C=C(O)C=C2O1 RNQBLQALVMHBKH-HHGOQMMWSA-N 0.000 claims abstract description 19
- QOPUSVUZHPIYER-QKOWHPQASA-N neochamaejasmin B Natural products COc1ccc(cc1)[C@H]2Oc3cc(O)cc(O)c3C(=O)[C@H]2[C@@H]4[C@H](Oc5cc(O)cc(O)c5C4=O)c6ccc(O)cc6 QOPUSVUZHPIYER-QKOWHPQASA-N 0.000 claims abstract description 19
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims abstract description 18
- 241001263603 Stellera Species 0.000 claims abstract description 15
- 241000196324 Embryophyta Species 0.000 claims abstract description 13
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 13
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 239000002904 solvent Substances 0.000 claims abstract description 5
- 238000000605 extraction Methods 0.000 claims abstract description 3
- 238000001914 filtration Methods 0.000 claims abstract description 3
- 238000000227 grinding Methods 0.000 claims abstract description 3
- 239000003945 anionic surfactant Substances 0.000 claims description 8
- -1 fatty acid alkyl alcohol amide Chemical class 0.000 claims description 8
- 239000004094 surface-active agent Substances 0.000 claims description 8
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 6
- 229930195729 fatty acid Natural products 0.000 claims description 6
- 239000000194 fatty acid Substances 0.000 claims description 6
- 239000000047 product Substances 0.000 claims description 5
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims description 4
- 150000001875 compounds Chemical class 0.000 claims description 4
- 239000012141 concentrate Substances 0.000 claims description 4
- 239000000600 sorbitol Substances 0.000 claims description 4
- DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 claims description 2
- 125000006539 C12 alkyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 claims description 2
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 2
- 239000002202 Polyethylene glycol Substances 0.000 claims description 2
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims description 2
- ULUAUXLGCMPNKK-UHFFFAOYSA-N Sulfobutanedioic acid Chemical compound OC(=O)CC(C(O)=O)S(O)(=O)=O ULUAUXLGCMPNKK-UHFFFAOYSA-N 0.000 claims description 2
- 239000004480 active ingredient Substances 0.000 claims description 2
- 150000004703 alkoxides Chemical class 0.000 claims description 2
- 125000000217 alkyl group Chemical group 0.000 claims description 2
- 150000008052 alkyl sulfonates Chemical class 0.000 claims description 2
- 150000002148 esters Chemical class 0.000 claims description 2
- 150000004665 fatty acids Chemical class 0.000 claims description 2
- 239000000706 filtrate Substances 0.000 claims description 2
- 239000000463 material Substances 0.000 claims description 2
- 239000003208 petroleum Substances 0.000 claims description 2
- 229920001223 polyethylene glycol Polymers 0.000 claims description 2
- 229920006395 saturated elastomer Polymers 0.000 claims description 2
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims description 2
- 239000002736 nonionic surfactant Substances 0.000 claims 1
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 abstract description 8
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 abstract description 4
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical compound CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 abstract description 4
- 231100000053 low toxicity Toxicity 0.000 abstract description 2
- 239000000203 mixture Substances 0.000 abstract description 2
- HXVNBWAKAOHACI-UHFFFAOYSA-N 2,4-dimethyl-3-pentanone Chemical compound CC(C)C(=O)C(C)C HXVNBWAKAOHACI-UHFFFAOYSA-N 0.000 abstract 2
- 239000000084 colloidal system Substances 0.000 description 6
- 238000001035 drying Methods 0.000 description 6
- 239000012530 fluid Substances 0.000 description 6
- 238000003756 stirring Methods 0.000 description 5
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 239000003905 agrochemical Substances 0.000 description 2
- 230000002950 deficient Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 230000000749 insecticidal effect Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000001228 spectrum Methods 0.000 description 2
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 1
- CYEJMVLDXAUOPN-UHFFFAOYSA-N 2-dodecylphenol Chemical compound CCCCCCCCCCCCC1=CC=CC=C1O CYEJMVLDXAUOPN-UHFFFAOYSA-N 0.000 description 1
- 241001600407 Aphis <genus> Species 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 240000006927 Foeniculum vulgare Species 0.000 description 1
- 235000004204 Foeniculum vulgare Nutrition 0.000 description 1
- 244000068988 Glycine max Species 0.000 description 1
- 235000010469 Glycine max Nutrition 0.000 description 1
- 241000219146 Gossypium Species 0.000 description 1
- 241000255967 Helicoverpa zea Species 0.000 description 1
- NTIZESTWPVYFNL-UHFFFAOYSA-N Methyl isobutyl ketone Chemical compound CC(C)CC(C)=O NTIZESTWPVYFNL-UHFFFAOYSA-N 0.000 description 1
- 241000409991 Mythimna separata Species 0.000 description 1
- 244000061176 Nicotiana tabacum Species 0.000 description 1
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 241000255969 Pieris brassicae Species 0.000 description 1
- 235000021307 Triticum Nutrition 0.000 description 1
- 244000098338 Triticum aestivum Species 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
- 240000008042 Zea mays Species 0.000 description 1
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 1
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 1
- 150000004996 alkyl benzenes Chemical class 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 239000002280 amphoteric surfactant Substances 0.000 description 1
- 229930101531 artemisinin Natural products 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- BLUAFEHZUWYNDE-XRNKLDBLSA-N chembl77 Chemical compound C([C@@](OO1)(C)O2)C[C@H]3[C@H](C)CC[C@@H]4C31[C@@H]2OC(=O)[C@@H]4C BLUAFEHZUWYNDE-XRNKLDBLSA-N 0.000 description 1
- 235000005822 corn Nutrition 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 229960002715 nicotine Drugs 0.000 description 1
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 1
- NHOIBRJOQAYBJT-IMGVWCFESA-N nimbin Chemical compound C=1([C@@H]2C[C@H]3O[C@H]4[C@](C3=C2C)(C)[C@@H]([C@]2(C(=O)C=C[C@](C)([C@@H]2[C@H]4OC(C)=O)C(=O)OC)C)CC(=O)OC)C=COC=1 NHOIBRJOQAYBJT-IMGVWCFESA-N 0.000 description 1
- ZQIYJHBQRBBBRZ-UHFFFAOYSA-N nimbin Natural products COC(=O)CC1C2C(C(OC(=O)C)C3OC4CC(C(=C4C13C)C)c5cocc5)C(C)(C=CC2=O)C(=O)OC ZQIYJHBQRBBBRZ-UHFFFAOYSA-N 0.000 description 1
- 244000144977 poultry Species 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 239000001397 quillaja saponaria molina bark Substances 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 229930182490 saponin Natural products 0.000 description 1
- 150000007949 saponins Chemical class 0.000 description 1
- 210000004894 snout Anatomy 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
Description
Claims (2)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 02133769 CN1201662C (en) | 2002-09-18 | 2002-09-18 | Preparation technique of biopesticide stellerin emulsion |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 02133769 CN1201662C (en) | 2002-09-18 | 2002-09-18 | Preparation technique of biopesticide stellerin emulsion |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1409968A CN1409968A (en) | 2003-04-16 |
CN1201662C true CN1201662C (en) | 2005-05-18 |
Family
ID=4747378
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN 02133769 Expired - Fee Related CN1201662C (en) | 2002-09-18 | 2002-09-18 | Preparation technique of biopesticide stellerin emulsion |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN1201662C (en) |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102939874B (en) * | 2012-10-19 | 2013-12-04 | 岭南园林股份有限公司 | Landscape plant pest control method |
CN103598265A (en) * | 2013-11-11 | 2014-02-26 | 丹阳市清云农业发展有限公司 | Insect-expelling and disinsection composition for organic rice and preparation method thereof |
CN103621504A (en) * | 2013-11-26 | 2014-03-12 | 内蒙古自治区农牧业科学院 | Stellera chamaejasme microemulsion and preparation method thereof |
CN103651594B (en) * | 2013-12-18 | 2015-08-05 | 青岛百瑞吉生物工程有限公司 | A kind of composite biological insecticide |
CN106973946A (en) * | 2017-05-25 | 2017-07-25 | 中国科学院西北高原生物研究所 | A kind of compounded pesticides of the extract containing The Leaves And Stems of Stellera Chamaejasme |
-
2002
- 2002-09-18 CN CN 02133769 patent/CN1201662C/en not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
CN1409968A (en) | 2003-04-16 |
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Legal Events
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C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
C57 | Notification of unclear or unknown address | ||
DD01 | Delivery of document by public notice |
Addressee: Zhang Jieke Document name: payment instructions |
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C56 | Change in the name or address of the patentee |
Owner name: GANSU GUOLI BIO-TECHNOLOGY DEVELOPMENT CO., LTD. Free format text: FORMER NAME OR ADDRESS: ZHANG JIEKE |
|
CP03 | Change of name, title or address |
Address after: 730030, twenty, International Trade Building or Cetra Building, 258 Qingyang Road, Chengguan District, Gansu, Lanzhou Patentee after: Gansu Guoli biological science and Technology Development Co Ltd Address before: 610072, Chengdu, Sichuan province Jinli Street West Road, No. 78 force industry Co., Ltd. Patentee before: Zhang Jieke |
|
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20050518 Termination date: 20140918 |
|
EXPY | Termination of patent right or utility model |