CN117757620B - Production equipment and production method of ginseng peptide with oxidation resistance and aging resistance - Google Patents
Production equipment and production method of ginseng peptide with oxidation resistance and aging resistance Download PDFInfo
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- CN117757620B CN117757620B CN202310918938.0A CN202310918938A CN117757620B CN 117757620 B CN117757620 B CN 117757620B CN 202310918938 A CN202310918938 A CN 202310918938A CN 117757620 B CN117757620 B CN 117757620B
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- 238000004519 manufacturing process Methods 0.000 title claims abstract description 44
- 241000208340 Araliaceae Species 0.000 title claims abstract description 42
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 title claims abstract description 42
- 235000003140 Panax quinquefolius Nutrition 0.000 title claims abstract description 42
- 235000008434 ginseng Nutrition 0.000 title claims abstract description 42
- 108090000765 processed proteins & peptides Proteins 0.000 title claims abstract description 41
- 230000032683 aging Effects 0.000 title claims abstract description 18
- 230000003647 oxidation Effects 0.000 title claims abstract description 18
- 238000007254 oxidation reaction Methods 0.000 title claims abstract description 18
- 239000007788 liquid Substances 0.000 claims abstract description 230
- 238000005070 sampling Methods 0.000 claims abstract description 96
- 238000003756 stirring Methods 0.000 claims abstract description 24
- 230000003712 anti-aging effect Effects 0.000 claims abstract description 17
- 230000000694 effects Effects 0.000 claims abstract description 9
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- 238000003860 storage Methods 0.000 claims description 93
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- 238000000034 method Methods 0.000 abstract description 14
- 239000011550 stock solution Substances 0.000 abstract description 10
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- 238000001514 detection method Methods 0.000 abstract description 4
- 238000000605 extraction Methods 0.000 abstract description 4
- 108010009736 Protein Hydrolysates Proteins 0.000 abstract 1
- 230000007071 enzymatic hydrolysis Effects 0.000 abstract 1
- 238000006047 enzymatic hydrolysis reaction Methods 0.000 abstract 1
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- 238000010586 diagram Methods 0.000 description 11
- 239000003963 antioxidant agent Substances 0.000 description 10
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Abstract
The invention discloses production equipment and a production method of ginseng peptide with oxidation resistance and aging resistance, and relates to the technical field of ginseng peptide production. This production facility with antioxidation and anti-aging's ginseng peptide can realize filling the stock solution bottle that is equipped with enzymatic hydrolysate on the sampling device automatically, later realize injecting enzymatic hydrolysate, cooperation stirring frame makes enzymatic hydrolysate and wait to extract liquid misce bene, sampling device can set up a plurality ofly, thereby can inject same enzymatic hydrolysate simultaneously many times, perhaps inject different enzymatic hydrolysate by many times, after enzymolysis for a period of time, through retrieving the subassembly, the upset subassembly, send the bottle subassembly to bottled empty stock solution on sampling device, can realize automatic sampling through sampling device and sampling pipe fitting, and finally retrieve the subassembly through retrieving, be convenient for carry out sampling detection at the in-process of enzymolysis, the inconvenient extraction liquid that detects in the enzymatic hydrolysate bucket of some enzymatic hydrolysis devices now has been solved, can lead to the enzymolysis condition uncontrollable, the problem of enzymolysis effect is poor.
Description
Technical Field
The invention relates to the technical field of ginseng peptide production, in particular to production equipment and a production method of ginseng peptide with oxidation resistance and aging resistance.
Background
The ginseng peptide is a bioactive peptide extracted from ginseng, has various health care effects including oxidation resistance and aging resistance, has large working pressure, reduced exercise quantity, and reduced physique of people along with the acceleration of the work and life rhythm of people, and is greatly increased for sub-healthy people, so that a tonic with high nutritive value is required to be eaten to improve the autoimmune power of the human body, strengthen the physique and improve the life quality, and the ginseng has various effects of tonifying original qi, promoting the production of body fluid, soothing the nerves, relaxing blood vessels, exciting nerves, improving blood circulation, enhancing heart contraction and the like, and often plays a role in the first choice of people.
The Chinese patent publication No. CN108077550B discloses a ginseng peptide production device, which is fast and convenient to assemble and disassemble through a rotating shaft, a connecting component and a stirring paddle, can be conveniently maintained and replaced, has reasonable design, can realize maximized stirring area, improves stirring efficiency and uniformity, can accelerate enzymolysis speed and enzymolysis efficiency, can meet the requirement of dissolution of various enzymes, simplifies operation and improves production efficiency.
The Chinese patent publication No. CN114231411A discloses a ginseng peptide production device and a production process, wherein a stirring gear is arranged above a stirring shaft in a clamping connection mode, the stirring gear adopts a detachable structure, the stirring gear is convenient to replace, at least two sizes are provided, the rotation speed of the stirring shaft connected with the stirring gear can be changed by replacing stirring gears with different gear tooth numbers, and then the material stirring speeds at different upper and lower positions in an enzymolysis tank body are changed, so that the device is suitable for different enzymolysis requirements.
The effect of enzymolysis is guaranteed to some measures that above prior art all adopted, but foretell enzymolysis device has inconvenient sampling detection to the extract in the enzymolysis bucket, probably can lead to the enzymolysis condition uncontrollable, problem that enzymolysis effect is poor.
Disclosure of Invention
Aiming at the defects of the prior art, the invention provides production equipment and production method of ginseng peptide with oxidation resistance and aging resistance, and solves the problems that the prior enzymolysis devices are inconvenient to sample and detect the extracting solution in the enzymolysis barrel, possibly cause uncontrollable enzymolysis condition and poor enzymolysis effect.
In order to achieve the above purpose, the invention is realized by the following technical scheme: production facility with antioxidation and anti-aging's ginseng peptide, including enzymolysis bucket and the closing cap of setting on enzymolysis bucket, install agitator motor on the closing cap, agitator motor output shaft runs through closing cap and fixedly connected with stirring frame, its characterized in that: the sealing cover is fixedly connected with a supporting block, the supporting block is fixedly connected with a sampling device, and the bottom of the sampling device is provided with a sampling pipe fitting penetrating through the sealing cover; the liquid storage bottle is movably inserted on the sampling device, a supporting frame is integrally formed on the surface of the sealing cover, a bottle conveying assembly is arranged on the sealing cover, a turnover assembly and a recovery assembly are respectively arranged on the supporting frame, the bottle conveying assembly is used for conveying the liquid storage bottle to a turnover position after being separated from the sampling device, the turnover assembly is used for clamping the liquid storage bottle and then turning the liquid storage bottle upwards, and the recovery assembly is used for recovering the liquid storage bottle.
Further, the sampling device comprises a buffer tube, a liquid inlet electromagnetic valve, a liquid outlet electromagnetic valve and a one-way air outlet valve, wherein the buffer tube is fixedly connected to the supporting block, the liquid inlet electromagnetic valve is fixedly connected to the bottom of the buffer tube, the liquid outlet electromagnetic valve is fixedly connected to the upper part of the buffer tube and corresponds to the liquid outlet electromagnetic valve in an up-down mode, and the one-way air outlet valve is fixedly connected to the upper part of the buffer tube; one end of the buffer tube is fixedly connected with a sampling electric push rod, an output shaft of the sampling electric push rod movably penetrates through the buffer tube and is fixedly connected with a rubber plug, and the surface of the rubber plug is attached to the inner side wall of the buffer tube; the sampling pipe fitting is fixedly connected with the liquid inlet end of the liquid inlet electromagnetic valve, the liquid outlet end of the liquid outlet electromagnetic valve is fixedly connected with a clamping ring, and the liquid storage bottle is inserted on the clamping ring and clamped and fixed by the bottle feeding component.
Further, the sampling pipe fitting includes main pipe and back flow, the one end of main pipe and the feed liquor end fixed connection of feed liquor solenoid valve, its other end runs through the closing cap and extends to the inside of enzymolysis bucket, the one end of back flow and the fixed surface of main pipe of taking out are connected with and inside are linked together between them, the other end fixedly connected with backward flow solenoid valve of back flow, backward flow solenoid valve fixed connection is keeping away from the one end that the sampling electric putter was kept away from to the buffer tube.
Further, a half-cone notch is formed in the surface of the rubber plug, the half-cone notch faces the liquid outlet electromagnetic valve, and the liquid outlet electromagnetic valve and the one-way air outlet valve are located on the same straight line.
Further, the surface of main pipe of taking out has seted up the pressure release hole, fixedly connected with lift cylinder on the closing cap, the output shaft of lift cylinder runs through the closing cap and fixedly connected with sealing member, sealing member activity cup joints the surface at main pipe of taking out.
Further, send the bottle subassembly to include the mount, vertical electric putter and horizontal electric putter, vertical electric putter fixed connection is on the surface of mount, and its output shaft passes through connecting block and crane fixed connection, horizontal electric putter fixed connection is on the crane, horizontal electric putter's output shaft fixedly connected with movable plate, the bottom fixedly connected with machinery clamping jaw of movable plate, machinery clamping jaw is connected with the stock solution bottle.
Further, the surface fixedly connected with guide bar of crane, guide bar and mount swing joint, the surface fixedly connected with gag lever post of movable plate, gag lever post and crane swing joint.
Further, the overturning assembly comprises two guide frames symmetrically arranged on the supporting frame, the two guide frames are fixedly connected with reciprocating cylinders, the output shafts of the reciprocating cylinders are fixedly connected with retracting cylinders, the output shafts of the retracting cylinders movably penetrate through the guide frames and are movably connected with the surfaces of the rotating gears, the opposite sides of the two rotating gears are fixedly connected with connecting rods, one end of one connecting rod is fixedly connected with a first clamping piece, one end of the other connecting rod is fixedly connected with a second clamping piece, and the surfaces of the second clamping pieces are movably connected with the inner side walls of the first clamping pieces; the surfaces of the two guide frames are provided with a plurality of racks in a linear array, and the racks are meshed with the rotating gears.
Further, retrieve the subassembly including retrieving frame and reciprocal electric putter, reciprocal electric putter fixed connection is on the support frame, reciprocal electric putter's output shaft passes through connecting piece and retrieves frame fixed connection, be provided with the notch that is used for placing the stock solution bottle on retrieving the frame.
The production method of the ginseng peptide with the functions of oxidation resistance and aging resistance, which is used for the production equipment of the ginseng peptide with the functions of oxidation resistance and aging resistance, comprises the following steps: s1, placing to-be-enzymolyzed extracting solution into an enzymolysis barrel, and sealing the extracting solution by using a sealing cover; s2, placing a liquid storage bottle filled with enzymolysis liquid on the recovery assembly, starting a control switch, clamping the liquid storage bottle filled with the enzymolysis liquid by the overturning assembly, overturning the liquid storage bottle by the overturning assembly after the liquid storage bottle is separated from the recovery assembly, and then clamping and fixing the overturned liquid storage bottle by the bottle feeding assembly to the sampling device; s3, the sampling device injects the enzymolysis liquid in the liquid storage bottle into the enzymolysis barrel through a sampling pipe fitting, the stirring frame enables the enzymolysis liquid and the liquid to be extracted to be uniformly mixed under the driving of the stirring motor, and the liquid storage bottle is dismantled after the enzymolysis liquid is injected; s4, after enzymolysis for a period of time, placing an empty liquid storage bottle on the recovery assembly, conveying the empty liquid storage bottle to the bottle conveying assembly through the overturning assembly, mounting the empty liquid storage bottle on the sampling device through the bottle conveying assembly, and sucking the extracting solution in the enzymolysis barrel into the liquid storage bottle through the sampling device; and S5, after sampling is finished, the liquid storage bottle stored with the sampling liquid is conveyed to the recovery assembly by the bottle conveying assembly and the overturning assembly.
The invention has the following beneficial effects:
(1) This production facility with antioxidation and anti-aging ginseng peptide through setting up recovery unit, upset subassembly, send bottle subassembly and sampling device, can realize will be equipped with the stock solution bottle automatic packing of zymolysis liquid to sampling device on, later realize injecting zymolysis liquid, cooperation stirring frame, make zymolysis liquid and wait to draw liquid misce bene, sampling device can set up a plurality of, thereby can inject same zymolysis liquid simultaneously many times, perhaps inject different zymolysis liquid for many times, after enzymolysis for a period, through recovery unit, upset subassembly, send bottle subassembly to empty stock solution bottle to be on sampling device, can realize automatic sampling through sampling device and sampling pipe fitting, and finally retrieve through recovery unit, be convenient for carry out sampling detection at the in-process of enzymolysis, know the enzymolysis condition as early as possible, thereby can adjust according to the enzymolysis condition, the inconvenient extraction liquid that detects of carrying out in the enzymolysis bucket of some current enzymolysis devices, probably can lead to the enzymolysis condition uncontrollable, the problem of enzymolysis effect is poor.
(2) This production facility with antioxidation and anti-aging ginseng peptide through setting up the buffer tube, feed liquor solenoid valve, go out the liquid solenoid valve, one-way air outlet valve, main pull tube and back flow, through control feed liquor solenoid valve, go out liquid solenoid valve and reflux control valve, can realize the injection of enzymolysis liquid and the extraction of sample liquid to utilize the negative pressure to realize that enzymolysis liquid pours into the buffer tube automatically, also can utilize the negative pressure to realize the extraction of large capacity sample liquid simultaneously, guarantee the reliability of testing result.
(3) This production facility with antioxidation and anti-aging ginseng peptide through setting up recovery unit, upset subassembly, send a bottle subassembly, place the stock solution bottle or the empty stock solution bottle that are equipped with enzymatic hydrolysate and retrieve the price back, upset subassembly and send a bottle subassembly to realize autoloading and retrieve, convenient operation, efficient.
Of course, it is not necessary for any one product to practice the invention to achieve all of the advantages set forth above at the same time.
Drawings
FIG. 1 is a schematic diagram showing the overall structure of an apparatus for producing ginseng peptide having antioxidant and antiaging properties according to the present invention.
FIG. 2 is a schematic diagram of the internal structure of an enzymolysis tank of a production facility for producing ginseng peptide with antioxidant and anti-aging effects.
FIG. 3 is a schematic diagram showing the structure of turnover components of the production facility for ginseng peptide with oxidation resistance and aging resistance.
FIG. 4 is a schematic diagram showing the structure of a rotating gear of a production facility for ginseng peptide having antioxidant and antiaging properties according to the present invention.
Fig. 5 is a schematic diagram showing the split structure of the first clamping member and the second clamping member of the production equipment of ginseng peptide with oxidation resistance and aging resistance.
FIG. 6 is a schematic diagram showing the structure of a bottle feeding assembly of a production facility for ginseng peptide having antioxidant and anti-aging properties.
FIG. 7 is a schematic diagram showing the structure of a sealing member of a production facility for ginseng peptide having antioxidant and antiaging properties according to the present invention.
FIG. 8 is a schematic diagram showing the structure of a rubber stopper of a production facility for ginseng peptide having antioxidant and antiaging properties according to the present invention.
FIG. 9 is a schematic diagram showing the internal structure of a buffer tube of a production facility for ginseng peptide having antioxidant and antiaging properties according to the present invention.
FIG. 10 is a schematic diagram showing the structure of a semi-conical notch of a production facility for ginseng peptide having antioxidant and antiaging properties according to the invention.
FIG. 11 is a schematic diagram showing the structure of recovery components of the production facility for ginseng peptide having antioxidant and anti-aging properties of the present invention.
FIG. 12 is a flow chart of a process for producing ginseng peptide having antioxidant and antiaging properties according to the invention.
In the figure, 1, an enzymolysis barrel; 2. a closing cap; 3. a stirring motor; 4. a stirring rack; 5. a support block; 6. a sampling device; 601. a buffer tube; 602. a liquid inlet electromagnetic valve; 603. a liquid outlet electromagnetic valve; 604. a one-way air outlet valve; 7. sampling the pipe fitting; 701. a main suction pipe; 702. a return pipe; 8. a liquid storage bottle; 9. a support frame; 10. sampling an electric push rod; 11. a rubber stopper; 12. a clamping ring; 13. a semi-conical notch; 14. a pressure relief hole; 15. a lifting cylinder; 16. a sealing member; 17. a fixing frame; 18. a longitudinal electric push rod; 19. a transverse electric push rod; 20. a lifting frame; 21. a moving plate; 22. mechanical clamping jaws; 23. a guide rod; 24. a limit rod; 25. a guide frame; 26. a reciprocating cylinder; 27. a retraction cylinder; 28. rotating the gear; 29. a connecting rod; 30. a first clamping member; 31. a second clamping member; 32. a rack; 33. a recovery rack; 34. a reciprocating electric push rod; 35. a return solenoid valve.
Detailed Description
The following description of the embodiments of the present invention will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present invention, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
In the description of the present invention, it should be understood that the terms "open," "upper," "lower," "thickness," "top," "middle," "length," "inner," "peripheral," and the like indicate orientation or positional relationships, merely for convenience in describing the present invention and to simplify the description, and do not indicate or imply that the components or elements referred to must have a particular orientation, be constructed and operated in a particular orientation, and thus should not be construed as limiting the present invention.
Referring to fig. 1 to 11, the embodiment of the present invention provides a technical solution: production facility with antioxidation and anti-aging's ginseng peptide, including enzymolysis bucket 1 and closing cap 2 of setting on enzymolysis bucket 1, install agitator motor 3 on the closing cap 2, agitator motor 3 output shaft runs through closing cap 2 and fixedly connected with stirring frame 4, its characterized in that: the sealing cover 2 is fixedly connected with a supporting block 5, the supporting block 5 is fixedly connected with a sampling device 6, and the bottom of the sampling device 6 is provided with a sampling pipe fitting 7 penetrating through the sealing cover 2; the sampling device 6 is movably inserted with a liquid storage bottle 8, a support frame 9 is integrally formed on the surface of the sealing cover 2, a bottle conveying component is arranged on the sealing cover 2, a turnover component and a recovery component are respectively arranged on the support frame 9, the bottle conveying component is used for conveying the liquid storage bottle 8 to a turnover position after being separated from the sampling device 6, the liquid storage bottle 8 is clamped by the turnover component and then turned upwards to a bottle mouth, and the liquid storage bottle is recovered by the recovery component.
Specifically, the sampling device 6 includes a buffer tube 601, a liquid inlet electromagnetic valve 602, a liquid outlet electromagnetic valve 603 and a one-way air outlet valve 604, the buffer tube 601 is fixedly connected to the support block 5, the liquid inlet electromagnetic valve 602 is fixedly connected to the bottom of the buffer tube 601, the liquid outlet electromagnetic valve 603 is fixedly connected to the upper part of the buffer tube 601 and corresponds to the liquid outlet electromagnetic valve 603 in an up-down manner, and the one-way air outlet valve 604 is fixedly connected to the upper part of the buffer tube 601; one end of the buffer tube 601 is fixedly connected with a sampling electric push rod 10, an output shaft of the sampling electric push rod 10 movably penetrates through the buffer tube 601 and is fixedly connected with a rubber plug 11, and the surface of the rubber plug 11 is attached to the inner side wall of the buffer tube 601; the sampling pipe fitting 7 is fixedly connected with the liquid inlet end of the liquid inlet electromagnetic valve 602, the liquid outlet end of the liquid outlet electromagnetic valve 603 is fixedly connected with the clamping ring 12, and the liquid storage bottle 8 is inserted on the clamping ring 12 and clamped and fixed by the bottle feeding component.
The sampling pipe fitting 7 comprises a main pumping pipe 701 and a return pipe 702, one end of the main pumping pipe 701 is fixedly connected with the liquid inlet end of the liquid inlet electromagnetic valve 602, the other end of the main pumping pipe 701 penetrates through the sealing cover 2 and extends to the inside of the enzymolysis barrel 1, one end of the return pipe 702 is fixedly connected with the surface of the main pumping pipe 701 and is communicated with the inside of the main pumping pipe 701 and the inside of the main pumping pipe 701, the other end of the return pipe 702 is fixedly connected with the return electromagnetic valve 35, and the return electromagnetic valve 35 is fixedly connected with one end, far away from the buffer pipe 601, of the sampling electric push rod 10.
The surface of the rubber plug 11 is provided with a semi-conical gap 13, the semi-conical gap 13 faces the liquid outlet electromagnetic valve 603, and the liquid outlet electromagnetic valve 603 and the one-way air outlet valve 604 are positioned on the same straight line.
In this embodiment, by switching the reflux solenoid valve 35, the liquid inlet solenoid valve 602 and the liquid outlet solenoid valve 603, the enzymolysis liquid can be injected and the sampling liquid can be pumped, and simultaneously, a large amount of air can be prevented from being pumped into the liquid storage bottle 8 in the sampling process, so that enough sampling liquid can be ensured.
Specifically, the surface of the main suction pipe 701 is provided with a pressure relief hole 14, the sealing cover 2 is fixedly connected with a lifting cylinder 15, an output shaft of the lifting cylinder 15 penetrates through the sealing cover 2 and is fixedly connected with a sealing piece 16, and the sealing piece 16 is movably sleeved on the surface of the main suction pipe 701.
In this embodiment, the sealing member 16 is used to seal and open the pressure relief hole 14, so as to facilitate sampling with different depths, and simultaneously ensure that the sample liquid in the reflux pipe 702 and the main pumping pipe 701 can flow back after sampling.
Specifically, send a bottle subassembly to include mount 17, vertical electric putter 18 and horizontal electric putter 19, and vertical electric putter 18 fixed connection is on the surface of mount 17, and its output shaft passes through connecting block and crane 20 fixed connection, and horizontal electric putter 19 fixed connection is on crane 20, and the output shaft of horizontal electric putter 19 fixedly connected with movable plate 21, the bottom fixedly connected with mechanical clamping jaw 22 of movable plate 21, mechanical clamping jaw 22 is connected with stock solution bottle 8.
The surface of the lifting frame 20 is fixedly connected with a guide rod 23, the guide rod 23 is movably connected with the fixed frame 17, the surface of the moving plate 21 is fixedly connected with a limit rod 24, and the limit rod 24 is movably connected with the lifting frame 20.
In this embodiment, in the process of making the liquid storage bottle 8 move, the guide rod 23 and the limit rod 24 can play a role in guiding and limiting, prevent to deviate, and then can make the liquid storage bottle 8 accurately install on the clamping ring 12.
Specifically, the turnover assembly comprises two guide frames 25 symmetrically arranged on the support frame 9, wherein the two guide frames 25 are fixedly connected with a reciprocating cylinder 26, an output shaft of the reciprocating cylinder 26 is fixedly connected with a retracting cylinder 27, the output shaft of the retracting cylinder 27 movably penetrates through the guide frames 25 and is movably connected with the surface of a rotating gear 28, the opposite sides of the two rotating gears 28 are fixedly connected with connecting rods 29, one end of one connecting rod 29 is fixedly connected with a first clamping piece 30, one end of the other connecting rod 29 is fixedly connected with a second clamping piece 31, and the surface of the second clamping piece 31 is movably connected with the inner side wall of the first clamping piece 30; the surfaces of both guide frames 25 are provided with a plurality of racks 32 in a linear array, and the racks 32 are engaged with the rotation gear 28.
In this embodiment, under the action of the rack 32 and the rotating gear 28, the liquid storage bottle 8 will turn over, and the bottle mouth of the recovery assembly is changed into the bottle mouth downward state, so that the mechanical clamping jaw 22 is convenient to clamp, and the liquid storage bottle 8 is mounted on the clamping ring 12, which is beneficial to realizing subsequent work.
Specifically, retrieve the subassembly and include retrieving frame 33 and reciprocal electric putter 34, reciprocal electric putter 34 fixed connection is on support frame 9, and the output shaft of reciprocal electric putter 34 passes through connecting piece and retrieves frame 33 fixed connection, is provided with the notch that is used for placing stock solution bottle 8 on retrieving frame 33.
In this embodiment, the liquid storage bottle 8 can be prevented or the liquid storage bottle 8 can be recovered through the notch on the recovery frame 33, so that batch operation is facilitated, and time is saved.
The production method of the ginseng peptide with oxidation resistance and aging resistance, which is used for the production equipment of the ginseng peptide with oxidation resistance and aging resistance, is shown in fig. 12, comprises the following steps: s1, placing to-be-enzymolyzed extracting solution into an enzymolysis barrel 1, and sealing the extracting solution by using a sealing cover 2; s2, placing a liquid storage bottle 8 filled with enzymolysis liquid on a recovery component, starting a control switch, clamping the liquid storage bottle 8 filled with the enzymolysis liquid by a turnover component, turning over the liquid storage bottle 8 by the turnover component after the liquid storage bottle 8 is separated from the recovery component, and then clamping and fixing the turned liquid storage bottle 8 by a bottle feeding component to a sampling device 6; s3, the sampling device 6 injects the enzymolysis liquid in the liquid storage bottle 8 into the enzymolysis barrel 1 through the sampling pipe fitting 7, the stirring frame 4 uniformly mixes the enzymolysis liquid and the liquid to be extracted under the driving of the stirring motor 3, and the liquid storage bottle 8 is dismantled after the enzymolysis liquid is injected; s4, after enzymolysis for a period of time, placing an empty liquid storage bottle 8 on the recovery assembly, conveying the empty liquid storage bottle 8 to the bottle conveying assembly by the overturning assembly, mounting the empty liquid storage bottle 8 on the sampling device 6 by the bottle conveying assembly, and sucking the extracting solution in the enzymolysis barrel 1 into the liquid storage bottle 8 by the sampling device 6; and S5, after sampling is finished, the liquid storage bottle 8 stored with the sampling liquid is sent to the recovery assembly by the bottle sending assembly and the overturning assembly.
When the enzymolysis barrel 1 is used, firstly, to-be-extracted liquid is placed into the enzymolysis barrel 1, then, the sealing cover 2 is packaged, the liquid storage bottle 8 filled with the enzymolysis liquid is placed through the recovery component, the recovery component comprises the recovery frame 33 and the reciprocating electric push rod 34, wherein the reciprocating electric push rod 34 is fixedly connected to the support frame 9, a connecting piece is fixedly connected to an output shaft of the reciprocating electric push rod 34, the recovery frame 33 is fixedly connected through the connecting piece, a notch for placing the liquid storage bottle 8 is formed in the recovery frame 33, a plurality of liquid storage bottles 8 filled with the enzymolysis liquid can be placed, and after the placement is completed, the reciprocating electric push rod 34 stretches to enable the recovery frame 33 to move upwards, so that the reciprocating electric push rod can be just in butt joint with the overturning component.
As shown in fig. 3, the turnover assembly comprises two guide frames 25 symmetrically arranged on the support frame 9, a reciprocating cylinder 26 is fixedly connected to the guide frames 25, a retracting cylinder 27 is fixedly connected to an output shaft of the reciprocating cylinder 26, a connecting rod 29 is fixedly connected to the retracting cylinder 27 through a rotating gear 28, one end of one connecting rod 29 is fixedly connected with a first clamping piece 30, one end of the other connecting rod 29 is fixedly connected with a second clamping piece 31, the first clamping piece 30 and the second clamping piece 31 are in a shape as shown in fig. 5, the surfaces of the second clamping piece 31 are movably connected with the inner side wall of the first clamping piece 30, when the liquid storage bottle 8 is required to be clamped, the two retracting cylinders are contracted, the first clamping piece 30 and the second clamping piece 31 are pulled by the connecting rod 29 to clamp the liquid storage bottle 8, after the clamping is firm, a reciprocating electric push rod 34 drives the retracting frame to move downwards, a notch on the retracting frame 33 is separated from the liquid storage bottle 8, the reciprocating cylinder 26 is contracted, a long rod penetrating the retracting cylinder 27 is arranged on the guide frame 25, the first clamping piece 30 and the second clamping piece can be guided and limited by the long rod penetrating the retracting cylinder 27, the surface of the second clamping piece 31 is movably connected with the first clamping piece 30, and then the second clamping piece is rotated by the reciprocating rod 28, and the second clamping piece is driven by the reciprocating electric push rod 34 to rotate the second clamping piece 28 to rotate the second clamping piece 32, and the liquid storage bottle 8, and the second clamping piece is rotated by the first clamping piece and can rotate the second clamping piece and can rotate under the action of the driving the rod and the second clamping piece and can rotate.
As shown in fig. 6, the bottle feeding assembly comprises a fixing frame 17, a longitudinal electric push rod 18 and a transverse electric push rod 19, wherein the longitudinal electric push rod 18 is fixedly connected to the surface of the fixing frame 17, an output shaft of the longitudinal electric push rod 18 is fixedly connected with a lifting frame 20 through a connecting block, an output shaft of the transverse electric push rod 19 is fixedly connected with a moving plate 21, a mechanical clamping jaw 22 is fixedly connected to the bottom of the moving plate 21, after the mechanical clamping jaw 22 clamps and stabilizes the liquid storage bottle 8, a retraction cylinder 27 is extended, a second clamping piece 31 is separated from the first clamping piece 30 and is in contact with the liquid storage bottle 8, then the transverse electric push rod 19 drives the moving plate 21 to move until the liquid storage bottle 8 corresponds to the position of the sampling device 6, and then the longitudinal electric push rod 18 moves downwards to enable the lifting frame 20 to move downwards, so that the liquid storage bottle 8 is installed on the sampling device 6 to prepare for injecting enzymolysis liquid.
As shown in fig. 8 and 9, the sampling device 6 includes a buffer tube 601, a liquid inlet electromagnetic valve 602, a liquid outlet electromagnetic valve 603 and a one-way air outlet valve 604, the buffer tube 601 is fixedly connected to the supporting block 5, the liquid inlet electromagnetic valve 602 is fixedly connected to the bottom of the buffer tube 601, the liquid outlet electromagnetic valve 603 is fixedly connected to the upper part of the buffer tube 601 and corresponds to the liquid outlet electromagnetic valve 603 vertically, the one-way air outlet valve 604 is fixedly connected to the upper part of the buffer tube 601, the liquid outlet end of the liquid outlet electromagnetic valve 603 is fixedly connected with a clamping ring 12, the liquid storage bottle 8 is spliced on the clamping ring 12 and clamped and fixed by a bottle feeding assembly, when the enzymolysis liquid is injected, the liquid inlet electromagnetic valve 602 is closed, the liquid outlet electromagnetic valve 603 is opened, the sampling electric push rod 10 drives the rubber plug 11 to move, so that the negative pressure inside the buffer tube 601 is enabled to suck the enzymolysis liquid in the liquid storage bottle 8 into the buffer tube 601, and in the process of the movement of the rubber plug 11, the one-way air outlet valve 604 can discharge compressed air out of the buffer tube 601, the liquid outlet electromagnetic valve 603 is closed, the liquid inlet electromagnetic valve 602 is opened, the sampling electric push rod 10 drives the rubber plug 11 to reset, so that enzymolysis liquid is fed into the sampling pipe fitting 7 through the liquid inlet electromagnetic valve 602, injection of the enzymolysis liquid is realized, after injection is finished, the bottle feeding component, the overturning component and the recycling component are used for recycling the empty liquid storage bottle 8, the rubber plug 11 needs to be restored to the position shown in fig. 8 after recycling, the next use is convenient, the liquid outlet electromagnetic valve 603 can be opened to enable external air to enter the buffer tube 601 to restore normal pressure, the one-way air outlet valve 604 is prevented from being in a state extruded by external air pressure for a long time, in order to shorten the stroke amount of the rubber plug 11, the semi-conical notch 13 is formed on the rubber plug, the semi-conical notch 13 can be incompletely avoided from the position of the liquid outlet electromagnetic valve 603, and external air can be enabled to enter the inside of the buffer tube 601, as shown in fig. 1, the sampling device 6 and the sampling pipe 7 are provided in plural numbers, so that the same enzymatic hydrolysate can be injected at the same time, or different enzymatic hydrolysates can be injected at intervals.
After enzymolysis for a period of time, the enzymolysis condition needs to be detected to determine whether the enzymolysis liquid needs to be continuously added or other control parameters such as rotation speed, temperature and the like need to be adjusted, and the unused liquid storage bottle 8 is mounted on the clamping ring 12 through the steps, so that sampling is prepared.
The sampling is divided into three stages, in the first stage, the liquid inlet electromagnetic valve 602, the liquid outlet electromagnetic valve 603 and the reflux electromagnetic valve 35 are all closed, the sampling electric push rod 10 is started to drive the rubber plug 11 to move, so that air in the buffer tube 601 is discharged through the one-way air outlet valve 604, at the moment, the negative pressure in the buffer tube 601 is generated, the rubber plug 11 is reset, the liquid outlet electromagnetic valve 603 is opened, air in the liquid storage bottle 8 enters the buffer tube 601 through the semi-conical notch 13, the inside of the buffer tube is restored to normal pressure, the above operation is repeated, the air in the liquid storage bottle 8 is pumped out, the inside of the buffer tube is provided with a certain negative pressure, after the first stage is completed, the rubber plug 11 is in the original position, and the liquid inlet electromagnetic valve 602, the liquid outlet electromagnetic valve 603 and the reflux electromagnetic valve 35 are all closed again.
In the second stage, the lifting cylinder 15 fixedly connected to the closing cap 2 drives the sealing piece 16 to move downwards, the pressure relief hole 14 on the surface of the main pumping pipe 701 is closed, then the liquid inlet electromagnetic valve 602 is opened, the sampling electric push rod 10 drives the rubber plug 11 to retreat, air in the main pumping pipe 701 is pumped into the buffer pipe 601, then the liquid inlet electromagnetic valve 602 is closed, the liquid outlet electromagnetic valve 603 is opened, gas in the buffer pipe 601 automatically enters the buffer pipe 8 due to negative pressure in the liquid storage bottle 8 in the first stage, meanwhile, the sampling electric push rod 10 drives the rubber plug 11 to reset, so that the rest of air enters the liquid storage bottle 8, after the rubber plug 11 resets, the air in the liquid storage bottle 8 enters the buffer pipe 601 through the semi-conical notch 13, the sampling electric push rod 10 drives the rubber plug 11 to retreat again, the air is discharged through the one-way air outlet valve 604, the operation is repeated for a plurality of times, and at the end of the second stage, the rubber plug 11 is in situ, the liquid storage bottle 8 and the buffer pipe 601 approaches normal pressure, and the air in the main pumping pipe 701 is emptied.
The third settlement is divided into two sub-stages, the first sub-stage requiring the negative pressure in the reservoir 8 and the second sub-stage starting the injection of sample liquid into the reservoir 8.
Humidity sensors are fixedly connected to the bottom and the top of the inner side wall of the buffer tube 601, in the first sub-stage, the sample liquid in the main pumping tube 701 can be pumped into the buffer tube 601 by the first backward movement of the rubber plug 11, but the buffer tube 601 cannot be completely filled with the sample liquid for the first time or the later times, if the sample liquid is directly extruded into the liquid storage bottle 8 in the stage, too little sample liquid can be caused, part of gas can be extruded into the liquid storage bottle 8 in the process, so that the sample liquid amount is further limited, even the conditions of bottle explosion or blowout can be caused due to too high pressure, therefore, in the first sub-stage, as long as the humidity sensor positioned at the top of the inner side wall of the buffer tube 601 does not detect enough humidity, the liquid inlet electromagnetic valve 602 and the reflux electromagnetic valve 35 are in a closed state and the liquid outlet electromagnetic valve 603 is opened in the process of resetting the rubber plug 11, in this case, air is squeezed into the liquid storage bottle 8, the buffer tube 601 is gradually raised in the resetting process until the humidity sensor at the top detects enough humidity, the liquid outlet electromagnetic valve 603 is closed, the reflux electromagnetic valve 35 is opened, sample liquid is refluxed into the main pumping tube 701 through the reflux tube 702, after the rubber plug 11 is reset, the negative pressure in the buffer tube 601 can suck out the air in the liquid storage bottle 8, then the reflux electromagnetic valve 35 and the liquid outlet electromagnetic valve 603 are closed, the liquid inlet electromagnetic valve 602 is opened, the rubber plug 11 is retreated, the first sub-stage is repeated once or a plurality of times until the humidity sensor at the top can always detect enough humidity, the stage can also be controlled by adopting theoretical data, the humidity sensor is not used, the repeated times of the first sub-stage is calculated through the theoretical data, after the first sub-stage is finished, the rubber plug 11 is in place, the buffer tube 601 and the liquid storage bottle 8 are both under negative pressure.
In the second sub-stage, each time the rubber stopper 11 retreats, the return electromagnetic valve 35 and the liquid outlet electromagnetic valve 603 are closed, the liquid inlet electromagnetic valve 602 is opened, each time the return electromagnetic valve 35 and the liquid inlet electromagnetic valve 602 are closed, the liquid outlet electromagnetic valve 603 is opened, the rubber stopper 11 is not completely reset, so that the sample liquid is prevented from being sucked into the rubber stopper 11 under the action of the negative pressure of the buffer tube 601, the process is repeated for a plurality of times, after enough sample liquid is extracted, the liquid outlet electromagnetic valve 603 is closed, and the rubber stopper 11 is reset. The length of each sampling pipe fitting 7 is different, so that sampling with different depths can be realized, and the accuracy of a detection result is ensured.
After sampling, the sealing piece 16 is reset, the pressure relief hole 14 is exposed, the sample liquid in the main suction pipe 701 can flow downwards under the action of gravity, the pressure in the main suction pipe 701 and the pressure in the return pipe 702 are maintained through the pressure relief hole 14, the pressure in the enzymolysis barrel 1 after sampling can be prevented from being nearly unchanged by using the liquid storage bottle 8 with proper size, the backflow of the sample liquid in the main suction pipe 701 and the return pipe 702 is facilitated, in addition, the empty liquid storage bottle 8 is mounted on the clamping ring 12, the liquid outlet electromagnetic valve 603 is opened, the gas in the liquid storage bottle is sucked into the buffer pipe 601, the liquid outlet electromagnetic valve 603 is closed, the liquid inlet electromagnetic valve 602 and the backflow electromagnetic valve 35 are opened, and the gas is extruded into the return pipe 702 and the main suction pipe 701 through the rubber plug 11, so that the forced backflow of the sample liquid is realized.
The empty liquid storage bottle 8 is recovered through the bottle conveying assembly, the overturning assembly and the recovery assembly, and is detected through a professional detecting instrument, and the enzymolysis condition is analyzed so as to extract the ginseng peptide.
It is noted that relational terms such as first and second, and the like are used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Moreover, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
The preferred embodiments of the invention disclosed above are intended only to assist in the explanation of the invention. The preferred embodiments are not exhaustive or to limit the invention to the precise form disclosed. Obviously, many modifications and variations are possible in light of the above teaching. The embodiments were chosen and described in order to best explain the principles of the invention and the practical application, to thereby enable others skilled in the art to best understand and utilize the invention. The invention is limited only by the claims and the full scope and equivalents thereof.
Claims (6)
1. Production facility with antioxidation and anti-aging's ginseng peptide, including enzymolysis bucket (1) and closing cap (2) of setting on enzymolysis bucket (1), install agitator motor (3) on closing cap (2), agitator motor (3) output shaft runs through closing cap (2) and fixedly connected with stirring frame (4), its characterized in that: a supporting block (5) is fixedly connected to the sealing cover (2), a sampling device (6) is fixedly connected to the supporting block (5), and a sampling pipe fitting (7) penetrating through the sealing cover (2) is arranged at the bottom of the sampling device (6);
The liquid storage bottle (8) is movably inserted on the sampling device (6), a supporting frame (9) is integrally formed on the surface of the sealing cover (2), a bottle conveying assembly is arranged on the sealing cover (2), a turnover assembly and a recovery assembly are respectively arranged on the supporting frame (9), the bottle conveying assembly is used for separating the liquid storage bottle (8) from the sampling device (6) and then conveying the liquid storage bottle to a turnover position, the turnover assembly clamps the liquid storage bottle (8) and then turns upwards to a bottle opening, and the recovery assembly recovers the liquid storage bottle;
The sampling device (6) comprises a buffer tube (601), a liquid inlet electromagnetic valve (602), a liquid outlet electromagnetic valve (603) and a one-way air outlet valve (604), wherein the buffer tube (601) is fixedly connected to the supporting block (5), the liquid inlet electromagnetic valve (602) is fixedly connected to the bottom of the buffer tube (601), the liquid outlet electromagnetic valve (603) is fixedly connected to the upper part of the buffer tube (601) and corresponds to the liquid outlet electromagnetic valve (603) up and down, and the one-way air outlet valve (604) is fixedly connected to the upper part of the buffer tube (601);
One end of the buffer tube (601) is fixedly connected with a sampling electric push rod (10), an output shaft of the sampling electric push rod (10) movably penetrates through the buffer tube (601) and is fixedly connected with a rubber plug (11), and the surface of the rubber plug (11) is attached to the inner side wall of the buffer tube (601);
the sampling pipe fitting (7) is fixedly connected with the liquid inlet end of the liquid inlet electromagnetic valve (602), the liquid outlet end of the liquid outlet electromagnetic valve (603) is fixedly connected with a clamping ring (12), and the liquid storage bottle (8) is inserted on the clamping ring (12) and clamped and fixed by the bottle feeding component;
The sampling pipe fitting (7) comprises a main suction pipe (701) and a return pipe (702), one end of the main suction pipe (701) is fixedly connected with the liquid inlet end of the liquid inlet electromagnetic valve (602), the other end of the main suction pipe penetrates through the sealing cover (2) and extends to the inside of the enzymolysis barrel (1), one end of the return pipe (702) is fixedly connected with the surface of the main suction pipe (701) and is communicated with the inside of the main suction pipe and the inside of the main suction pipe, the other end of the return pipe (702) is fixedly connected with a return electromagnetic valve (35), and the return electromagnetic valve (35) is fixedly connected with one end far away from the buffer pipe (601) and far away from the sampling electric push rod (10);
A semi-conical gap (13) is formed in the surface of the rubber plug (11), the semi-conical gap (13) faces the liquid outlet electromagnetic valve (603), and the liquid outlet electromagnetic valve (603) and the one-way air outlet valve (604) are positioned on the same straight line;
The surface of main pipe (701) has seted up pressure release hole (14), fixedly connected with lift cylinder (15) on closing cap (2), the output shaft of lift cylinder (15) runs through closing cap (2) and fixedly connected with sealing piece (16), sealing piece (16) activity cup joints the surface at main pipe (701).
2. The production facility of ginseng peptide having oxidation resistance and aging resistance according to claim 1, wherein: the bottle conveying assembly comprises a fixing frame (17), a longitudinal electric push rod (18) and a transverse electric push rod (19), wherein the longitudinal electric push rod (18) is fixedly connected to the surface of the fixing frame (17), an output shaft of the longitudinal electric push rod is fixedly connected with a lifting frame (20) through a connecting block, the transverse electric push rod (19) is fixedly connected to the lifting frame (20), an output shaft of the transverse electric push rod (19) is fixedly connected with a moving plate (21), the bottom of the moving plate (21) is fixedly connected with a mechanical clamping jaw (22), and the mechanical clamping jaw (22) is connected with a liquid storage bottle (8).
3. The production facility of ginseng peptide having oxidation resistance and aging resistance according to claim 2, wherein: the lifting frame is characterized in that a guide rod (23) is fixedly connected to the surface of the lifting frame (20), the guide rod (23) is movably connected with the fixed frame (17), a limiting rod (24) is fixedly connected to the surface of the moving plate (21), and the limiting rod (24) is movably connected with the lifting frame (20).
4. The production facility of ginseng peptide having oxidation resistance and aging resistance according to claim 2, wherein: the turnover assembly comprises two guide frames (25) symmetrically arranged on a support frame (9), wherein reciprocating cylinders (26) are fixedly connected to the two guide frames (25), retracting cylinders (27) are fixedly connected to output shafts of the reciprocating cylinders (26), the output shafts of the retracting cylinders (27) movably penetrate through the guide frames (25) and are movably connected with surfaces of rotating gears (28), connecting rods (29) are fixedly connected to opposite sides of the rotating gears (28), one end of one connecting rod (29) is fixedly connected with a first clamping piece (30), one end of the other connecting rod (29) is fixedly connected with a second clamping piece (31), and the surfaces of the second clamping pieces (31) are movably connected with inner side walls of the first clamping pieces (30);
The surfaces of the two guide frames (25) are provided with a plurality of racks (32) in a linear array, and the racks (32) are meshed with the rotating gears (28).
5. The production facility of ginseng peptide having oxidation resistance and aging resistance according to claim 4, wherein: the recovery assembly comprises a recovery frame (33) and a reciprocating electric push rod (34), wherein the reciprocating electric push rod (34) is fixedly connected to the support frame (9), an output shaft of the reciprocating electric push rod (34) is fixedly connected with the recovery frame (33) through a connecting piece, and a notch for placing a liquid storage bottle (8) is formed in the recovery frame (33).
6. A method for producing a ginseng peptide having oxidation resistance and aging resistance, which is used for the production apparatus of a ginseng peptide having oxidation resistance and aging resistance according to claim 1, characterized by comprising the steps of:
s1, placing to-be-enzymolyzed extracting solution into an enzymolysis barrel (1), and sealing the extracting solution by using a sealing cover (2);
S2, placing a liquid storage bottle (8) filled with enzymolysis liquid on the recovery assembly, starting a control switch, clamping the liquid storage bottle (8) filled with the enzymolysis liquid by the overturning assembly, overturning the liquid storage bottle (8) after the liquid storage bottle is separated from the recovery assembly, and then clamping and fixing the overturned liquid storage bottle (8) by the bottle conveying assembly to the sampling device (6);
S3, the sampling device (6) injects the enzymolysis liquid in the liquid storage bottle (8) into the enzymolysis barrel (1) through the sampling pipe fitting (7), the stirring frame (4) enables the enzymolysis liquid to be uniformly mixed with the liquid to be extracted under the driving of the stirring motor (3), and the liquid storage bottle (8) is removed after the enzymolysis liquid is injected;
S4, after enzymolysis for a period of time, placing an empty liquid storage bottle (8) on the recovery assembly, conveying the empty liquid storage bottle (8) to the bottle conveying assembly through the overturning assembly, mounting the empty liquid storage bottle (8) on the sampling device (6) through the bottle conveying assembly, and sucking the extracting solution in the enzymolysis barrel (1) into the liquid storage bottle (8) through the sampling device (6);
And S5, after sampling is finished, the liquid storage bottle (8) storing the sampling liquid is sent to the recovery assembly through the bottle sending assembly and the overturning assembly.
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