CN117282124B - 一种基于红外加热的植物原露析取工艺及其设备 - Google Patents
一种基于红外加热的植物原露析取工艺及其设备 Download PDFInfo
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0269—Solid material in other moving receptacles
- B01D11/0273—Solid material in other moving receptacles in rotating drums
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Abstract
Description
序号 | 升温温度(℃) | 停留时间(min) | 物质名称 | 分子式 |
1 | 35 | 10~11 | 隐酮 | C9H14O |
2 | 37 | 14~15 | 草蒿脑 | C10H12O |
3 | 39 | 10~11 | 胡椒酮 | C10H16O |
4 | 42 | 5~6 | 香茅醇 | C10H20O |
5 | 44 | 5~6 | α-乙酸松油酯 | C12H20O2 |
序号 | 升温温度(℃) | 停留时间(min) | 物质名称 | 分子式 |
1 | 34 | 7~8 | 对甲酚 | C7H8O |
2 | 36 | 9~10 | 草蒿脑 | C10H12O |
3 | 43 | 11~12 | 十三烷酸甲酯 | C14H28O2 |
序号 | 升温温度(℃) | 停留时间(min) | 物质名称 | 分子式 |
1 | 35.5 | 8~9 | 苯乙醇 | C8H10O |
2 | 37.5 | 9~10 | 1-顺马鞭草烯醇 | C10H14O |
3 | 39.5 | 8~9 | L-松香芹醇 | C10H16O |
4 | 43.5 | 7~8 | 十三烷酸甲酯 | C14H28O2 |
序号 | 升温温度(℃) | 停留时间(min) | 物质名称 | 分子式 | 原露质量(g) | 目标成分相对含量(%) |
1 | 35 | 10.3 | 隐酮 | C9H14O | 910 | 0.47 |
2 | 37 | 14.8 | 草蒿脑 | C10H12O | 1360 | 0.53 |
3 | 39 | 10.5 | 胡椒酮 | C10H16O | 971 | 1.22 |
4 | 42 | 5.5 | 香茅醇 | C10H20O | 1257 | 0.11 |
5 | 44 | 5.8 | α-乙酸松油酯 | C12H20O2 | 846 | 0.39 |
序号 | 物质名称 | 分子式 | 浓缩液质量(g) | 目标成分相对含量(%) |
1 | 隐酮 | C9H14O | 250 | 1.40 |
2 | 草蒿脑 | C10H12O | 250 | 2.45 |
3 | 胡椒酮 | C10H16O | 250 | 3.81 |
4 | 香茅醇 | C10H20O | 250 | 0.05 |
5 | α-乙酸松油酯 | C12H20O2 | 250 | 1.13 |
序号 | 升温温度(℃) | 停留时间(min) | 物质名称 | 分子式 | 原露质量(g) | 目标成分相对含量(%) |
1 | 34 | 7.5 | 对甲酚 | C7H8O | 875 | 0.34 |
2 | 36 | 9.2 | 草蒿脑 | C10H12O | 1160 | 0.13 |
3 | 43 | 11.5 | 十三烷酸甲酯 | C14H28O2 | 1092 | 0.17 |
序号 | 物质名称 | 分子式 | 浓缩提取液质量(g) | 目标成分相对含量(%) |
1 | 对甲酚 | C7H8O | 39 | 2.98 |
2 | 草蒿脑 | C10H12O | 39 | 0.45 |
3 | 十三烷酸甲酯 | C14H28O2 | 39 | 0.67 |
序号 | 升温温度(℃) | 停留时间(min) | 物质名称 | 分子式 | 原露质量(g) | 目标成分相对含量(%) |
1 | 35.5 | 8.2 | 苯乙醇 | C8H10O | 862 | 0.09 |
2 | 37.5 | 9.8 | 1-顺马鞭草烯醇 | C10H14O | 1083 | 0.16 |
3 | 39.5 | 8.8 | L-松香芹醇 | C10H16O | 1159 | 0.07 |
4 | 43.5 | 7.3 | 十三烷酸甲酯 | C14H28O2 | 941 | 0.04 |
序号 | 物质名称 | 分子式 | 浓缩液质量(g) | 目标性成分含量(%) |
1 | 苯乙醇 | C8H10O | 28 | 0.12 |
2 | 1-顺马鞭草烯醇 | C10H14O | 28 | 0.78 |
3 | L-松香芹醇 | C10H16O | 28 | 0.65 |
4 | 十三烷酸甲酯 | C14H28O2 | 28 | 0.00 |
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