CN116270366B - Hair restoration care composition containing rose extract and preparation method thereof - Google Patents
Hair restoration care composition containing rose extract and preparation method thereof Download PDFInfo
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- CN116270366B CN116270366B CN202310529375.6A CN202310529375A CN116270366B CN 116270366 B CN116270366 B CN 116270366B CN 202310529375 A CN202310529375 A CN 202310529375A CN 116270366 B CN116270366 B CN 116270366B
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- 239000000284 extract Substances 0.000 title claims abstract description 128
- 210000004209 hair Anatomy 0.000 title claims abstract description 110
- 241000220317 Rosa Species 0.000 title claims abstract description 55
- 238000002360 preparation method Methods 0.000 title claims abstract description 41
- 239000000203 mixture Substances 0.000 title claims abstract description 39
- 238000000605 extraction Methods 0.000 title claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 53
- 240000001548 Camellia japonica Species 0.000 claims abstract description 40
- 235000018597 common camellia Nutrition 0.000 claims abstract description 40
- 241001289529 Fallopia multiflora Species 0.000 claims abstract description 26
- 229940051841 polyoxyethylene ether Drugs 0.000 claims abstract description 21
- 229920000056 polyoxyethylene ether Polymers 0.000 claims abstract description 21
- -1 vinyl dimethyl siloxane Chemical class 0.000 claims abstract description 20
- 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 claims abstract description 19
- 239000004354 Hydroxyethyl cellulose Substances 0.000 claims abstract description 18
- 229920000663 Hydroxyethyl cellulose Polymers 0.000 claims abstract description 18
- 235000019447 hydroxyethyl cellulose Nutrition 0.000 claims abstract description 18
- 239000003999 initiator Substances 0.000 claims abstract description 17
- 239000003755 preservative agent Substances 0.000 claims abstract description 16
- 230000002335 preservative effect Effects 0.000 claims abstract description 16
- 239000002562 thickening agent Substances 0.000 claims abstract description 16
- 229920002554 vinyl polymer Polymers 0.000 claims abstract description 16
- 239000002738 chelating agent Substances 0.000 claims abstract description 15
- 238000000034 method Methods 0.000 claims abstract description 15
- 239000008213 purified water Substances 0.000 claims abstract description 13
- 238000002137 ultrasound extraction Methods 0.000 claims abstract description 13
- 238000002156 mixing Methods 0.000 claims description 43
- 238000010438 heat treatment Methods 0.000 claims description 24
- ROOXNKNUYICQNP-UHFFFAOYSA-N ammonium persulfate Chemical group [NH4+].[NH4+].[O-]S(=O)(=O)OOS([O-])(=O)=O ROOXNKNUYICQNP-UHFFFAOYSA-N 0.000 claims description 20
- BXWNKGSJHAJOGX-UHFFFAOYSA-N hexadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCO BXWNKGSJHAJOGX-UHFFFAOYSA-N 0.000 claims description 20
- 239000012153 distilled water Substances 0.000 claims description 19
- 241000628997 Flos Species 0.000 claims description 18
- 238000010298 pulverizing process Methods 0.000 claims description 18
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 17
- 239000008367 deionised water Substances 0.000 claims description 14
- 229910021641 deionized water Inorganic materials 0.000 claims description 14
- 238000003756 stirring Methods 0.000 claims description 12
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims description 10
- 229910001870 ammonium persulfate Inorganic materials 0.000 claims description 10
- 229960000541 cetyl alcohol Drugs 0.000 claims description 10
- 229960005323 phenoxyethanol Drugs 0.000 claims description 10
- 239000003795 chemical substances by application Substances 0.000 claims description 9
- 238000005406 washing Methods 0.000 claims description 8
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonium chloride Substances [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 claims description 7
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical group COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 claims description 7
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 7
- 235000019270 ammonium chloride Nutrition 0.000 claims description 7
- 238000006243 chemical reaction Methods 0.000 claims description 7
- 238000001816 cooling Methods 0.000 claims description 6
- 238000007599 discharging Methods 0.000 claims description 6
- 238000000265 homogenisation Methods 0.000 claims description 6
- 239000012299 nitrogen atmosphere Substances 0.000 claims description 6
- 230000001376 precipitating effect Effects 0.000 claims description 6
- 230000008961 swelling Effects 0.000 claims description 6
- 230000003750 conditioning effect Effects 0.000 claims description 5
- CHHHXKFHOYLYRE-UHFFFAOYSA-M 2,4-Hexadienoic acid, potassium salt (1:1), (2E,4E)- Chemical compound [K+].CC=CC=CC([O-])=O CHHHXKFHOYLYRE-UHFFFAOYSA-M 0.000 claims description 2
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 2
- 239000003109 Disodium ethylene diamine tetraacetate Substances 0.000 claims description 2
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 claims description 2
- 229920002125 Sokalan® Polymers 0.000 claims description 2
- 241001122767 Theaceae Species 0.000 claims description 2
- 229960001631 carbomer Drugs 0.000 claims description 2
- 235000019301 disodium ethylene diamine tetraacetate Nutrition 0.000 claims description 2
- RGUVUPQQFXCJFC-UHFFFAOYSA-N n-hydroxyoctanamide Chemical compound CCCCCCCC(=O)NO RGUVUPQQFXCJFC-UHFFFAOYSA-N 0.000 claims description 2
- 239000004302 potassium sorbate Substances 0.000 claims description 2
- 235000010241 potassium sorbate Nutrition 0.000 claims description 2
- 229940069338 potassium sorbate Drugs 0.000 claims description 2
- 230000035484 reaction time Effects 0.000 claims description 2
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 claims description 2
- 235000010234 sodium benzoate Nutrition 0.000 claims description 2
- 239000004299 sodium benzoate Substances 0.000 claims description 2
- 229960003885 sodium benzoate Drugs 0.000 claims description 2
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 2
- 229960003010 sodium sulfate Drugs 0.000 claims description 2
- 235000011152 sodium sulphate Nutrition 0.000 claims description 2
- GQOKIYDTHHZSCJ-UHFFFAOYSA-M dimethyl-bis(prop-2-enyl)azanium;chloride Chemical compound [Cl-].C=CC[N+](C)(C)CC=C GQOKIYDTHHZSCJ-UHFFFAOYSA-M 0.000 abstract description 10
- 238000000874 microwave-assisted extraction Methods 0.000 abstract description 8
- 239000000126 substance Substances 0.000 abstract description 6
- 238000004821 distillation Methods 0.000 abstract description 4
- 230000009471 action Effects 0.000 abstract description 3
- 230000000638 stimulation Effects 0.000 abstract 1
- 230000000052 comparative effect Effects 0.000 description 18
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 15
- 238000012360 testing method Methods 0.000 description 14
- 230000000694 effects Effects 0.000 description 11
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 10
- 239000006228 supernatant Substances 0.000 description 10
- 238000010025 steaming Methods 0.000 description 9
- LXAHHHIGZXPRKQ-UHFFFAOYSA-N 5-fluoro-2-methylpyridine Chemical compound CC1=CC=C(F)C=N1 LXAHHHIGZXPRKQ-UHFFFAOYSA-N 0.000 description 8
- 239000000047 product Substances 0.000 description 6
- 230000008439 repair process Effects 0.000 description 6
- 238000000944 Soxhlet extraction Methods 0.000 description 5
- 231100000344 non-irritating Toxicity 0.000 description 4
- 235000016709 nutrition Nutrition 0.000 description 4
- 210000004761 scalp Anatomy 0.000 description 4
- 241000196324 Embryophyta Species 0.000 description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 230000003779 hair growth Effects 0.000 description 3
- 230000000474 nursing effect Effects 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 239000002453 shampoo Substances 0.000 description 3
- 239000000341 volatile oil Substances 0.000 description 3
- 241000894006 Bacteria Species 0.000 description 2
- XUMBMVFBXHLACL-UHFFFAOYSA-N Melanin Chemical compound O=C1C(=O)C(C2=CNC3=C(C(C(=O)C4=C32)=O)C)=C2C4=CNC2=C1C XUMBMVFBXHLACL-UHFFFAOYSA-N 0.000 description 2
- 239000008280 blood Substances 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 125000002091 cationic group Chemical group 0.000 description 2
- LQGUBLBATBMXHT-UHFFFAOYSA-N chrysophanol Chemical compound C1=CC=C2C(=O)C3=CC(C)=CC(O)=C3C(=O)C2=C1O LQGUBLBATBMXHT-UHFFFAOYSA-N 0.000 description 2
- 230000006378 damage Effects 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 230000001804 emulsifying effect Effects 0.000 description 2
- 239000000686 essence Substances 0.000 description 2
- 125000001033 ether group Chemical group 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 239000006260 foam Substances 0.000 description 2
- 230000009477 glass transition Effects 0.000 description 2
- 210000003128 head Anatomy 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 230000005764 inhibitory process Effects 0.000 description 2
- 230000001050 lubricating effect Effects 0.000 description 2
- 239000002932 luster Substances 0.000 description 2
- 230000003020 moisturizing effect Effects 0.000 description 2
- 239000000178 monomer Substances 0.000 description 2
- 210000005036 nerve Anatomy 0.000 description 2
- 235000015097 nutrients Nutrition 0.000 description 2
- 230000035764 nutrition Effects 0.000 description 2
- 230000035699 permeability Effects 0.000 description 2
- 229920001296 polysiloxane Polymers 0.000 description 2
- 230000001105 regulatory effect Effects 0.000 description 2
- 210000002374 sebum Anatomy 0.000 description 2
- 230000028327 secretion Effects 0.000 description 2
- 210000000582 semen Anatomy 0.000 description 2
- 210000003491 skin Anatomy 0.000 description 2
- 230000000087 stabilizing effect Effects 0.000 description 2
- 239000004094 surface-active agent Substances 0.000 description 2
- 230000003664 tensile strength of the hair Effects 0.000 description 2
- 235000013343 vitamin Nutrition 0.000 description 2
- 239000011782 vitamin Substances 0.000 description 2
- 229940088594 vitamin Drugs 0.000 description 2
- 229930003231 vitamin Natural products 0.000 description 2
- TUSDEZXZIZRFGC-UHFFFAOYSA-N 1-O-galloyl-3,6-(R)-HHDP-beta-D-glucose Natural products OC1C(O2)COC(=O)C3=CC(O)=C(O)C(O)=C3C3=C(O)C(O)=C(O)C=C3C(=O)OC1C(O)C2OC(=O)C1=CC(O)=C(O)C(O)=C1 TUSDEZXZIZRFGC-UHFFFAOYSA-N 0.000 description 1
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 description 1
- 201000004384 Alopecia Diseases 0.000 description 1
- 241001391944 Commicarpus scandens Species 0.000 description 1
- 208000001840 Dandruff Diseases 0.000 description 1
- 239000001263 FEMA 3042 Substances 0.000 description 1
- 206010019049 Hair texture abnormal Diseases 0.000 description 1
- LRBQNJMCXXYXIU-PPKXGCFTSA-N Penta-digallate-beta-D-glucose Natural products OC1=C(O)C(O)=CC(C(=O)OC=2C(=C(O)C=C(C=2)C(=O)OC[C@@H]2[C@H]([C@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)O2)OC(=O)C=2C=C(OC(=O)C=3C=C(O)C(O)=C(O)C=3)C(O)=C(O)C=2)O)=C1 LRBQNJMCXXYXIU-PPKXGCFTSA-N 0.000 description 1
- 240000004980 Rheum officinale Species 0.000 description 1
- 235000008081 Rheum officinale Nutrition 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 235000010208 anthocyanin Nutrition 0.000 description 1
- 229930002877 anthocyanin Natural products 0.000 description 1
- 239000004410 anthocyanin Substances 0.000 description 1
- 150000004636 anthocyanins Chemical class 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000017531 blood circulation Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- NZPQWZZXRKZCDU-UHFFFAOYSA-N chrysophanol Natural products Cc1cc(O)c2C(=O)c3c(O)cccc3Oc2c1 NZPQWZZXRKZCDU-UHFFFAOYSA-N 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
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- 239000006185 dispersion Substances 0.000 description 1
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- 150000002148 esters Chemical class 0.000 description 1
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- 230000005802 health problem Effects 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 238000010409 ironing Methods 0.000 description 1
- 239000000787 lecithin Substances 0.000 description 1
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- 235000010445 lecithin Nutrition 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
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- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 239000001397 quillaja saponaria molina bark Substances 0.000 description 1
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- 229930182490 saponin Natural products 0.000 description 1
- 150000007949 saponins Chemical class 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 235000019605 sweet taste sensations Nutrition 0.000 description 1
- 235000015523 tannic acid Nutrition 0.000 description 1
- LRBQNJMCXXYXIU-NRMVVENXSA-N tannic acid Chemical compound OC1=C(O)C(O)=CC(C(=O)OC=2C(=C(O)C=C(C=2)C(=O)OC[C@@H]2[C@H]([C@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)O2)OC(=O)C=2C=C(OC(=O)C=3C=C(O)C(O)=C(O)C=3)C(O)=C(O)C=2)O)=C1 LRBQNJMCXXYXIU-NRMVVENXSA-N 0.000 description 1
- 229940033123 tannic acid Drugs 0.000 description 1
- 229920002258 tannic acid Polymers 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
- A61K8/894—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone modified by a polyoxyalkylene group, e.g. cetyl dimethicone copolyol
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Botany (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to the technical field of daily chemicals, and particularly discloses a hair restoration care composition containing rose extract and a preparation method thereof. 2 to 3.5 parts of rose extract, 1.2 to 2.8 parts of camellia seed extract, 2.4 to 4 parts of polygonum multiflorum extract, 3 to 8 parts of conditioner, 1 to 2 parts of thickener, 0.05 to 0.3 part of chelating agent, 0.01 to 0.1 part of preservative and the balance of purified water; preparing a rose extract by a distillation extraction method, preparing a camellia seed extract by an ultrasonic extraction method, and preparing a polygonum multiflorum extract by a microwave extraction method, wherein each extract is mild and has no stimulation; the preparation method has the advantages that the hydroxyethyl cellulose, the allyl polyoxyethylene ether, the dimethyl diallyl ammonium chloride and the vinyl dimethyl siloxane are copolymerized under the action of the initiator to prepare the conditioner, the compatibility between the conditioner and other components is good, the conditioner has positive charges, the wet comb property and the dry comb property of hair can be obviously improved, damaged hair is repaired and nursed, and the toughness of the hair is enhanced.
Description
Technical Field
The invention relates to the technical field of daily chemicals, in particular to a hair restoration care composition containing rose extract and a preparation method thereof.
Background
Healthy hair and hair scales are orderly arranged, scalp is not dry, sebum secretion is normal, and the healthy hair and hair scales have normal microbial ecological environment. With the rapid development of modern economy, the life rhythm of people is faster and faster, and life habits such as life pressure and stay up night lead to health problems of different degrees of scalp of most people. With the development of the hair-dressing industry, more and more people dye hair by ironing, the hair-washing and hair-care products are improperly used, and a large amount of chemical substances are used, so that hair is easy to damage, hair is dry, hair quality is fragile and hair is easy to lose, and meanwhile, sebum secretion of hair is abnormal, and a large amount of dandruff is generated.
Chinese patent CN104814890B discloses an agilawood hair care and hair growth essential oil and a preparation method thereof, and the agilawood hair care and hair growth essential oil is prepared by extracting various plant essential oils, so that multiple nutrients required by hair growth are provided, hair follicles are rapidly activated, and the purposes of hair care and hair care are achieved.
Chinese patent application CN105163713A discloses a hair care shampoo, which relates to a cleaning cosmetic composition, takes a surfactant as a main body and is matched with other auxiliary components to effectively clean hair, but the shampoo has no ideal use effect and cannot effectively play a role in repairing and nursing for the hair injury and the group needing nursing.
Chinese patent application CN105232365A discloses a hair care film and a preparation method thereof, wherein the hair care film comprises a thickening agent, an emulsifying agent, a hair conditioning agent, a preservative, essence, citric acid and a coloring agent CI42090, and the balance deionized water is a solvent.
It is of great value to develop a mild, non-irritating restoration care composition that can restore and care damaged hair and enhance the toughness of hair.
Disclosure of Invention
In order to solve the technical problems, the invention provides a hair restoration care composition containing rose extract and a preparation method thereof, and provides a mild and non-irritating hair restoration care composition capable of restoring and caring damaged hair and enhancing hair toughness.
In order to achieve the above purpose, the invention discloses a hair restoration care composition containing rose extract, which comprises the following components in parts by weight, based on 100 parts by weight:
2-3.5 parts of rose extract, 1.2-2.8 parts of camellia seed extract, 2.4-4 parts of polygonum multiflorum extract, 3-8 parts of conditioner, 1-2 parts of thickener, 0.05-0.3 part of chelating agent, 0.01-0.1 part of preservative and the balance of purified water;
the preparation method of the rose extract comprises the following steps:
pulverizing flos Rosae Rugosae, mixing with distilled water, heating, distilling, collecting distillate, and absorbing excessive water with anhydrous sodium sulfate to obtain flos Rosae Rugosae extract;
the preparation method of the camellia seed extract comprises the following steps:
pulverizing semen Camelliae sinensis, mixing with anhydrous ethanol, ultrasonic extracting, centrifuging at 3500-4500rpm for 6-8min, collecting supernatant, and rotary steaming to obtain semen Camelliae sinensis extract;
the preparation method of the polygonum multiflorum extract comprises the following steps:
pulverizing Polygoni Multiflori radix, mixing with distilled water, microwave extracting, centrifuging at 3500-4500rpm for 6-8min, collecting supernatant, and rotary steaming to obtain Polygoni Multiflori radix extract;
the preparation method of the conditioner comprises the following steps:
adding hydroxyethyl cellulose into deionized water, heating to 70-80 ℃, swelling for 20-25min, adding an initiator, allyl polyoxyethylene ether, dimethyl diallyl ammonium chloride and vinyl dimethyl siloxane into the deionized water in a nitrogen atmosphere, uniformly mixing, reacting, precipitating with acetone after the reaction is finished, washing with absolute ethyl alcohol, and performing Soxhlet extraction with methanol to obtain the conditioner.
Preferably, in the preparation process of the rose extract, the mass ratio of the rose to distilled water is 100:280-350, the distillation extraction temperature is 100-105 ℃, and the distillation extraction time is 1-2h.
Preferably, in the preparation process of the camellia seed extract, the mass ratio of the camellia seed to the absolute ethyl alcohol is 100:1450-1550, the ultrasonic extraction temperature is 55-65 ℃, the ultrasonic extraction time is 0.5-1h, and the ultrasonic intensity of ultrasonic extraction is 300W.
Preferably, in the preparation process of the polygonum multiflorum extract, the mass ratio of the polygonum multiflorum to distilled water is 100:520-600, the power of microwave extraction is 300-350W, and the time of microwave extraction is 0.5-1h.
Preferably, in the preparation process of the conditioner, the mass ratio of deionized water to hydroxyethyl cellulose to an initiator to allyl polyoxyethylene ether to dimethyl diallyl ammonium chloride to vinyl dimethyl siloxane is 1800-2500:100:2-5:15-25:8-12:30-50, the reaction temperature is 65-75 ℃, the reaction time is 4-7 hours, and the initiator is ammonium persulfate.
Preferably, the chelating agent comprises one or two of disodium EDTA and octanoyl hydroxamic acid.
Preferably, the thickener comprises one or more of cetyl alcohol, carbomer and sodium sulfate.
Preferably, the preservative comprises one or more of sodium benzoate, phenoxyethanol and potassium sorbate.
Preferably, the preparation method of the hair restoration care composition containing the rose extract comprises the following steps:
s1, adding rose extract, camellia seed extract and polygonum multiflorum extract into purified water, heating to 45-50 ℃, and stirring and mixing uniformly to obtain a component A;
s2, adding a conditioning agent, a thickening agent and a chelating agent into the component A, heating to 75-80 ℃, stirring and mixing uniformly, and cooling to obtain a component B;
s3, homogenizing the component B, adding a preservative after homogenizing, mixing uniformly, and discharging to obtain the hair restoration care composition containing the rose extract.
Preferably, the speed of the homogenization treatment in the step S3 is 3500-5000rpm, the time of the homogenization treatment is 3-5min, and the temperature of the homogenization treatment is 70-75 ℃.
Compared with the prior art, the invention has the beneficial effects that:
the hair restoration care composition containing the rose extract contains extracts of natural plant raw materials, wherein the extracts are respectively prepared by distillation extraction to prepare the rose extract, ultrasonic extraction to prepare the camellia seed extract and microwave extraction to prepare the polygonum multiflorum extract, and the extracts are mild and non-irritating, can provide nutritional ingredients required by hair, and can well restore the hair. The flos Rosae Rugosae extract is rich in various nutrients, vitamins, tannic acid and anthocyanin, 18 amino acids and various microelements required by human body, and has effects of promoting blood circulation and metabolism. Meanwhile, the hair restoration care composition has aromatic smell and sweet taste, and has pleasant fragrance without adding essence. The tea saponin contained in the camellia seed extract is a natural surfactant with excellent performance, can play a role in good dispersion, foaming and wetting when used in a hair restoration care composition, contains active ingredients such as unsaturated fatty acid, vitamin and the like, can effectively repair and nourish hair, prevent hair loss, dryness and bifurcation, and deeply nourish and nourish hair and scalp. The polygonum multiflorum extract is rich in active substances such as lecithin, chrysophanol, rheum officinale ester and the like, has good effects of tonifying qi and nourishing blood, regulating nerves and nourishing hair roots, can nourish the skin of the head, promote the hair to absorb nutrition, and can promote the generation of hair melanin to play a good role in nourishing hair.
The hydroxyethyl cellulose used for preparing the conditioner has mild performance and good adhesiveness, and can form a net-shaped nursing film on the surface of hair, so that the hair is endowed with excellent combing performance and bright and smooth feeling; can repair damaged hair, improve the appearance of the damaged hair, provide excellent moisturizing performance, effectively increase the toughness of hair, endow the hair with good elasticity, ensure that the hair is not easy to break, take hydroxyethyl cellulose as raw material, polymerize with allyl polyoxyethylene ether, cationic monomer dimethyl diallyl ammonium chloride and vinyl dimethyl siloxane under the action of an initiator, the polysiloxane has the special surface properties of high air permeability, low glass transition temperature, physiological inertia, excellent flexibility and the like, and the polyoxyethylene ether group has hydrophilicity, can endow the product with water solubility and surface activity, has good emulsifying, foam stabilizing, soft and lubricating properties and the like, can obtain smooth and soft hand feeling, and endows the hair with the properties of luster, static resistance, bacteria inhibition and the like. The conditioner has good compatibility with other components and has positive charges, so that the wet comb property and the dry comb property of the hair can be obviously improved, the damaged hair can be repaired and nursed, and the toughness of the hair can be enhanced.
Drawings
FIG. 1 is a flow chart of the preparation of a hair restoration care composition containing rose extract according to the present invention;
FIG. 2 is a chart of hair elasticity test for the volunteers of examples 1-4, comparative examples 1-3 and blank test in the present invention.
Detailed Description
The technical solutions of the embodiments of the present invention will be clearly and completely described below in conjunction with the embodiments of the present invention, and it is apparent that the described embodiments are only some embodiments of the present invention, but not all embodiments, and all other embodiments obtained by those skilled in the art without making any inventive effort based on the embodiments of the present invention are within the scope of protection of the present invention.
Example 1
A method for preparing a hair restoration care composition containing rose extract, comprising the steps of:
s1, adding rose extract, camellia seed extract and polygonum multiflorum extract into purified water, heating to 45 ℃, and stirring and mixing uniformly to obtain a component A;
s2, adding a conditioner, a thickener cetyl alcohol and a chelating agent EDTA disodium into the component A, heating to 75 ℃, stirring and mixing uniformly, and cooling to obtain a component B;
s3, homogenizing the component B at 3500rpm for 5min at 70 ℃, adding a preservative phenoxyethanol after homogenizing, mixing uniformly, and discharging to obtain a hair restoration care composition containing rose extract;
wherein the mass portion of the rose extract is 2 portions, the camellia seed extract is 1.2 portions, the polygonum multiflorum extract is 2.4 portions, the conditioner is 3 portions, the thickener cetyl alcohol is 1 portion, the chelating agent EDTA disodium is 0.05 portion, the preservative phenoxyethanol is 0.01 portion, and the purified water is 90.34 portions.
The preparation method of the rose extract comprises the following steps:
pulverizing flos Rosae Rugosae, mixing with distilled water at a mass ratio of flos Rosae Rugosae to distilled water of 100:280, heating, distilling at 100deg.C for 2 hr, collecting distillate, and absorbing excessive water with anhydrous sodium sulfate to obtain flos Rosae Rugosae extract.
The preparation method of the camellia seed extract comprises the following steps:
pulverizing camellia seed, mixing with absolute ethanol uniformly, wherein the mass ratio of camellia seed to absolute ethanol is 100:1450, performing ultrasonic extraction at 55 ℃ for 1h, wherein the ultrasonic intensity is 300W, centrifuging at 3500rpm for 8min after extraction is completed, collecting supernatant, and performing rotary evaporation to obtain camellia seed extract.
The preparation method of the polygonum multiflorum extract comprises the following steps:
pulverizing Polygoni Multiflori radix, mixing with distilled water at a mass ratio of 100:520, performing microwave extraction with power of 300W for 1 hr, centrifuging at 3500rpm for 8min, collecting supernatant, and steaming to obtain Polygoni Multiflori radix extract.
The preparation method of the conditioner comprises the following steps:
adding hydroxyethyl cellulose into deionized water, heating to 70 ℃, swelling for 25min, adding initiator ammonium persulfate, allyl polyoxyethylene ether, dimethyl diallyl ammonium chloride and vinyl dimethyl siloxane in a nitrogen atmosphere, uniformly mixing, wherein the mass ratio of the deionized water to the hydroxyethyl cellulose to the initiator ammonium persulfate to the allyl polyoxyethylene ether to the dimethyl diallyl ammonium chloride to the vinyl dimethyl siloxane is 1800:100:2:15:8:30, reacting for 7h at 65 ℃, precipitating by using acetone after the reaction is finished, washing by using absolute ethyl alcohol, and carrying out Soxhlet extraction by using methanol as an extracting agent to obtain the conditioner.
Example 2
A method for preparing a hair restoration care composition containing rose extract, comprising the steps of:
s1, adding rose extract, camellia seed extract and polygonum multiflorum extract into purified water, heating to 48 ℃, and stirring and mixing uniformly to obtain a component A;
s2, adding a conditioner, a thickener cetyl alcohol and a chelating agent EDTA disodium into the component A, heating to 78 ℃, stirring and mixing uniformly, and cooling to obtain a component B;
s3, homogenizing the component B at 4000rpm for 4min at 72 ℃, adding a preservative phenoxyethanol after homogenizing, and discharging after uniform mixing to obtain a hair restoration care composition containing rose extract;
wherein the mass portion of the rose extract is 2.5 portions, the camellia seed extract is 1.8 portions, the polygonum multiflorum extract is 3 portions, the conditioner is 5 portions, the thickener cetyl alcohol is 1.4 portions, the chelating agent EDTA disodium is 0.1 portion, the preservative phenoxyethanol is 0.03 portion, and the purified water is 86.17 portions.
The preparation method of the rose extract comprises the following steps:
pulverizing flos Rosae Rugosae, mixing with distilled water at a mass ratio of flos Rosae Rugosae to distilled water of 100:305, heating, distilling at 102deg.C for 1.5 hr, collecting distillate, and absorbing excessive water with anhydrous sodium sulfate to obtain flos Rosae Rugosae extract.
The preparation method of the camellia seed extract comprises the following steps:
pulverizing camellia seed, mixing with absolute ethanol uniformly, wherein the mass ratio of camellia seed to absolute ethanol is 100:1480, performing ultrasonic extraction at 60 ℃ for 0.8h, the ultrasonic intensity is 300W, centrifuging at 4000rpm for 7min after extraction is completed, collecting supernatant, and performing rotary steaming to obtain camellia seed extract.
The preparation method of the polygonum multiflorum extract comprises the following steps:
pulverizing Polygoni Multiflori radix, mixing with distilled water at a mass ratio of 100:550, performing microwave extraction with power of 320W for 0.8 hr, centrifuging at 4000rpm for 7min after extraction, collecting supernatant, and rotary steaming to obtain Polygoni Multiflori radix extract.
The preparation method of the conditioner comprises the following steps:
adding hydroxyethyl cellulose into deionized water, heating to 75 ℃, swelling for 24min, adding initiator ammonium persulfate, allyl polyoxyethylene ether, dimethyl diallyl ammonium chloride and vinyl dimethyl siloxane in a nitrogen atmosphere, uniformly mixing, wherein the mass ratio of the deionized water to the hydroxyethyl cellulose to the initiator ammonium persulfate to the allyl polyoxyethylene ether to the dimethyl diallyl ammonium chloride to the vinyl dimethyl siloxane is 2100:100:3:18:9:38, reacting for 5h at 70 ℃, precipitating by using acetone after the reaction is finished, washing by using absolute ethyl alcohol, and carrying out Soxhlet extraction by using methanol as an extracting agent to obtain the conditioner.
Example 3
A method for preparing a hair restoration care composition containing rose extract, comprising the steps of:
s1, adding rose extract, camellia seed extract and polygonum multiflorum extract into purified water, heating to 48 ℃, and stirring and mixing uniformly to obtain a component A;
s2, adding a conditioner, a thickener cetyl alcohol and a chelating agent EDTA disodium into the component A, heating to 78 ℃, stirring and mixing uniformly, and cooling to obtain a component B;
s3, homogenizing the component B at 4500rpm for 4min at 72 ℃, adding a preservative phenoxyethanol after homogenizing, mixing uniformly, and discharging to obtain a hair restoration care composition containing rose extract;
wherein the mass portion of the rose extract is 3 portions, the camellia seed extract is 2.4 portions, the polygonum multiflorum extract is 3.5 portions, the conditioner is 7 portions, the thickener cetyl alcohol is 1.8 portions, the chelating agent EDTA disodium is 0.2 portion, the preservative phenoxyethanol is 0.06 portion, and the purified water is 82.04 portions.
The preparation method of the rose extract comprises the following steps:
pulverizing flos Rosae Rugosae, mixing with distilled water at a mass ratio of flos Rosae Rugosae to distilled water of 100:335, heating, distilling at 102deg.C for 1.5 hr, collecting distillate, and absorbing excessive water with anhydrous sodium sulfate to obtain flos Rosae Rugosae extract.
The preparation method of the camellia seed extract comprises the following steps:
pulverizing camellia seed, mixing with absolute ethanol uniformly, wherein the mass ratio of camellia seed to absolute ethanol is 100:1520, performing ultrasonic extraction at 60 ℃ for 0.8h, performing ultrasonic intensity of 300W, centrifuging at 4200rpm for 7min after extraction, collecting supernatant, and performing rotary steaming to obtain camellia seed extract.
The preparation method of the polygonum multiflorum extract comprises the following steps:
pulverizing Polygoni Multiflori radix, mixing with distilled water at a mass ratio of 100:580, performing microwave extraction with power of 340W for 0.8 hr, centrifuging at 4000rpm for 7min after extraction, collecting supernatant, and rotary steaming to obtain Polygoni Multiflori radix extract.
The preparation method of the conditioner comprises the following steps:
adding hydroxyethyl cellulose into deionized water, heating to 75 ℃, swelling for 24min, adding initiator ammonium persulfate, allyl polyoxyethylene ether, dimethyl diallyl ammonium chloride and vinyl dimethyl siloxane in a nitrogen atmosphere, uniformly mixing, wherein the mass ratio of deionized water to hydroxyethyl cellulose to initiator ammonium persulfate to allyl polyoxyethylene ether to dimethyl diallyl ammonium chloride to vinyl dimethyl siloxane is 2400:100:4:22:11:45, reacting for 6h at 70 ℃, precipitating by using acetone after the reaction is finished, washing by using absolute ethyl alcohol, and performing Soxhlet extraction by using methanol as an extracting agent to obtain the conditioner.
Example 4
A method for preparing a hair restoration care composition containing rose extract, comprising the steps of:
s1, adding rose extract, camellia seed extract and polygonum multiflorum extract into purified water, heating to 50 ℃, and stirring and mixing uniformly to obtain a component A;
s2, adding a conditioner, a thickener cetyl alcohol and a chelating agent EDTA disodium into the component A, heating to 80 ℃, stirring and mixing uniformly, and cooling to obtain a component B;
s3, homogenizing the component B at a speed of 5000rpm for 3min at a temperature of 75 ℃, adding a preservative phenoxyethanol after homogenizing, and discharging after uniform mixing to obtain a hair restoration care composition containing rose extract;
wherein the mass portion of the rose extract is 3.5 portions, the camellia seed extract is 2.8 portions, the polygonum multiflorum extract is 4 portions, the conditioner is 8 portions, the thickener cetyl alcohol is 2 portions, the chelating agent EDTA disodium is 0.3 portion, the preservative phenoxyethanol is 0.1 portion, and the purified water is 79.3 portions.
The preparation method of the rose extract comprises the following steps:
pulverizing flos Rosae Rugosae, mixing with distilled water at a mass ratio of flos Rosae Rugosae to distilled water of 100:350, heating, distilling at 105deg.C for 1 hr, collecting distillate, and absorbing excessive water with anhydrous sodium sulfate to obtain flos Rosae Rugosae extract.
The preparation method of the camellia seed extract comprises the following steps:
pulverizing camellia seed, mixing with absolute ethanol uniformly, wherein the mass ratio of camellia seed to absolute ethanol is 100:1550, performing ultrasonic extraction at 65 ℃ for 0.5h, the ultrasonic intensity is 300W, centrifuging at 4500rpm for 6min after extraction, collecting supernatant, and performing rotary steaming to obtain camellia seed extract.
The preparation method of the polygonum multiflorum extract comprises the following steps:
pulverizing Polygoni Multiflori radix, mixing with distilled water at a mass ratio of 100:600, performing microwave extraction with power of 350W for 0.5 hr, centrifuging at 4500rpm for 6min, collecting supernatant, and steaming to obtain Polygoni Multiflori radix extract.
The preparation method of the conditioner comprises the following steps:
adding hydroxyethyl cellulose into deionized water, heating to 80 ℃, swelling for 20min, adding initiator ammonium persulfate, allyl polyoxyethylene ether, dimethyl diallyl ammonium chloride and vinyl dimethyl siloxane in a nitrogen atmosphere, uniformly mixing, wherein the mass ratio of the deionized water to the hydroxyethyl cellulose to the initiator ammonium persulfate to the allyl polyoxyethylene ether to the dimethyl diallyl ammonium chloride to the vinyl dimethyl siloxane is 2500:100:5:25:12:50, reacting for 4h at 75 ℃, precipitating by using acetone after the reaction is finished, washing by using absolute ethyl alcohol, and performing Soxhlet extraction by using methanol as an extracting agent to obtain the conditioner.
Comparative example 1
The difference between this comparative example and example 3 is that no conditioning agent was added.
Comparative example 2
The difference between this comparative example and example 3 is that no allyl polyoxyethylene ether was added to the conditioner during the preparation.
Comparative example 3
The difference between this comparative example and example 3 is that no vinyldimethylsiloxane is added to the conditioning agent during the preparation process.
Hydroxyethyl cellulose in the present invention was purchased from the dow chemical (china) limited.
The allyl polyoxyethylene ether is purchased from Nantong Xitai chemical industry Co., ltd, and the model is APEG2400.
In the invention, the dimethyl diallyl ammonium chloride is purchased from Shandong Luyue chemical industry Co., ltd, and is a 60wt% dimethyl diallyl ammonium chloride aqueous solution.
The hair restoration care compositions containing rose extract in examples 1 to 4 and comparative examples 1 to 3 were subjected to performance tests, specifically as follows:
(1) 160 volunteers aged 25-35 years were selected to participate in the experiment, hair of the volunteers generally appeared to be dry and lose elasticity, and other diseases which might not affect the result of the experiment were randomly divided into 8 groups of 20 persons each, after washing hair with the same commercial shampoo, eight groups of volunteers respectively used the hair restoration care compositions prepared in examples 1-4 and comparative examples 1-3 and did not use any hair restoration care products, none of the hair restoration care products was blank test, the hair restoration care compositions prepared in examples 1-4 and comparative examples 1-3 were used once every two days, the use period was two months, no other similar products were used during the test, and the hair of the volunteers had no significant difference in elasticity and frictional properties, and were comparable. Recording the curative effect after use, wherein the curative effect standard is divided into: 1) The effect is shown: the comb property and the tensile strength of the hair are obviously improved; 2) The method is effective: the comb property and the tensile strength of the hair are slightly improved; 3) Invalidation: no change is caused before and after use; the specific test results are shown in table 1:
TABLE 1
From the test results of Table 1, it can be seen that the hair combing properties and tensile strength of the volunteers corresponding to examples 1 to 4 were significantly improved by comparison with those of the blank test after using the hair restoration care composition containing the rose extract. The rose extract, the camellia seed extract and the polygonum multiflorum extract extracted from natural plant raw materials are mild and non-irritating, can provide nutritional ingredients required by hair, and can well repair the hair. The hydroxyethyl cellulose, allyl polyoxyethylene ether, cationic monomer dimethyl diallyl ammonium chloride and vinyl dimethyl siloxane in the conditioner are polymerized under the action of an initiator, and the obtained polysiloxane has special surface properties such as high air permeability, low glass transition temperature, physiological inertia, excellent flexibility and the like, and the polyoxyethylene ether group has hydrophilicity, so that the product can be endowed with water solubility and surface activity, and has good emulsifying, foam stabilizing, softening, lubricating and other properties, and can obtain smooth and soft hand feeling, and endow hair with luster, antistatic property, bacteria inhibition and other properties. No conditioner was added in comparative example 1, no allyl polyoxyethylene ether was added in comparative example 2, no vinyl dimethylsiloxane was added in comparative example 3, and the test performance was significantly reduced.
(2) The elasticity of the hair of 160 volunteers was tested using a yarn elastometer model Y391, available from second textile Instrument factory, inc. Measurement conditions: traction force was 199g, pre-tension was 2.5g, hair length was 50mm, and the test results were averaged. The specific test results are shown in table 2.
TABLE 2
From the test results in Table 2, it can be seen that the hair elasticity of the volunteers of examples 1 to 4 after using the hair restoration care composition containing the rose extract was significantly higher than that of the volunteers of comparative examples 1 to 3 and the blank test, and that the hair elasticity was higher than 82.67% for each of the examples. The rose extract can quickly and deeply nourish hair, reproduce healthy and tough hair, the camellia seed extract can effectively nourish and repair hair and scalp deeply, the polygonum multiflorum extract has the effects of tonifying qi and nourishing blood, regulating nerves and nourishing hair roots, can nourish head skin, promote hair to absorb nutrition, has good hair nourishing effect, hydroxyethyl cellulose can repair damaged hair, improve the appearance of damaged hair, provide excellent moisturizing performance, effectively increase the toughness of hair, endow the hair with good elasticity, enable the hair not to be broken easily, and the hair repair care composition containing the rose extract can effectively improve the elasticity of hair. No conditioner is added in comparative example 1, no allyl polyoxyethylene ether is added in comparative example 2, no vinyl dimethyl siloxane is added in comparative example 3, the test results are reduced compared with those of examples 1-4, which shows that each component in the conditioner has important effect in hair restoration care compositions, and the elasticity of the hair is obviously improved compared with that of blank test hair in comparative examples 1-3.
Although embodiments of the present invention have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made hereto without departing from the spirit and scope of the invention as defined by the appended claims.
Claims (7)
1. A method for preparing a hair restoration care composition containing rose extract, which is characterized in that: the method comprises the following steps:
s1, adding rose extract, camellia seed extract and polygonum multiflorum extract into purified water, heating to 45-50 ℃, and stirring and mixing uniformly to obtain a component A;
s2, adding a conditioning agent, a thickening agent and a chelating agent into the component A, heating to 75-80 ℃, stirring and mixing uniformly, and cooling to obtain a component B;
s3, homogenizing the component B, adding a preservative after homogenizing, uniformly mixing, and discharging to obtain a hair restoration care composition containing rose extract;
wherein, the total amount is calculated by 100 parts, and the mass parts of each component are as follows:
2-3.5 parts of rose extract, 1.2-2.8 parts of camellia seed extract, 2.4-4 parts of polygonum multiflorum extract, 3-8 parts of conditioner, 1-2 parts of thickener, 0.05-0.3 part of chelating agent, 0.01-0.1 part of preservative and the balance of purified water;
the preparation method of the conditioner in the step S2 comprises the following steps:
mixing hydroxyethyl cellulose and deionized water, heating to 70-80 ℃, swelling for 20-25min, adding an initiator, allyl polyoxyethylene ether, dimethyl diallyl ammonium chloride and vinyl dimethyl siloxane in a nitrogen atmosphere, uniformly mixing, reacting, precipitating, washing and Soxhlet extracting to obtain a conditioner;
in the preparation process of the conditioner in S2, the mass ratio of deionized water, hydroxyethyl cellulose, an initiator, allyl polyoxyethylene ether, dimethyl diallyl ammonium chloride and vinyl dimethyl siloxane is 1800-2500:100:2-5:15-25:8-12:30-50, the reaction temperature is 65-75 ℃, the reaction time is 4-7 hours, and the initiator is ammonium persulfate;
the chelating agent in the S2 comprises one or two of disodium EDTA and octanoyl hydroxamic acid;
the thickening agent in the S2 comprises one or more of cetyl alcohol, carbomer and sodium sulfate.
2. A method of preparing a hair restoration care composition containing rose extract as set forth in claim 1, wherein: the preparation method of the rose extract in the step S1 comprises the following steps: pulverizing flos Rosae Rugosae, mixing with distilled water, heating, and distilling at 100:280-350 (mass ratio of flos Rosae Rugosae to distilled water) and 100-105deg.C for 1-2 hr to obtain flos Rosae Rugosae extract.
3. A method of preparing a hair restoration care composition containing rose extract as set forth in claim 1, wherein: the preparation method of the oil tea seed extract in the step S1 comprises the following steps: pulverizing camellia seed, mixing with absolute ethanol uniformly, performing ultrasonic extraction, wherein the mass ratio of the camellia seed to the absolute ethanol is 100:1450-1550, the ultrasonic extraction temperature is 55-65 ℃, the ultrasonic extraction time is 0.5-1h, the ultrasonic intensity of ultrasonic extraction is 300W, and obtaining the camellia seed extract after the extraction is completed.
4. A method of preparing a hair restoration care composition containing rose extract as set forth in claim 1, wherein: the preparation method of the polygonum multiflorum extract in the S1 comprises the following steps: pulverizing Polygoni Multiflori radix, mixing with distilled water, and microwave extracting at a mass ratio of 100:520-600 with power of 300-350W for 0.5-1 hr to obtain Polygoni Multiflori radix extract.
5. A method of preparing a hair restoration care composition containing rose extract as set forth in claim 1, wherein: the preservative in the step S3 comprises one or more of sodium benzoate, phenoxyethanol and potassium sorbate.
6. A method of preparing a hair restoration care composition containing rose extract as set forth in claim 1, wherein: the speed of the homogenization treatment in the step S3 is 3500-5000rpm, the time of the homogenization treatment is 3-5min, and the temperature of the homogenization treatment is 70-75 ℃.
7. A hair restoration care composition containing rose extract prepared by the method for preparing a hair restoration care composition containing rose extract according to any one of claims 1 to 6.
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