CN115997910A - Preparation method of beef marrow oil refined powder - Google Patents
Preparation method of beef marrow oil refined powder Download PDFInfo
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- CN115997910A CN115997910A CN202211732413.XA CN202211732413A CN115997910A CN 115997910 A CN115997910 A CN 115997910A CN 202211732413 A CN202211732413 A CN 202211732413A CN 115997910 A CN115997910 A CN 115997910A
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- 235000015278 beef Nutrition 0.000 title claims abstract description 110
- 239000000843 powder Substances 0.000 title claims abstract description 103
- 238000002360 preparation method Methods 0.000 title claims abstract description 27
- 239000003921 oil Substances 0.000 claims abstract description 150
- 238000000605 extraction Methods 0.000 claims abstract description 85
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 74
- 230000001804 emulsifying effect Effects 0.000 claims abstract description 62
- 210000001185 bone marrow Anatomy 0.000 claims abstract description 59
- 241000283690 Bos taurus Species 0.000 claims abstract description 55
- 235000014347 soups Nutrition 0.000 claims abstract description 54
- 238000001694 spray drying Methods 0.000 claims abstract description 32
- 239000007788 liquid Substances 0.000 claims abstract description 28
- 238000010411 cooking Methods 0.000 claims abstract description 26
- 239000000463 material Substances 0.000 claims abstract description 25
- 238000007670 refining Methods 0.000 claims abstract description 25
- 238000004140 cleaning Methods 0.000 claims abstract description 23
- 239000007921 spray Substances 0.000 claims abstract description 22
- 210000002082 fibula Anatomy 0.000 claims abstract description 19
- GUOCOOQWZHQBJI-UHFFFAOYSA-N 4-oct-7-enoxy-4-oxobutanoic acid Chemical compound OC(=O)CCC(=O)OCCCCCCC=C GUOCOOQWZHQBJI-UHFFFAOYSA-N 0.000 claims abstract description 18
- 229920002774 Maltodextrin Polymers 0.000 claims abstract description 18
- 239000005913 Maltodextrin Substances 0.000 claims abstract description 18
- 239000010779 crude oil Substances 0.000 claims abstract description 18
- 229940035034 maltodextrin Drugs 0.000 claims abstract description 18
- 229940080313 sodium starch Drugs 0.000 claims abstract description 18
- 238000002156 mixing Methods 0.000 claims abstract description 16
- 238000001914 filtration Methods 0.000 claims abstract description 15
- 238000005191 phase separation Methods 0.000 claims abstract description 13
- 239000000839 emulsion Substances 0.000 claims abstract description 7
- 210000000988 bone and bone Anatomy 0.000 claims description 66
- 238000007599 discharging Methods 0.000 claims description 22
- 238000000034 method Methods 0.000 claims description 21
- 238000010008 shearing Methods 0.000 claims description 18
- 239000012141 concentrate Substances 0.000 claims description 13
- 210000001930 leg bone Anatomy 0.000 claims 1
- 239000007787 solid Substances 0.000 abstract description 12
- 239000002994 raw material Substances 0.000 description 41
- 235000013305 food Nutrition 0.000 description 36
- 239000004519 grease Substances 0.000 description 26
- 238000005086 pumping Methods 0.000 description 20
- 238000000926 separation method Methods 0.000 description 20
- 238000010025 steaming Methods 0.000 description 20
- 239000002699 waste material Substances 0.000 description 20
- 239000000796 flavoring agent Substances 0.000 description 12
- 235000019634 flavors Nutrition 0.000 description 12
- 235000016709 nutrition Nutrition 0.000 description 12
- 230000035764 nutrition Effects 0.000 description 12
- 230000000694 effects Effects 0.000 description 11
- 235000011194 food seasoning agent Nutrition 0.000 description 11
- 239000004615 ingredient Substances 0.000 description 11
- 239000002245 particle Substances 0.000 description 11
- 239000000126 substance Substances 0.000 description 11
- 238000004321 preservation Methods 0.000 description 10
- 239000000203 mixture Substances 0.000 description 7
- 230000009286 beneficial effect Effects 0.000 description 1
- 244000309466 calf Species 0.000 description 1
- 210000001699 lower leg Anatomy 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000003760 tallow Substances 0.000 description 1
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Abstract
The invention discloses a preparation method of beef marrow oil refined powder, which comprises the following steps: s10, selecting pollution-free calf bones, cleaning, and then sending the calf bones into a crusher for crushing treatment; s20, throwing the crushed calf bones into a cooking pot for bone marrow extraction to obtain feed liquid to be treated; s30, standing the feed liquid to be treated obtained in the step S20 in a standing tank to naturally separate oil from soup; s40, carrying out three-phase separation on the materials prepared in the step S30 through a centrifugal machine to obtain crude oil; s50, refining the crude oil obtained in the step S40 after filtering to obtain bovine bone marrow oil; s60, adding sodium starch octenyl succinate, maltodextrin and water into the beef marrow oil obtained in the step S50, and emulsifying and blending in an emulsifying tank to obtain an emulsion; and S70, feeding the emulsion obtained in the step S60 into a spray dryer for spray drying to obtain the beef marrow fat refined powder. Since it is in a solid powder state, it is less affected by temperature, and storage stability is increased.
Description
Technical Field
The invention relates to the technical field of food processing, in particular to a preparation method of beef marrow oil refined powder.
Background
The oil can be used as an important raw material of food, and can be used as nutrition source to improve taste and flavor of food. The general grease is obviously affected by temperature, solidifies when cold, softens into liquid when hot, is easy to deteriorate and has poor storage stability. The existing beef tallow eating method cannot meet the increasing demands of people, and along with the increasing of the daily living standard of people, the demands for grease are increasing, and a grease product with good storage stability and less influence of temperature is needed.
Disclosure of Invention
In view of the above, the invention provides a preparation method of bovine bone marrow oil concentrate, which is used for solving the problems that in the prior art, oil is obviously affected by temperature and has poor storage stability.
In order to achieve one or a part or all of the above objects or other objects, the present invention provides a method for preparing bovine bone marrow oil fine powder, comprising the steps of:
s10, selecting pollution-free calf bones, cleaning, and then sending the calf bones into a crusher for crushing treatment;
s20, throwing the crushed calf bones into a cooking pot for bone marrow extraction to obtain feed liquid to be treated;
s30, standing the feed liquid to be treated obtained in the step S20 in a standing tank to naturally separate oil from soup;
s40, carrying out three-phase separation on the materials prepared in the step S30 through a centrifugal machine to obtain crude oil;
s50, refining the crude oil obtained in the step S40 after filtering to obtain bovine bone marrow oil;
s60, adding sodium starch octenyl succinate, maltodextrin and water into the beef marrow oil obtained in the step S50, and emulsifying and blending in an emulsifying tank to obtain an emulsion;
and S70, feeding the emulsion obtained in the step S60 into a spray dryer for spray drying to obtain the beef marrow fat refined powder.
Further, the step of putting the crushed calf shank into a cooking pot for bone marrow extraction specifically comprises the following steps:
s201, adding the crushed corbel bones into a cooking pot, adding water with the weight ratio of 1-2 times of the corbel bones, preserving heat for 1-5 hours at 100-136 ℃ and discharging;
s202, adding water with the weight ratio of 0.5-1 times of the weight of the bracket bone into the material obtained in the step S201, and preserving heat for 1-2 h at 100-136 ℃.
Further, in the step S30, the time for which the feed liquid to be treated is kept stand in the standing tank is 30min to 2h.
Further, the rotational speed of the centrifugal machine is controlled to be 5000-7200 revolutions/h, and the feeding flow of the centrifugal machine is controlled to be 2-10T/h.
Further, the step S50 specifically includes:
filtering the crude oil obtained in the step S40 by a plate-frame filter and refining at the temperature of 101-120 ℃ to obtain the bovine bone marrow oil.
Further, the step S60 specifically includes:
and (3) emulsifying the beef marrow oil obtained in the step (S50) in an emulsifying tank by adding water, shearing and emulsifying for 30 min-2 h after the beef marrow oil contains 50% -70% of the beef marrow oil, 18% -35% of sodium starch octenyl succinate and 10% -20% of maltodextrin.
Further, the content of the bovine bone marrow oil is 60%, the content of the sodium starch octenyl succinate is 25%, and the content of maltodextrin is 15%.
Further, the temperature is controlled at 45-70 ℃ in the step of shearing and emulsifying for 30 min-2 h.
Further, the shearing and emulsifying time is 1h, and the shearing and emulsifying temperature is controlled at 60 ℃.
Further, the working conditions of the spray dryer are: the inlet temperature of the spray dryer is 130-215 ℃, and the outlet temperature of the spray dryer is 80-108 ℃.
The implementation of the embodiment of the invention has the following beneficial effects:
after the preparation method of the beef marrow fat refined powder is adopted, the obtained beef marrow fat refined powder maintains the nutrition characteristics of grease, improves the flavor and the dispersibility, is easier to mix with other foods, and has better mouthfeel; because the powder is in a solid powder state, the influence of temperature is small, and the storage stability is improved; because the conventional grease is difficult to mix with water, but the beef marrow fat refined powder wraps the grease particles by utilizing hydrophilic substances, is easy to mix with water in food, has good emulsifying and dispersing effects, improves the water solubility, expands the application range of the beef marrow fat refined powder, and is particularly suitable for seasoning bags, chaffy dish and spicy soup base ingredients of instant food.
Detailed Description
Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs; the terminology used in the description of the applications herein is for the purpose of describing particular embodiments only and is not intended to be limiting of the invention.
Reference herein to "an embodiment" means that a particular feature, structure, or characteristic described in connection with the embodiment may be included in at least one embodiment of the invention. The appearances of such phrases in various places in the specification are not necessarily all referring to the same embodiment, nor are separate or alternative embodiments mutually exclusive of other embodiments. Those of skill in the art will explicitly and implicitly appreciate that the embodiments described herein may be combined with other embodiments.
In order to enable those skilled in the art to better understand the present invention, the following description will clearly and completely describe the technical solutions in the embodiments of the present invention.
Example 1
The preparation method of the beef marrow oil refined powder provided by the invention comprises the following process steps:
(1) Selecting, cleaning and crushing raw materials
Selecting pollution-free calf bones as raw materials, cleaning and then sending into a crusher for crushing treatment;
(2) Extracting by steaming
Putting the beef bones subjected to the crushing treatment in the step (1) into a cooking pot for extraction: primary extraction: adding bone into a steaming pot, adding water with the weight ratio of 1 time to the bone, preserving heat at 100 ℃ for 1 hour, and discharging;
and (3) secondary extraction: after the primary material is beaten, adding water with the weight ratio of 0.5 times to the bone, preserving heat for 1h at 100 ℃ and discharging;
in the step, more bone marrow in the bovine bone is extracted in a secondary extraction mode, so that the residue and waste of raw materials are reduced; wherein, either the primary extraction or the secondary extraction can be carried out under normal pressure or under proper pressure, for example, under the condition of 0.1MPA to 0.12MPA for heat preservation;
(3) Standing separation
Standing the feed liquid obtained in the step (2) in a standing tank for 30min; naturally separating oil from soup;
(4) Disc separation
Carrying out three-phase separation on the materials prepared in the step (3) through a centrifugal machine, controlling the rotating speed of the centrifugal machine to 5000 revolutions per hour, controlling the feeding flow of the centrifugal machine to 5T/h, and pumping the separated soup into a soup temporary storage tank and pumping the oil into a crude oil tank, wherein the oil content of the separated soup is less than 2 per mill; the centrifuge used in the embodiments of the present invention may be a disk centrifuge;
(5) Refining
Filtering the oil obtained in the step (4) through a plate frame and refining at 110 ℃ to obtain bovine bone marrow oil;
(6) Blending
Adding a proper amount of water into the bovine bone marrow oil obtained in the step (5) according to the content of the bovine bone marrow oil in the bovine bone marrow oil refined powder product of 62 percent, the content of the sodium starch octenyl succinate of 18 percent and the content of maltodextrin of 20 percent, emulsifying and blending in an emulsifying tank, for example, adding 1.2 times of the weight ratio of the bovine bone marrow oil, shearing and emulsifying for 30 minutes, and controlling the emulsifying temperature at 45 ℃; it should be noted that the ratio in this step is mass percent, and the following embodiments are mass percent as well; adding a proper amount of water means that the bovine bone marrow oil, the sodium starch octenyl succinate and the maltodextrin can be converted into emulsion, and the added water amount can be properly adjusted according to different proportions, and the embodiment is not repeated;
(7) Spray drying
Feeding the feed liquid obtained in the step (6) into a spray dryer for spray drying to obtain beef marrow fat refined powder;
wherein, the working conditions of the spray dryer are as follows: the inlet temperature of the spray dryer was 130℃and the outlet temperature of the spray dryer was 80 ℃.
According to the preparation method of the beef marrow oil refined powder, provided by the embodiment, the marrow in the beef bones is extracted more in a secondary extraction mode during cooking and extraction, so that the residual waste of raw materials is reduced; the obtained beef marrow fat refined powder retains the nutrition of fat, improves the flavor and dispersibility, and is easier to mix with other foods; because the powder is in a solid powder state, the influence of temperature is small, and the storage stability is improved; compared with the characteristic that conventional grease is difficult to mix with water, the beef marrow oil concentrate powder provided by the invention wraps grease particles by utilizing hydrophilic substances, is easy to mix with water in food, has good emulsifying and dispersing effects, improves water solubility, expands application range, and is especially suitable for seasoning bags of instant food, hot pot and spicy soup base ingredients.
Example 2
The preparation method of the beef marrow oil refined powder provided by the invention comprises the following process steps:
(1) Selecting, cleaning and crushing raw materials
Selecting pollution-free calf bones as raw materials, cleaning and then sending into a crusher for crushing treatment;
(2) Extracting by steaming
Putting the beef bones subjected to the crushing treatment in the step (1) into a cooking pot for extraction: primary extraction: adding bone into a steaming pot, adding water with the weight ratio of 2 times of that of the bone, preserving heat at 136 ℃ for 5 hours, and discharging;
and (3) secondary extraction: after the primary material is beaten, adding water with the weight ratio of 1 time to the bone, preserving heat for 2 hours at 136 ℃ and discharging;
in the step, more bone marrow in the bovine bone is extracted in a secondary extraction mode, so that the residue and waste of raw materials are reduced; wherein, either the primary extraction or the secondary extraction can be carried out under normal pressure or under proper pressure, for example, under the condition of 0.12MPA for heat preservation;
(3) Standing separation
Standing the feed liquid obtained in the step (2) for 2 hours in a standing tank; naturally separating oil from soup;
(4) Disc separation
Carrying out three-phase separation on the materials prepared in the step (3) through a centrifugal machine, controlling the rotation speed of the centrifugal machine to 7200 r/h and the feeding flow of the centrifugal machine to 5T/h, wherein the oil content of the separated soup is less than 2 per mill, and pumping the soup into a soup temporary storage tank and pumping the oil into a crude oil tank;
(5) Refining
Filtering the oil obtained in the step (4) through a plate frame and refining at 110 ℃ to obtain bovine bone marrow oil;
(6) Blending
Adding a proper amount of water into the bovine bone marrow oil obtained in the step (5) according to the content of the bovine bone marrow oil in the bovine bone marrow oil refined powder product of 70%, the content of sodium starch octenyl succinate of 25% and the content of maltodextrin of 5%, emulsifying and blending in an emulsifying tank, for example, adding 1.1 times of the weight ratio of the bovine bone marrow oil, shearing and emulsifying for 2 hours, and controlling the emulsifying temperature at 65 ℃;
(7) Spray drying
Feeding the feed liquid obtained in the step (6) into a spray dryer for spray drying to obtain beef marrow fat refined powder;
the working conditions of spray drying are: the inlet temperature was 215℃and the outlet temperature was 108 ℃.
According to the preparation method of the beef marrow oil refined powder, provided by the embodiment, the marrow in the beef bones is extracted more in a secondary extraction mode during cooking and extraction, so that the residual waste of raw materials is reduced; the obtained beef marrow fat refined powder retains the nutrition of fat, improves the flavor and dispersibility, and is easier to mix with other foods; because the powder is in a solid powder state, the influence of temperature is small, and the storage stability is improved; compared with the characteristic that conventional grease is difficult to mix with water, the beef marrow oil concentrate powder provided by the invention wraps grease particles by utilizing hydrophilic substances, is easy to mix with water in food, has good emulsifying and dispersing effects, improves water solubility, expands application range, and is especially suitable for seasoning bags of instant food, hot pot and spicy soup base ingredients.
Example 3
The preparation method of the beef marrow oil refined powder provided by the invention comprises the following process steps:
(1) Selecting, cleaning and crushing raw materials
Selecting pollution-free calf bones as raw materials, cleaning and then sending into a crusher for crushing treatment;
(2) Extracting by steaming
Putting the beef bones subjected to the crushing treatment in the step (1) into a cooking pot for extraction: primary extraction: adding bone into a steaming pot, adding water with the weight ratio of 1.5 times of that of the bone, preserving heat at 130 ℃ for 2 hours, and discharging;
and (3) secondary extraction: after the primary material is beaten, adding water with the weight ratio of 1 time to the bone, preserving heat for 1.5 hours at 120 ℃ and discharging;
in the step, more bone marrow in the bovine bone is extracted in a secondary extraction mode, so that the residue and waste of raw materials are reduced; wherein, either the primary extraction or the secondary extraction can be carried out under normal pressure or under proper pressure, for example, under the condition of 0.11MPA for heat preservation;
(3) Standing separation
Standing the feed liquid obtained in the step (2) for 1h in a standing tank; naturally separating oil from soup;
(4) Disc separation
Carrying out three-phase separation on the materials prepared in the step (3) through a centrifugal machine, controlling the rotating speed of the centrifugal machine to 10000 revolutions per hour, controlling the feeding flow of the centrifugal machine to 5T/h, and pumping the separated soup into a soup temporary storage tank and pumping the oil into a crude oil tank, wherein the oil content of the separated soup is less than 2 per mill;
(5) Refining
Filtering the oil obtained in the step (4) through a plate frame and refining at 110 ℃ to obtain bovine bone marrow oil;
(6) Blending
Adding a proper amount of water into the bovine bone marrow oil obtained in the step (5) to emulsify and blend in an emulsifying tank according to the content of the bovine bone marrow oil in the bovine bone marrow oil refined powder product of 60 percent, the content of the sodium starch octenyl succinate of 20 percent and the content of maltodextrin of 20 percent, shearing and emulsifying for 1h, and controlling the emulsifying temperature at 50 ℃;
(7) Spray drying
Feeding the feed liquid obtained in the step (6) into a spray dryer for spray drying to obtain beef marrow fat refined powder;
the working conditions of spray drying are: the inlet temperature was 200℃and the outlet temperature was 101 ℃.
According to the preparation method of the beef marrow oil refined powder, provided by the embodiment, the marrow in the beef bones is extracted more in a secondary extraction mode during cooking and extraction, so that the residual waste of raw materials is reduced; the obtained beef marrow fat refined powder retains the nutrition of fat, improves the flavor and dispersibility, and is easier to mix with other foods; because the powder is in a solid powder state, the influence of temperature is small, and the storage stability is improved; compared with the characteristic that conventional grease is difficult to mix with water, the beef marrow oil concentrate powder provided by the invention wraps grease particles by utilizing hydrophilic substances, is easy to mix with water in food, has good emulsifying and dispersing effects, improves water solubility, expands application range, and is especially suitable for seasoning bags of instant food, hot pot and spicy soup base ingredients.
Example 4
The preparation method of the beef marrow oil refined powder provided by the invention comprises the following process steps:
(1) Selecting, cleaning and crushing raw materials
Selecting pollution-free calf bones as raw materials, cleaning and then sending into a crusher for crushing treatment;
(2) Extracting by steaming
Putting the beef bones subjected to the crushing treatment in the step (1) into a cooking pot for extraction: primary extraction: adding bone into a steaming pot, adding water with the weight ratio of 1.2 times of that of the bone, preserving heat for 3 hours at 110 ℃, and discharging;
and (3) secondary extraction: after the primary material is beaten, adding water with the weight ratio of 0.6 times to the bone, preserving heat for 1h at 110 ℃ and discharging;
in the step, more bone marrow in the bovine bone is extracted in a secondary extraction mode, so that the residue and waste of raw materials are reduced; wherein, either the primary extraction or the secondary extraction can be carried out under normal pressure or under proper pressure, for example, under the condition of 0.11MPA for heat preservation;
(3) Standing separation
Standing the feed liquid obtained in the step (2) for 1.5 hours in a standing tank; naturally separating oil from soup;
(4) Disc separation
Carrying out three-phase separation on the materials prepared in the step (3) through a centrifugal machine, controlling the rotating speed of the centrifugal machine to 6000 revolutions per hour, controlling the feeding flow of the centrifugal machine to 5T/h, and pumping the separated soup into a soup temporary storage tank and pumping the oil into a crude oil tank, wherein the oil content of the separated soup is less than 2 per mill;
(5) Refining
Filtering the oil obtained in the step (4) through a plate frame and refining at 110 ℃ to obtain bovine bone marrow oil;
(6) Blending
Adding a proper amount of water into the bovine bone marrow oil obtained in the step (5) according to the content of the bovine bone marrow oil in the bovine bone marrow oil refined powder product of 65%, the content of sodium starch octenyl succinate of 20% and the content of maltodextrin of 15%, emulsifying and blending in an emulsifying tank, for example, adding 1.3 times of the weight ratio of the bovine bone marrow oil, shearing and emulsifying for 1.5h, and controlling the emulsifying temperature at 55 ℃;
(7) Spray drying
Feeding the feed liquid obtained in the step (6) into a spray dryer for spray drying to obtain beef marrow fat refined powder;
the working conditions of spray drying are: the inlet temperature was 170℃and the outlet temperature was 105 ℃.
According to the preparation method of the beef marrow oil refined powder, provided by the embodiment, the marrow in the beef bones is extracted more in a secondary extraction mode during cooking and extraction, so that the residual waste of raw materials is reduced; the obtained beef marrow fat refined powder retains the nutrition of fat, improves the flavor and dispersibility, and is easier to mix with other foods; because the powder is in a solid powder state, the influence of temperature is small, and the storage stability is improved; compared with the characteristic that conventional grease is difficult to mix with water, the beef marrow oil concentrate powder provided by the invention wraps grease particles by utilizing hydrophilic substances, is easy to mix with water in food, has good emulsifying and dispersing effects, improves water solubility, expands application range, and is especially suitable for seasoning bags of instant food, hot pot and spicy soup base ingredients.
Example 5
The preparation method of the beef marrow oil refined powder provided by the invention comprises the following process steps:
(1) Selecting, cleaning and crushing raw materials
Selecting pollution-free calf bones as raw materials, cleaning and then sending into a crusher for crushing treatment;
(2) Extracting by steaming
Putting the beef bones subjected to the crushing treatment in the step (1) into a cooking pot for extraction: primary extraction: adding bone into a steaming pot, adding water with the weight ratio of 1.5 times of that of the bone, preserving heat for 4 hours at 100 ℃, and discharging;
and (3) secondary extraction: after the primary material is beaten, adding water with the weight ratio of 0.6 times to the bone, preserving heat for 1.5 hours at 100 ℃ and discharging;
in the step, more bone marrow in the bovine bone is extracted in a secondary extraction mode, so that the residue and waste of raw materials are reduced; wherein, either the primary extraction or the secondary extraction can be carried out under normal pressure or under proper pressure, for example, under the condition of 0.10MPA for heat preservation;
(3) Standing separation
Standing the feed liquid obtained in the step (2) for 1.5 hours in a standing tank; naturally separating oil from soup;
(4) Disc separation
Carrying out three-phase separation on the materials prepared in the step (3) through a centrifugal machine, controlling the rotating speed of the centrifugal machine to 5400 r/h and the feeding flow of the centrifugal machine to 5T/h, wherein the oil content of the separated soup is less than 2 per mill, and pumping the soup into a soup temporary storage tank and pumping the oil into a crude oil tank;
(5) Refining
Filtering the oil obtained in the step (4) through a plate frame and refining at 110 ℃ to obtain bovine bone marrow oil;
(6) Blending
Adding a proper amount of water into the beef marrow oil obtained in the step (5) to emulsify and blend in an emulsifying tank according to the content of the beef marrow oil in the beef marrow oil refined powder product of 65%, the content of sodium starch octenyl succinate of 25% and the content of maltodextrin of 10%, shearing and emulsifying for 1.5h, and controlling the emulsifying temperature at 60 ℃;
(7) Spray drying
Feeding the feed liquid obtained in the step (6) into a spray dryer for spray drying to obtain beef marrow fat refined powder;
the working conditions of spray drying are: the inlet temperature was 180℃and the outlet temperature was 90 ℃.
According to the preparation method of the beef marrow oil refined powder, provided by the embodiment, the marrow in the beef bones is extracted more in a secondary extraction mode during cooking and extraction, so that the residual waste of raw materials is reduced; the obtained beef marrow fat refined powder retains the nutrition of fat, improves the flavor and dispersibility, and is easier to mix with other foods; because the powder is in a solid powder state, the influence of temperature is small, and the storage stability is improved; compared with the characteristic that conventional grease is difficult to mix with water, the beef marrow oil concentrate powder provided by the invention wraps grease particles by utilizing hydrophilic substances, is easy to mix with water in food, has good emulsifying and dispersing effects, improves water solubility, expands application range, and is especially suitable for seasoning bags of instant food, hot pot and spicy soup base ingredients.
Example 6
The preparation method of the beef marrow oil refined powder provided by the invention comprises the following process steps:
(1) Selecting, cleaning and crushing raw materials
Selecting pollution-free calf bones as raw materials, cleaning and then sending into a crusher for crushing treatment;
(2) Extracting by steaming
Putting the beef bones subjected to the crushing treatment in the step (1) into a cooking pot for extraction: primary extraction: adding bone into a steaming pot, adding water with the weight ratio of 1.5 times of that of the bone, preserving heat for 4 hours at 100 ℃, and discharging;
and (3) secondary extraction: after the primary material is beaten, adding water with the weight ratio of 0.6 times to the bone, preserving heat for 1.5 hours at 100 ℃ and discharging;
in the step, more bone marrow in the bovine bone is extracted in a secondary extraction mode, so that the residue and waste of raw materials are reduced; wherein, either the primary extraction or the secondary extraction can be carried out under normal pressure or under proper pressure, for example, under the condition of 0.10MPA for heat preservation;
(3) Standing separation
Standing the feed liquid obtained in the step (2) for 1.5 hours in a standing tank; naturally separating oil from soup;
(4) Disc separation
Carrying out three-phase separation on the materials prepared in the step (3) through a centrifugal machine, controlling the rotating speed of the centrifugal machine to 5400 r/h and the feeding flow of the centrifugal machine to 5T/h, wherein the oil content of the separated soup is less than 2 per mill, and pumping the soup into a soup temporary storage tank and pumping the oil into a crude oil tank;
(5) Refining
Filtering the oil obtained in the step (4) through a plate frame and refining at 110 ℃ to obtain bovine bone marrow oil;
(6) Blending
Adding a proper amount of water into the beef marrow oil obtained in the step (5) to emulsify and blend in an emulsifying tank according to the content of the beef marrow oil in the beef marrow oil refined powder product of 65%, the content of sodium starch octenyl succinate of 25% and the content of maltodextrin of 10%, shearing and emulsifying for 1.5h, and controlling the emulsifying temperature at 60 ℃;
(7) Spray drying
Feeding the feed liquid obtained in the step (6) into a spray dryer for spray drying to obtain beef marrow fat refined powder;
the working conditions of spray drying are: the inlet temperature was 180℃and the outlet temperature was 90 ℃.
According to the preparation method of the beef marrow oil refined powder, provided by the embodiment, the marrow in the beef bones is extracted more in a secondary extraction mode during cooking and extraction, so that the residual waste of raw materials is reduced; the obtained beef marrow fat refined powder retains the nutrition of fat, improves the flavor and dispersibility, and is easier to mix with other foods; because the powder is in a solid powder state, the influence of temperature is small, and the storage stability is improved; compared with the characteristic that conventional grease is difficult to mix with water, the beef marrow oil concentrate powder provided by the invention wraps grease particles by utilizing hydrophilic substances, is easy to mix with water in food, has good emulsifying and dispersing effects, improves water solubility, expands application range, and is especially suitable for seasoning bags of instant food, hot pot and spicy soup base ingredients.
Example 7
The preparation method of the beef marrow oil refined powder provided by the invention comprises the following process steps:
(1) Selecting, cleaning and crushing raw materials
Selecting pollution-free calf bones as raw materials, cleaning and then sending into a crusher for crushing treatment;
(2) Extracting by steaming
Putting the beef bones subjected to the crushing treatment in the step (1) into a cooking pot for extraction: primary extraction: adding bone into a steaming pot, adding water with the weight ratio of 1.8 times of that of the bone, preserving heat for 2.5 hours at 105 ℃, and discharging;
and (3) secondary extraction: after the primary material is beaten, adding water with the weight ratio of 0.7 times to the bone, preserving heat for 1.2 hours at 105 ℃ and discharging;
in the step, more bone marrow in the bovine bone is extracted in a secondary extraction mode, so that the residue and waste of raw materials are reduced; wherein, either the primary extraction or the secondary extraction can be carried out under normal pressure or under proper pressure, for example, under the condition of 0.11MPA for heat preservation;
(3) Standing separation
Standing the feed liquid obtained in the step (2) for 1.8 hours in a standing tank; naturally separating oil from soup;
(4) Disc separation
Carrying out three-phase separation on the materials prepared in the step (3) through a centrifugal machine, controlling the rotating speed of the centrifugal machine to 7000 r/h, controlling the feeding flow of the centrifugal machine to 5T/h, and pumping the separated soup into a soup temporary storage tank, wherein the oil content of the soup is less than 2 per mill, and pumping the oil into a crude oil tank;
(5) Refining
Filtering the oil obtained in the step (4) through a plate frame and refining at 110 ℃ to obtain bovine bone marrow oil;
(6) Blending
Adding a proper amount of water into the beef marrow oil obtained in the step (5) to emulsify and blend in an emulsifying tank according to the content of the beef marrow oil in the beef marrow oil refined powder product of 67%, the content of sodium starch octenyl succinate of 18% and the content of maltodextrin of 15%, shearing and emulsifying for 1.4h, and controlling the emulsifying temperature at 58 ℃;
(7) Spray drying
Feeding the feed liquid obtained in the step (6) into a spray dryer for spray drying to obtain beef marrow fat refined powder;
the working conditions of spray drying are: the inlet temperature was 150℃and the outlet temperature was 95 ℃.
According to the preparation method of the beef marrow oil refined powder, provided by the embodiment, the marrow in the beef bones is extracted more in a secondary extraction mode during cooking and extraction, so that the residual waste of raw materials is reduced; the obtained beef marrow fat refined powder retains the nutrition of fat, improves the flavor and dispersibility, and is easier to mix with other foods; because the powder is in a solid powder state, the influence of temperature is small, and the storage stability is improved; compared with the characteristic that conventional grease is difficult to mix with water, the beef marrow oil concentrate powder provided by the invention wraps grease particles by utilizing hydrophilic substances, is easy to mix with water in food, has good emulsifying and dispersing effects, improves water solubility, expands application range, and is especially suitable for seasoning bags of instant food, hot pot and spicy soup base ingredients.
Example 8
The preparation method of the beef marrow oil refined powder provided by the invention comprises the following process steps:
(1) Selecting, cleaning and crushing raw materials
Selecting pollution-free calf bones as raw materials, cleaning and then sending into a crusher for crushing treatment;
(2) Extracting by steaming
Putting the beef bones subjected to the crushing treatment in the step (1) into a cooking pot for extraction: primary extraction: adding bone into a steaming pot, adding water with the weight ratio of 2 times of that of the bone, preserving heat for 4.5 hours at 125 ℃, and discharging;
and (3) secondary extraction: after the primary material is beaten, adding water with the weight ratio of 0.8 times to the bone, preserving heat for 1.6 hours at 125 ℃ and discharging;
in the step, more bone marrow in the bovine bone is extracted in a secondary extraction mode, so that the residue and waste of raw materials are reduced; wherein, either the primary extraction or the secondary extraction can be carried out under normal pressure or under proper pressure, for example, under the condition of 0.12MPA for heat preservation;
(3) Standing separation
Standing the feed liquid obtained in the step (2) for 1.2 hours in a standing tank; naturally separating oil from soup;
(4) Disc separation
Carrying out three-phase separation on the materials prepared in the step (3) through a centrifugal machine, controlling the rotating speed of the centrifugal machine to be 6300 revolutions per hour, controlling the feeding flow of the centrifugal machine to be 5T/h, and pumping the separated soup into a soup temporary storage tank, wherein the oil content of the soup is less than 2 per mill, and pumping the oil into a crude oil tank;
(5) Refining
Filtering the oil obtained in the step (4) through a plate frame and refining at 105 ℃ to obtain bovine bone marrow oil;
(6) Blending
Adding a proper amount of water into the beef marrow oil obtained in the step (5) to emulsify and blend in an emulsifying tank according to the content of the beef marrow oil in the beef marrow oil refined powder product of 68%, the content of sodium starch octenyl succinate of 15% and the content of maltodextrin of 17%, shearing and emulsifying for 1.6h, and controlling the emulsifying temperature at 62 ℃;
(7) Spray drying
Feeding the feed liquid obtained in the step (6) into a spray dryer for spray drying to obtain beef marrow fat refined powder;
the working conditions of spray drying are: the inlet temperature was 160℃and the outlet temperature was 85 ℃.
According to the preparation method of the beef marrow oil refined powder, provided by the embodiment, the marrow in the beef bones is extracted more in a secondary extraction mode during cooking and extraction, so that the residual waste of raw materials is reduced; the obtained beef marrow fat refined powder retains the nutrition of fat, improves the flavor and dispersibility, and is easier to mix with other foods; because the powder is in a solid powder state, the influence of temperature is small, and the storage stability is improved; compared with the characteristic that conventional grease is difficult to mix with water, the beef marrow oil concentrate powder provided by the invention wraps grease particles by utilizing hydrophilic substances, is easy to mix with water in food, has good emulsifying and dispersing effects, improves water solubility, expands application range, and is especially suitable for seasoning bags of instant food, hot pot and spicy soup base ingredients.
Example 9
The preparation method of the beef marrow oil refined powder provided by the invention comprises the following process steps:
(1) Selecting, cleaning and crushing raw materials
Selecting pollution-free calf bones as raw materials, cleaning and then sending into a crusher for crushing treatment;
(2) Extracting by steaming
Putting the beef bones subjected to the crushing treatment in the step (1) into a cooking pot for extraction: primary extraction: adding bone into a steaming pot, adding water with the weight ratio of 2 times of that of the bone, preserving heat for 4 hours at 115 ℃ and discharging;
and (3) secondary extraction: after the primary material is beaten, adding water with the weight ratio of 1 time to the bone, preserving heat for 1.2 hours at 115 ℃ and discharging;
in the step, more bone marrow in the bovine bone is extracted in a secondary extraction mode, so that the residue and waste of raw materials are reduced; wherein, either the primary extraction or the secondary extraction can be carried out under normal pressure or under proper pressure, for example, under the condition of 0.11MPA for heat preservation;
(3) Standing separation
Standing the feed liquid obtained in the step (2) for 2 hours in a standing tank; naturally separating oil from soup;
(4) Disc separation
Carrying out three-phase separation on the materials prepared in the step (3) through a centrifugal machine, controlling the rotating speed of the centrifugal machine to 5000 revolutions per hour, controlling the feeding flow of the centrifugal machine to 5T/h, and pumping the separated soup into a soup temporary storage tank and pumping the oil into a crude oil tank, wherein the oil content of the separated soup is less than 2 per mill;
(5) Refining
Filtering the oil obtained in the step (4) through a plate frame and refining at 108 ℃ to obtain bovine bone marrow oil;
(6) Blending
Adding a proper amount of water into the beef marrow oil obtained in the step (5) to emulsify and blend in an emulsifying tank according to the content of the beef marrow oil in the beef marrow oil refined powder product of 68%, the content of sodium starch octenyl succinate of 17% and the content of maltodextrin of 15%, shearing and emulsifying for 1.5h, and controlling the emulsifying temperature at 63 ℃;
(7) Spray drying
Feeding the feed liquid obtained in the step (6) into a spray dryer for spray drying to obtain beef marrow fat refined powder;
the working conditions of spray drying are: the inlet temperature was 190℃and the outlet temperature was 98 ℃.
According to the preparation method of the beef marrow oil refined powder, provided by the embodiment, the marrow in the beef bones is extracted more in a secondary extraction mode during cooking and extraction, so that the residual waste of raw materials is reduced; the obtained beef marrow fat refined powder retains the nutrition of fat, improves the flavor and dispersibility, and is easier to mix with other foods; because the powder is in a solid powder state, the influence of temperature is small, and the storage stability is improved; compared with the characteristic that conventional grease is difficult to mix with water, the beef marrow oil concentrate powder provided by the invention wraps grease particles by utilizing hydrophilic substances, is easy to mix with water in food, has good emulsifying and dispersing effects, improves water solubility, expands application range, and is especially suitable for seasoning bags of instant food, hot pot and spicy soup base ingredients.
Example 10
The preparation method of the beef marrow oil refined powder provided by the invention comprises the following process steps:
(1) Selecting, cleaning and crushing raw materials
Selecting pollution-free calf bones as raw materials, cleaning and then sending into a crusher for crushing treatment;
(2) Extracting by steaming
Putting the beef bones subjected to the crushing treatment in the step (1) into a cooking pot for extraction: primary extraction: adding bone into a steaming pot, adding water with the weight ratio of 2 times of that of the bone, preserving heat for 3 hours at 100 ℃, and discharging;
and (3) secondary extraction: after the primary material is beaten, adding water with the weight ratio of 0.5 times to the bone, preserving heat for 1.5 hours at 100 ℃ and discharging;
in the step, more bone marrow in the bovine bone is extracted in a secondary extraction mode, so that the residue and waste of raw materials are reduced; wherein, either the primary extraction or the secondary extraction can be carried out under normal pressure or under proper pressure, for example, under the condition of 0.11MPA for heat preservation;
(3) Standing separation
Standing the feed liquid obtained in the step (2) for 2 hours in a standing tank; naturally separating oil from soup;
(4) Disc separation
Carrying out three-phase separation on the materials prepared in the step (3) through a centrifugal machine, controlling the rotating speed of the centrifugal machine to 5000 revolutions per hour, controlling the feeding flow of the centrifugal machine to 5T/h, and pumping the separated soup into a soup temporary storage tank and pumping the oil into a crude oil tank, wherein the oil content of the separated soup is less than 2 per mill;
(5) Refining
Filtering the oil obtained in the step (4) through a plate frame and refining at 110 ℃ to obtain bovine bone marrow oil;
(6) Blending
Adding a proper amount of water into the beef marrow oil obtained in the step (5) to emulsify and blend in an emulsifying tank according to the content of the beef marrow oil in the beef marrow oil refined powder product of 66 percent, the content of sodium starch octenyl succinate of 18 percent and the content of maltodextrin of 16 percent, shearing and emulsifying for 1.5 hours, and controlling the emulsifying temperature at 64 ℃;
(7) Spray drying
Feeding the feed liquid obtained in the step (6) into a spray dryer for spray drying to obtain beef marrow fat refined powder;
the working conditions of spray drying are: the inlet temperature was 135℃and the outlet temperature was 100 ℃.
According to the preparation method of the beef marrow oil refined powder, provided by the embodiment, the marrow in the beef bones is extracted more in a secondary extraction mode during cooking and extraction, so that the residual waste of raw materials is reduced; the obtained beef marrow fat refined powder retains the nutrition of fat, improves the flavor and dispersibility, and is easier to mix with other foods; because the powder is in a solid powder state, the influence of temperature is small, and the storage stability is improved; compared with the characteristic that conventional grease is difficult to mix with water, the beef marrow oil concentrate powder provided by the invention wraps grease particles by utilizing hydrophilic substances, is easy to mix with water in food, has good emulsifying and dispersing effects, improves water solubility, expands application range, and is especially suitable for seasoning bags of instant food, hot pot and spicy soup base ingredients.
It should be apparent that the embodiments described above are only some, but not all, embodiments of the invention and do not limit the scope of the invention. This invention may be embodied in many different forms, but rather, embodiments are provided in order to provide a thorough and complete understanding of the present disclosure. Although the invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications may be made to the embodiments described in the foregoing description, or equivalents may be substituted for elements thereof.
Claims (10)
1. The preparation method of the beef marrow oil refined powder is characterized by comprising the following steps:
s10, selecting pollution-free calf bones, cleaning, and then sending the calf bones into a crusher for crushing treatment;
s20, throwing the crushed calf bones into a cooking pot for bone marrow extraction to obtain feed liquid to be treated;
s30, standing the feed liquid to be treated obtained in the step S20 in a standing tank to naturally separate oil from soup;
s40, carrying out three-phase separation on the materials prepared in the step S30 through a centrifugal machine to obtain crude oil;
s50, refining the crude oil obtained in the step S40 after filtering to obtain bovine bone marrow oil;
s60, adding sodium starch octenyl succinate, maltodextrin and water into the beef marrow oil obtained in the step S50, and emulsifying and blending in an emulsifying tank to obtain an emulsion;
and S70, feeding the emulsion obtained in the step S60 into a spray dryer for spray drying to obtain the beef marrow fat refined powder.
2. The method for preparing bovine bone marrow oil powder according to claim 1, wherein the step of putting the crushed bovine leg bones into a digester for bone marrow extraction comprises:
s201, adding the crushed corbel bones into a cooking pot, adding water with the weight ratio of 1-2 times of the corbel bones, preserving heat for 1-5 hours at 100-136 ℃ and discharging;
s202, adding water with the weight ratio of 0.5-1 times of the weight of the bracket bone into the material obtained in the step S201, and preserving heat for 1-2 h at 100-136 ℃.
3. The method for preparing bovine bone marrow oil fine powder according to claim 1, wherein in the step S30, the solution to be treated is left in a still pot for 30min to 2h.
4. The method for preparing bovine bone marrow oil fine powder according to claim 1, wherein the rotational speed of the centrifuge is controlled to be 5000/h to 7200 rpm, and the feed flow rate of the centrifuge is controlled to be 2T/h to 10T/h.
5. The method for preparing bovine bone marrow oil powder according to claim 1, wherein the step S50 specifically comprises:
filtering the crude oil obtained in the step S40 by a plate-frame filter and refining at the temperature of 101-120 ℃ to obtain the bovine bone marrow oil.
6. The method for preparing bovine bone marrow oil powder according to claim 1, wherein step S60 specifically comprises:
and (3) emulsifying the beef marrow oil obtained in the step (S50) in an emulsifying tank by adding water, shearing and emulsifying for 30 min-2 h after the beef marrow oil contains 50% -70% of the beef marrow oil, 18% -35% of sodium starch octenyl succinate and 10% -20% of maltodextrin.
7. The method for preparing bovine bone marrow oil concentrate according to claim 6, wherein the bovine bone marrow oil content is 60%, the sodium starch octenyl succinate content is 25%, and the maltodextrin content is 15%.
8. The method for preparing bovine bone marrow oil powder according to claim 6, wherein the temperature is controlled to be 45-70 ℃ in the step of shearing and emulsifying for 30 min-2 h.
9. The method for preparing bovine bone marrow oil fine powder according to claim 8, wherein the shearing and emulsifying time is 1h, and the shearing and emulsifying temperature is controlled at 60 ℃.
10. The method for preparing bovine bone marrow oil concentrate according to claim 1, wherein the spray dryer is operated under the following conditions: the inlet temperature of the spray dryer is 130-215 ℃, and the outlet temperature of the spray dryer is 80-108 ℃.
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| CN116941690A (en) * | 2023-07-28 | 2023-10-27 | 东莞汉朔建元生物科技有限公司 | Formula of bone marrow soup milk tea raw material and preparation method thereof |
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