CN115634177A - Tartary buckwheat rutin sun cream and preparation method thereof - Google Patents
Tartary buckwheat rutin sun cream and preparation method thereof Download PDFInfo
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- CN115634177A CN115634177A CN202211104918.1A CN202211104918A CN115634177A CN 115634177 A CN115634177 A CN 115634177A CN 202211104918 A CN202211104918 A CN 202211104918A CN 115634177 A CN115634177 A CN 115634177A
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- Cosmetics (AREA)
Abstract
The invention discloses tartary buckwheat rutin sun cream and a preparation method thereof, wherein the tartary buckwheat rutin sun cream comprises the following raw materials in parts by weight: 4-6 parts of tartary buckwheat rutin, 6-8 parts of quinoa extract, 20-30 parts of glycerol, 2-6 parts of emulsifier, 2-5 parts of olive oil, 1-2 parts of preservative, 3-6 parts of nano titanium dioxide, 2-4 parts of nano silicon dioxide, 5-10 parts of natural beewax, 2-4 parts of graphene oxide, 5-10 parts of medical stone powder and 15-25 parts of deionized water; the tartary buckwheat rutin sun cream disclosed by the invention can reflect and absorb ultraviolet rays, has excellent oxidation resistance and moisture retention performance, can reduce free radicals generated in skin tissues, further reduces the generation of melanin, and finally achieves an excellent sun protection effect.
Description
Technical Field
The invention relates to the technical field of cosmetics, and particularly relates to tartary buckwheat rutin sunscreen cream and a preparation method thereof.
Background
Skin refers to the tissue covered on the surface of human body and directly contacted with the external environment, has the functions of protection, sensation, secretion, excretion, respiration and the like, and is formed by tightly combining epidermis and dermis. The skin is irradiated by ultraviolet rays for a long time to induce generation of melanin, so that the skin is blackened, and simultaneously, the skin is damaged, so that the problems of aging, wrinkling and the like of the skin occur.
In order to avoid the skin problem caused by ultraviolet radiation generated by outdoor activities, various sunscreen creams are developed on the market, and the sunscreen principle of the sunscreen cream is mainly to directly reduce the ultraviolet radiation on the skin so as to achieve the purpose of sunscreen; however, even the better sunscreen cream cannot completely block ultraviolet rays, and thus, ultraviolet irradiation for a long time after the sunscreen cream is applied has a certain effect on the skin.
In view of the above, the present invention is particularly proposed.
Disclosure of Invention
The invention aims to provide tartary buckwheat rutin sun cream and a preparation method thereof.
In order to achieve the above purpose of the present invention, the following technical solutions are adopted:
the invention provides tartary buckwheat rutin sun cream in a first aspect, which comprises the following raw materials in parts by weight:
4-6 parts of tartary buckwheat rutin, 6-8 parts of quinoa extract, 20-30 parts of glycerol, 2-6 parts of emulsifier, 2-5 parts of olive oil, 1-2 parts of preservative, 3-6 parts of nano titanium dioxide, 2-4 parts of nano silicon dioxide, 5-10 parts of natural beewax, 2-4 parts of graphene oxide, 5-10 parts of medical stone powder and 15-25 parts of deionized water.
Preferably, the tartary buckwheat rutin sun cream comprises the following raw materials in parts by weight:
4-5 parts of tartary buckwheat rutin, 7-8 parts of quinoa extract, 24-26 parts of glycerol, 4-6 parts of emulsifier, 3-5 parts of olive oil, 1-2 parts of preservative, 3-5 parts of nano titanium dioxide, 2-3 parts of nano silicon dioxide, 6-8 parts of natural beewax, 3-4 parts of graphene oxide, 6-8 parts of medical stone powder and 18-22 parts of deionized water.
Preferably, the tartary buckwheat rutin sun cream comprises the following raw materials in parts by weight:
the tartary buckwheat rutin compound premix comprises 5 parts of tartary buckwheat rutin, 7 parts of quinoa extract, 25 parts of glycerol, 5 parts of emulsifier, 4 parts of olive oil, 1 part of preservative, 4 parts of nano titanium dioxide, 3 parts of nano silicon dioxide, 7 parts of natural beewax, 3 parts of graphene oxide, 7 parts of medical stone powder and 20 parts of deionized water.
Preferably, the emulsifier is selected from at least one of carbomer, liquid paraffin, and glyceryl stearate.
Preferably, the preservative is phenoxyethanol or sorbitan caprylate.
Preferably, the particle size of the medical stone powder is 10-20 μm.
The second aspect of the invention provides a preparation method of tartary buckwheat rutin sunscreen cream, which comprises the following steps:
(a) Heating and uniformly mixing olive oil, an emulsifier and natural beeswax to obtain a first mixture;
(b) Mixing glycerol, tartary buckwheat rutin, quinoa extract, graphene oxide and deionized water uniformly to obtain a second mixture;
(c) And (3) uniformly mixing the first mixture and the second mixture, adding a preservative, nano titanium dioxide, nano silicon dioxide and medical stone powder, and uniformly stirring to obtain the tartary buckwheat rutin sunscreen cream.
Preferably, in the step (a), the heating is carried out to 60 to 70 ℃.
Preferably, in the step (c), the mixing of the first mixture and the second mixture specifically includes:
the first mixture and the second mixture are mixed and heated to 50-60 ℃, and then stirred for 5-15 min at the speed of 300-500 r/min.
Compared with the prior art, the invention has the beneficial effects that at least:
according to the technical scheme, the tartary buckwheat rutin has anti-inflammatory and antioxidant effects, can absorb ultraviolet rays, and can achieve a better antioxidant effect by combining with a quinoa extract; in addition, the glycerin and the natural beeswax have a certain moisturizing effect, so that a moist environment can be provided for the skin, the skin tissue can keep vitality, and the resistance of ultraviolet rays is improved; in addition, the nano titanium dioxide, the nano silicon dioxide, the graphene oxide and the medical stone powder are added into the sunscreen cream, so that physical protection on ultraviolet rays can be realized, meanwhile, the components can generate certain heat after absorbing the ultraviolet rays, the medical stone can be promoted to excite far infrared rays, absorption of tartary buckwheat rutin and quinoa extract is promoted, and a better antioxidation effect is achieved.
Detailed Description
The following describes embodiments of the present invention in detail with reference to the following embodiments. The following examples are only for illustrating the technical solutions of the present invention more clearly, and therefore are only used as examples, and the protection scope of the present invention is not limited thereby.
It is to be noted that, unless otherwise specified, technical or scientific terms used herein shall have the ordinary meaning as understood by those skilled in the art to which the invention pertains.
The following examples used the following starting materials:
the tartary buckwheat rutin is prepared by the following method:
(a) Selecting fresh tartary buckwheat flowers in a flowering period, and then carrying out freeze grinding on the tartary buckwheat flowers for 0.2h to obtain tartary buckwheat powder;
(b) Under the ultrasonic condition of 600W, according to the mass ratio of the tartary buckwheat powder to the extracting solution of 1: 10, putting the tartary buckwheat powder into the extracting solution with the pH value of 8.8, extracting for 0.5h at room temperature, and filtering to obtain the tartary buckwheat extracting solution, wherein the extracting solution comprises the following components: ethanol, sodium sulfite and water; the volume concentration of ethanol in the extracting solution is 60 percent, and the mass concentration of sodium sulfite is 0.2 percent;
(c) Adjusting the pH value of the tartary buckwheat extracting solution to 3.5, standing for 5 hours, and filtering to obtain a tartary buckwheat rutin crude product;
(d) And (3) washing the buckwheat rutin crude product with water, and drying in vacuum to obtain the buckwheat rutin.
The quinoa water extract: obtained by common market purchase;
and (3) graphene oxide: obtained by ordinary commercial purchase;
medical stone powder: the particle size is 10-20 μm, and is generally commercially available.
Example 1
1. Tartary buckwheat rutin sun cream
The tartary buckwheat rutin sun cream comprises the following raw materials in parts by weight:
4 parts of tartary buckwheat rutin, 8 parts of quinoa extract, 20 parts of glycerin, 2 parts of emulsifier, 5 parts of olive oil, 1 part of preservative, 6 parts of nano titanium dioxide, 2 parts of nano silicon dioxide, 10 parts of natural beewax, 2 parts of graphene oxide, 10 parts of medical stone powder and 15 parts of deionized water; wherein, the first and the second end of the pipe are connected with each other,
the emulsifier is carbomer;
the preservative is sorbitan caprylate.
2. Preparation method
The preparation method of the tartary buckwheat rutin sun cream comprises the following steps:
(a) Heating olive oil, an emulsifier and natural beeswax to 60 ℃, and uniformly stirring to obtain a first mixture;
(b) Mixing glycerol, tartary buckwheat rutin, quinoa extract, graphene oxide and deionized water uniformly to obtain a second mixture;
(c) And mixing the first mixture and the second mixture, heating to 50 ℃, then stirring for 15min at 300r/min, adding the preservative, the nano titanium dioxide, the nano silicon dioxide and the medical stone powder, and stirring and uniformly mixing to obtain the tartary buckwheat rutin sunscreen cream.
Example 2
1. Tartary buckwheat rutin sun cream
The tartary buckwheat rutin sun cream comprises the following raw materials in parts by weight:
6 parts of tartary buckwheat rutin, 6 parts of quinoa extract, 30 parts of glycerol, 6 parts of emulsifier, 2 parts of olive oil, 2 parts of preservative, 3 parts of nano titanium dioxide, 4 parts of nano silicon dioxide, 5 parts of natural beewax, 4 parts of graphene oxide, 5 parts of medical stone powder and 25 parts of deionized water; wherein the content of the first and second substances,
the emulsifier is glyceryl stearate;
the antiseptic is phenoxyethanol.
2. Preparation method
The preparation method of the tartary buckwheat rutin sun cream comprises the following steps:
(a) Heating olive oil, an emulsifier and natural beeswax to 70 ℃, and uniformly stirring to obtain a first mixture;
(b) Mixing glycerol, tartary buckwheat rutin, quinoa extract, graphene oxide and deionized water uniformly to obtain a second mixture;
(c) And mixing the first mixture and the second mixture, heating to 60 ℃, stirring at 500r/min for 5min, adding the preservative, the nano titanium dioxide, the nano silicon dioxide and the medical stone powder, and uniformly stirring to obtain the tartary buckwheat rutin sunscreen cream.
Example 3
1. Tartary buckwheat rutin sun cream
The tartary buckwheat rutin sun cream comprises the following raw materials in parts by weight:
4 parts of tartary buckwheat rutin, 8 parts of quinoa extract, 24 parts of glycerol, 4 parts of emulsifier, 5 parts of olive oil, 1 part of preservative, 5 parts of nano titanium dioxide, 2 parts of nano silicon dioxide, 8 parts of natural beewax, 3 parts of graphene oxide, 8 parts of medical stone powder and 18 parts of deionized water; wherein the content of the first and second substances,
the emulsifier is liquid paraffin;
the antiseptic is phenoxyethanol.
2. Preparation method
The preparation method of the tartary buckwheat rutin sun cream comprises the following steps:
(a) Heating olive oil, an emulsifier and natural beeswax to 65 ℃, and uniformly stirring to obtain a first mixture;
(b) Mixing glycerol, tartary buckwheat rutin, quinoa extract, graphene oxide and deionized water uniformly to obtain a second mixture;
(c) And mixing the first mixture and the second mixture, heating to 55 ℃, stirring at 400r/min for 10min, adding the preservative, the nano titanium dioxide, the nano silicon dioxide and the medical stone powder, and uniformly stirring to obtain the tartary buckwheat rutin sunscreen cream.
Example 4
1. Tartary buckwheat rutin sun cream
The tartary buckwheat rutin sun cream comprises the following raw materials in parts by weight:
buckwheat rutin 5 parts, quinoa extract 7 parts, glycerin 26 parts, emulsifier 6 parts, olive oil 3 parts, preservative 2 parts, nano titanium dioxide 3 parts, nano silicon dioxide 3 parts, natural beeswax 6 parts, graphene oxide 4 parts, medical stone powder 6 parts and deionized water 22 parts; wherein, the first and the second end of the pipe are connected with each other,
the emulsifier is carbomer, liquid paraffin and glyceryl stearate;
the preservative is phenoxyethanol or sorbitan caprylate.
2. Preparation method
The preparation method of the tartary buckwheat rutin sun cream comprises the following steps:
(a) Heating olive oil, an emulsifier and natural beeswax to 65 ℃, and uniformly stirring to obtain a first mixture;
(b) Mixing glycerol, tartary buckwheat rutin, quinoa extract, graphene oxide and deionized water uniformly to obtain a second mixture;
(c) And mixing the first mixture and the second mixture, heating to 55 ℃, stirring at 400r/min for 10min, adding the preservative, the nano titanium dioxide, the nano silicon dioxide and the medical stone powder, and uniformly stirring to obtain the tartary buckwheat rutin sunscreen cream.
Example 5
1. Tartary buckwheat rutin sun cream
The tartary buckwheat rutin sun cream comprises the following raw materials in parts by weight:
buckwheat rutin 5 parts, quinoa extract 7 parts, glycerin 25 parts, emulsifier 5 parts, olive oil 4 parts, preservative 1 part, nano titanium dioxide 4 parts, nano silicon dioxide 3 parts, natural beeswax 7 parts, graphene oxide 3 parts, medical stone powder 7 parts and deionized water 20 parts; wherein the content of the first and second substances,
the emulsifier is carbomer, liquid paraffin and glyceryl stearate;
the preservative is phenoxyethanol or sorbitan caprylate.
2. Preparation method
The preparation method of the tartary buckwheat rutin sun cream comprises the following steps:
(a) Heating olive oil, an emulsifier and natural beeswax to 65 ℃, and uniformly stirring to obtain a first mixture;
(b) Mixing glycerol, tartary buckwheat rutin, quinoa extract, graphene oxide and deionized water uniformly to obtain a second mixture;
(c) And mixing the first mixture and the second mixture, heating to 55 ℃, then stirring for 10min at 400r/min, adding the preservative, the nano titanium dioxide, the nano silicon dioxide and the medical stone powder, and uniformly stirring to obtain the tartary buckwheat rutin sunscreen cream.
Comparative example 1
The comparison example is tartary buckwheat rutin sun cream, which is basically the same as the tartary buckwheat rutin sun cream in the embodiment 5, and is different only in that the quinoa extract is replaced by equal amount of tartary buckwheat rutin;
the preparation method of the tartary buckwheat rutin sun cream is the same as that in the embodiment 5.
Comparative example 2
The comparison example is a tartary buckwheat rutin sun cream, which is basically the same as the tartary buckwheat rutin sun cream in the embodiment 5, and is different only in that tartary buckwheat rutin is replaced by an equal amount of quinoa extract;
the preparation method of the tartary buckwheat rutin sun cream is the same as that in the embodiment 5.
Comparative example 3
The comparison example is a tartary buckwheat rutin sun cream, which is basically the same as the tartary buckwheat rutin sun cream in the embodiment 5, and the difference is that the medical stone powder is replaced by the same amount of nano titanium dioxide;
the preparation method of the tartary buckwheat rutin sun cream is the same as that in the embodiment 5.
Examples of the experiments
1. A certain amount of DPPH is weighed and prepared into 0.06mg/mL DPPH solution by absolute ethyl alcohol.
Taking 1mL of sunscreen cream (sample) in example 5, adding 2mL of DPPH solution, stirring and dispersing uniformly, standing at room temperature for 30min, and centrifuging at 5000r/min for 10min; taking the supernatant, and measuring the light absorption value at 517 nm; repeating the steps for 3 times, taking an average value, and then calculating the clearance rate of the sample to DPPH free radicals, wherein the calculation formula is as follows:
DPPH clearance = [ A0- (A1-A2) ]/A0 × 100%; wherein, A is the light absorption value of 0-1 mL of absolute ethyl alcohol and 2mL of DPPH solution; a1-1 mL sample +2mL light absorption value of DPPH solution; a2-absorbance of 1mL sample +2mL absolute ethanol.
The radical scavenging performance of the sunscreen creams of example 5 and comparative examples 1-3 were tested according to the above method, and the test results are shown in table 1:
TABLE 1
| Group of | Clearance rate |
| Example 5 | 28.2％ |
| Comparative example 1 | 21.7％ |
| Comparative example 2 | 23.9％ |
| Comparative example 3 | 28.4％ |
As can be seen from Table 1:
compared with comparative examples 1 and 2, the sunscreen cream prepared by the embodiment of the invention has more excellent effect of removing free radicals, and compared with comparative example 3, the sunscreen cream has equivalent effect of removing free radicals.
2. Purchasing 20 SD rats, carrying out back unhairing treatment, then randomly dividing the SD rats into 4 groups, 5 rats in each group, selecting a position with the diameter of 1cm at the same position on the back of the rats for testing, and respectively smearing the sunscreen creams of example 5 and comparative examples 1-3 on rats in different groups at different experimental positions; the coating amount is 0.5 ml/mouse, ultraviolet rays with the wavelength of 310nm are adopted to irradiate an experimental area (the other areas are protected by ultraviolet rays as much as possible), the irradiation time is 30 hours, the coating is performed once every 5 hours, and whether the skin of a group of mice test has erythema is counted; in addition, skin texture measurement was performed on the skin of a rat having a back diameter of 1.5cm before and after the experiment using VISIA-CR, and the average increase in surface wrinkles was calculated, and the specific results are shown in table 2:
TABLE 2
As can be seen from Table 2:
compared with a comparative example, the sunscreen cream prepared by the invention has the best sunscreen effect and can better prevent ultraviolet rays from damaging skin.
Finally, it should be noted that: the above embodiments are only used to illustrate the technical solution of the present invention, and not to limit the same; while the invention has been described in detail and with reference to the foregoing embodiments, it will be understood by those skilled in the art that: the technical solutions described in the foregoing embodiments may still be modified, or some or all of the technical features may be equivalently replaced; such modifications and substitutions do not depart from the spirit and scope of the present invention, and they should be construed as being included in the following claims and description.
Claims (9)
1. The tartary buckwheat rutin sun cream is characterized by comprising the following raw materials in parts by weight:
4-6 parts of tartary buckwheat rutin, 6-8 parts of quinoa extract, 20-30 parts of glycerol, 2-6 parts of emulsifier, 2-5 parts of olive oil, 1-2 parts of preservative, 3-6 parts of nano titanium dioxide, 2-4 parts of nano silicon dioxide, 5-10 parts of natural beewax, 2-4 parts of graphene oxide, 5-10 parts of medical stone powder and 15-25 parts of deionized water.
2. The tartary buckwheat rutin sunscreen cream according to claim 1, is characterized by comprising the following raw materials in parts by weight:
4-5 parts of tartary buckwheat rutin, 7-8 parts of quinoa extract, 24-26 parts of glycerol, 4-6 parts of emulsifier, 3-5 parts of olive oil, 1-2 parts of preservative, 3-5 parts of nano titanium dioxide, 2-3 parts of nano silicon dioxide, 6-8 parts of natural beewax, 3-4 parts of graphene oxide, 6-8 parts of medical stone powder and 18-22 parts of deionized water.
3. The tartary buckwheat rutin sunscreen cream according to claim 1, is characterized by comprising the following raw materials in parts by weight:
the tartary buckwheat rutin compound preparation comprises, by weight, 5 parts of tartary buckwheat rutin, 7 parts of a quinoa extract, 25 parts of glycerin, 5 parts of an emulsifier, 4 parts of olive oil, 1 part of a preservative, 4 parts of nano titanium dioxide, 3 parts of nano silicon dioxide, 7 parts of natural beeswax, 3 parts of graphene oxide, 7 parts of medical stone powder and 20 parts of deionized water.
4. The tartary buckwheat rutin sun cream as claimed in claim 1, wherein the emulsifier is at least one selected from carbomer, liquid paraffin and glyceryl stearate.
5. The tartary buckwheat rutin sunscreen cream as claimed in claim 1, wherein the preservative is phenoxyethanol or sorbitan caprylate.
6. The tartary buckwheat rutin sun cream as claimed in claim 1, wherein the particle size of the medical stone powder is 10-20 μm.
7. The preparation method of tartary buckwheat rutin sunscreen cream as claimed in any one of claims 1 to 6, is characterized by comprising the following steps:
(a) Heating and uniformly mixing olive oil, an emulsifier and natural beeswax to obtain a first mixture;
(b) Mixing glycerol, tartary buckwheat rutin, quinoa extract, graphene oxide and deionized water uniformly to obtain a second mixture;
(c) And (3) uniformly mixing the first mixture and the second mixture, adding the preservative, the nano titanium dioxide, the nano silicon dioxide and the medical stone powder, and uniformly stirring to obtain the tartary buckwheat rutin sunscreen cream.
8. The method according to claim 7, wherein in the step (a), the heating is carried out at 60 to 70 ℃.
9. The preparation method according to claim 7, wherein in the step (c), the uniformly mixing the first mixture and the second mixture specifically comprises:
the first mixture and the second mixture are mixed and heated to 50-60 ℃, and then stirred for 5-15 min at the speed of 300-500 r/min.
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