CN115475114A - Essential oil for conditioning shoulder and neck and preparation method thereof - Google Patents

Essential oil for conditioning shoulder and neck and preparation method thereof Download PDF

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Publication number
CN115475114A
CN115475114A CN202111667012.6A CN202111667012A CN115475114A CN 115475114 A CN115475114 A CN 115475114A CN 202111667012 A CN202111667012 A CN 202111667012A CN 115475114 A CN115475114 A CN 115475114A
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oil
neck
shoulder
conditioning
essential oil
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向子科
房和军
孟令健
曹俊乐
李玉华
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Xiangji Shanghai Biotechnology Co ltd
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P19/00—Drugs for skeletal disorders
    • A61P19/02—Drugs for skeletal disorders for joint disorders, e.g. arthritis, arthrosis
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P29/00—Non-central analgesic, antipyretic or antiinflammatory agents, e.g. antirheumatic agents; Non-steroidal antiinflammatory drugs [NSAID]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59—Mixtures
    • A61K2800/592—Mixtures of compounds complementing their respective functions
    • A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18

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  • Pharmacology & Pharmacy (AREA)
  • Physical Education & Sports Medicine (AREA)
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  • Orthopedic Medicine & Surgery (AREA)
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Abstract

The invention relates to A61K8, in particular to essential oil for conditioning shoulder and neck and a preparation method thereof. The raw materials of the essential oil for conditioning the shoulder and neck comprise natural components and auxiliary materials. Fresh ginger oil with specific optical rotation is added into the system, so that the obtained essential oil for conditioning the shoulder and neck has lasting fragrance, and the temperature resistance of the system can be improved. The obtained plant essential oil has high stability, does not deteriorate after long-term storage, does not generate precipitate, does not change color, can improve shoulder and neck stiffness, joint dampness and cold and the like, can play a role in auxiliary alleviation of pains caused by traumatic injury, is good in use comfort, and does not generate burning sensation.

Description

Essential oil for conditioning shoulder and neck and preparation method thereof
Technical Field
The invention relates to A61K8, in particular to essential oil for conditioning shoulder and neck and a preparation method thereof.
Background
Many office people experience varying degrees of shoulder and neck problems with maintaining the same sitting position for extended periods of time, and this problem is becoming more and more youthful. These problems occur because the muscles are tense for a long time, and waste materials such as lactic acid accumulated in the human body cannot be smoothly discharged, and the essential oil for conditioning is carried out.
However, many essential oils cause some irritation to the skin, and not only do not last the original fragrance for a long time, but also may generate bad taste, which may adversely affect the user.
Patent No. CN109432369A provides compound essential oil for relieving shoulder and neck ache, pure plant distilled and extracted essential oil is added, and the obtained product is transparent and clear in color and luster, has aromatic taste and has the effect of relieving muscle stiffness.
Disclosure of Invention
In order to solve the above problems, the present invention provides, in a first aspect, an essential oil for conditioning shoulder and neck, which comprises natural components and auxiliary materials as raw materials.
Preferably, the raw materials of the essential oil for conditioning the shoulder and neck comprise 30-40 parts of natural components and 0.7-1.2 parts of auxiliary materials in parts by weight.
As a preferable technical scheme, the natural components are selected from one or more of ginger oil, wormwood oil, garden balsam stem oil, ganoderma oil, radix codonopsitis oil, orange flower oil and chamomile oil.
As a preferable technical scheme of the invention, the weight ratio of the ginger oil, the wormwood oil, the garden balsam stem oil, the ganoderma lucidum oil and the radix codonopsitis oil in the natural components is (10.5-13): (8-11): (5-7): (4-7).
Preferably, the weight ratio of the ginger oil, the wormwood oil, the garden balsam stem oil, the ganoderma lucidum oil and the radix codonopsitis oil in the natural components is 12:10:6:6.
as a preferred technical scheme of the invention, the ginger oil is fresh ginger oil.
The ginger oil is divided into fresh ginger oil and dry ginger oil.
As a preferable technical scheme of the invention, the optical rotation of the ginger oil is-30-50.
The optical rotation is a constant, without units. The optical rotation can be used for measuring the purity of the active substance, and other characteristics of the substance can be known through researching the reaction mechanism of the optical rotation substance. Some optically active substances have differences in biological actions in the left or right rotation, the optical rotation of the left-handed substance is negative, and the optical rotation of the right-handed substance is positive.
The applicant finds that the addition of the fresh ginger oil with specific optical rotation in the system can not only make the fragrance of the obtained essential oil for conditioning the shoulder and neck more lasting, but also improve the temperature resistance of the system. The applicant guesses that the fresh ginger oil under the specific optical rotation has specific purity, and the contained ketone substances, alkene substances, alcohol substances and phenol substances have specific proportions, so that the fresh ginger oil can generate specific synergistic effect with molecules in the wormwood oil, the ganoderma lucidum oil and the garden balsam stem oil in the system, the stability of the system is improved, the fragrance is lasting, and the temperature resistance is obviously improved.
As a preferred technical scheme, the auxiliary material comprises an antioxidant.
Preferably, the antioxidant is alpha-tocopherol.
As a preferable technical scheme, the wormwood oil is obtained by an alcohol extraction process.
Preferably, the alcohol extraction process specifically comprises the steps of crushing 500g of wormwood by using a crusher, sieving by using a 30-mesh sieve, soaking for 14 days by using 17 times of ethyl acetate, taking out the wormwood, drying in a 70-DEG C oven for 12 hours, adding 10 times of absolute ethyl alcohol, soaking for 15 days, filtering, distilling the filtered liquid under reduced pressure for 5 hours at the temperature of 40 ℃ and the vacuum degree of 10mbar to obtain extract, namely wormwood oil.
As a preferable technical scheme, the ganoderma lucidum oil is obtained by an alcohol extraction process.
Preferably, the alcohol extraction process specifically comprises the steps of crushing 500g of ganoderma lucidum by using a crusher, sieving by using a 20-mesh sieve, soaking for 14 days by using 18 times of ethyl acetate, taking out the ganoderma lucidum, drying in a 60-DEG C oven for 12 hours, adding 11 times of absolute ethyl alcohol, soaking for 15 days, filtering, distilling the filtered liquid under reduced pressure for 5 hours at the temperature of 40 ℃ and the vacuum degree of 10mbar to obtain extract, namely the ganoderma oil.
The second aspect of the invention provides a preparation method of essential oil for conditioning shoulder and neck, which comprises the following steps: (1) mixing; and (2) carrying out ultrasound.
In a preferred embodiment of the present invention, the mixing temperature is 35 ℃.
Preferably, the step (1) is to mix the raw materials of the shoulder and neck conditioning essential oil at 35 ℃ and stir for 30min.
In the step (2), the ultrasonic treatment time is 1.5h.
Compared with the prior art, the invention has the following beneficial effects:
(1) Fresh ginger oil with specific optical rotation is added into the system, so that the obtained essential oil for conditioning the shoulder and neck has lasting fragrance, and the temperature resistance of the system can be improved.
(2) The obtained plant essential oil has high stability, and can be stored for a long time without deterioration, precipitation, and color change.
(3) The obtained plant essential oil can improve shoulder and neck stiffness, joint dampness and cold, etc.
(4) The obtained plant essential oil can also relieve pain caused by traumatic injury in an auxiliary way.
(5) The essential oil for conditioning shoulder and neck provided by the invention is good in use comfort and free from burning.
Detailed Description
Examples
The raw materials for preparing the compositions in the examples are commercially available, wherein ginger (ginger of fiscilar Roscoe) oil is obtained from Chenopodium alpinum L.with an optical rotation of-28-45, garden balsam stem (Phryma leptostachya L.subsp.asitica (Hara) Kitamura) oil is obtained from Hadamard, mugwort (Artemisia argyi H.L em v. & Vaniot) is obtained from Aikest, ganoderma lucidum (Curtis) P.Karst.) is obtained from Guilin Hongkun speciality Co., ltd., ethyl acetate is obtained from Chunda, density is 0.Karst. and alpha-902 tocopherol is obtained from Topices Biotech Co., ltd.
Example 1
The present example provides an essential oil for conditioning shoulders and necks, wherein the raw materials of the essential oil for conditioning shoulders and necks comprise, by weight, 32 parts of natural components and 0.86 part of auxiliary materials.
The natural components comprise ginger oil, wormwood oil, lopseed oil, ganoderma oil and radix Codonopsis oil.
In the natural components, the weight ratio of ginger oil, wormwood oil, garden balsam stem oil, ganoderma lucidum oil and radix codonopsitis oil is 12:10:6:6.
the ginger oil is fresh ginger oil.
The auxiliary material comprises an antioxidant. The antioxidant is alpha-tocopherol.
The wormwood oil is obtained by an alcohol extraction process.
The alcohol extraction process specifically comprises the steps of crushing 500g of wormwood by using a crusher, sieving by using a 30-mesh sieve, soaking for 14 days by using 17 times of ethyl acetate, taking out the wormwood, drying for 12 hours in a 70-DEG C oven, adding 10 times of absolute ethyl alcohol, soaking for 15 days, filtering, distilling the filtered liquid for 5 hours under reduced pressure at the temperature of 40 ℃ and the vacuum degree of 10mbar, and obtaining extract, namely wormwood oil.
The ganoderma oil is obtained by an alcohol extraction process.
The alcohol extraction process specifically comprises the steps of crushing 500g of lucid ganoderma by using a crusher, sieving the crushed lucid ganoderma by using a 20-mesh sieve, soaking the lucid ganoderma in 18 times of ethyl acetate for 14 days, taking out the lucid ganoderma, drying the lucid ganoderma in an oven at 60 ℃ for 12 hours, adding 11 times of absolute ethyl alcohol, soaking for 15 days, filtering, and distilling the filtered filtrate under reduced pressure for 5 hours at 40 ℃ and under the vacuum degree of 10mbar to obtain extract, namely the lucid ganoderma oil.
The embodiment also provides a preparation method of the essential oil for conditioning the shoulder and the neck, which comprises the following steps: (1) mixing; and (2) carrying out ultrasound.
The step (1) is to mix the raw materials of the shoulder and neck conditioning essential oil at 35 ℃ and stir for 30min.
In the step (2), the ultrasonic treatment time is 1.5h.
Example 2
The present example provides an essential oil for conditioning shoulders and necks and a preparation method thereof, and the essential oil for conditioning shoulders and necks is different from example 1 in that raw materials of the essential oil for conditioning shoulders and necks comprise 37 parts of natural components and 0.97 part of auxiliary materials.
The example also provides a preparation method of the essential oil for conditioning the shoulder and neck, which is the same as the example 1.
Example 3
The present example provides an essential oil for conditioning shoulder and neck and a preparation method thereof, and is different from example 1 in that, in the natural components, the weight ratio of ginger oil, wormwood oil, garden balsam stem oil, ganoderma lucidum oil and codonopsis pilosula oil is 12.4:10.5:6.6:6.5.
the example also provides a preparation method of the essential oil for conditioning the shoulder and neck, which is the same as the example 1.
Example 4
The present example provides an essential oil for conditioning shoulder and neck and a preparation method thereof, and is different from example 1 in that, in the natural components, the weight ratio of ginger oil, wormwood oil, garden balsam stem oil, ganoderma lucidum oil and codonopsis pilosula oil is 6.3:8.1:5.3:4.8.
the example also provides a preparation method of the essential oil for conditioning the shoulder and the neck, which is the same as the example 1.
Example 5
The present example provides an essential oil for conditioning shoulder and neck and a preparation method thereof, and differs from example 1 in that the raw materials of the essential oil for conditioning shoulder and neck comprise 28 parts of natural components and 0.7 part of auxiliary materials.
The example also provides a preparation method of the essential oil for conditioning the shoulder and neck, which is the same as the example 1.
And (4) performance testing:
1. and (3) testing the stability: after the essential oils for neck and shoulder conditioning obtained in examples 1 to 5 were left at a low temperature of 5 deg.C, a high temperature of 25 deg.C and a high temperature of 35 deg.C for 15 days, it was observed whether the odor was strong and whether an offensive odor was generated, and the results are shown in Table 1:
TABLE 1
Figure BDA0003451398790000041
Figure BDA0003451398790000051
It was found that the essential oil for conditioning the neck and shoulder obtained in examples 1 to 3 was still strong in taste when left at a low temperature of 5 ℃, a high temperature of 25 ℃ and a high temperature of 35 ℃ in 15 days, did not generate any unpleasant odor, and was long in storage time and high in stability.

Claims (10)

1. Essential oil for conditioning shoulder and neck is characterized in that the raw materials of the essential oil for conditioning shoulder and neck comprise natural components and auxiliary materials.
2. The essential oil for conditioning shoulder and neck as claimed in claim 1, wherein the natural component is one or more selected from ginger oil, wormwood oil, speranskia herb oil, ganoderma lucidum oil, codonopsis pilosula oil, neroli oil and chamomile oil.
3. The essential oil for conditioning shoulder and neck as claimed in claim 2, wherein the natural components comprise ginger oil, wormwood oil, garden balsam stem oil, ganoderma lucidum oil and radix codonopsis oil, and the weight ratio of the ginger oil, the wormwood oil, the garden balsam stem oil, the ganoderma lucidum oil and the radix codonopsis oil is (10.5-13): (8-11): (5-7): (4-7).
4. The essential oil for conditioning shoulder and neck as claimed in claim 2, wherein the ginger oil is fresh ginger oil.
5. The essential oil for conditioning shoulder and neck as claimed in claim 4, wherein the ginger oil has an optical rotation of-30 to 50.
6. An essential oil for conditioning the shoulder and neck as claimed in any one of claims 1 to 5, wherein the auxiliary material comprises an antioxidant.
7. The essential oil for conditioning the shoulder and neck as claimed in claim 2, wherein the wormwood oil is obtained by an alcohol extraction process.
8. The essential oil for conditioning shoulder and neck as claimed in claim 2, wherein the ganoderma lucidum oil is obtained by an alcohol extraction process.
9. The preparation method of the essential oil for conditioning the shoulder and the neck according to claim 1, which is characterized by comprising the following steps of: (1) mixing; and (2) carrying out ultrasound.
10. The method for preparing essential oil for conditioning shoulder and neck as claimed in claim 9, wherein the temperature of the mixing is 35 ℃.
CN202111667012.6A 2021-12-31 2021-12-31 Essential oil for conditioning shoulder and neck and preparation method thereof Pending CN115475114A (en)

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Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106421720A (en) * 2016-11-28 2017-02-22 深圳汉草药研纳米生物科技有限公司 Essential oil for relaxing tendons, activating collaterals, invigorating blood, dissolving stasis, and relieving neck aching pain and shoulder aching pain
CN107929681A (en) * 2017-10-30 2018-04-20 岳阳市翻天应生物科技有限公司 One kind palm moxibustion essential oil
CN108158966A (en) * 2018-03-22 2018-06-15 合肥仙之峰农业科技有限公司 A kind of body massaging volatile oil for the pressure that can releive
CN108721592A (en) * 2018-09-03 2018-11-02 湖南鑫球贸易有限责任公司 It is a kind of to be used to treat essential oil of shoulder and neck and preparation method thereof
CN109925359A (en) * 2017-12-17 2019-06-25 株洲千金药业股份有限公司 A kind of shoulder neck nursing essential oil and preparation method thereof
CN110200857A (en) * 2019-07-08 2019-09-06 江苏康地源生态农场有限公司 It is a kind of with anti-oxidant, delaying skin aging effect compound wormwood essential oil
CN110917318A (en) * 2018-09-19 2020-03-27 广州思谋信息科技有限公司 Shoulder and neck qi and blood guiding essential oil and preparation method thereof
CN111450227A (en) * 2020-04-25 2020-07-28 福建百想生物科技有限公司 Plant essential oil for relieving shoulder and neck ache

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106421720A (en) * 2016-11-28 2017-02-22 深圳汉草药研纳米生物科技有限公司 Essential oil for relaxing tendons, activating collaterals, invigorating blood, dissolving stasis, and relieving neck aching pain and shoulder aching pain
CN107929681A (en) * 2017-10-30 2018-04-20 岳阳市翻天应生物科技有限公司 One kind palm moxibustion essential oil
CN109925359A (en) * 2017-12-17 2019-06-25 株洲千金药业股份有限公司 A kind of shoulder neck nursing essential oil and preparation method thereof
CN108158966A (en) * 2018-03-22 2018-06-15 合肥仙之峰农业科技有限公司 A kind of body massaging volatile oil for the pressure that can releive
CN108721592A (en) * 2018-09-03 2018-11-02 湖南鑫球贸易有限责任公司 It is a kind of to be used to treat essential oil of shoulder and neck and preparation method thereof
CN110917318A (en) * 2018-09-19 2020-03-27 广州思谋信息科技有限公司 Shoulder and neck qi and blood guiding essential oil and preparation method thereof
CN110200857A (en) * 2019-07-08 2019-09-06 江苏康地源生态农场有限公司 It is a kind of with anti-oxidant, delaying skin aging effect compound wormwood essential oil
CN111450227A (en) * 2020-04-25 2020-07-28 福建百想生物科技有限公司 Plant essential oil for relieving shoulder and neck ache

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