CN115428976A - Coconut-flavored heating cigarette sheet and preparation method thereof - Google Patents
Coconut-flavored heating cigarette sheet and preparation method thereof Download PDFInfo
- Publication number
- CN115428976A CN115428976A CN202211240162.3A CN202211240162A CN115428976A CN 115428976 A CN115428976 A CN 115428976A CN 202211240162 A CN202211240162 A CN 202211240162A CN 115428976 A CN115428976 A CN 115428976A
- Authority
- CN
- China
- Prior art keywords
- coconut
- flavored
- cigarette
- meat
- pulp
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
Abstract
The invention provides a coconut-flavored heating cigarette sheet and a preparation method thereof, wherein the preparation method comprises the following steps: (1) Mixing deoiled coconut meat, coconut water, tobacco leaf and pulp to obtain coconut cigarette pulp, wherein the pulp comprises fiber raw material, adhesive and smoke agent; (2) And (2) performing flow-extending tabletting on the coconut cigarette pulp obtained in the step (1) to obtain the coconut-flavored heating cigarette slice. The coconut-flavored heating cigarette sheet disclosed by the invention is added with the deoiled coconut meat on the basis of the original heating cigarette sheet preparation method, so that the fragrance of the heating cigarette can be enriched, the smoking stimulation can be relieved, the smoke release amount of the heating cigarette can be adjusted, the tensile strength of the heating cigarette sheet can be improved, and the probability of deformation or breakage of the sheet can be reduced. In addition, coconut water is added into the preparation raw materials, the coconut water can be cooperated with the deoiled coconut meat for synergism, and the prepared coconut-flavored heating cigarette slice is fragrant in smell, sweet but not greasy. In addition, the preparation method is simple to operate and suitable for industrial amplification.
Description
Technical Field
The invention belongs to the technical field of tobacco products, and particularly relates to a coconut-flavored heating cigarette sheet and a preparation method thereof.
Background
With the acceleration of global smoking control movement, the tobacco industry has entered a new period of seeking revolution and breakthrough, and the research and development of novel tobacco products (mainly heating non-combustion type cigarettes, electronic cigarettes, buccal cigarettes and the like) are accelerated. The heating non-combustion cigarette (also known as heating cigarette, hnB cigarette) is an important component of novel tobacco products, and is characterized in that: firstly, low-temperature heating (below 500 ℃) is non-combustion; secondly, nicotine is provided, so that the physiological needs of consumers can be met; and thirdly, compared with the traditional cigarette, the reduction of most harmful components in the smoke of the heated cigarette is more than 90%. However, the existing heating cigarette is affected by unstable heating temperature and flavoring mode, the taste is single, and the sensory quality of the product is unstable.
The coconut is a plant of the genus Cocos in the family Tung, and is mainly distributed in Wenchang, qinhai, wanning, lingshui county and Suanshi, etc. of the southeast coast of Hainan province, and the area and yield of the coconut account for about 80% of the country. Coconut water is present in the cavity and the coconut water in the young fruit is sour and astringent before coconut meat has not yet formed. After the coconut meat is formed, the coconut water has higher sugar content and sweet taste. The matured coconut has a light taste but an increased fat and mineral content. The coconut meat is pure white in color and fragrant in smell, and comprises the following components: 35-40% of fat, 5-10% of carbohydrate, 4-5% of protein, 2-4% of crude fiber, 1-1.5% of ash and a small amount of vitamins B1, A, C, E, magnesium, calcium and the like. The coconut water comprises the following main components: reducing sugar 0.8%, sucrose 4.2%, protein 0.03%, and small amount of amino acids, vitamin C, B2, calcium, magnesium, etc. (comprehensive analysis and utilization of coconut substance composition, chenlimei, lideluo, tropical agricultural science, vol.22, no. 6, pages 50-75)
There are three main forms of heated cigarette smoking media in the current market: the first is mainly granular bulk material, such as Japanese tobacco Ploom; the second is an orderly arranged thin sheet, such as the 'wide and narrow kungfu' of cigarette in Sichuan; the third is the same disorder of tobacco shreds or flakes as conventional cigarettes, such as Revo by Renuo, COO by Hubei, etc. From the market products, the smoking media in the form of cigarettes are still the mainstream in the market, and the third randomly arranged cut tobacco or thin slices are easier to realize on the existing production line and are widely applied.
Patent document CN109207267A discloses a compound coconut oil for cigarettes and a preparation method thereof, which comprises the following steps: (1) Selecting mature fresh coconuts, breaking shells, and respectively taking coconut juice and coconut meat for later use; (2) Pulping coconut pulp, adding food-grade 95% ethanol which is 3-5 times of the weight of the coconut pulp to prepare a mixture, and freezing a container filled with the mixture in a refrigerator at a set temperature of-50 to-80 ℃ for 1-3 hours; (3) Taking out the container, unfreezing, adding coconut juice which is 1 to 1 percent of the weight ratio of the coconut juice to the food grade 95 percent ethanol in the step (2), stirring for 10 to 15min, and then placing the mixture at 4 ℃ for cold soaking for 8 to 10 hours; (4) And (4) after the mixture obtained in the step three is subjected to vacuum filtration, the mixture is subjected to vacuum concentration at the temperature of 40-60 ℃ until the relative density is 1.01-1.20, and the coconut oil for the compound cigarette is obtained. The natural tobacco flavor with the sweet coconut fragrance prepared by the invention is applied to cigarettes, has good harmony with smoke gas, and can improve smoking taste and reduce stimulation.
Patent document CN103396887B discloses a preparation method of coconut essence for cigarettes, which comprises the following steps: (1) cutting fresh coconut, and taking out coconut meat and coconut juice; (2) Cleaning and crushing coconut meat, adding 50-80% of ethanol into the coconut meat according to 4-8 times of the weight of the coconut meat, soaking for 10-20 days under a backlight condition, taking a soaking solution, and concentrating under reduced pressure until no alcohol smell exists to obtain a concentrated solution; (3) Adding alcohol into the coconut juice to make the content of the alcohol reach 30-50%, standing for 18-30 hours, and then filtering with a 0.5-1.2 mu m filter membrane to obtain filtrate for later use; (4) And (3) mixing the concentrated solution obtained in the step (2) with the filtrate obtained in the step (3) according to a volume ratio of 1. The coconut essence prepared by the invention can enrich the cigarette fragrance of cigarettes, smooth the smoke and improve the taste, and compared with the existing coconut essence, the coconut essence has softer, smoother and more refreshing fragrance.
However, due to the low heating temperature of the heated cigarette and the inherent structural characteristics of the heating appliance and the cigarette, the smoke release characteristic of the heated cigarette is obviously different from that of the traditional cigarette, and the problems of monotonous aroma, large strength, irritation and the like in sensory characteristics are particularly shown, so that the adjustment of raw material components, the optimization of a preparation process and the improvement of the aroma performance, the smoking performance and the sensory experience of the heated cigarette are very significant.
Disclosure of Invention
Aiming at the defects of the prior art, the invention aims to provide a coconut-flavored heating cigarette sheet and a preparation method thereof.
In order to achieve the purpose, the invention adopts the following technical scheme:
on one hand, the invention provides a preparation method of coconut-flavored heating cigarette slices, which comprises the following steps:
(1) Mixing deoiled coconut meat, coconut water, tobacco leaf and pulp to obtain coconut cigarette pulp, wherein the pulp comprises fiber raw material, adhesive and smoke agent;
(2) And (2) performing flow-extending tabletting on the coconut cigarette pulp obtained in the step (1) to obtain the coconut-flavored heating cigarette slice.
The preparation method of the coconut-flavored heating cigarette sheet is to add deoiled coconut meat and coconut water on the basis of the original preparation method of the heating cigarette sheet. The coconut meat without oil is added in the preparation raw materials of the heating cigarette slice, firstly, the fragrance of the coconut meat can enrich the fragrance of the heating cigarette and relieve the stimulation of nicotine to respiratory tract and oral cavity; secondly, the coconut meat has certain moisture-keeping components and can be compounded with a smoke agent in the heated cigarette, so that the smoke release amount and the smoke release speed of the heated cigarette slice during use are adjusted, and the problem that a user is choked and stimulated due to too large smoke amount or the satisfaction of the user is low due to too small smoke amount is avoided; and thirdly, the tensile strength of the heated cigarette sheet can be adjusted by adding the deoiled coconut meat, the tissue structure of the sheet is loose when the coconut oil in the heated cigarette is excessive, the tensile strength of the sheet is low, and the tensile strength of the heated cigarette sheet can be improved and the probability of deformation or breakage of the sheet is reduced when the heated cigarette sheet is added after the coconut meat is deoiled. In addition, coconut water is added into the raw materials for preparing the heating cigarette slices, so that the coconut water and the deoiled coconut meat can be synergized, and the prepared coconut-flavor heating cigarette slices are fragrant in smell and sweet but not greasy. In addition, the preparation method is simple to operate and suitable for industrial amplification.
Preferably, the preparation method of the de-oiled coconut meat in the step (1) comprises the following steps:
mixing and drying the coconut meat and the organic solvent, and drying again to obtain the deoiled coconut meat.
The method is simple to operate, suitable for industrial amplification and high in coconut oil removing efficiency.
Preferably, the dried coconut meat is obtained by crushing coconut meat and then drying the crushed coconut meat through the following temperature program: oven drying at 50-80 deg.C for 1-5 hr, standing at 20-30 deg.C for 0.5-3 hr, and oven drying at 90-130 deg.C for 0.5-2 hr to obtain oven-dried coconut meat.
The dried coconut meat needs to be firstly crushed and then dried under a corresponding temperature program to prepare the dried coconut meat, and the crushed coconut meat is beneficial to improving the subsequent drying and extraction efficiency. The dried coconut meat prepared by the temperature program of firstly drying for 1-5h at the temperature of 50-80 ℃, then standing for 0.5-3h at the temperature of 20-30 ℃, and then drying for 0.5-2h at the temperature of 90-130 ℃ has good quality, and the drying efficiency of the method is high.
The specific value of 50-80 deg.C can be selected from 50 deg.C, 55 deg.C, 60 deg.C, 65 deg.C, 70 deg.C, 75 deg.C or 80 deg.C etc.
The specific value of 1-5h can be selected from 1h, 1.5h, 2h, 2.5h, 3h, 3.5h, 4h, 4.5h or 5h, etc.
The specific value of 20-30 deg.C can be selected from 20 deg.C, 22 deg.C, 24 deg.C, 26 deg.C, 28 deg.C or 30 deg.C etc.
Specific values in the 0.5-3h can be selected from 0.5h, 1h, 1.5h, 2h, 2.5h or 3h and the like.
The specific value of 90-130 deg.C can be selected from 90 deg.C, 95 deg.C, 100 deg.C, 105 deg.C, 110 deg.C, 115 deg.C, 120 deg.C, 125 deg.C or 130 deg.C etc.
The specific value of 0.5-2h can be selected from 0.5h, 1h, 1.5h or 2h, etc.
Other specific point values within the above numerical ranges can be selected, and are not described in detail herein.
Preferably, the mass ratio of the organic solvent to the dried coconut meat is (0.5-3): 1.
When the mass ratio of the organic solvent to the dried coconut meat is (0.5-3): 1, the efficiency of extracting coconut oil by the organic solvent is high, the required total extraction times are few, the content of the organic solvent is proper, and the subsequent drying operation is facilitated.
The specific value of (0.5-3) can be selected from 0.5, 0.8, 1.1, 1.4, 1.7, 2, 2.3, 2.6, 2.9 or 3, etc.
Preferably, the organic solvent includes any one or a combination of at least two of ethanol, dichloromethane or n-hexane, the combination of at least two includes, for example, a combination of ethanol and dichloromethane, a combination of dichloromethane and n-hexane, a combination of ethanol and n-hexane, and the like, and any other combination mode can be selected, which is not described in detail herein.
Preferably, the mixing is specifically operated by stirring at a speed of 50-300rpm for 0.3-3h.
When the organic solvent is mixed with the dried coconut pulp, the stirring speed is 50-300rpm, and the stirring time is 0.3-3h, so that the coconut oil in the coconut pulp can be effectively removed.
The specific value of 50-300rpm can be selected from 50rpm, 100rpm, 150rpm, 200rpm, 250rpm, 300rpm, etc.
The specific value of 0.3-3h can be selected from 0.3h, 0.6h, 0.9h, 1.2h, 1.5h, 1.8h, 2.1h, 2.4h, 2.7h or 3h, etc.
Other specific values within the above ranges can be selected, and are not described in detail herein.
Preferably, the temperature for drying again is 60-90 ℃, and the time for drying again is 0.5-5h.
In the invention, the dried coconut meat is mixed with the organic solvent, the coconut oil in the coconut meat can be effectively extracted by the organic solvent, and then the coconut meat is dried again for 0.5 to 5 hours at the temperature of between 60 and 90 ℃, so that the organic solvent in the coconut meat can be effectively removed, therefore, the method for removing the solvent impurities in the system is simple, and the production efficiency is higher.
The specific value of 60-90 deg.C can be 60 deg.C, 65 deg.C, 70 deg.C, 75 deg.C, 80 deg.C, 85 deg.C or 90 deg.C.
The specific value of 0.5-5h can be selected from 0.5h, 1h, 1.5h, 2h, 2.5h, 3h, 3.5h, 4h, 4.5h or 5h, etc.
Preferably, the mass ratio of the de-oiled coconut meat, the coconut water, the tobacco leaves and the pulp in the preparation raw materials in the step (1) is 1 (30-80): 50-100): 500-700;
the specific value of (30-80) can be 30, 35, 40, 45, 50, 55, 60, 65, 70, 75 or 80, and the like.
The specific value in (50-100) can be 50, 55, 60, 65, 70, 75, 80, 85, 90, 95 or 100, and the like.
The specific value in (500-700) can be selected from 500, 520, 540, 560, 580, 600, 620, 640, 660, 680 or 700, and the like.
Other specific values within the above ranges can be selected, and are not described in detail herein.
According to the invention, when the mass ratio of the coconut meat, the coconut water, the tobacco leaves and the pulp is specifically selected from 1 (30-80) to 50-100 (500-700), the coconut meat, the coconut water, the tobacco leaves and the pulp are removed, and the coconut meat and the coconut oil in the finished product heated cigarette are matched with each other, so that the coconut meat and the coconut oil in the finished product heated cigarette are moderate, the coconut-flavored heated cigarette has rich fragrance and fresh and sweet taste, and a user does not choke in the smoking process.
Preferably, before the mixing in step (1), the method further comprises the step of crushing and sieving the deoiled coconut meat.
Preferably, the mesh number of the screen mesh for sieving is 180-260 meshes.
The specific numerical value in the 180-260 meshes can be selected from 180 meshes, 200 meshes, 220 meshes, 240 meshes, 260 meshes and the like.
Other specific point values within the above numerical ranges can be selected, and are not described in detail herein.
Preferably, before the mixing in the step (1), the tobacco leaves are crushed and sieved.
Preferably, the mesh number of the screen mesh for sieving is 180-260 meshes.
The specific numerical value in the 180-260 meshes can be selected from 180 meshes, 200 meshes, 220 meshes, 240 meshes, 260 meshes and the like.
Other specific point values within the above numerical ranges can be selected, and are not described in detail herein.
Preferably, the fiber raw material in step (1) includes any one of wood pulp fiber, straw pulp fiber, hemp pulp fiber or tobacco stalk fiber or a combination of at least two of them, and the combination of at least two of them includes, for example, a combination of wood pulp fiber and straw pulp fiber, a combination of wood pulp fiber and hemp pulp fiber or a combination of straw pulp fiber and hemp pulp fiber, and the like, and any other combination mode can be selected, and is not repeated herein.
Preferably, the binder in step (1) includes any one of carboxymethyl cellulose, guar gum or pectin, or a combination of at least two of carboxymethyl cellulose, guar gum or pectin, and the combination of at least two of carboxymethyl cellulose and guar gum, guar gum and pectin, or a combination of carboxymethyl cellulose and pectin, and any other combination may be selected, and will not be described herein again.
Preferably, the smoke agent in step (1) includes any one of glycerin, propylene glycol or ethylene glycol or a combination of at least two of glycerin, propylene glycol or ethylene glycol, and the combination of at least two of glycerin and propylene glycol, propylene glycol and ethylene glycol, glycerin and ethylene glycol, and the like, and any other combination mode can be selected, and is not described in detail herein.
Preferably, the slurry in the step (1) comprises 0.5-3 parts of fiber raw materials, 0.5-3 parts of adhesives and 3-10 parts of smoke agents in parts by mass.
The fiber raw material can be selected from 0.5 part, 0.8 part, 1.1 part, 1.4 parts, 1.7 parts, 2 parts, 2.3 parts, 2.6 parts or 3 parts by weight.
The mass portion of the adhesive can be selected from 0.5 portion, 0.8 portion, 1.1 portion, 1.4 portions, 1.7 portions, 2 portions, 2.3 portions, 2.6 portions, 3 portions and the like.
The mass parts of the smoke agent can be 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts, 9 parts or 10 parts and the like.
Other specific values within the above ranges can be selected, and are not described in detail herein.
Preferably, the step (2) of drying is further included after the delayed flow tabletting.
Preferably, the drying temperature is 80-100 ℃, and the drying time is 0.5-5h.
The specific value of 80-100 deg.C can be selected from 80 deg.C, 85 deg.C, 90 deg.C, 95 deg.C or 100 deg.C etc.
The specific value of 0.5-5h can be selected from 0.5h, 1h, 1.5h, 2h, 2.5h, 3h, 3.5h, 4h, 4.5h or 5h, etc.
Other specific values within the above ranges can be selected, and are not described in detail herein.
Preferably, the thickness of the coconut-flavored heating cigarette slice in the step (2) is 0.1-0.3mm, and the moisture content is 5-15%.
The specific value of 0.1-0.3mm can be 0.1mm, 0.2mm or 0.3 mm.
Specific values of 5-15% can be selected from 5%, 6%, 7%, 8%, 9%, 10%, 11%, 12%, 13%, 14%, 15%, etc.
Other specific values within the above ranges can be selected, and are not described in detail herein.
In a second aspect, the invention provides a coconut-flavored heated cigarette sheet prepared according to the preparation method of the first aspect.
The coconut-flavored heating cigarette sheet prepared by the invention is not easy to deform or break and has excellent tensile property; when the cigarette is smoked by matching with a heating cigarette appliance, the smoke amount is suitable, the choking stimulation is not easy to cause, the fragrance is fragrant, and the taste is sweet but not greasy.
Compared with the prior art, the invention has the following beneficial effects:
the preparation method of the coconut-flavored heating cigarette sheet is to add deoiled coconut meat and coconut water on the basis of the original preparation method of the heating cigarette sheet. The coconut meat without oil is added in the preparation raw materials of the heating cigarette slice, firstly, the fragrance of the coconut meat can enrich the fragrance of the heating cigarette and relieve the stimulation of nicotine to respiratory tract and oral cavity; secondly, the coconut meat has certain moisture-keeping components and can be compounded with a smoke agent in the heated cigarette, so that the smoke release amount and the smoke release speed of the heated cigarette slice during use are adjusted, and the problem that a user is choked and stimulated due to too large smoke amount or the satisfaction of the user is low due to too small smoke amount is avoided; and thirdly, the tensile strength of the heated cigarette sheet can be adjusted by adding the deoiled coconut meat, the tissue structure of the sheet is loose when the coconut oil in the heated cigarette is excessive, the tensile strength of the sheet is low, and the tensile strength of the heated cigarette sheet can be improved and the probability of deformation or breakage of the sheet is reduced when the heated cigarette sheet is added after the coconut meat is deoiled. In addition, coconut water is added into the raw materials for preparing the heating cigarette slices, so that the coconut water and the deoiled coconut meat can be synergized, and the prepared coconut-flavor heating cigarette slices are fragrant in smell and sweet but not greasy. In addition, the preparation method is simple to operate and suitable for industrial amplification.
Detailed Description
The technical solution of the present invention is further described below by way of specific embodiments. It should be understood by those skilled in the art that the examples are only for the understanding of the present invention and should not be construed as the specific limitations of the present invention.
The tobacco leaves related to the following examples, comparative examples and test examples are Yunyan 87 flue-cured tobacco leaves produced in Yunyan Chuxiong; the wood pulp fibers are hardwood pulp fibers.
The examples do not show the specific techniques or conditions, according to the technical or conditions described in the literature in the field, or according to the product specifications. The reagents or apparatus used are conventional products commercially available from normal sources, not indicated by the manufacturer.
Example 1
The embodiment provides a coconut-flavored heating cigarette sheet, which is prepared by the following steps: crushing 100 parts of fresh coconut meat into pulp, drying at 70 ℃ for 2h, standing at 25 ℃ for 2h, and then drying at 120 ℃ for 1h to obtain the dried coconut meat.
Mixing dichloromethane and the dried coconut meat according to the mass ratio of 2, rotating at 100rpm, stirring for 0.5h, filtering, repeating the operation for 3 times, and drying again for 2h at 70 ℃ to obtain the deoiled coconut meat.
Drying tobacco leaf at 70 deg.C for 2 hr, pulverizing, sieving with 180 mesh sieve, removing oil, pulverizing, and sieving with 180 mesh sieve. Then 1 part of deoiled coconut pulp, 60 parts of coconut water, 80 parts of tobacco leaves and 540 parts of pulp (12 parts of wood pulp fiber, 18 parts of carboxymethyl cellulose, 48 parts of glycerol and 462 parts of water) are mixed uniformly to prepare the coconut cigarette pulp.
And (3) performing flow casting tabletting on coconut cigarette pulp, drying for 3 hours at the temperature of 90 ℃, controlling the thickness of the slices to be 0.18mm and the water content to be 10%, and thus obtaining the coconut aroma heating cigarette slices.
Example 2
The embodiment provides a coconut-flavored heating cigarette sheet, which is prepared by the following steps: crushing 90 parts of fresh coconut meat into pulp, firstly drying at the temperature of 60 ℃ for 2.5h, standing at the temperature of 27 ℃ for 1h, and then drying at the temperature of 110 ℃ for 2h to prepare the dried coconut meat.
Mixing dichloromethane and the dried coconut meat according to the mass ratio of 1.5, rotating at 150rpm, stirring for 1h, filtering, repeating the operation for 3 times, and drying again for 3h at 60 ℃ to obtain the deoiled coconut meat.
Drying tobacco leaf at 80 deg.C for 2 hr, pulverizing, sieving with 220 mesh sieve, removing oil, pulverizing, and sieving with 220 mesh sieve. Then 1 part of deoiled coconut meat, 40 parts of coconut water, 90 parts of tobacco leaves and 550 parts of pulp (18 parts of wood pulp fiber, 18 parts of carboxymethyl cellulose, 60 parts of glycerol and 454 parts of water) are mixed uniformly to prepare the coconut cigarette pulp.
And (3) performing flow casting tabletting on coconut cigarette pulp, drying at 80 ℃ for 4 hours, wherein the thickness of the slice is 0.2mm, and the moisture is controlled at 13%, so as to prepare the coconut-flavored heating cigarette slice.
Example 3
The embodiment provides a coconut-flavored heating cigarette slice, which is prepared by the following steps: crushing 90 parts of fresh coconut meat into pulp, firstly drying for 1.5h at the temperature of 80 ℃, standing for 2.5h at the temperature of 24 ℃, and then drying for 1.5h at the temperature of 125 ℃ to obtain the dried coconut meat.
And mixing the dichloromethane solution and the dried coconut meat according to the mass ratio of 2.5.
Drying tobacco leaf at 75 deg.C for 2.5h, pulverizing, sieving with 200 mesh sieve, removing oil, pulverizing, and sieving with 200 mesh sieve. And then 1 part of deoiled coconut pulp, 70 parts of coconut water, 100 parts of tobacco leaves and 600 parts of pulp (10 parts of wood pulp fiber, 10 parts of carboxymethyl cellulose, 80 parts of glycerol and 500 parts of water) are mixed uniformly to prepare the coconut cigarette pulp.
And (3) performing flow-casting tabletting on coconut cigarette pulp, drying at the temperature of 100 ℃ for 2h, wherein the thickness of the thin sheet is 0.2mm, and the moisture content is controlled at 8%, so as to prepare the coconut-flavored heating cigarette thin sheet.
Example 4
This example prepared a coconut-flavored heated cigarette sheet which differed from example 1 only in that 60 parts of coconut water was replaced with 85 parts of coconut water, 1 part of coconut meat was replaced with 0.5 part of coconut meat, and 80 parts of tobacco was replaced with 105 parts of tobacco, and the rest was the same as example 1.
Example 5
This example prepared a coconut-flavored heated cigarette sheet which differed from example 1 only in that 60 parts of coconut water was replaced with 25 parts of coconut water, 1 part of coconut meat was replaced with 2.5 parts of coconut meat, and 80 parts of tobacco leaf was replaced with 45 parts of tobacco leaf, and the rest was the same as example 1.
Comparative example 1
This comparative example prepared a coconut-flavored heated cigarette sheet, which was prepared in the same manner as in example 1 except that the starting materials were prepared without removing oil-removed coconut meat, and the mass portions of the oil-removed coconut meat were all distributed to the smoking agent glycerin, except that the rest was the same as in example 1.
Comparative example 2
This comparative example prepared a coconut-flavored heated cigarette sheet, which was prepared using the same procedure as in example 1 except that the starting materials were prepared without the use of fuming agent glycerol, and the glycerol was distributed in parts by mass to the deoiled coconut meat, except that the remainder was the same as in example 1.
Comparative example 3
This comparative example prepared a coconut-flavored heated cigarette sheet that differed from example 1 only in that the starting materials were prepared without coconut meat removed, and the entire mass fraction of coconut meat removed was distributed to coconut water, with the remainder being the same as in example 1.
Comparative example 4
This comparative example prepared a coconut-flavored heated cigarette sheet which was prepared in the same manner as in example 1 except that no coconut water was contained in the starting materials and the coconut water was distributed in parts by mass to the coconut meat removed, the remainder being the same as in example 1.
Comparative example 5
This comparative example prepared a heated cigarette sheet, the preparation method of which differed from example 1 only in that no oil-removed coconut meat and coconut water were contained in the preparation raw materials, namely: drying tobacco leaf at 70 deg.C for 2 hr, pulverizing, and sieving with 180 mesh sieve. Then, 80 parts of tobacco leaves, 540 parts of a slurry (12 parts of wood pulp fiber, 18 parts of carboxymethyl cellulose, 48 parts of glycerin, 462 parts of water) were mixed well to prepare a tobacco slurry.
And (3) performing continuous casting tabletting on the tobacco pulp, drying for 3 hours at the temperature of 90 ℃, controlling the thickness of the slice to be 0.18mm and the water content to be 10%, and preparing the heated cigarette slice.
Comparative example 6
This comparative example prepared a coconut-flavored heated cigarette sheet, the method of preparation differing from example 1 only in that no coconut meat deoiling operation was involved in the preparation, namely: crushing 100 parts of fresh coconut meat into pulp, drying at 70 ℃ for 2h, standing at 25 ℃ for 2h, and then drying at 120 ℃ for 1h to obtain the dried coconut meat.
Drying tobacco leaf at 70 deg.C for 2 hr, pulverizing, sieving with 180 mesh sieve, pulverizing dried coconut meat, and sieving with 180 mesh sieve. Then, 1 part of dried coconut meat, 60 parts of coconut water, 80 parts of tobacco leaves and 540 parts of pulp (12 parts of wood pulp fiber, 18 parts of carboxymethyl cellulose, 48 parts of glycerol and 462 parts of water) are mixed uniformly to prepare the coconut cigarette pulp.
And (3) performing flow-casting tabletting on coconut cigarette pulp, drying at the temperature of 90 ℃ for 3h, wherein the thickness of the thin slice is 0.18mm, and the moisture content is controlled at 10%, so as to prepare the coconut-flavored heating cigarette thin slice.
Test example 1
The products obtained in the examples and comparative examples were subjected to smoking sensory evaluation. The specific evaluation method comprises the following steps: (1) 55 volunteers were selected for sensory evaluation, and 5 volunteers were divided into 1 group and 11 groups, and each group evaluated 1 heated cigarette sheet prepared in the examples or comparative examples, and used in combination with IQOS 3.0 smoking set, and each person smoked 15 mouthfuls. (2) The evaluation criteria are as shown in table 1, and the total sensory evaluation scores were calculated from the average values of the aroma characteristics, smoke characteristics, harmony, taste characteristics, and the like of each group of samples.
TABLE 1
TABLE 2
As can be seen from the data in Table 2, the mass ratios of the coconut meat removed, the coconut water removed, the tobacco leaves and the pulp in examples 4 to 5 are all not in the range of 1 (30-80): 50-100): 500-700, and the total sensory evaluation score for the heated cigarette sheet prepared in the examples 1 is lower than that in the example 1, indicating that the overall sensory experience of the coconut-flavored heated cigarette sheet in use is better when the mass ratios of the coconut meat removed, the coconut water removed, the tobacco leaves and the pulp are in the range of 1 (30-80): 50-100): 500-700.
Compared with the example 1, the coconut-flavored heating cigarette slices have poor smoke characteristics and mouthfeel characteristics when used, are low in choking cough and low in satisfaction of users due to overhigh or overlow smoke and unstable release, show that the coconut-flavored and smoking agent glycerin synergizes, and have better smoke characteristics when used; when the heated cigarette slice prepared in the example 1 is used, smoke has faint scent of coconut meat and sweet taste of coconut water, the coconut meat does not lose sweetness and greasiness when being deoiled, and the product fragrance property is excellent, while the preparation raw materials in the comparative examples 3 and 4 do not contain the deoiled coconut meat and the coconut water respectively, so that the preparation method has poor fragrance property, low fragrance amount and slightly poor fragrance quality compared with the example 1, and shows that the deoiled coconut meat and the coconut water have a synergistic effect in the aspect of fragrance property, the preparation raw materials in the comparative example 5 do not contain the deoiled coconut meat and the coconut water and have poorer overall sensory experience compared with the example 1, and the sensory experience of the heated cigarette slice is greatly improved by adding the coconut meat and the coconut water.
Test example 2
Tensile strength tests were conducted on the heated cigarette sheets obtained in example 1 and comparative example 6. The specific detection method is carried out according to the GB/T12914-2018 standard.
TABLE 3
As can be seen from the data in Table 3, the comparative example 6, which does not include the coconut oil removal operation in the preparation method compared with example 1, produced the heated cigarette sheet with low tensile strength, which indicates that the heated cigarette sheet has loose structure, easy breakage and poor product quality caused by excessive coconut oil contained in the preparation raw material, and the coconut-flavored heated cigarette sheet produced by using the coconut oil removed as the raw material has high tensile strength, strong toughness and difficult fragmentation.
The applicant states that the invention is illustrated by the above examples, but the invention is not limited to the above examples, i.e. it is not intended that the invention must rely on them to be practiced. It should be understood by those skilled in the art that any modification of the present invention, equivalent substitutions of the raw materials of the product of the present invention, addition of auxiliary components, selection of specific modes, etc., are within the scope and disclosure of the present invention.
Claims (10)
1. The preparation method of the coconut-flavored heating cigarette slice is characterized by comprising the following steps:
(1) Mixing oil-removed coconut meat, coconut water, tobacco leaves and pulp to prepare coconut cigarette pulp, wherein the pulp comprises fiber raw materials, adhesive and smoke agent;
(2) And (2) performing flow-extending tabletting on the coconut cigarette pulp obtained in the step (1) to obtain the coconut-flavored heating cigarette slice.
2. The method of making coconut-flavored heated cigarette flakes of claim 1, wherein the method of making de-oiled coconut meat of step (1) comprises:
mixing and drying the coconut meat and the organic solvent, and drying again to obtain the deoiled coconut meat;
preferably, the dried coconut meat is obtained by crushing coconut meat and then drying the crushed coconut meat through the following temperature program: firstly, drying for 1-5h at the temperature of 50-80 ℃, then standing for 0.5-3h at the temperature of 20-30 ℃, and then drying for 0.5-2h at the temperature of 90-130 ℃ to prepare dried coconut meat;
preferably, the mass ratio of the organic solvent to the dried coconut meat is (0.5-3) to 1;
preferably, the organic solvent comprises any one of ethanol, dichloromethane or n-hexane or a combination of at least two of the same;
preferably, the mixing operation is stirring at a rotating speed of 50-300rpm for 0.3-3h;
preferably, the temperature of the secondary drying is 60-90 ℃, and the time of the secondary drying is 0.5-5h.
3. The method for preparing coconut-flavored heated cigarette flakes according to claim 1 or 2, wherein the mass ratio of the de-oiled coconut meat, the coconut water, the tobacco leaves and the slurry in the preparation raw materials in the step (1) is 1 (30-80): 50-100): 500-700;
preferably, before the mixing in the step (1), the method further comprises the operation of crushing and sieving the deoiled coconut meat;
preferably, the mesh number of the screen mesh for sieving is 180-260 meshes;
preferably, before the mixing in the step (1), the tobacco leaves are crushed and sieved;
preferably, the mesh number of the screen mesh for sieving is 180-260 meshes.
4. The method of producing coconut-flavored heated cigarette sheets as claimed in any one of claims 1-3, wherein the fibrous feedstock of step (1) comprises any one or a combination of at least two of wood pulp fiber, straw pulp fiber, hemp pulp fiber or tobacco rod fiber.
5. The method of making coconut-flavored heated cigarette flakes according to any one of claims 1-4, wherein the binder of step (1) comprises any one or a combination of at least two of carboxymethylcellulose, guar gum, or pectin.
6. The method of producing coconut-flavored heated cigarette flakes according to any one of claims 1-5, wherein said smoking agent of step (1) comprises any one of glycerin, propylene glycol or ethylene glycol or a combination of at least two thereof.
7. The method for preparing coconut-flavored heated cigarette sheets as claimed in any one of claims 1-6, wherein the slurry in step (1) comprises, in parts by mass, 0.5-3 parts of fiber raw materials, 0.5-3 parts of binders, and 3-10 parts of smoke agents.
8. The process for preparing a coconut-flavored heated rolled cigarette sheet as claimed in any one of claims 1 to 7, wherein the step (2) of delayed flaking is followed by a drying step;
preferably, the drying temperature is 80-100 ℃, and the drying time is 0.5-5h.
9. The process for preparing coconut-flavored heated cigarette flakes according to any one of claims 1 to 8, wherein the coconut-flavored heated cigarette flakes of step (2) have a thickness of 0.1 to 0.3mm and a moisture content of 5 to 15%.
10. A coconut-flavored heated cigarette sheet, characterized in that it is produced according to the production method of any one of claims 1 to 9.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211240162.3A CN115428976A (en) | 2022-10-11 | 2022-10-11 | Coconut-flavored heating cigarette sheet and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211240162.3A CN115428976A (en) | 2022-10-11 | 2022-10-11 | Coconut-flavored heating cigarette sheet and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN115428976A true CN115428976A (en) | 2022-12-06 |
Family
ID=84251917
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202211240162.3A Pending CN115428976A (en) | 2022-10-11 | 2022-10-11 | Coconut-flavored heating cigarette sheet and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN115428976A (en) |
Citations (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004283358A (en) * | 2003-03-20 | 2004-10-14 | Daio Paper Corp | Tissue paper |
| JP2009041156A (en) * | 2007-08-10 | 2009-02-26 | Nof Corp | Paper softener |
| CN103396887A (en) * | 2013-07-29 | 2013-11-20 | 湖北中烟工业有限责任公司 | Preparation method of cocos nucifera essence for cigarettes |
| CN103866629A (en) * | 2014-02-28 | 2014-06-18 | 苏州恒康新材料有限公司 | Papermaking processing aid and preparation method thereof |
| CN104099178A (en) * | 2014-07-16 | 2014-10-15 | 湖南中烟工业有限责任公司 | Preparation method and application of coconut concentrate |
| CN104213460A (en) * | 2014-08-05 | 2014-12-17 | 江守仲 | Smoke-content-reducing fragrant base paper of tipping paper with addition of nano kieselguhr and preparation method thereof |
| CN105421147A (en) * | 2015-11-25 | 2016-03-23 | 赖清甜 | High-tensile-strength paper and preparation method thereof |
| CN105747269A (en) * | 2016-04-19 | 2016-07-13 | 滁州卷烟材料厂 | Tobacco sheet tobacco shreds containing coconut fiber and preparing method thereof |
| CN106522030A (en) * | 2016-11-11 | 2017-03-22 | 广州市极合技术咨询有限公司 | Wear-resistant packing paper with high structure strength, and production method thereof |
| CN106714590A (en) * | 2014-09-30 | 2017-05-24 | 菲利普莫里斯生产公司 | Method for the production of homogenized tobacco material |
| CN107118848A (en) * | 2017-07-05 | 2017-09-01 | 湖北中烟工业有限责任公司 | A kind of fine processing method of coconut oil and its application |
| US20180310608A1 (en) * | 2015-11-05 | 2018-11-01 | Philip Morris Products S.A. | Homogenized tobacco material with improved volatile transfer |
| CN110903606A (en) * | 2019-12-10 | 2020-03-24 | 安徽农业大学 | Plant oil-based composite material and preparation method thereof |
| US20210000158A1 (en) * | 2017-12-20 | 2021-01-07 | Philip Morris Products S.A. | Aerosol-generating substrate comprising an oil additive |
| CN112900146A (en) * | 2021-03-03 | 2021-06-04 | 东莞市贝辉装饰材料有限公司 | Impregnated adhesive film paper with fragrance and preparation method thereof |
| US20220167659A1 (en) * | 2019-03-11 | 2022-06-02 | Nicoventures Trading Limited | Tobacco composition comprising a tobacco component and an aerosol forming material |
| CN114568732A (en) * | 2022-04-11 | 2022-06-03 | 湖北中烟工业有限责任公司 | Dry-process tobacco sheet and preparation method thereof |
| CN115553487A (en) * | 2022-10-13 | 2023-01-03 | 云南中烟新材料科技有限公司 | Heating cigarette sheet and manufacturing method thereof |
-
2022
- 2022-10-11 CN CN202211240162.3A patent/CN115428976A/en active Pending
Patent Citations (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004283358A (en) * | 2003-03-20 | 2004-10-14 | Daio Paper Corp | Tissue paper |
| JP2009041156A (en) * | 2007-08-10 | 2009-02-26 | Nof Corp | Paper softener |
| CN103396887A (en) * | 2013-07-29 | 2013-11-20 | 湖北中烟工业有限责任公司 | Preparation method of cocos nucifera essence for cigarettes |
| CN103866629A (en) * | 2014-02-28 | 2014-06-18 | 苏州恒康新材料有限公司 | Papermaking processing aid and preparation method thereof |
| CN104099178A (en) * | 2014-07-16 | 2014-10-15 | 湖南中烟工业有限责任公司 | Preparation method and application of coconut concentrate |
| CN104213460A (en) * | 2014-08-05 | 2014-12-17 | 江守仲 | Smoke-content-reducing fragrant base paper of tipping paper with addition of nano kieselguhr and preparation method thereof |
| CN106714590A (en) * | 2014-09-30 | 2017-05-24 | 菲利普莫里斯生产公司 | Method for the production of homogenized tobacco material |
| US20180310608A1 (en) * | 2015-11-05 | 2018-11-01 | Philip Morris Products S.A. | Homogenized tobacco material with improved volatile transfer |
| CN105421147A (en) * | 2015-11-25 | 2016-03-23 | 赖清甜 | High-tensile-strength paper and preparation method thereof |
| CN105747269A (en) * | 2016-04-19 | 2016-07-13 | 滁州卷烟材料厂 | Tobacco sheet tobacco shreds containing coconut fiber and preparing method thereof |
| CN106522030A (en) * | 2016-11-11 | 2017-03-22 | 广州市极合技术咨询有限公司 | Wear-resistant packing paper with high structure strength, and production method thereof |
| CN107118848A (en) * | 2017-07-05 | 2017-09-01 | 湖北中烟工业有限责任公司 | A kind of fine processing method of coconut oil and its application |
| US20210000158A1 (en) * | 2017-12-20 | 2021-01-07 | Philip Morris Products S.A. | Aerosol-generating substrate comprising an oil additive |
| US20220167659A1 (en) * | 2019-03-11 | 2022-06-02 | Nicoventures Trading Limited | Tobacco composition comprising a tobacco component and an aerosol forming material |
| CN110903606A (en) * | 2019-12-10 | 2020-03-24 | 安徽农业大学 | Plant oil-based composite material and preparation method thereof |
| CN112900146A (en) * | 2021-03-03 | 2021-06-04 | 东莞市贝辉装饰材料有限公司 | Impregnated adhesive film paper with fragrance and preparation method thereof |
| CN114568732A (en) * | 2022-04-11 | 2022-06-03 | 湖北中烟工业有限责任公司 | Dry-process tobacco sheet and preparation method thereof |
| CN115553487A (en) * | 2022-10-13 | 2023-01-03 | 云南中烟新材料科技有限公司 | Heating cigarette sheet and manufacturing method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN109393543B (en) | Ultra-micro powder plant slice and preparation method thereof | |
| DE60122883T2 (en) | SMOKING FILLING MATERIAL CONTAINING A FRUIT PRODUCT | |
| CN102415613B (en) | Method for improving quality of tobacco stalks by using grape wine | |
| AU2001264076A1 (en) | Smokable filler material containing a fruit material | |
| CN109082344B (en) | Tobacco essence perfume, cigarette paper containing tobacco essence perfume and application of cigarette paper | |
| CH643120A5 (en) | METHOD FOR PRODUCING A SMOKABLE MATERIAL. | |
| US4969477A (en) | Smoking materials | |
| CN108998241B (en) | Cured flue-cured tobacco flavor essence for heating non-combustible cigarettes and preparation method and application thereof | |
| CN108618192A (en) | A kind of 15 are formulated electronic cigarette tobacco tar and preparation method thereof | |
| CN112772965A (en) | Cigar flavor cigarette flavor and cigar flavor cigarette paper preparation method | |
| CN101461561B (en) | Conversion agent of fire-cured tobacco odor type as well as preparation method and use method thereof | |
| CN110484369B (en) | Method for preparing tobacco flavor based on increase of extraction rate of dark plums | |
| CN115428976A (en) | Coconut-flavored heating cigarette sheet and preparation method thereof | |
| CN115553487A (en) | Heating cigarette sheet and manufacturing method thereof | |
| CN105441187A (en) | Roasted pumpkin essence, preparation method thereof and application of roasted pumpkin essence in cigarettes | |
| JPS6023830B2 (en) | Tobacco flavor improvement method | |
| JPS606194B2 (en) | Method for improving tobacco aroma and taste | |
| CN113679087A (en) | Cigarette spice and cigarette product | |
| CA1184756A (en) | Substitute smoking tobacco product | |
| CN111084418A (en) | Degradable composite filter stick capable of being cooled and preparation method thereof | |
| CN115413811B (en) | Preparation method and application of burnt sweet tea flavored heating cigarette | |
| GB2234663A (en) | Smoking materials. | |
| GB2203022A (en) | Smoking material | |
| CN112064406B (en) | Special aroma forming paper prepared from jatropha roots of Dai nationality traditional edible spice plants of Xishuangbanna, method and application thereof | |
| CN112064405B (en) | Special fragrant forming paper prepared from rice dyeing flower and method and application thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination |