CN115245686A - Purification device for production of ethylene glycol phenyl ether - Google Patents
Purification device for production of ethylene glycol phenyl ether Download PDFInfo
- Publication number
- CN115245686A CN115245686A CN202210730641.7A CN202210730641A CN115245686A CN 115245686 A CN115245686 A CN 115245686A CN 202210730641 A CN202210730641 A CN 202210730641A CN 115245686 A CN115245686 A CN 115245686A
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- fixedly connected
- rotating shaft
- ethylene glycol
- stirring
- phenyl ether
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- 238000000746 purification Methods 0.000 title claims abstract description 24
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 title claims abstract description 21
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 12
- 238000012545 processing Methods 0.000 claims abstract description 78
- 238000010438 heat treatment Methods 0.000 claims abstract description 60
- 238000003756 stirring Methods 0.000 claims abstract description 58
- 235000017166 Bambusa arundinacea Nutrition 0.000 claims abstract description 33
- 235000017491 Bambusa tulda Nutrition 0.000 claims abstract description 33
- 241001330002 Bambuseae Species 0.000 claims abstract description 33
- 235000015334 Phyllostachys viridis Nutrition 0.000 claims abstract description 33
- 239000011425 bamboo Substances 0.000 claims abstract description 33
- 238000007599 discharging Methods 0.000 claims abstract description 21
- 238000001125 extrusion Methods 0.000 claims description 15
- 230000006978 adaptation Effects 0.000 claims description 3
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 20
- 239000000463 material Substances 0.000 description 7
- 238000012546 transfer Methods 0.000 description 7
- 238000001704 evaporation Methods 0.000 description 3
- 230000008020 evaporation Effects 0.000 description 3
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 238000005096 rolling process Methods 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 229910002651 NO3 Inorganic materials 0.000 description 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 1
- 239000002202 Polyethylene glycol Substances 0.000 description 1
- 229920004933 Terylene® Polymers 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000007910 cell fusion Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- USIUVYZYUHIAEV-UHFFFAOYSA-N diphenyl ether Chemical compound C=1C=CC=CC=1OC1=CC=CC=C1 USIUVYZYUHIAEV-UHFFFAOYSA-N 0.000 description 1
- 150000002170 ethers Chemical class 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- 238000003780 insertion Methods 0.000 description 1
- 230000037431 insertion Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 231100000053 low toxicity Toxicity 0.000 description 1
- 230000009965 odorless effect Effects 0.000 description 1
- 239000003444 phase transfer catalyst Substances 0.000 description 1
- 229920001223 polyethylene glycol Polymers 0.000 description 1
- 239000005020 polyethylene terephthalate Substances 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 235000019605 sweet taste sensations Nutrition 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/0082—Regulation; Control
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/30—Accessories for evaporators ; Constructional details thereof
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
- B01F27/95—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with stirrers having planetary motion, i.e. rotating about their own axis and about a sun axis
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/10—Maintenance of mixers
- B01F35/12—Maintenance of mixers using mechanical means
- B01F35/123—Maintenance of mixers using mechanical means using scrapers for cleaning mixers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B9/00—Cleaning hollow articles by methods or apparatus specially adapted thereto
- B08B9/08—Cleaning containers, e.g. tanks
- B08B9/087—Cleaning containers, e.g. tanks by methods involving the use of tools, e.g. brushes, scrapers
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The invention discloses a purification device for producing ethylene glycol phenyl ether, which specifically comprises: the processing cylinder is provided with a cylindrical structure and a support frame arranged at the bottom of the processing cylinder, a discharging device is fixedly connected at the center position in the support frame, and the top of the discharging device is communicated with the bottom of the processing cylinder; the device comprises a rotating shaft and a fixing sleeve, wherein the rotating shaft is provided with a shaft body structure, the fixing sleeve is arranged on the rotating shaft and is rotatably connected with the rotating shaft, a heating device is fixedly connected to the outer side of the fixing sleeve, a stirring device is fixedly connected to the rotating shaft in a sleeved mode, and the rotating shaft is arranged inside a processing cylinder. This a be used for ethylene glycol phenyl ether production to use purification device, accessible heat-conducting plate increase heating area makes things convenient for the inside solution of a processing section of thick bamboo to be heated fast to the convenient stirring degree of stirring the board to the inside solution of a processing section of thick bamboo that improves makes the inside solution heating of a processing section of thick bamboo more even.
Description
Technical Field
The invention relates to the technical field of purification, in particular to a purification device for producing ethylene glycol phenyl ether.
Background
Along with the development of society, the application of ethylene glycol is more and more extensive, and ethylene glycol is also named as "glycol", "1,2-ethylene glycol", EG for short, is the simplest dihydric alcohol, and the ethylene glycol is colorless and odorless liquid with sweet taste, has low toxicity to animals, can be mutually dissolved with water and acetone, but has low solubility in ethers, and is used as a solvent, an antifreezing agent and a raw material for synthesizing terylene, and the high polymer polyethylene glycol of the ethylene glycol is a phase transfer catalyst and is also used for cell fusion, and the nitrate thereof is an explosive. The heating device used in the current glycol phenyl ether purification can not uniformly heat the glycol in the container, which is also an important reason for influencing the purity, and the residue is easy to exist on the plane of the bottom of the inner wall of the container when discharging after the purification is finished.
Disclosure of Invention
In order to achieve the purpose, the invention is realized by the following technical scheme: a be used for production of ethylene glycol phenyl ether to use purification device specifically includes:
the processing cylinder is provided with a cylindrical structure and a support frame arranged at the bottom of the processing cylinder, a discharging device is fixedly connected at the center position in the support frame, and the top of the discharging device is communicated with the bottom of the processing cylinder;
the rotating shaft is provided with a shaft body structure and a fixing sleeve arranged on the rotating shaft, the fixing sleeve is sleeved on the rotating shaft and is rotationally connected with the rotating shaft, a heating device is fixedly connected to the outer side of the fixing sleeve, a stirring device is sleeved and fixedly connected on the rotating shaft, the rotating shaft is arranged in the processing cylinder, and the top of the rotating shaft penetrates through the processing cylinder and is fixedly connected with a driving shaft of a driving motor;
the bottom of the exhaust pipe is communicated with the top of the processing cylinder, and one end of the exhaust pipe, which is far away from the processing cylinder, is communicated with the condensing device;
the heating device includes:
the supporting rod is provided with a supporting rod body and a heating rod arranged at the top of the supporting rod, the bottom of the heating rod is fixedly connected with the top of the supporting rod, and a heat-conducting sleeve is sleeved and fixedly connected outside the heating rod;
the sliding groove has the rectangle inner wall to and set up the inside extrusion piston of sliding groove, the sliding groove is seted up in the heat-conducting sleeve side, extrusion piston and sliding groove inner wall sliding connection, extrusion piston one side fixedly connected with heat-conducting plate, it has the thermal expansion medium to fill between one side that the extrusion piston kept away from the heat-conducting plate and the sliding groove inner wall.
Be provided with when using through the inside heating device of a processing section of thick bamboo solution heating inside, with the inside moisture evaporation of solution can, be provided with heating device, when the inside heating rod during operation of heating device, heat transfer to on heat-conducting sleeve and the heat-conducting plate on the heating rod, heat the inside solution of a processing section of thick bamboo through heat-conducting sleeve and heat-conducting plate, be provided with the multiunit heat-conducting plate, accessible heat-conducting plate increase heating area, make things convenient for the inside solution of a processing section of thick bamboo to be heated fast, the heating rod heats the thermal energy medium of sliding tray inside simultaneously, the thermal energy medium is heated the inflation and is promoted extrusion piston and heat-conducting plate and move to the sliding tray outside, when the convenience rises at the heating rod temperature, increase the area of contact between the inside solution of heat-conducting plate and a processing section of thick bamboo, make the heat on the heating rod of higher temperature can be faster with heat transfer to the inside solution of a processing section of thick bamboo, the convenient self-adaptive regulation rate of heat exchange according to the temperature of heating rod, and convenient use.
Preferably, one end of the support rod is fixedly connected with the fixing sleeve, and the bottom of the support rod is fixedly connected with the bottom of the inner wall of the processing cylinder.
Preferably, the sliding groove is provided with a plurality of groups and is uniformly distributed on the side surface of the heat-conducting sleeve, and the side surface of the heat-conducting plate is connected with the inner wall of the sliding groove in a sliding manner.
Preferably, the stirring device comprises a rotating disc, a connecting rod is fixedly connected to the side face of the rotating disc, one end, far away from the rotating disc, of the connecting rod penetrates through and is rotatably connected with a stirring plate, a friction disc is fixedly connected to the top of the stirring plate, a friction ring is slidably connected to the side face of the friction disc, stirring grooves are formed in two sides of the stirring plate, a stirring device is arranged, when the heating device heats the solution inside the processing cylinder, a driving motor drives a rotating shaft to rotate, the rotating shaft drives the rotating disc to rotate, the rotating disc drives the stirring plate to rotate through the connecting rod, the solution inside the processing cylinder can be subjected to stirring through the stirring plate, the solution at each position inside the processing cylinder can be uniformly heated, the stirring plate drives the friction disc to rotate when rotating, the friction disc is driven to rotate through friction force between the friction disc and the friction ring, the friction disc drives the stirring plate to rotate, the stirring plate to conveniently improve the stirring degree of the stirring plate on the solution inside the processing cylinder, and the solution inside the processing cylinder can be heated more uniformly.
Preferably, the rotating shaft penetrates through the rotating disc and is fixedly connected with the rotating disc, and the top of the friction ring is fixedly connected with the top of the processing cylinder.
Preferably, the stirring grooves are provided with a plurality of groups and are uniformly distributed on the stirring plate, and the stirring grooves on two sides of the stirring plate are distributed in a staggered manner.
Preferably, discharging device includes a feed cylinder, go out feed cylinder inner wall bottom threaded connection and have the end cap, the taut spring of end cap outside fixedly connected with, taut spring top and a feed cylinder outside fixed connection, end cap top fixedly connected with telescopic link, telescopic link outside cover is established and fixedly connected with rotating collar, rotating collar side fixedly connected with arc scraper blade is provided with discharging device, and when needs the ejection of compact, the telescopic link extension drives inside the draw-in groove of fixture block insertion pivot bottom, and the pivot can drive the telescopic link and rotate, and the telescopic link drives the end cap and rotates, can rotate the end cap from a feed cylinder one end, and storage cylinder one end discharge can be followed to the inside material of a processing section of thick bamboo, and the telescopic link pivoted drives rotating collar and arc scraper blade rotation simultaneously, and accessible arc scraper blade scrapes processing section of thick bamboo inner wall bottom, makes the material of processing section of thick bamboo inner wall bottom gather and discharge from a feed cylinder to the centre, conveniently avoids the material extravagant.
Preferably, go out feed cylinder top and processing bobbin base intercommunication, arc scraper blade bottom and processing bobbin inner wall bottom sliding connection, the telescopic link top is provided with the fixture block, the draw-in groove with fixture block looks adaptation is seted up to the pivot bottom.
The invention provides a purification device for producing ethylene glycol phenyl ether. The method has the following beneficial effects:
1. this a be used for ethylene glycol phenyl ether production to use purification device, be provided with when using through the inside heating device of a processing section of thick bamboo to the inside solution heating of a processing section of thick bamboo, with the inside moisture evaporation of solution can, be provided with heating device, when the inside heating rod during operation of heating device, heat transfer on the heating rod is to on heat conduction sleeve and the heat-conducting plate, heat the inside solution of a processing section of thick bamboo through heat conduction sleeve and heat-conducting plate, be provided with the multiunit heat-conducting plate, accessible heat-conducting plate increase heating area, make things convenient for the inside solution of a processing section of thick bamboo to be heated fast.
2. This a be used for ethylene glycol phenyl ether production to use purification device, be provided with sliding tray and heat-conducting plate, the heating rod heats the thermal energy medium of sliding tray inside, the thermal energy medium is heated the inflation and promotes extrusion piston and heat-conducting plate to the outside removal of sliding tray, conveniently when the heating rod temperature risees, increase the area of contact between the inside solution of heat-conducting plate and processing section of thick bamboo, make heat on the heating rod of higher temperature can be faster with heat transfer to the inside solution of processing section of thick bamboo, the convenient temperature self-adaptation according to the heating rod adjusts the rate of heat transfer, and convenient use.
3. This a be used for ethylene glycol phenyl ether production to use purification device, be provided with agitating unit, when heating device heats the inside solution of a processing section of thick bamboo, driving motor drives the pivot and rotates, the pivot drives the rolling disc and rotates, the rolling disc drives through the connecting rod and stirs the board rotation, can go on the inside solution of a processing section of thick bamboo through stirring the board, the solution that conveniently makes the inside each position of a processing section of thick bamboo can the thermally equivalent, and stir the board when rotating, it rotates to drive the friction disk, friction power through with between the friction ring drives the friction disk rotation, the friction disk drives stirs the board rotation, conveniently improve the stirring degree of stirring the board to the inside solution of a processing section of thick bamboo, make the inside solution heating of a processing section of thick bamboo more even.
4. This a be used for ethylene glycol phenyl ether production to use purification device, be provided with discharging device, when the needs ejection of compact, the telescopic link extension, it is inside to drive the draw-in groove that the fixture block inserted the pivot bottom, the pivot can drive the telescopic link and rotate, the telescopic link drives the end cap and rotates, can roll out the end cap from play feed cylinder one end, storage barrel one end discharge can be followed to the inside material of processing section of thick bamboo, drive rotation circle and arc scraper blade rotation when the telescopic link rotates, accessible arc scraper blade scrapes processing section of thick bamboo inner wall bottom, make the material of processing section of thick bamboo inner wall bottom to middle gathering and discharge from a feed cylinder, conveniently avoid the material extravagant.
Drawings
FIG. 1 is a schematic structural view of the present invention;
FIG. 2 is a schematic view of the internal structure of the present invention;
FIG. 3 is a schematic view of the connection structure of the heating apparatus according to the present invention;
FIG. 4 is a schematic view of a heating apparatus according to the present invention;
FIG. 5 is a schematic view of the stirring device of the present invention;
FIG. 6 is a schematic view of the structure of the discharging device of the present invention;
FIG. 7 is a schematic view of the internal structure of the discharging device of the present invention.
In the figure: 1. processing the cylinder; 2. a support frame; 3. a discharging device; 31. a discharging barrel; 32. a plug; 33. tensioning the spring; 34. a telescopic rod; 35. rotating the ring; 36. an arc-shaped scraper plate; 4. a rotating shaft; 5. fixing a sleeve; 6. a heating device; 61. a support bar; 62. a heating rod; 63. a thermally conductive sleeve; 64. a sliding groove; 65. a squeeze piston; 66. a heat conducting plate; 7. a stirring device; 71. rotating the disc; 72. a connecting rod; 73. stirring the plate; 74. a friction disk; 75. a friction ring; 76. a stirring tank; 8. a drive motor; 9. and (4) exhausting the gas.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The first embodiment is as follows:
referring to fig. 1-4, the present invention provides a technical solution: a be used for production of ethylene glycol phenyl ether to use purification device specifically includes:
the processing cylinder 1 is of a cylindrical structure, the supporting frame 2 is arranged at the bottom of the processing cylinder 1, the central position in the supporting frame 2 is fixedly connected with the discharging device 3, and the top of the discharging device 3 is communicated with the bottom of the processing cylinder 1;
the rotating shaft 4 is provided with a shaft body structure, the fixing sleeve 5 is arranged on the rotating shaft 4, the fixing sleeve 5 is sleeved on the rotating shaft 4 and is connected with the rotating shaft 4 in a rotating mode, the heating device 6 is fixedly connected to the outer side of the fixing sleeve 5, the stirring device 7 is sleeved and fixedly connected on the rotating shaft 4, the rotating shaft 4 is arranged inside the processing cylinder 1, and the top of the rotating shaft 4 penetrates through the processing cylinder 1 and is fixedly connected with a driving shaft of a driving motor 8;
the bottom of the exhaust pipe 9 is communicated with the top of the processing cylinder 1, and one end of the exhaust pipe 9, which is far away from the processing cylinder 1, is communicated with a condensing device;
the heating device 6 includes:
the supporting rod 61 is provided with a supporting rod body, the heating rod 62 is arranged at the top of the supporting rod 61, the bottom of the heating rod 62 is fixedly connected with the top of the supporting rod 61, and the heating rod 62 is sleeved and fixedly connected with a heat conduction sleeve 63;
the sliding groove 64 is provided with a rectangular inner wall, the extrusion piston 65 is arranged in the sliding groove 64, the sliding groove 64 is arranged on the side surface of the heat-conducting sleeve 63, the extrusion piston 65 is in sliding connection with the inner wall of the sliding groove 64, a heat-conducting plate 66 is fixedly connected to one side of the extrusion piston 65, and a thermal expansion medium is filled between one side of the extrusion piston 65, which is far away from the heat-conducting plate 66, and the inner wall of the sliding groove 64.
One end of the support rod 61 is fixedly connected with the fixed sleeve 5, and the bottom of the support rod 61 is fixedly connected with the bottom of the inner wall of the processing cylinder 1.
The sliding grooves 64 are provided with a plurality of groups and are evenly distributed on the side surface of the heat conducting sleeve 63, and the side surface of the heat conducting plate 66 is connected with the inner wall of the sliding groove 64 in a sliding way.
Be provided with when using through the inside heating device 6 of a processing section of thick bamboo 1 solution heating inside through processing section of thick bamboo 1, with the inside moisture evaporation of solution can, be provided with heating device 6, when the inside heating rod 62 during operation of heating device 6, heat transfer on the heating rod 62 is to on heat conduction sleeve 63 and the heat-conducting plate 66, heat the inside solution of a processing section of thick bamboo 1 through heat conduction sleeve 63 and heat-conducting plate 66, be provided with multiunit heat-conducting plate 66, accessible heat-conducting plate 66 increases the heating area, the inside solution of a convenient processing section of thick bamboo 1 is heated fast, simultaneously the heating rod 62 heats the thermal expansion medium of sliding tray 64 inside, the thermal expansion medium is heated the inflation and is promoted extrusion piston 65 and heat-conducting plate 66 and is removed to sliding tray 64 outside, when the convenient temperature of heating rod 62 risees, increase the area of contact between heat-conducting plate 66 and the inside solution of a processing section of thick bamboo 1, make the heat on the heating rod 62 of higher temperature can be faster with heat transfer to the inside solution of a processing section of thick bamboo 1, the convenience is according to the self-adaptive adjustment heat exchange speed of heating rod 62, and convenient use.
Example two:
referring to fig. 1-5, the present invention provides a technical solution based on the first embodiment: the stirring device 7 comprises a rotating disc 71, a connecting rod 72 is fixedly connected to the side face of the rotating disc 71, one end, far away from the rotating disc 71, of the connecting rod 72 is penetrated and rotatably connected with a stirring plate 73, a friction disc 74 is fixedly connected to the top of the stirring plate 73, a friction ring 75 is slidably connected to the side face of the friction disc 74, stirring grooves 76 are formed in two sides of the stirring plate 73, a rotating shaft 4 penetrates through the rotating disc 71 and is fixedly connected with the rotating disc 71, the tops of the friction ring 75 and the top of the processing barrel 1 are fixedly connected, the stirring grooves 76 are formed in multiple groups and are uniformly distributed on the stirring plate 73, the stirring grooves 76 in two sides of the stirring plate 73 are mutually distributed in a staggered mode, the stirring device 7 is arranged, when the heating device 6 heats the solution in the processing barrel 1, a driving motor 8 drives the rotating shaft 4 to rotate, the rotating shaft 4 drives the rotating disc 71 to rotate, the rotating disc 71 drives the stirring plate 73 to rotate through the connecting rod 72, the stirring plate 73 can be carried out on the solution in the processing barrel 1 through the stirring plate 73, the solution in each position in the processing barrel 1 can be uniformly heated by the stirring plate 73, and the stirring plate 73 can be driven by the friction disc 74, and the friction disc 75, and the self-rotation force can be used for improving the uniformity of the solution in the processing barrel 1, and the processing barrel 1.
Example three:
referring to fig. 1-7, the present invention provides a technical solution based on the first embodiment and the second embodiment: discharging device 3, discharging device 3 includes a barrel 31, 31 inner wall bottom threaded connection of a barrel has end cap 32, 32 outside fixedly connected with straining spring 33 of end cap 32, straining spring 33 top and 31 outside fixed connection of a barrel, end cap 32 top fixedly connected with telescopic link 34, 34 outside cover of telescopic link establishes and fixedly connected with turns around 35, 35 side fixedly connected with arc scraper 36 of turning around, 31 top and 1 bottom intercommunication of a barrel, 36 bottom and 1 inner wall bottom sliding connection of arc scraper, telescopic link 34 top is provided with the fixture block, pivot 4 bottom is seted up the draw-in groove with fixture block looks adaptation, be provided with discharging device 3, when needing the ejection of compact, telescopic link 34 extension, it inserts inside the draw-in groove of pivot 4 bottom to drive the fixture block, pivot 4 can drive telescopic link 34 and rotate, telescopic link 34 drives end cap 32 and rotates, can be with going out from 31 one end of a barrel, the inside material of a barrel 1 can be discharged from 31 one end of a barrel, drive turning around 35 and arc scraper 36 rotates when needing the ejection of compact, accessible scraper 36 scrapes the bottom the inner wall of a barrel 1 inner wall and scrapes the waste material from the barrel 31 in the centre of messenger's.
It is to be understood that the described embodiments are merely a few embodiments of the invention, and not all embodiments. All other embodiments, which can be derived by one of ordinary skill in the art and related arts based on the embodiments of the present invention without any creative effort, shall fall within the protection scope of the present invention. Structures, devices, and methods of operation not specifically described or illustrated herein are generally practiced in the art without specific recitation or limitation.
Claims (8)
1. A be used for production of ethylene glycol phenyl ether to use purification device specifically includes:
the processing cylinder (1) is of a cylindrical structure, the supporting frame (2) is arranged at the bottom of the processing cylinder (1), the center position in the supporting frame (2) is fixedly connected with the discharging device (3), and the top of the discharging device (3) is communicated with the bottom of the processing cylinder (1);
the processing device comprises a rotating shaft (4), the rotating shaft (4) is provided with a shaft body structure and a fixing sleeve (5) arranged on the rotating shaft (4), the fixing sleeve (5) is sleeved on the rotating shaft (4) and is rotationally connected with the rotating shaft (4), a heating device (6) is fixedly connected to the outer side of the fixing sleeve (5), a stirring device (7) is sleeved and fixedly connected on the rotating shaft (4), the rotating shaft (4) is arranged in a processing barrel (1), and the top of the rotating shaft (4) penetrates through the processing barrel (1) and is fixedly connected with a driving shaft of a driving motor (8);
the bottom of the exhaust pipe (9) is communicated with the top of the processing cylinder (1), and one end, far away from the processing cylinder (1), of the exhaust pipe (9) is communicated with a condensing device;
the purification device for the production of the ethylene glycol phenyl ether is characterized in that: the heating device (6) comprises:
the supporting rod (61) is provided with a supporting rod body and a heating rod (62) arranged at the top of the supporting rod (61), the bottom of the heating rod (62) is fixedly connected with the top of the supporting rod (61), and a heat-conducting sleeve (63) is sleeved and fixedly connected outside the heating rod (62);
the heat-conducting sleeve is characterized by comprising a sliding groove (64), wherein the sliding groove (64) is provided with a rectangular inner wall, and an extrusion piston (65) is arranged inside the sliding groove (64), the sliding groove (64) is formed in the side face of the heat-conducting sleeve (63), the extrusion piston (65) is in sliding connection with the inner wall of the sliding groove (64), a heat-conducting plate (66) is fixedly connected to one side of the extrusion piston (65), and a thermal expansion medium is filled between one side, away from the heat-conducting plate (66), of the extrusion piston (65) and the inner wall of the sliding groove (64).
2. The purification device for the production of ethylene glycol phenyl ether according to claim 1, wherein: one end of the support rod (61) is fixedly connected with the fixed sleeve (5), and the bottom of the support rod (61) is fixedly connected with the bottom of the inner wall of the processing cylinder (1).
3. The purification device for producing ethylene glycol phenyl ether according to claim 1, wherein: the sliding groove (64) is provided with a plurality of groups and is uniformly distributed on the side surface of the heat-conducting sleeve (63), and the side surface of the heat-conducting plate (66) is in sliding connection with the inner wall of the sliding groove (64).
4. The purification device for producing ethylene glycol phenyl ether according to claim 1, wherein: the stirring device (7) comprises a rotating disc (71), a connecting rod (72) is fixedly connected to the side face of the rotating disc (71), one end, far away from the rotating disc (71), of the connecting rod (72) penetrates through and is rotatably connected with a stirring plate (73), a friction disc (74) is fixedly connected to the top of the stirring plate (73), a friction ring (75) is slidably connected to the side face of the friction disc (74), and stirring grooves (76) are formed in two sides of the stirring plate (73).
5. The purification device for producing ethylene glycol phenyl ether according to claim 4, wherein: the rotating shaft (4) penetrates through the rotating disc (71) and is fixedly connected with the rotating disc (71), and the top of the friction ring (75) is fixedly connected with the top of the processing cylinder (1).
6. The purification device for producing ethylene glycol phenyl ether according to claim 4, wherein: the stirring grooves (76) are provided with a plurality of groups and are uniformly distributed on the stirring plate (73), and the stirring grooves (76) on two sides of the stirring plate (73) are distributed in a staggered mode.
7. The purification device for producing ethylene glycol phenyl ether according to claim 1, wherein: discharging device (3), discharging device (3) are including going out feed cylinder (31), go out feed cylinder (31) inner wall bottom threaded connection has end cap (32), end cap (32) outside fixedly connected with straining spring (33), straining spring (33) top and play feed cylinder (31) outside fixed connection, end cap (32) top fixedly connected with telescopic link (34), telescopic link (34) outside cover is established and fixedly connected with and is rotated circle (35), rotate circle (35) side fixedly connected with arc scraper blade (36).
8. The purification device for producing ethylene glycol phenyl ether according to claim 7, wherein: go out feed cylinder (31) top and processing section of thick bamboo (1) bottom intercommunication, arc scraper blade (36) bottom and processing section of thick bamboo (1) inner wall bottom sliding connection, telescopic link (34) top is provided with the fixture block, the draw-in groove with fixture block looks adaptation is seted up to pivot (4) bottom.
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Denomination of invention: A purification device for the production of ethylene glycol phenyl ether Granted publication date: 20230704 Pledgee: Agricultural Bank of China Limited Dongzhi County Branch Pledgor: Anhui Sanhe Chemical Technology Co.,Ltd. Registration number: Y2024980007901 |