CN115227614B - Blackhead-removing facial cleanser and preparation method thereof - Google Patents
Blackhead-removing facial cleanser and preparation method thereof Download PDFInfo
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- 238000002360 preparation method Methods 0.000 title claims abstract description 84
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- 239000002253 acid Substances 0.000 claims abstract description 35
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- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 34
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Classifications
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/362—Polycarboxylic acids
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/368—Carboxylic acids; Salts or anhydrides thereof with carboxyl groups directly bound to carbon atoms of aromatic rings
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- A—HUMAN NECESSITIES
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
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- A—HUMAN NECESSITIES
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Abstract
The application relates to the technical field of daily chemicals, in particular to blackhead-removing facial cleanser and a preparation method thereof. The blackhead-removing facial cleanser comprises a facial cleanser matrix and blackhead-removing components, wherein the blackhead-removing components are prepared by blending nano carbon powder, plant extracts and compound fruit acid; the dosage of the cleansing matrix and the blackhead removing component is 1 (0.1-0.3) in weight ratio; the plant extract is prepared from the following raw materials: peppermint leaf, red seaweed, lavender, litchi rind, tian Huang, licorice and purslane. The blackhead removing component is prepared by blending the nano carbon powder, the plant extract and the composite fruit acid, can effectively guide out and remove blackheads, simultaneously reduces the damage to skin, is beneficial to shrinking pores and reduces the repeated phenomenon of the blackheads.
Description
Technical Field
The application relates to the technical field of daily chemicals, in particular to blackhead-removing facial cleanser and a preparation method thereof.
Background
The facial cleanser has the function of cleaning the face, is also called as facial cleanser, belongs to cleaning cosmetics, and along with the increasing promotion of the material condition and living standard of people in recent years, the pursuit of the facial cleanser is not only kept for cleaning, but also various functional facial cleansers are generated, wherein the blackhead-removing facial cleanser is taken as an example.
It is well known that the nature of blackheads is essentially sebum that plugs pores, and that the surface layer, when exposed directly to the outside and in contact with air, dust in the air, oxidizes to form a hardened grease obstruction, which is usually present in the forehead and nose of the face and is difficult to remove and cure.
The blackhead removing facial cleanser in the related art comprises a facial cleanser matrix and blackhead removing components, wherein the facial cleanser matrix comprises a surfactant, a humectant, an emollient, an antiseptic and antioxidant auxiliary agent and the like, the blackhead removing components are activated carbon powder, and the blackhead removing facial cleanser can achieve the purpose of removing blackheads by means of the strong adsorption performance of the activated carbon powder.
The blackhead-removing facial cleanser is characterized in that the blackhead can be taken out, but is limited by the reason that the active carbon powder only can play a physical role, the active carbon powder damages the dermis layer along with the increase of the use frequency, and pores are large after a long time, so that blackhead cannot be removed and radically treated in a deeper level, and the blackhead-removing facial cleanser which has good blackhead-removing effect and can shrink the pores and the preparation method thereof are provided.
Disclosure of Invention
The application provides a blackhead-removing facial cleanser and a preparation method thereof, which are used for endowing facial cleanser with excellent blackhead-removing performance and simultaneously have the advantages of low irritation and deep radical treatment, so that the phenomenon of blackhead recurrence is reduced.
In a first aspect, the application provides a blackhead-removing facial cleanser, which adopts the following technical scheme:
the blackhead-removing facial cleanser comprises a facial cleanser matrix and blackhead-removing components, wherein the blackhead-removing components are prepared by blending nano carbon powder, plant extracts and compound fruit acid;
the dosage of the cleansing matrix and the blackhead removing component is 1 (0.1-0.3) in weight ratio;
the plant extract is prepared from the following raw materials: peppermint leaf, red seaweed, litchi rind, tian Huang, licorice and purslane.
By adopting the technical scheme, the facial cleanser with the components has excellent blackhead removing performance and also has the advantages of low stimulation and deep radical treatment by adding the blackhead removing components, namely nano carbon powder, plant extracts and compound fruit acid, so that the recurrence of blackheads can be effectively reduced;
the reason for this analysis may be due to: the blackhead removing component can not only play a basic adsorption and blackhead removing effect through nano carbon powder, but also play a synergistic effect with the nano carbon powder through the stimulation of the composite fruit acid to the skin, so that the delivery and dissolution of the blackhead are accelerated;
in addition, after the blackheads are led out from pores, the plant extracts can stimulate the pores to shrink and strengthen the removal effect of the blackheads by means of strong adsorptivity and dispersibility of nano carbon powder, so that the purposes of reducing blackheads and recurrence are achieved, and the plant extracts can also repair skin, can be used continuously compared with pure fruit acid skin replacement, and basically have no side effect.
Preferably, the blackhead removing component is prepared by blending (0.6-1.2) 1.8-2.4 of nano carbon powder, plant extract and compound fruit acid according to the weight ratio.
By adopting the technical scheme, the blackhead removing component with the proportion has the advantages that the compounding effect of nano carbon powder, plant extract and compound fruit acid is optimal, blackhead can be effectively removed, and meanwhile, the blackhead removing component is not easy to damage skin, and is suitable for daily use.
Preferably, the plant extract is prepared from the following components in parts by weight:
20-30 parts of mint leaves, 3-5 parts of red seaweed, 5-10 parts of litchi shells, 3-5 parts of field yellow, 5-10 parts of liquorice and 3-5 parts of purslane.
Preferably, the preparation method of the plant extract comprises the following steps:
a1, breaking the wall of an extraction raw material of a plant extract, crushing, pouring an ethanol aqueous solution with the concentration of 10-20% into the wall, immersing the extraction raw material completely, and carrying out constant-temperature water bath at 40-60 ℃ for 20-40min;
and A2, after the water bath is completed, adding deionized water which is 3-5 times of the total amount of the extracted raw materials, heating to 90-100 ℃, then carrying out constant-temperature reaction for 1-2 hours, and filtering the residue powder in a vacuum environment after the liquid level is lower than the extracted raw materials, thus obtaining the plant extract.
By adopting the technical scheme, the plant extract prepared from the components and the raw materials in proportion has a better compounding effect with nano carbon powder, can effectively stimulate pores to shrink and discharge residual blackheads, is green in finished product, has low stimulation, and is suitable for long-time continuous use;
in addition, the plant extract obtained by the extraction method has relatively uniform and stable performance, high effective component retention amount, easier cost control, higher utilization efficiency of the components in the plant extract compared with an ethanol extraction method and a water decoction method, and capability of relieving the greasy feeling of the facial cleanser.
Preferably, the average particle diameter of the nano carbon powder is 20-30nm, and the specific surface area is 200-300m 2 /g
By adopting the technical scheme, the nano carbon powder with the characteristics has remarkable effect on removing blackheads, is not easy to remain in pores, and further reduces the phenomena of large pores or skin injury caused by frequent use.
Preferably, the compound fruit acid is an aqueous solution of one or more of glycolic acid, malic acid, salicylic acid and citric acid.
Preferably, the compound fruit acid comprises the following components in percentage by weight: 5-9% of glycollic acid, 3-5% of malic acid, 3-5% of salicylic acid and the balance of deionized water.
By adopting the technical scheme, the compound fruit acid with the proportion can effectively promote the leading-out and dissolution of blackheads and the peeling of aged cornifi layers, and overcomes the defects that the traditional fruit acid can not be frequently used for skin replacement and the subsequent nursing and protection are complicated.
In a second aspect, the application provides a preparation method of a blackhead-removing facial cleanser, which adopts the following technical scheme: a preparation method of a blackhead-removing facial cleanser comprises the following specific steps:
s1, cleaning all the appliances and sterilizing for later use;
s2, heating the phase A in a water bath, heating to 70-90 ℃, adding the phase B into the phase A, and stirring until A, B two phases are completely dissolved;
s3, additionally taking the phase C, placing the phase C into an emulsifying pot, and stirring at 70-80 ℃ for 10-30r/min until the phase C is completely dissolved;
s4, pumping the A, B mixed phase in the S2 into an emulsifying pot in vacuum, adding the D phase after the pumping is finished, and stirring for 30-60min at 10-20 r/min;
s5, finally, starting a cooling mode, adding the E phase and the blackhead removing component when the temperature is reduced to 40-50 ℃, and continuing to keep the temperature and stir for 10-30min;
s6, sampling and detecting to be qualified, namely the blackhead-removing facial cleanser finished product, and then packaging and warehousing.
By adopting the technical scheme, the blackhead-removing facial cleanser prepared by the steps and the conditions has good blackhead-removing performance, is green and low in stimulation, is suitable for long-term use, and is easy to control in various operation conditions and the quality of a final finished product.
In summary, the application has the following beneficial effects:
1. the application endows the facial cleanser with excellent blackhead removing performance and also has the advantage of low stimulation by compounding the nano carbon powder, the plant extract and the compound fruit acid, and can effectively reduce the recurrence phenomenon of blackheads by long-time continuous use;
2. the plant extract disclosed by the application not only achieves a better compounding effect with nano carbon powder through multi-component compounding, but also can effectively stimulate pores to shrink and discharge residual blackheads, is acceptable to a human body, and is suitable for long-time continuous use;
3. the compound fruit acid with the specific proportion can effectively peel the aged cuticle, promote the blackhead to be guided out and dissolved, can be frequently used compared with the traditional fruit acid for skin replacement, does not need subsequent tedious nursing, and only needs to be washed cleanly;
4. the preparation method provided by the application has the advantages that various conditions are easy to control, the final quality of the obtained product is easy to control, the product has excellent blackhead removing performance, the whole product is green and low in stimulation, and the product is suitable for long-term use, and is easy to treat and rinse.
Detailed Description
The present application will be described in further detail with reference to examples.
Preparation example
Preparation examples 1 to 6
A plant extract, the components and their corresponding weights (kg) are shown in the following table and are prepared by the following preparation method:
a1, breaking the wall of an extraction raw material of a plant extract, crushing, pouring an ethanol aqueous solution with the concentration of 10 percent into the wall, immersing the extraction raw material completely, and then carrying out constant-temperature water bath at 60 ℃ for 40min;
and A2, after the water bath is completed, adding deionized water which is 3 times of the total amount of the extracted raw materials, heating to 100 ℃, then carrying out constant-temperature reaction for 2 hours, and filtering the residue powder in a vacuum environment after the liquid level is lower than the extracted raw materials, thus obtaining the plant extract.
Table: each component of the plant extract in preparation examples 1 to 6 and its weight (kg)
Preparation example 7
The plant extract differs from preparation example 1 in that the preparation steps are as follows:
a1, breaking the wall of an extraction raw material of a plant extract, crushing, pouring an ethanol aqueous solution with the concentration of 10 percent into the wall, immersing the extraction raw material completely, and then carrying out constant-temperature water bath at 40 ℃ for 20min;
and A2, after the water bath is completed, adding deionized water which is 3 times of the total amount of the extracted raw materials, heating to 100 ℃, then carrying out constant-temperature reaction for 2 hours, and filtering the residue powder in a vacuum environment after the liquid level is lower than the extracted raw materials, thus obtaining the plant extract.
Preparation example 8
The plant extract differs from preparation example 1 in that the preparation steps are as follows:
a1, breaking the wall of an extraction raw material of a plant extract, crushing, pouring an ethanol aqueous solution with the concentration of 20 percent into the wall, immersing the extraction raw material completely, and then carrying out constant-temperature water bath at 60 ℃ for 40min;
and A2, after the water bath is completed, adding deionized water which is 3 times of the total amount of the extracted raw materials, heating to 100 ℃, then carrying out constant-temperature reaction for 2 hours, and filtering the residue powder in a vacuum environment after the liquid level is lower than the extracted raw materials, thus obtaining the plant extract.
Preparation example 9
The plant extract differs from preparation example 1 in that the preparation steps are as follows:
a1, breaking the wall of an extraction raw material of a plant extract, crushing, pouring an ethanol aqueous solution with the concentration of 10 percent into the wall, immersing the extraction raw material completely, and then carrying out constant-temperature water bath at 60 ℃ for 40min;
and A2, after the water bath is completed, adding deionized water which is 5 times of the total amount of the extracted raw materials, heating to 100 ℃, then carrying out constant-temperature reaction for 1h, and filtering the residue powder in a vacuum environment after the liquid level is lower than the extracted raw materials, thus obtaining the plant extract.
Preparation examples 10 to 15
A composite fruit acid, the components and their corresponding weights (kg) are shown in the following table:
table: each component of the plant extract in preparation examples 10 to 15 and its weight (kg)
PREPARATION EXAMPLE 16
A blackhead removing component is prepared by blending nano carbon powder, plant extract and compound fruit acid according to the weight ratio of 1:0.3:1.5; wherein the average grain diameter of the nano carbon powder is 30nm, and the specific surface area is 200m 2 /g；
The plant extract was prepared in preparation example 1; the compound fruit acid was prepared in preparation example 10.
Preparation example 17
The blackhead removing component is different from preparation example 16 in that the blackhead removing component is prepared by blending nano carbon powder, plant extract and compound fruit acid according to the weight ratio of 1:0.6:1.8.
PREPARATION EXAMPLE 18
The blackhead removing component is different from preparation example 16 in that the blackhead removing component is prepared by blending nano carbon powder, plant extract and compound fruit acid according to the weight ratio of 1:0.8:2.4.
Preparation example 19
The blackhead removing component is different from preparation example 16 in that the blackhead removing component is prepared by blending nano carbon powder, plant extract and compound fruit acid according to a weight ratio of 1:1.2:2.4.
Preparation example 20
The blackhead removing component is different from preparation example 16 in that the blackhead removing component is prepared by blending nano carbon powder, plant extract and compound fruit acid according to a weight ratio of 1:1.5:2.4.
Preparation examples 21 to 28
The blackhead removing component is different from preparation example 16 in the use of the plant extract, specifically as shown in the following table.
Table: table comparing usage of plant extracts in preparation examples 21 to 29
| Group of | Plant extracts |
| Preparation example 21 | Prepared from preparation example 2 |
| PREPARATION EXAMPLE 22 | Prepared from preparation example 3 |
| Preparation example 23 | Prepared from preparation 4 |
| PREPARATION EXAMPLE 24 | Prepared from preparation 5 |
| Preparation example 25 | From preparation 6 |
| PREPARATION EXAMPLE 26 | Prepared from preparation 7 |
| Preparation example 27 | Prepared from preparation 8 |
| PREPARATION EXAMPLE 28 | Prepared in preparation example 9 |
Preparation examples 29 to 33
The blackhead removing component is different from preparation example 16 in the use condition of the compound fruit acid, and is shown in the following table.
Table: table for comparing usage of Compound fruit acid in preparation examples 29-33
Preparation examples 34 to 36
A cleansing base comprising the following ingredients and their respective weights (per 100 kg):
table: preparation examples 34-36 cleansing base Each component and its corresponding weight (kg)
Wherein ARC03-95FGY and YCS03-30HGY are both cocoylglycine surfactant purchased from Guiguanite chemical (Shanghai) Inc.; HTmuls Dss is glycerol stearate, HTsoft 5688 is isovalerdiol, all purchased from Shanghai Biotech Co., ltd; 10-1-S is polyglycerol stearate, purchased from Shanghai Pu En Biochemical technology Co., ltd; LT-60 is disodium lauryl sulfosuccinate, purchased from Guangzhou Star technology Co., ltd.
Performance test
The blackhead-removing facial cleanser prepared in each example and comparative example is selected as a test object group, volunteers with blackheads at the noses of 20-40 years old are taken as test objects (10 boxes per group, each person releases one box/120 g for free and leaves a contact way, and statistics is carried out in the form of timely releasing questionnaires);
taking 1-2g of facial cleanser each time in the morning and evening, massaging the nose for 3-5min, and testing the blackhead removing effect after continuous use for 7d, 15d and 30d, wherein the specific evaluation criteria are as follows:
blackhead removing effect:
in order to facilitate the return visit statistics, scoring is carried out according to the five-point system, and the test results are counted by taking an average value, wherein 5 is divided into 5 with obvious effects, 4 is divided into 4 with good effects, 3 is divided into 3 with general effects, and 1-2 is divided into 1-2 with basically no effects;
if the subject does not participate in the questionnaire filling, the test subject is automatically counted as 3 points, and the effect is considered to be general, and if the subject has strong stimulation, allergy and other phenomena, the test subject is counted as 0 points, and the test subject is considered to be unqualified.
Note that: the product has refreshing feel and slight irritation after use and washing, such as irritation and allergy during continuous use, and can be used immediately after stopping use and in combination with feedback of me.
Examples
Example 1
A blackhead-removing facial cleanser consists of a facial cleanser matrix and blackhead-removing components in a weight ratio of 1:0.1, wherein the facial cleanser matrix is prepared from preparation example 35, the blackhead-removing components are prepared from preparation example 16, and the following method is adopted for preparation:
s1, cleaning all the appliances and sterilizing for later use;
s2, heating the phase A in a water bath, heating to 80 ℃, adding the phase B into the phase A, and stirring until A, B phases are completely dissolved;
s3, additionally taking the phase C, placing the phase C in an emulsifying pot, and stirring at 80 ℃ and 15r/min until the phase C is completely dissolved;
s4, pumping the A, B mixed phase in the S2 into an emulsifying pot in vacuum, adding the D phase after the pumping is finished, and stirring for 45min at 15 r/min;
s5, finally, starting a cooling mode, adding the E phase and the blackhead removing component when the temperature is reduced to 45 ℃, and continuing to keep the temperature and stir for 20 minutes;
s6, sampling and detecting to be qualified, namely the blackhead-removing facial cleanser finished product, and then packaging and warehousing.
It should be noted that, in other embodiments, the above operation conditions may be other parameter conditions within a limited range, which only have an influence on the final emulsification effect, but have no influence on the final blackhead removal performance, so that no detailed description and corresponding experiments are required.
Example 2
A blackhead-removing facial cleanser is different from example 1 in that the facial cleanser consists of a facial cleanser matrix and blackhead-removing components in a weight ratio of 1:0.2.
Example 3
A blackhead-removing facial cleanser is different from example 1 in that the facial cleanser consists of a facial cleanser matrix and blackhead-removing components in a weight ratio of 1:0.3.
Example 4
A blackhead-removing facial cleanser differs from example 1 in that a facial cleanser base was prepared from preparation example 35.
Example 5
A blackhead-removing facial cleanser differs from example 1 in that a facial cleanser base was prepared from preparation 36.
Comparative example 1
A facial cleanser was different from example 1 in that it did not contain a blackhead removing component.
The groups to which the facial washes of examples 1 to 5 and comparative example 1 described above were applied were extracted, and their blackhead removal performance was measured according to the above-described measurement procedures and measurement criteria, and the average value of the measurement results was recorded in the following table.
Table: examples 1 to 5, comparative example 1 Performance test results (score)
As can be seen from the above table, the facial cleanser prepared in examples 1 to 5 has excellent blackhead removing performance, and the 7d blackhead removing effect is 4.2 to 4.4 minutes; 15d, the blackhead removing effect is 4.5-4.6 minutes; the blackhead removing effect is 4.7-4.9 minutes after 30 days; has a remarkable effect compared with comparative example 1;
the reason for this analysis may be due to: the blackhead removing component can not only play a basic role in removing blackhead effect through the adsorption of the basis of the nano carbon powder, but also play a synergistic effect with the nano carbon powder through the stimulation of the composite fruit acid to the skin, so that the guiding-out and dissolution of the blackhead are accelerated, and a remarkable blackhead removing effect is achieved.
As can be seen from the table, the blackhead removing facial cleanser is suitable for long-term use, and has different degrees of blackhead removing performance along with the extension of the use time, thereby being beneficial to reducing the recurrence of blackheads; the corresponding improvement in blackhead removal performance for comparative example 1 was associated with good cleaning habits.
The reason for this analysis may be due to: the plant extract can stimulate pores to shrink and strengthen the removal effect of blackheads by means of strong adsorptivity and dispersibility of nano carbon powder so as to achieve the purpose of reducing blackheads and recurrence, and the plant extract can also repair skin, is sustainable to use compared with pure fruit acid skin replacement, and basically has no side effect.
In addition, the table shows that the facial cleanser formed by the components with the proportion can effectively endow the facial cleanser with excellent blackhead removing performance, has the advantages of low stimulation and low sensitization, and is suitable for long-term continuous use; the dosage of each component of the cleansing matrix is basically unaffected;
under the condition that the consumption of the facial substrate is certain, the blackhead removing effect of the facial substrate is correspondingly improved along with the increase of the consumption of blackhead removing components, and then the facial substrate tends to be saturated, see the examples 1-3; if the amount of the blackhead removing component is continuously increased (the amount ratio is 0.5), the blackhead removing effect cannot be continuously improved, and stronger irritation and sensitization (a mouse skin test) can be caused to the skin, so that the skin is clearly known to be harmful, and a corresponding comparative example is not designed.
Examples 6 to 9
A blackhead-removing facial cleanser differs from example 1 in that the blackhead-removing components are used differently, and the specific correspondence is shown in the following table.
Table: use condition comparison Table of blackhead removing Components in examples 6 to 9
| Group of | Blackhead removing component |
| Example 6 | Prepared in preparation example 17 |
| Example 7 | From preparation 18 |
| Example 8 | From preparation 19 |
| Example 9 | From preparation example 20 |
Comparative example 2
A facial cleanser is different from the facial cleanser in example 1 in that the blackhead removing component only comprises nano carbon powder, and is an adsorption type blackhead removing facial cleanser.
Comparative example 3
A facial cleanser is different from example 1 in that the blackhead removing component only comprises compound fruit acid, and is a skin-changing blackhead removing facial cleanser.
Comparative example 4
A facial cleanser differs from example 1 in that only a plant extract is included in the blackhead removing component.
Comparative example 5
A facial cleanser differs from example 1 in that the blackhead removing component does not include a plant extract.
The groups to which the facial washes of examples 6 to 9 and comparative examples 2 to 5 described above were applied were extracted, and their blackhead removing performance was tested according to the above-described measurement procedures and measurement criteria, and the test results were averaged and presented in the following table.
Table: examples 6 to 9, comparative examples 2 to 5, results of performance test (minutes)
As can be seen from the above table, the facial cleanser prepared in examples 1 and 6-9 has excellent blackhead removing performance, and the blackhead removing effect of 7d is 4.2-4.4 minutes; 15d, the blackhead removing effect is 4.5-4.6 minutes; the blackhead removing effect is 4.7-4.8 minutes after 30 days; to a different extent than in comparative examples 2-5;
therefore, the composition of the blackhead removing component in the proportion has the optimal compounding effect of the nano carbon powder, the plant extract and the compound fruit acid, can effectively remove blackheads, is not easy to damage skin, is suitable for daily use, and has increased blackhead removing effect along with the extension of the use time.
Furthermore, as can be seen from the data of comparative examples 2 to 5, which are incorporated in the above table, the use of either single or partial components does not achieve the desired effect, and the following analysis is specific:
the group of only using nano carbon powder and/or composite fruit acid has obvious effect only in 7 days, is not suitable for long-term use, and can cause negative effects along with the extension of the use time;
the reasons for this analysis may be: the effect of removing blackheads is affected by the blocking of pores by nano carbon powder; or excessive exfoliation of the skin horny layer gives the user a feeling of strong irritation or allergy to 0 point;
the plant extracts are only used, the effect of removing blackheads of the whole d1 is weak, the plant extracts are suitable for long-term maintenance and use, the plant extracts are improved to a certain extent compared with 7d in 15-30d, and the analysis is probably due to the improvement of skin epidermis microecology, so that the plant extracts are not easy to secrete grease.
Examples 10 to 17
A blackhead-removing facial cleanser differs from example 1 in that the blackhead-removing components are used differently, and the specific correspondence is shown in the following table.
Table: use condition comparison Table of blackhead removing component in examples 10 to 17
| Group of | Blackhead removing component |
| Example 10 | Prepared from preparation 21 |
| Example 11 | From preparation 22 |
| Example 12 | From preparation 23 |
| Example 13 | From preparation 24 |
| Example 14 | From preparation 25 |
| Example 15 | From preparation 26 |
| Example 16 | From preparation 27 |
| Example 17 | From preparation 28 |
The group of facial washes used in examples 10-17 above was extracted, and their blackhead removal performance was measured according to the above-mentioned measurement procedure and measurement standard, and the average value of the measurement results was recorded in the following table.
Table: examples 10 to 18 Performance test results (score)
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As can be seen from the above table, the facial cleanser prepared in examples 1 and 10-17 has excellent blackhead removing performance, and the 7d blackhead removing effect is 4.2-4.3 minutes; 15d, the blackhead removing effect is 4.5-4.7 minutes; the blackhead removing effect is 4.7-4.9 minutes after 30 days;
the plant extract prepared from the components and the extraction raw materials in the proportion has a better compounding effect with nano carbon powder, can effectively stimulate pores to shrink and discharge residual blackheads, is green in finished product, has low stimulation, and is suitable for long-time continuous use, wherein the embodiment 12 is the most preferred embodiment;
the reason for this analysis may be due to the nature of the components of the preparation:
wherein the mint leaves mainly have the effects of stimulating skin and promoting pore shrinkage; the red seaweed can maintain capillary vessels around pores, so that damage to the pores is reduced; purslane and Tian Huangqi have antibacterial and anti-inflammatory effects, and are helpful for improving skin microecology; the litchi shells and the liquorice can effectively relieve the side effect of the fruit acid and the irritation of the mint leaves;
in addition, as is clear from examples 1, 15-17, the plant extract obtained by the above extraction method has relatively uniform and stable properties, high retention of effective components, and easy cost control of the whole process, and can fully utilize the components in the plant extract compared with ethanol extraction and water decoction.
Examples 18 to 22
A blackhead-removing facial cleanser differs from example 1 in that the blackhead-removing components are used differently, and the specific correspondence is shown in the following table.
Table: use condition comparison Table of blackhead removing component in examples 18 to 22
| Group of | Blackhead removing component |
| Example 18 | From preparation 29 |
| Example 19 | Prepared from preparation 30 |
| Example 20 | From preparation 31 |
| Example 21 | From preparation 32 |
| Example 22 | From preparation 33 |
The group of facial washes used in examples 18-22 above was extracted and tested for blackhead removal performance according to the above-described measurement procedure and measurement criteria, and the average of the test results was recorded in the following table.
Table: examples 18 to 22 Performance test results (score)
As can be seen from the above table, the facial cleanser prepared in examples 1 and 18-22 has excellent blackhead removing performance, and the 7d blackhead removing effect is 4.2-4.4 minutes; 15d, the blackhead removing effect is 4.5-4.6 minutes; the blackhead removing effect is 4.6-4.8 minutes after 30 days;
the compound fruit acid prepared by the proportion can effectively promote the leading-out and dissolution of blackheads and the peeling of aged corneas, and overcomes the defects that the traditional fruit acid can not be frequently used for skin replacement and the subsequent nursing and protection are complicated, wherein the embodiment 19 is a preferred example.
The present embodiment is only for explanation of the present application and is not to be construed as limiting the present application, and modifications to the present embodiment, which may not creatively contribute to the present application as required by those skilled in the art after reading the present specification, are all protected by patent laws within the scope of claims of the present application.
Claims (4)
1. The blackhead-removing facial cleanser comprises a facial cleanser matrix and blackhead-removing components, and is characterized in that the blackhead-removing components are prepared by blending (0.6-1.2) 1.8-2.4 of nano carbon powder, plant extracts and composite fruit acid according to the weight ratio;
the dosage of the cleansing matrix and the blackhead removing component is 1 (0.1-0.3) in weight ratio;
the plant extract is prepared from the following components in parts by weight:
20-30 parts of mint leaves, 3-5 parts of red seaweed, 5-10 parts of litchi shells, 3-5 parts of field yellow, 5-10 parts of liquorice and 3-5 parts of purslane;
the preparation method of the plant extract comprises the following steps:
a1, breaking the wall of an extraction raw material of a plant extract, crushing, pouring an ethanol aqueous solution with the concentration of 10-20% into the wall, immersing the extraction raw material completely, and carrying out constant-temperature water bath at 40-60 ℃ for 20-40min;
and A2, after the water bath is completed, adding deionized water which is 3-5 times of the total amount of the extracted raw materials, heating to 90-100 ℃, then carrying out constant-temperature reaction for 1-2 hours, and filtering the residue powder in a vacuum environment after the liquid level is lower than the extracted raw materials, thus obtaining the plant extract.
2. The blackhead removal facial cleanser according to claim 1, characterized in that the average particle diameter of the nano carbon powder is 20-30nm, and the specific surface area is 200-300m 2 /g。
3. The blackhead removal facial cleanser of claim 1, wherein the complex fruit acid is an aqueous solution of two or more of glycolic acid, malic acid, salicylic acid, and citric acid.
4. A blackhead removal facial cleanser according to claim 3, characterized in that the compound fruit acid consists of the following components in weight percentage: 5-9% of glycollic acid, 3-5% of malic acid, 3-5% of salicylic acid and the balance of deionized water.
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