CN115227585A - Preparation method and process of oily solid cosmetic - Google Patents
Preparation method and process of oily solid cosmetic Download PDFInfo
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- CN115227585A CN115227585A CN202210938224.1A CN202210938224A CN115227585A CN 115227585 A CN115227585 A CN 115227585A CN 202210938224 A CN202210938224 A CN 202210938224A CN 115227585 A CN115227585 A CN 115227585A
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- 239000002537 cosmetic Substances 0.000 title claims abstract description 29
- 239000007787 solid Substances 0.000 title claims abstract description 27
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 230000008569 process Effects 0.000 title abstract description 6
- 239000000341 volatile oil Substances 0.000 claims abstract description 37
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- 239000002994 raw material Substances 0.000 claims abstract description 30
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- 244000025254 Cannabis sativa Species 0.000 claims abstract description 28
- 240000000560 Citrus x paradisi Species 0.000 claims abstract description 26
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 22
- 238000004945 emulsification Methods 0.000 claims abstract description 20
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- 238000000034 method Methods 0.000 claims abstract description 18
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- 238000006243 chemical reaction Methods 0.000 claims description 30
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- KIUKXJAPPMFGSW-DNGZLQJQSA-N (2S,3S,4S,5R,6R)-6-[(2S,3R,4R,5S,6R)-3-Acetamido-2-[(2S,3S,4R,5R,6R)-6-[(2R,3R,4R,5S,6R)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2-carboxylic acid Chemical compound CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 KIUKXJAPPMFGSW-DNGZLQJQSA-N 0.000 claims description 11
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- 239000003963 antioxidant agent Substances 0.000 claims description 10
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- 229930003935 flavonoid Natural products 0.000 claims description 10
- 150000002215 flavonoids Chemical class 0.000 claims description 10
- 235000017173 flavonoids Nutrition 0.000 claims description 10
- 239000003906 humectant Substances 0.000 claims description 10
- 238000004806 packaging method and process Methods 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 8
- QTWJRLJHJPIABL-UHFFFAOYSA-N 2-methylphenol;3-methylphenol;4-methylphenol Chemical compound CC1=CC=C(O)C=C1.CC1=CC=CC(O)=C1.CC1=CC=CC=C1O QTWJRLJHJPIABL-UHFFFAOYSA-N 0.000 claims description 7
- 229940069521 aloe extract Drugs 0.000 claims description 7
- 125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 claims description 7
- 230000035484 reaction time Effects 0.000 claims description 5
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- 238000004519 manufacturing process Methods 0.000 claims description 3
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- 235000014787 Vitis vinifera Nutrition 0.000 claims 3
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- 241000219784 Sophora Species 0.000 claims 1
- 229930003944 flavone Natural products 0.000 claims 1
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- 208000002874 Acne Vulgaris Diseases 0.000 abstract description 4
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- 240000000785 Tagetes erecta Species 0.000 abstract 1
- 238000001914 filtration Methods 0.000 description 6
- DCXXMTOCNZCJGO-UHFFFAOYSA-N Glycerol trioctadecanoate Natural products CCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC DCXXMTOCNZCJGO-UHFFFAOYSA-N 0.000 description 4
- 239000004519 grease Substances 0.000 description 4
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Images
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0216—Solid or semisolid forms
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/347—Phenols
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- A—HUMAN NECESSITIES
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/645—Proteins of vegetable origin; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/925—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of animal origin
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/981—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of mammals or bird
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- A—HUMAN NECESSITIES
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- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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- Cosmetics (AREA)
Abstract
The invention discloses a preparation method and a process of oily solid cosmetics, wherein the preparation method of the cosmetics comprises the following steps: step one, pretreating plant raw materials, namely pretreating marigold, rose, alfalfa whole grass and grape fruits; step two, pre-emulsification, namely preparing an emulsifier by using ionized water, coconut oil, glycerol, natural triglyceride and glyceryl stearate; step three, preparing essential oil, namely preparing the pretreated plant raw materials into the essential oil; the invention is prepared from natural vegetable oil, is green and safe, and has no stimulation to skin; by adding the lanolin oil, the coconut oil, the glycerin, the milk and the like, the whitening and oil hole-removing oil has good effects; but also has good effects of lightening pigmentation, repairing sensitive skin, and repairing scars such as acne marks and pockmarks left by pimples and whelk.
Description
Technical Field
The invention relates to the technical field of cosmetics, in particular to a preparation method and a process of an oily solid cosmetic.
Background
In the metabolism process of human body, various free radicals are formed; among them, 95% of free radicals are harmful oxygen radicals, which attack cells to generate oxidation, damage cell functions, reduce human vitality, cause aging phenomena such as wrinkles and spots on the face, and make the skin dark. In addition, when the temperature is high in summer, the moisture of the skin is seriously lost, the skin can secrete a large amount of grease to prevent further loss of moisture, excessive grease is excessively secreted to cause the excessive grease to stay on the surface layer of the skin, pores can be blocked if the skin is not cleaned in time to form acne, and the acne and the like cannot be caused after the skin is not cleaned; meanwhile, the grease can easily adsorb dust, peroxide and the like in the air, so that the skin aging can be accelerated, and the skin shows dark and lusterless; therefore, maintaining skin health is a very interesting problem for every girl, and therefore we propose a preparation method and a process of an oily solid cosmetic.
Disclosure of Invention
The invention aims to solve the defects in the prior art and provides a preparation method and a process of an oily solid cosmetic.
In order to achieve the purpose, the invention adopts the following technical scheme:
a method for preparing oily solid cosmetic comprises the following steps:
step one, pretreating plant raw materials, namely pretreating marigold, rose, alfalfa whole grass and grape fruits;
step two, pre-emulsification, namely preparing an emulsifier from ionized water, coconut oil, glycerol, natural triglyceride and glyceryl stearate;
step three, preparing essential oil, namely preparing the pretreated plant raw materials into the essential oil;
emulsifying, namely emulsifying deionized water, plant essential oil, hyaluronic acid, milk, vaseline, lanolin oil and the flos sophorae flavonoid extract by using the prepared emulsifier to obtain an emulsion;
step five, preparing mixed emulsion, namely adding lauric acid, stearic acid, special additive solution, antioxidant, humectant and vegetable protein into the emulsion, and then stirring and mixing to obtain the mixed emulsion;
removing impurities, namely removing impurities from the mixed emulsion through a filter screen;
step seven, concentration, namely concentrating the mixed emulsion after impurity removal;
and step eight, packaging and warehousing, namely packaging the concentrated emulsion and warehousing.
As further preferable in the present technical solution: in the first step, the calendula, the rose, the alfalfa whole grass and the grape fruit are cleaned and then placed at the temperature of 3-10 ℃ for storage for 1-4 hours, and then the cleaned calendula, the rose, the alfalfa whole grass and the grape fruit are respectively cut into pieces to obtain the cut calendula, rose, alfalfa whole grass and grape fruit raw materials.
As further preferable in the present technical solution: in the second step, a proper amount of ionized water, coconut oil, glycerol, natural triglyceride and glyceryl stearate are put into an emulsification reaction kettle, the rotation speed of a main shaft of the emulsification reaction kettle is 600-800r/min, the time is 50-120min, the internal temperature is 40-50 ℃, and the internal pressure is 4-6MPa, so that the emulsion is obtained.
As further preferable in the present technical solution: in the third step, the cut raw materials of the calendula, the rose, the alfalfa and the grape fruit are put into a squeezer, the rotating speed of a main shaft of the squeezer is 60-100r/min, the squeezing temperature is 60-80 ℃, and the squeezing time is 30-50min, so that crude essential oil mixed liquid is obtained, and the crude essential oil mixed liquid is filtered through a filter screen of 300-500 meshes and filtered to obtain the essential oil mixed liquid.
As further preferable in the present technical solution: in the fourth step, deionized water, hyaluronic acid, flos sophorae flavonoid and vaseline are weighed according to the proportion and then sequentially added into a stirrer to be stirred, wherein the rotating speed of a main shaft of the stirrer is 80-100r/min for 15-30min, then the mixture is added into a reaction kettle, then the mixed liquid of milk, lanolin oil and essential oil is added into the reaction kettle according to the proportion, the rotating speed of the main shaft of the reaction kettle is 800-1000r/min for 20-40min, the internal temperature is 60-70 ℃, and the internal pressure is 1-3MPa, so that a solvent is obtained, the solvent is cooled and stands for 4-6h for later use, then the solvent is injected into an emulsifying machine, and then pre-emulsified liquid and thickening agent are added until complete emulsification is achieved.
As further preferable in the present technical solution: and fifthly, putting the lauric acid and stearic acid raw materials into a container, heating to 80-90 ℃ to completely dissolve the lauric acid and stearic acid raw materials, then adding the mixed emulsion after deslagging into a stirrer to stir and mix, wherein the rotating speed of a main shaft of the stirrer is 400-600r/min, the time is 60-90min, the liquid obtained after uniform mixing is an oil phase, then adding the special additive liquid, the antioxidant, the humectant and the vegetable protein, and mixing and stirring again, wherein the rotating speed of the main shaft of the stirrer is 200-500r/min, and the time is 20-30min.
As further preferable in the present technical solution: and seventhly, adding the mixed solution into a concentrator to be concentrated into cream, wherein the concentration temperature is 80-100 ℃, and the concentration time is 15-25h.
The invention also provides a preparation process of the oily solid cosmetic, wherein the special additive solution comprises the following components: tert-butyl, methyl phenol, aloe extract, and vegetable protein extract.
As further preferable in the present technical solution: adding appropriate amount of tert-butyl, methyl phenol, aloe extract, and vegetable protein extract into a reaction kettle, placing the kettle at main shaft rotation speed of 500-600r/min, reaction time of 20-40min, internal temperature of 40-50 deg.C, and internal pressure of 0.3-0.7MPa into a high pressure steam furnace, distilling, and condensing to obtain mixed steam, wherein the pressure of the high pressure steam furnace is controlled at 0.2-0.4MPa, and the mixed steam is condensed to obtain the special additive solution.
Compared with the prior art, the invention has the beneficial effects that:
the invention is prepared from natural vegetable oil, is green and safe, and has no stimulation to skin; by adding the lanolin oil, the coconut oil, the glycerol, the milk and the like, the whitening and oil-hole-removing oil has good whitening and oil-hole-removing effects; but also has good effects of lightening pigmentation, repairing sensitive skin, and repairing scars such as acne marks and pockmarks left by pimples and whelks.
Drawings
FIG. 1 is a flow chart of a method and a process for preparing an oily solid cosmetic provided by the present invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments.
Example one
Referring to fig. 1, a method for preparing an oily solid cosmetic includes the steps of:
step one, pretreating plant raw materials, namely pretreating calendula, roses, alfalfa whole grass and grape fruits, cleaning the calendula, the roses, the alfalfa whole grass and the grape fruits, placing the cleaned calendula, the roses, the alfalfa whole grass and the grape fruits at a temperature of 4 ℃ for storage for 3 hours, and then respectively cutting the cleaned calendula, the roses, the alfalfa whole grass and the grape fruits into pieces to obtain the cut calendula, rose, alfalfa whole grass and grape fruit raw materials;
step two, pre-emulsifying, namely preparing an emulsifier by using ionized water, coconut oil, glycerol, natural triglyceride and glyceryl stearate, and putting a proper amount of ionized water, coconut oil, glycerol, natural triglyceride and glyceryl stearate into an emulsification reaction kettle, wherein the main shaft rotation speed of the emulsification reaction kettle is 780r/min, the time is 110min, the internal temperature is 50 ℃, and the internal pressure is 5MPa, so that an emulsion is obtained;
step three, preparing essential oil, namely preparing the pretreated plant raw materials into the essential oil, putting the cut raw materials of the calendula, the rose, the alfalfa whole grass and the grape fruit into a squeezer, wherein the rotating speed of a main shaft of the squeezer is 80r/min, the squeezing temperature is 70 ℃, and the squeezing time is 45min, so that a crude essential oil mixed solution is obtained, filtering the crude essential oil mixed solution through a 450-mesh filter screen, and filtering to obtain an essential oil mixed solution;
emulsifying, namely emulsifying deionized water, plant essential oil, hyaluronic acid, milk, vaseline, lanolin oil and a flos sophorae flavonoid extract by using a prepared emulsifier to obtain an emulsion, weighing the deionized water, hyaluronic acid, flos sophorae flavonoid and vaseline according to a ratio, sequentially adding the weighed substances into a stirrer to stir, wherein the rotating speed of a main shaft of the stirrer is 90r/min and the time is 25min, then adding the obtained mixture into a reaction kettle, adding a mixed solution of the milk, the lanolin oil and the essential oil according to the ratio into the reaction kettle, the rotating speed of a main shaft of the reaction kettle is 900r/min and the time is 35min, the internal temperature is 67 ℃, and the internal pressure is 2.6MPa to obtain a solvent, cooling and standing for 5 hours, injecting the solvent into the emulsifier for later use, and then adding the pre-emulsified liquid and a thickener until complete emulsification is achieved;
step five, preparing a mixed emulsion, adding lauric acid, stearic acid, special additive solution, antioxidant, humectant and vegetable protein into the emulsion, stirring and mixing to obtain the mixed emulsion, putting the lauric acid and stearic acid raw materials into a container, heating to 70 ℃ to completely dissolve the lauric acid and stearic acid raw materials, then adding the mixed emulsion after deslagging into a stirrer, stirring and mixing, wherein the rotating speed of a main shaft of the stirrer is 560r/min for 75min, the liquid obtained after uniform mixing is an oil phase, then adding the special additive solution, antioxidant, humectant and vegetable protein, and mixing and stirring again, wherein the rotating speed of the main shaft of the stirrer is 300r/min for 30min;
removing impurities, namely removing impurities from the mixed emulsion through a filter screen;
concentrating, namely concentrating the mixed emulsion after impurity removal, adding the mixed solution into a concentrator, and concentrating into frost, wherein the concentration temperature is 90 ℃, and the concentration time is 20 hours;
and step eight, packaging and warehousing, namely packaging the concentrated emulsion and warehousing.
The embodiment also discloses a preparation process of the oily solid cosmetic, wherein the special additive solution comprises the following components: the method comprises the steps of adding a proper amount of tert-butyl, methyl phenol, aloe extract and vegetable protein extract into a reaction kettle, controlling the rotation speed of a main shaft of the kettle to be 600r/min, the reaction time to be 40min, the internal temperature to be 45 ℃ and the internal pressure to be 0.6MPa, then putting the kettle into a high-pressure steam furnace for distillation, controlling the pressure of the high-pressure steam furnace to be 0.3MPa, thus obtaining mixed steam, and then condensing the mixed steam to obtain the special additive solution.
Example two
Referring to fig. 1, a method for preparing an oily solid cosmetic includes the steps of:
step one, pretreating plant raw materials, namely pretreating calendula, roses, alfalfa whole grass and grape fruits, cleaning the calendula, the roses, the alfalfa whole grass and the grape fruits, then placing the cleaned calendula, the roses, the alfalfa whole grass and the grape fruits at the temperature of 0 ℃ for storage for 2 hours, and then respectively cutting the cleaned calendula, the roses, the alfalfa whole grass and the grape fruits into pieces to obtain the cut calendula, rose, alfalfa whole grass and grape fruit raw materials;
step two, pre-emulsification, namely preparing an emulsifier by using ionized water, coconut oil, glycerol, natural triglyceride and stearin, and putting a proper amount of ionized water, coconut oil, glycerol, natural triglyceride and stearin into an emulsification reaction kettle, wherein the main shaft rotation speed of the emulsification reaction kettle is 700r/min, the time is 100min, the internal temperature is 40 ℃, and the internal pressure is 4MPa, so as to obtain an emulsion;
step three, preparing essential oil, namely preparing the pretreated plant raw materials into the essential oil, putting the cut raw materials of the calendula, the rose, the alfalfa whole grass and the grape fruit into a squeezer, wherein the rotating speed of a main shaft of the squeezer is 60r/min, the squeezing temperature is 60 ℃, and the squeezing time is 30min, so that crude essential oil mixed liquid is obtained, filtering the crude essential oil mixed liquid through a 300-mesh filter screen, and filtering to obtain the essential oil mixed liquid;
emulsifying, namely emulsifying deionized water, plant essential oil, hyaluronic acid, milk, vaseline, lanolin oil and a flos sophorae flavonoid extract by using a prepared emulsifier to obtain an emulsion, weighing the deionized water, hyaluronic acid, flos sophorae flavonoid and vaseline according to a ratio, sequentially adding the weighed substances into a stirrer to stir, wherein the rotating speed of a main shaft of the stirrer is 85r/min and the time is 30min, then adding the obtained mixture into a reaction kettle, adding a mixed solution of the milk, the lanolin oil and the essential oil according to the ratio into the reaction kettle, the rotating speed of a main shaft of the reaction kettle is 800r/min and the time is 40min, the internal temperature is 60 ℃, and the internal pressure is 1MPa, so as to obtain a solvent, cooling and standing for 5 hours, injecting the solvent into the emulsifier for later use, and adding a pre-emulsifying liquid and a thickening agent until complete emulsification is achieved;
step five, preparing a mixed emulsion, adding lauric acid, stearic acid, special additive solution, antioxidant, humectant and vegetable protein into the emulsion, stirring and mixing to obtain the mixed emulsion, putting the lauric acid and stearic acid raw materials into a container, heating to 85 ℃ to completely dissolve the lauric acid and stearic acid raw materials, then adding the mixed emulsion after deslagging into a stirrer, stirring and mixing, wherein the rotating speed of a main shaft of the stirrer is 500r/min for 80min, the liquid obtained after uniform mixing is an oil phase, then adding the special additive solution, antioxidant, humectant and vegetable protein, and mixing and stirring again, wherein the rotating speed of the main shaft of the stirrer is 500r/min for 20min;
removing impurities, namely removing impurities from the mixed emulsion through a filter screen;
concentrating, namely concentrating the mixed emulsion after impurity removal, adding the mixed solution into a concentrator, and concentrating into frost at the concentration temperature of 80 ℃ for 24 hours;
and step eight, packaging and warehousing, namely packaging the concentrated emulsion and warehousing.
The embodiment also discloses a preparation process of the oily solid cosmetic, wherein the special additive solution comprises the following components: the method comprises the steps of adding a proper amount of tert-butyl, methyl phenol, aloe extract and vegetable protein extract into a reaction kettle, controlling the rotation speed of a main shaft of the kettle to be 600r/min, the reaction time to be 40min, the internal temperature to be 50 ℃ and the internal pressure to be 0.7MPa, then putting the kettle into a high-pressure steam furnace for distillation, controlling the pressure of the high-pressure steam furnace to be 0.5MPa, thus obtaining mixed steam, and then condensing the mixed steam to obtain the special additive solution.
EXAMPLE III
Referring to fig. 1, a method for preparing an oily solid cosmetic includes the steps of:
step one, pretreating plant raw materials, namely pretreating calendula, roses, alfalfa whole grass and grape fruits, cleaning the calendula, the roses, the alfalfa whole grass and the grape fruits, placing the cleaned calendula, the roses, the alfalfa whole grass and the grape fruits at the temperature of 10 ℃ for storage for 4 hours, and then respectively cutting the cleaned calendula, the roses, the alfalfa whole grass and the grape fruits into pieces to obtain the cut calendula, rose, alfalfa whole grass and grape fruit raw materials;
step two, pre-emulsification, namely preparing an emulsifier by using ionized water, coconut oil, glycerol, natural triglyceride and stearin, and putting a proper amount of ionized water, coconut oil, glycerol, natural triglyceride and stearin into an emulsification reaction kettle, wherein the rotating speed of a main shaft of the emulsification reaction kettle is 800r/min, the time is 50min, the internal temperature is 50 ℃, and the internal pressure is 4-6MPa, so that an emulsion is obtained;
step three, preparing essential oil, namely preparing the pretreated plant raw materials into the essential oil, putting the cut raw materials of the calendula, the rose, the alfalfa whole grass and the grape fruit into a squeezer, wherein the rotating speed of a main shaft of the squeezer is 100r/min, the squeezing temperature is 70 ℃, and the squeezing time is 35min, so that crude essential oil mixed liquid is obtained, filtering the crude essential oil mixed liquid through a 430-mesh filter screen, and filtering to obtain the essential oil mixed liquid;
step four, emulsifying, namely emulsifying deionized water, plant essential oil, hyaluronic acid, milk, vaseline, lanolin oil and the flos sophorae flavonoid extract by using a prepared emulsifier to obtain an emulsion, weighing the deionized water, hyaluronic acid, flos sophorae flavonoid and vaseline according to the proportion, sequentially adding the weighed deionized water, hyaluronic acid, flos sophorae flavonoid and vaseline into a stirrer to stir, wherein the rotating speed of a main shaft of the stirrer is 90r/min and the time is 25min, adding the obtained mixture into a reaction kettle, adding the milk, lanolin oil and essential oil mixed solution into the reaction kettle according to the proportion, the rotating speed of a main shaft of the reaction kettle is 950r/min and the time is 40min, the internal temperature is 60 ℃, and the internal pressure is 1MPa, so as to obtain a solvent, cooling and standing for later for 6 hours, then injecting the solvent into the emulsifier, and adding the pre-emulsified liquid and a thickener until complete emulsification is achieved;
step five, preparing a mixed emulsion, adding lauric acid, stearic acid, special additive solution, antioxidant, humectant and vegetable protein into the emulsion, stirring and mixing to obtain the mixed emulsion, putting the lauric acid and stearic acid raw materials into a container, heating to 80 ℃ to completely dissolve the lauric acid and stearic acid raw materials, then adding the mixed emulsion after deslagging into a stirrer, stirring and mixing, wherein the main shaft rotation speed of the stirrer is 600r/min for 60min, the liquid obtained after uniform mixing is an oil phase, then adding the special additive solution, antioxidant, humectant and vegetable protein, mixing and stirring again, wherein the main shaft rotation speed of the stirrer is 200r/min for 30min;
removing impurities, namely removing impurities from the mixed emulsion through a filter screen;
concentrating, namely concentrating the mixed emulsion after impurity removal, adding the mixed solution into a concentrator, and concentrating into frost, wherein the concentration temperature is 100 ℃, and the concentration time is 22 hours;
and step eight, packaging and warehousing, namely packaging the concentrated emulsion and warehousing.
The embodiment also discloses a preparation process of the oily solid cosmetic, wherein the special additive solution comprises the following components: the method comprises the steps of adding a proper amount of tert-butyl, methyl phenol, aloe extract and vegetable protein extract into a reaction kettle, controlling the rotation speed of a main shaft of the kettle to be 600r/min, the reaction time to be 40min, the internal temperature to be 50 ℃ and the internal pressure to be 0.7MPa, then putting the kettle into a high-pressure steam furnace for distillation, controlling the pressure of the high-pressure steam furnace to be 0.4MPa, thus obtaining mixed steam, and then condensing the mixed steam to obtain the special additive solution.
For the oily solid cosmetics prepared in examples one to three, experimental data are shown in the following table, compared with conventional oily solid cosmetics:
as can be seen from the above table, the oily solid cosmetic prepared by the present invention has significantly improved effects of repairing sensitive skin, tightening wrinkle, anti-aging and whitening, and is one preferred embodiment.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (9)
1. A method for preparing an oily solid cosmetic is characterized by comprising the following steps:
step one, pretreating plant raw materials, namely pretreating marigold, rose, alfalfa whole grass and grape fruits;
step two, pre-emulsification, namely preparing an emulsifier by using ionized water, coconut oil, glycerol, natural triglyceride and glyceryl stearate;
step three, preparing essential oil, namely preparing the pretreated plant raw materials into the essential oil;
emulsifying, namely emulsifying deionized water, plant essential oil, hyaluronic acid, milk, vaseline, lanolin oil and the flos sophorae flavonoid extract by using the prepared emulsifier to obtain an emulsion;
step five, preparing mixed emulsion, namely adding lauric acid, stearic acid, special additive solution, antioxidant, humectant and vegetable protein into the emulsion, and then stirring and mixing to obtain the mixed emulsion;
removing impurities, namely removing impurities from the mixed emulsion through a filter screen;
step seven, concentration, namely concentrating the mixed emulsion after impurity removal;
and step eight, packaging and warehousing, namely packaging the concentrated emulsion and warehousing.
2. The method for preparing an oily solid cosmetic according to claim 1, wherein in the first step, the calendula officinalis, the roses, the alfalfa whole grass and the grape berries are cleaned and stored at a temperature of 3-10 ℃ for 1-4h, and then the cleaned calendula officinalis, roses, alfalfa whole grass and grape berries are respectively cut into pieces to obtain the cut calendula officinalis, roses, alfalfa whole grass and grape berries.
3. The method for preparing an oily solid cosmetic according to claim 2, wherein in the second step, a proper amount of ionized water, coconut oil, glycerin, natural triglyceride and glyceryl stearate is added into an emulsification reaction vessel, the rotation speed of a main shaft of the emulsification reaction vessel is 600-800r/min, the time is 50-120min, the internal temperature is 40-50 ℃, and the internal pressure is 4-6MPa, thereby obtaining the emulsion.
4. The method for preparing an oily solid cosmetic as claimed in claim 3, wherein in the third step, the cut raw materials of the calendula, the rose, the alfalfa whole grass and the grape fruit are put into a squeezing machine, the rotating speed of a main shaft of the squeezing machine is 60-100r/min, the squeezing temperature is 60-80 ℃, and the squeezing time is 30-50min, so as to obtain a crude essential oil mixed solution, and the crude essential oil mixed solution is filtered through a 300-500 mesh filter screen to obtain an essential oil mixed solution.
5. The method for preparing an oily solid cosmetic according to claim 4, wherein in the fourth step, deionized water, hyaluronic acid, flavones of sophora flower and vaseline are weighed according to the ratio and then sequentially added into a stirrer for stirring, wherein the rotation speed of a main shaft of the stirrer is 80-100r/min for 15-30min, then the mixture is added into a reaction kettle, then the mixture of milk, lanolin oil and essential oil is added into the reaction kettle according to the ratio, the rotation speed of the main shaft of the reaction kettle is 800-1000r/min for 20-40min, the internal temperature is 60-70 ℃, and the internal pressure is 1-3MPa, so as to obtain the solvent, the solvent is cooled and kept stand for 4-6h, then the solvent is injected into an emulsifier, and then the pre-emulsion and the thickener are added until complete emulsification is achieved.
6. The method for producing an oily solid cosmetic as claimed in claim 5, wherein in the fifth step, the lauric acid and stearic acid raw materials are put into a container and heated to 80-90 ℃ to be completely dissolved, then the mixed emulsion after the slag removal is added into a stirrer to be stirred and mixed, the rotation speed of a main shaft of the stirrer is 400-600r/min for 60-90min, the liquid obtained after the uniform mixing is taken as an oil phase, and then the special additive liquid, the antioxidant, the humectant and the vegetable protein are added to be mixed and stirred again, the rotation speed of the main shaft of the stirrer is 200-500r/min for 20-30min.
7. The method for preparing an oily solid cosmetic as claimed in claim 6, wherein in the seventh step, the mixture is added into a concentrator to be concentrated into cream, the concentration temperature is 80-100 ℃, and the concentration time is 15-25h.
8. A preparation process of an oily solid cosmetic is characterized in that the components of a special additive solution are as follows: tert-butyl, methyl phenol, aloe extract, and vegetable protein extract.
9. The process for preparing an oily solid cosmetic according to claim 8, wherein a proper amount of t-butyl, methyl phenol, aloe extract, vegetable protein extract is added to a reaction vessel with a main shaft rotation speed of 500 to 600r/min, a reaction time of 20 to 40min, an internal temperature of 40 to 50 ℃ and an internal pressure of 0.3 to 0.7MPa, and then the vessel is put into a high pressure steam oven to be distilled, the pressure of the high pressure steam oven is controlled to be 0.2 to 0.4MPa, thereby obtaining mixed steam, and then the mixed steam is condensed to obtain the special additive solution.
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| WO2013149323A1 (en) * | 2012-04-02 | 2013-10-10 | Ntegrity | Natural products for skin care |
| CN105411965A (en) * | 2016-01-13 | 2016-03-23 | 广州丹奇日用化工厂有限公司 | Safe makeup removing cream and preparation method thereof |
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| WO2013149323A1 (en) * | 2012-04-02 | 2013-10-10 | Ntegrity | Natural products for skin care |
| CN105585601A (en) * | 2012-12-27 | 2016-05-18 | 株式会社林原 | Skin-Exterior Anti-Ageing Composition And Production Method Therefor |
| CN105411965A (en) * | 2016-01-13 | 2016-03-23 | 广州丹奇日用化工厂有限公司 | Safe makeup removing cream and preparation method thereof |
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