CN115215676A - Porous ceramic material, manufacturing method, porous ceramic and application - Google Patents

Porous ceramic material, manufacturing method, porous ceramic and application Download PDF

Info

Publication number
CN115215676A
CN115215676A CN202110408028.9A CN202110408028A CN115215676A CN 115215676 A CN115215676 A CN 115215676A CN 202110408028 A CN202110408028 A CN 202110408028A CN 115215676 A CN115215676 A CN 115215676A
Authority
CN
China
Prior art keywords
porous ceramic
binder
heating
ceramic
powder
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202110408028.9A
Other languages
Chinese (zh)
Inventor
齐会龙
聂革
宋文正
胡勇齐
李俊辉
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shenzhen Woody Vapes Technology Co Ltd
Original Assignee
Shenzhen Woody Vapes Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shenzhen Woody Vapes Technology Co Ltd filed Critical Shenzhen Woody Vapes Technology Co Ltd
Priority to CN202110408028.9A priority Critical patent/CN115215676A/en
Priority to PCT/CN2021/132963 priority patent/WO2022217932A1/en
Publication of CN115215676A publication Critical patent/CN115215676A/en
Pending legal-status Critical Current

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B38/00Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
    • C04B38/06Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof by burning-out added substances by burning natural expanding materials or by sublimating or melting out added substances
    • C04B38/063Preparing or treating the raw materials individually or as batches
    • C04B38/0635Compounding ingredients
    • C04B38/0645Burnable, meltable, sublimable materials
    • C04B38/067Macromolecular compounds
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24FSMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/40Constructional details, e.g. connection of cartridges and battery parts
    • A24F40/42Cartridges or containers for inhalable precursors
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/14Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silica
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/63Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B using additives specially adapted for forming the products, e.g.. binder binders
    • C04B35/632Organic additives
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/63Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B using additives specially adapted for forming the products, e.g.. binder binders
    • C04B35/632Organic additives
    • C04B35/634Polymers
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/63Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B using additives specially adapted for forming the products, e.g.. binder binders
    • C04B35/632Organic additives
    • C04B35/634Polymers
    • C04B35/63404Polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C04B35/63408Polyalkenes
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/63Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B using additives specially adapted for forming the products, e.g.. binder binders
    • C04B35/632Organic additives
    • C04B35/634Polymers
    • C04B35/63496Bituminous materials, e.g. tar, pitch
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/63Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B using additives specially adapted for forming the products, e.g.. binder binders
    • C04B35/638Removal thereof
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/64Burning or sintering processes
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B38/00Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
    • C04B38/06Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof by burning-out added substances by burning natural expanding materials or by sublimating or melting out added substances
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B38/00Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
    • C04B38/06Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof by burning-out added substances by burning natural expanding materials or by sublimating or melting out added substances
    • C04B38/063Preparing or treating the raw materials individually or as batches
    • C04B38/0635Compounding ingredients
    • C04B38/0645Burnable, meltable, sublimable materials
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3205Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
    • C04B2235/3206Magnesium oxides or oxide-forming salts thereof
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3205Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
    • C04B2235/3208Calcium oxide or oxide-forming salts thereof, e.g. lime
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3231Refractory metal oxides, their mixed metal oxides, or oxide-forming salts thereof
    • C04B2235/3232Titanium oxides or titanates, e.g. rutile or anatase
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3284Zinc oxides, zincates, cadmium oxides, cadmiates, mercury oxides, mercurates or oxide forming salts thereof
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3427Silicates other than clay, e.g. water glass
    • C04B2235/3463Alumino-silicates other than clay, e.g. mullite
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3427Silicates other than clay, e.g. water glass
    • C04B2235/3463Alumino-silicates other than clay, e.g. mullite
    • C04B2235/3481Alkaline earth metal alumino-silicates other than clay, e.g. cordierite, beryl, micas such as margarite, plagioclase feldspars such as anorthite, zeolites such as chabazite
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/349Clays, e.g. bentonites, smectites such as montmorillonite, vermiculites or kaolines, e.g. illite, talc or sepiolite
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/36Glass starting materials for making ceramics, e.g. silica glass
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/60Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
    • C04B2235/602Making the green bodies or pre-forms by moulding
    • C04B2235/6022Injection moulding
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/656Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
    • C04B2235/6567Treatment time
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/66Specific sintering techniques, e.g. centrifugal sintering
    • C04B2235/661Multi-step sintering

Abstract

The invention discloses a porous ceramic material, a manufacturing method, porous ceramic and application. The porous ceramic material comprises ceramic powder and a binder; the ceramic powder accounts for 55-80% by mass, and the balance is the binder. According to the manufacturing method of the porous ceramic, the porous ceramic material is adopted, the porous ceramic is manufactured through injection molding, inorganic powder does not need to be used for landfill high-temperature degreasing, the porous ceramic does not need to be cleaned, manpower and material resources are saved, the ceramic is not easy to damage, an aerosol generating device adopting the porous ceramic has no risk of powder falling, the safety is good, a metal heating circuit is not easy to fall off, and the risk of core pasting is small.

Description

Porous ceramic material, manufacturing method, porous ceramic and application
Technical Field
The invention relates to the field of porous ceramic manufacturing, in particular to a porous ceramic material, a manufacturing method, porous ceramic and application.
Background
Aerosol generating devices are used to generate aerosols, which are often atomized using a porous ceramic atomizing wick. The porous ceramic atomizing core is made of porous ceramic. At present, in the process of manufacturing porous ceramics for aerosol generating devices, after molding, inorganic powder is used for filling and high-temperature degreasing of molded bodies. The capillary formed by the inorganic powder is beneficial to degreasing, promotes the discharge of part of liquid-phase organic matters and the separation of decomposition products of organic materials, and on the other hand, the inorganic powder helps the formed body to maintain the shape of the formed body, so that the deformation and collapse of the blank body caused by the self gravity and the separation of the organic matters are avoided.
However, the inorganic powder landfill process has many disadvantages: (1) Inorganic powder needs to be cleaned after degreasing, time and labor are consumed, and the ceramic is easily damaged in the cleaning process; (2) Inorganic powder is adhered to the surface of the ceramic due to physical and chemical effects, so that the ceramic is difficult to clean; inorganic powder which cannot be completely removed has the risk of powder falling on the aerosol generating device, so that great potential safety hazards are brought to users; (3) Inorganic powder is stuck on the ceramic to influence the taste of the aerosol generating device, and meanwhile, the metal heating circuit on the surface of the ceramic is easy to fall off, so that the risk of core pasting is high.
Disclosure of Invention
The invention aims to provide a porous ceramic material, a manufacturing method, porous ceramic and application, so as to overcome the defects of the conventional porous ceramic manufacturing process and the porous ceramic.
The invention discloses a porous ceramic material, which comprises ceramic powder and a binder; the ceramic powder accounts for 55-80% by mass, and the balance is the binder.
Optionally, the ceramic powder comprises the following components in percentage by mass: 30-70% of diatomite, 1-20% of quartz sand, 1-20% of glass powder, 10-50% of pore-forming agent, 1-20% of kaolin, 0-10% of calcium carbonate, 0-10% of magnesium oxide, 0-10% of zinc oxide, 0-10% of titanium dioxide, 0-15% of talc, 0-15% of feldspar, 0-10% of sepiolite and 0-5% of bentonite.
Optionally, the ceramic powder comprises the following components in percentage by mass: 40-50% of diatomite, 5-10% of quartz sand, 5-10% of glass powder, 20-30% of pore-forming agent, 5-10% of kaolin, 2-5% of calcium carbonate, 0-10% of magnesium oxide, 0-10% of zinc oxide, 0-10% of titanium dioxide, 0-10% of talc, 2-10% of feldspar, 0-5% of sepiolite and 0-5% of bentonite.
Optionally, the binder comprises the following components in percentage by mass: 30-75% of paraffin, 1-20% of beeswax, 2-35% of low-density polyethylene, 1-10% of stearic acid, 0-5% of vegetable oil and 0-10% of plasticizer.
Optionally, the binder comprises the following components in percentage by mass: 50-60% of paraffin, 5-10% of beeswax, 15-20% of low-density polyethylene, 5-10% of stearic acid, 2-5% of vegetable oil and 3-8% of plasticizer.
The invention also discloses a manufacturing method of the porous ceramic, which comprises the following steps:
step 1: weighing the ceramic powder and the binder in proportion;
step 2: heating the binder in the step 1 to be in a molten state, and adding the ceramic powder in the step 1 for mixing to obtain a premixed material;
and 3, step 3: granulating the premixed material obtained in the step 2, and then performing injection molding to obtain an injection molding blank;
and 4, step 4: and (4) degreasing and sintering the injection molding blank body in the step (3) to obtain the porous ceramic.
Optionally, the step 2 specifically includes:
heating the binder in the step 1 to 70-170 ℃, and banburying, kneading or stirring to enable the binder to be in a molten state;
adding the ceramic powder obtained in the step (1) and mixing for 2-5 h to obtain a premixed material.
Optionally, step 4 specifically includes:
heating the sintering temperature from room temperature to 250 ℃, and preserving heat, wherein the heating time is 730min, and the heat preservation time is 240min;
heating the sintering temperature from 250 ℃ to 350 ℃, and preserving heat, wherein the heating time is 300min, and the heat preservation time is 60min;
heating the sintering temperature from 350 ℃ to 500 ℃, and preserving heat, wherein the heating time is 150min, and the heat preservation time is 60min;
heating the sintering temperature from 500 ℃ to 900 ℃ for 120min;
heating the sintering temperature from 900 ℃ to 1100 ℃, and preserving the heat, wherein the heating time is 120min, and the heat preservation time is 120min;
and (4) reducing the sintering temperature from 1100 ℃ to room temperature to finish sintering.
The invention also discloses a porous ceramic which is prepared by the preparation method.
The invention also discloses application of the porous ceramic in an aerosol generating device.
According to the manufacturing method of the porous ceramic, the porous ceramic material is adopted, the porous ceramic is manufactured through injection molding, inorganic powder does not need to be used for landfill high-temperature degreasing, the porous ceramic does not need to be cleaned, manpower and material resources are saved, the ceramic is not easy to damage, an aerosol generating device adopting the porous ceramic has no powder falling risk, the safety is good, a metal heating circuit is not easy to fall off, and the risk of core pasting is small.
Drawings
The accompanying drawings, which are included to provide a further understanding of the embodiments of the invention and are incorporated in and constitute a part of this specification, illustrate embodiments of the invention and together with the description serve to explain the principles of the invention. It is obvious that the drawings in the following description are only some embodiments of the invention, and that for a person skilled in the art, other drawings can be derived from them without inventive effort. In the drawings:
FIG. 1 is a flow chart of a method of making a porous ceramic according to an embodiment of the present invention;
FIG. 2 is a graph showing a thermal analysis of an injection-molded body according to an embodiment of the present invention.
Detailed Description
To better illustrate the invention and to facilitate the understanding of the technical solutions thereof, typical but non-limiting examples of the invention are as follows:
example 1
A porous ceramic material comprises ceramic powder and a binder; the ceramic powder accounts for 55-80% by mass, and the balance is the binder.
The porous ceramic material is used for manufacturing the porous ceramic for the sol device, realizes a powder embedding-free degreasing process, has high solid content and high sintering strength, is not easy to damage, has no risk of powder falling, has high safety, has good taste of the aerosol generating device, is not easy to fall off a metal heating circuit on the surface of the ceramic, and has small risk of core pasting.
In this embodiment, the ceramic powder accounts for 55-80% of the total mass of the porous ceramic material, the ceramic powder has a solid content, a high solid content is beneficial to maintaining the shape without collapsing and deforming in the degreasing process, but an excessively high solid content is not beneficial to injection molding, so the ceramic powder is selected to be 55-80%.
Specifically, the ceramic powder comprises the following components in percentage by mass: 30-70% of diatomite, 1-20% of quartz sand, 1-20% of glass powder, 10-50% of pore-forming agent, 1-20% of kaolin, 0-10% of calcium carbonate, 0-10% of magnesium oxide, 0-10% of zinc oxide, 0-10% of titanium dioxide, 0-15% of talc, 0-15% of feldspar, 0-10% of sepiolite and 0-5% of bentonite.
In this scheme, diatomaceous earth self has good porous structure, has fine adsorption and filtration characteristic, and density is little, and the heat accumulation nature is good, as main skeleton material in this scheme, makes porous ceramic, uses in aerosol generating device, in aerosol generating device use, and the atomizing filter effect is good, and the quality is light. The quartz sand, the glass powder, the kaolin, the talc and the bentonite are fluxing components, so that the sintering temperature can be reduced, and the sintering is promoted. The pore former may be removed during the debinding sintering of the porous ceramic to leave a pore structure. Magnesium oxide, zinc oxide and titanium dioxide are used as additives, and have the effects of adjusting phase components of inorganic phases, sterilizing and the like. The strength of the porous ceramic can be conveniently adjusted by adding the feldspar. The calcium carbonate can adjust the wettability and improve the sintering temperature, and the sepiolite can be added to adjust the comprehensive taste of the aerosol generating device.
Wherein, the diatomite may be 30%, 35%, 40%, 45%, 50%, 55%, 60%, 65%, 70%, the quartz sand may be 1%, 5%, 10%, 15%, 20%, the glass frit may be 1%, 5%, 10%, 15%, 20%, the pore-forming agent may be 10%, 15%, 20%, 25%, 30%, 35%, 40%, 45%, 50%, the kaolin may be 1%, 5%, 10%, 15%, 20%, the calcium carbonate may be 0-10%, the magnesium oxide may be 0%, 2%, 5%, 8%, 10%, the zinc oxide may be 0%, 2%, 5%, 8%, 10%, the titanium dioxide may be 0%, 2%, 5%, 8%, 10%, the talc may be 0%, 1%, 5%, 10%, 15%, the feldspar may be 0%, 1%, 5%, 10%, 15%, the sepiolite may be 0%, 2%, 5%, 8%, 10%, and the bentonite may be 0%, 1%, 2%, 3%, 4%, 5%.
As a further preferable technical scheme of the ceramic powder in this embodiment, the ceramic powder includes the following components by mass percent: 40-50% of diatomite, 5-10% of quartz sand, 5-10% of glass powder, 20-30% of pore-forming agent, 5-10% of kaolin, 2-5% of calcium carbonate, 0-10% of magnesium oxide, 0-10% of zinc oxide, 0-10% of titanium dioxide, 0-10% of talcum, 2-10% of feldspar, 0-5% of sepiolite and 0-5% of bentonite.
Wherein, by mass percentage, the diatomite can be 40%, 42%, 44%, 46%, 48%, the quartz sand can be 5%, 7%, 8%, 10%, the glass powder can be 5%, 7%, 8%, 10%, the pore-forming agent can be 20%, 22%, 24%, 26%, 28%, 30%, the kaolin can be 5%, 7%, 8%, 10%, the calcium carbonate can be 2%, 3%, 4%, 5%, the magnesium oxide can be 0%, 2%, 4%, 6%, 8%, 10%, the zinc oxide can be 0%, 2%, 4%, 6%, 8%, 10%, the titanium dioxide can be 0%, 2%, 4%, 6%, 8%, 10%, the talc can be 0%, 2%, 4%, 6%, 8%, 10%, the feldspar can be 2%, 4%, 6%, 8%, 10%, the sepiolite can be 0%, 1%, 2%, 3%, 4%, 5%, and the bentonite can be 0%, 1%, 2%, 3%, 4%, 5%. Among them, too much calcium carbonate results in large shrinkage ratio, poor dimensional consistency and reduced strength, and in the range of 2-5%, the shrinkage is small, the dimensional consistency is good, and the strength is large.
In another aspect, the binder comprises the following components in weight percent: 30-75% of paraffin, 1-20% of beeswax, 2-35% of low-density polyethylene, 1-10% of stearic acid, 0-5% of vegetable oil and 0-10% of plasticizer.
The main function of the binder in this embodiment is to impart fluidity to the ceramic powder, which is beneficial to molding, and the binder can be removed completely in the degreasing process to form a porous structure. In this embodiment, the paraffin wax, as a small molecular weight organic substance, has good thermochemical properties, and is easily removed at high temperature, and is used as a main material of a binder. The adhesive is applied to ceramic powder, and when the porous ceramic is manufactured, the adhesive is easy to remove and clean, and the aerosol generating device has better and clean mouthfeel. The melting point of the beeswax is higher than that of the paraffin wax, so that the range of removing temperature is widened, and bubbling caused by violent volatilization of the binder at the temperature for removing the paraffin wax is avoided. The low-density polyethylene is used as a high-viscosity high-elasticity material and is a high-temperature framework of the adhesive. Stearic acid facilitates the dispersion of the ceramic powder and the binder. The vegetable oil is used as a lubricant, which is beneficial to demoulding in the material forming process. The plasticizer can improve the plasticity of the injection-molded green body.
Wherein, the paraffin wax can be 30%, 35%, 40%, 45%, 55%, 60%, 65%, 70%, 75%, 1%, 5%, 10%, 15%, 20%, 2%, 5%, 10%, 15%, 20%, 30%, 35%, 1%, 2%, 4%, 6%, 8%, 10%, 0%, 1%, 2%, 3%, 4%, 5%, 0%, 2%, 4%, 6%, 8%, 10% by mass of vegetable oil.
As a further preferable technical scheme of the binder in this embodiment, the binder comprises the following components in percentage by mass: 50-60% of paraffin, 5-10% of beeswax, 15-20% of low-density polyethylene, 5-10% of stearic acid, 2-5% of vegetable oil and 3-8% of plasticizer.
Wherein, the mass percentage of the paraffin wax can be 50%, 52%, 54%, 56%, 58%, 60%, the mass percentage of the beeswax can be 5%, 7%, 9%, 10%, the mass percentage of the low-density polyethylene can be 15%, 16%, 18%, 20%, the mass percentage of the stearic acid can be 5%, 7%, 9%, 10%, the mass percentage of the vegetable oil can be 2%, 3%, 4%, 5%, and the mass percentage of the plasticizer can be 3%, 5%, 7%, 8%.
Example 2
The ceramic powder comprises the following components in percentage by mass: 50% of diatomite, 5% of quartz sand, 6% of glass powder, 30% of pore-forming agent, 5% of kaolin and 4% of feldspar.
Example 3
The ceramic powder comprises the following components in percentage by mass: 50% of diatomite, 5% of quartz sand, 10% of glass powder, 30% of pore-forming agent and 5% of kaolin.
Example 4
The ceramic powder comprises the following components in percentage by mass: 40% of diatomite, 5% of quartz sand, 5% of glass powder, 10% of pore-forming agent, 7% of kaolin, 5% of magnesium oxide, 5% of zinc oxide, 5% of titanium dioxide, 10% of talc, 5% of feldspar and 3% of bentonite.
Example 5
The ceramic powder comprises the following components in percentage by mass: 30% of diatomite, 5% of quartz sand, 5% of glass powder, 10% of pore-forming agent, 2% of kaolin, 5% of calcium carbonate, 5% of magnesium oxide, 5% of zinc oxide, 5% of titanium dioxide, 10% of talc, 5% of feldspar, 10% of sepiolite and 3% of bentonite.
Example 6
The adhesive comprises the following components in percentage by mass: 60% of paraffin, 10% of beeswax, 15% of low-density polyethylene, 5% of stearic acid, 5% of vegetable oil and 5% of plasticizer.
Example 7
The adhesive comprises the following components in percentage by mass: 70% of paraffin, 10% of beeswax, 15% of low-density polyethylene and 5% of stearic acid.
Example 8
The adhesive comprises the following components in percentage by mass: 70% of paraffin, 7% of beeswax, 15% of low-density polyethylene, 5% of stearic acid and 3% of vegetable oil.
Example 9
The adhesive comprises the following components in percentage by mass: 70% of paraffin, 7% of beeswax, 15% of low-density polyethylene, 3% of stearic acid and 5% of plasticizer.
Example 10
As shown in fig. 1, a method for manufacturing a porous ceramic includes:
step 1: weighing the ceramic powder and the binder in the embodiments in proportion;
and 2, step: heating the binder in the step 1 to be in a molten state, and adding the ceramic powder in the step 1 for mixing to obtain a premixed material;
and step 3: granulating the premixed material obtained in the step 2, and then performing injection molding to obtain an injection molding blank;
and 4, step 4: and (4) degreasing and sintering the injection molding blank body in the step (3) to obtain the porous ceramic.
According to the porous ceramic manufacturing method, the ceramic powder and the binder are adopted, the porous ceramic is manufactured through injection molding, inorganic powder does not need to be used for landfill high-temperature degreasing, the inorganic powder does not need to be cleaned, manpower and material resources are saved, and the ceramic is not easy to damage. The porous ceramic aerosol generating device is applied to the aerosol generating device, the aerosol generating device adopting the porous ceramic has no risk of powder falling, the safety is good, the metal heating circuit is not easy to fall off, and the risk of core pasting is low.
In the embodiment, the non-buried powder degreasing technology can realize the integration of burning and removing, and the product is finished by feeding into the furnace once, so that the time is saved. In the existing inorganic powder landfill process, the buried powder is degreased for about 40 hours, sticky powder on the surface is taken out and cleaned for about 4 hours, the buried powder is placed in a sintering furnace for high-temperature sintering and temperature rise for about 6 hours, the temperature is kept for 2 hours, and the buried powder is taken out after being cooled along with the furnace. The manufacturing method of the porous ceramic can save the time for cleaning the surface adhesive powder.
Step 4 may specifically be: and (3) degreasing the injection molding blank body in the step (3) and sintering the injection molding blank body to obtain the porous ceramic. Specifically, the injection molding blank is degreased for 40 hours, taken out and directly placed in a sintering furnace for high-temperature sintering, the temperature rise time is about 6 hours, the temperature is kept for 2 hours, and the injection molding blank is taken out after being cooled along with the furnace. Compared with the prior art, the method saves the time for cleaning the surface sticky powder and the step of cleaning the powder, thereby avoiding the damage of the ceramic substrate caused by the step, and increasing the yield from about 94 percent to about 99 percent.
In another embodiment, step 4 may also be: and (4) simultaneously carrying out high-temperature degreasing and sintering the injection molding blank body in the step (3) to obtain the porous ceramic. Specifically, degreasing at high temperature, sintering for 42 hours, cooling with a furnace, and taking out. This embodiment realizes degrease and sintering than current technology, just can realize two steps of degrease and sintering with same high temperature furnace, has reduced equipment quantity, has shortened degrease sintering total time, and need not to clear up and glue powder, and the product is cleaner, and is safer, and the yield is for being close to 100%.
In the step 2, the binder is heated to be in a molten state, so that the ceramic powder is fully mixed and fused, and in the step 3, the granules in the step 2 are uniformly injected into a blank.
Specifically, the step 1 further includes the steps of: drying the ceramic powder at 70-90 deg.c for 1.5-2.5 hr. Preferably, the drying temperature is 80 ℃ and the drying time is 2h. After drying, the product can be naturally cooled for later use. The drying is intended to remove the water from the ceramic powder and to prevent uncontrolled porosity during injection molding in the event of excessive water.
Specifically, the step 2 specifically comprises: heating the binder in the step 1 to 70-170 ℃, and carrying out banburying, kneading or stirring to enable the binder to be in a molten state; adding the ceramic powder obtained in the step (1) and mixing for 2-5 h to obtain a premixed material. One of banburying, kneading or stirring may be selected to mix the binder uniformly. The internal mixing, kneading or stirring is carried out by means of corresponding internal mixers, kneaders, stirrers.
Specifically, the step 3 specifically comprises: granulating the premixed material obtained in the step 2, wherein the granulation temperature is 50-140 ℃; and performing injection molding on the premixed material to obtain an injection molding blank, wherein the injection molding temperature is 50-140 ℃. And after the injection molding blank body is obtained, removing burrs and a joint line of the injection molding blank body.
The step 4 specifically comprises the following steps: heating the sintering temperature from room temperature to 250 ℃, and preserving heat, wherein the heating time is 730min, and the heat preservation time is 240min; heating the sintering temperature from 250 ℃ to 350 ℃, and preserving heat, wherein the heating time is 300min, and the heat preservation time is 60min; heating the sintering temperature from 350 ℃ to 500 ℃, and preserving heat, wherein the heating time is 150min, and the heat preservation time is 60min; heating the sintering temperature from 500 ℃ to 900 ℃ for 120min; heating the sintering temperature from 900 ℃ to 1100 ℃, and preserving the heat, wherein the heating time is 120min, and the heat preservation time is 120min; and (4) reducing the sintering temperature from 1100 ℃ to room temperature to finish sintering.
As shown in the thermal analysis curve (DG-DSC curve) of the injection molding blank body shown in FIG. 2, the injection molding blank body is slowly heated up from room temperature to 250 ℃, and the deformation of the blank body caused by too fast heating up is avoided; the temperature of 250-350 ℃ is a violent volatilization stage of the organic matters, the heating rate is reduced, and the organic matters are completely removed. And (3) volatilizing the organic matters at 500 ℃ completely, quickly heating, and carrying out heat preservation sintering at 1100 ℃ to obtain the porous ceramic with uniformly distributed pores.
Specifically, the ceramic powder weighed in the step 1 accounts for 55-80% of the total mass of the ceramic powder and the binder, and the balance is the binder. The ceramic powder has a solid content, and the high solid content is beneficial to keeping the shape without collapsing and deforming in the degreasing process. However, the solid content is too high to facilitate injection molding, and the ceramic powder is selected to be 55-80%.
More specifically, in one embodiment, the ceramic powder is 70% by weight and the binder is 30% by weight. Wherein, in the ceramic powder, the percentage of each component is as follows according to the mass percentage: 50% of diatomite, 5% of quartz sand, 6% of glass powder, 30% of pore-forming agent, 5% of kaolin and 4% of feldspar. In the binder, the percentage by mass of each component is as follows: 60% of paraffin, 10% of beeswax, 15% of low-density polyethylene, 5% of stearic acid, 5% of vegetable oil and 5% of plasticizer. As shown in Table 1, the porosity of the porous ceramic obtained by the formula is more than or equal to 60%, the pore diameter is about 20 mu m, the high reduction degree of the porous ceramic is met, and the taste is excellent.
TABLE 1
Sintering temperature Porosity of the material Pore diameter Taste of food
1100℃ 63.97% 25.53um Superior food
In one embodiment, the ceramic powder is 75% by weight and the binder is 25% by weight. The ratio of each component in the ceramic powder and the ratio of each component in the binder are the same as above, and are not described again. As shown in Table 2, the porosity of the porous ceramic obtained by the formula is more than or equal to 60%, the pore diameter is about 20 mu m, the high reduction degree of the porous ceramic is met, and the mouthfeel is excellent.
TABLE 2
Sintering temperature Porosity factor Pore diameter Taste of food
1120℃ 63.16% 20.7um Superior food
Example 11
The porous ceramic is prepared by the above porous ceramic preparation method. The porous ceramic prepared by the method does not need to be cleaned of inorganic powder, so that manpower and material resources are saved, the ceramic is not easy to damage, the risk of powder falling is avoided, the safety is good, the metal heating circuit of the aerosol generating device is not easy to fall off, and the risk of core pasting is small.
Example 12
Use of a porous ceramic as described above in an aerosol generating device. The porous ceramic is used in the aerosol generating device, the aerosol generating device has no risk of powder falling, the safety is good, the metal heating circuit is not easy to fall off, and the risk of core pasting is low.
It should be noted that, the limitations of the steps involved in the present disclosure are not considered to limit the order of the steps without affecting the implementation of the specific embodiments, and the steps written in the foregoing may be executed first, or executed later, or even executed simultaneously, and as long as the present disclosure can be implemented, all should be considered to belong to the protection scope of the present disclosure.
The foregoing is a more detailed description of the invention in connection with specific alternative embodiments, and the practice of the invention should not be construed as limited to those descriptions. For those skilled in the art to which the invention pertains, numerous simple deductions or substitutions may be made without departing from the spirit of the invention, which shall be deemed to belong to the scope of the invention.

Claims (10)

1. The porous ceramic material comprises ceramic powder and a binder, and is characterized in that the ceramic powder accounts for 55-80% by mass, and the balance is the binder.
2. The porous ceramic material of claim 1 wherein the ceramic powder comprises the following composition in weight percent: 30-70% of diatomite, 1-20% of quartz sand, 1-20% of glass powder, 10-50% of pore-forming agent, 1-20% of kaolin, 0-10% of calcium carbonate, 0-10% of magnesium oxide, 0-10% of zinc oxide, 0-10% of titanium dioxide, 0-15% of talc, 0-15% of feldspar, 0-10% of sepiolite and 0-5% of bentonite.
3. The porous ceramic material of claim 2 wherein the ceramic powder comprises the following components in weight percent: 40-50% of diatomite, 5-10% of quartz sand, 5-10% of glass powder, 20-30% of pore-forming agent, 5-10% of kaolin, 2-5% of calcium carbonate, 0-10% of magnesium oxide, 0-10% of zinc oxide, 0-10% of titanium dioxide, 0-10% of talcum, 2-10% of feldspar, 0-5% of sepiolite and 0-5% of bentonite.
4. The porous ceramic material of claim 1 wherein the binder comprises the components in weight percent: 30-75% of paraffin, 1-20% of beeswax, 2-35% of low-density polyethylene, 1-10% of stearic acid, 0-5% of vegetable oil and 0-10% of plasticizer.
5. The porous ceramic material of claim 4 wherein the binder comprises the following components in weight percent: 50-60% of paraffin, 5-10% of beeswax, 15-20% of low-density polyethylene, 5-10% of stearic acid, 2-5% of vegetable oil and 3-8% of plasticizer.
6. A method for manufacturing porous ceramics is characterized by comprising the following steps:
step 1: weighing the ceramic powder material as claimed in any one of claims 1 to 5 and a binder in proportion;
step 2: heating the binder in the step 1 to be in a molten state, and adding the ceramic powder in the step 1 for mixing to obtain a premixed material;
and step 3: granulating the premixed material obtained in the step 2, and then performing injection molding to obtain an injection molding blank;
and 4, step 4: and (4) degreasing and sintering the injection molding blank body in the step (3) to obtain the porous ceramic.
7. The method for manufacturing porous ceramics according to claim 6, wherein the step 2 is specifically:
heating the binder in the step 1 to 70-170 ℃, and banburying, kneading or stirring to enable the binder to be in a molten state;
adding the ceramic powder obtained in the step (1) and mixing for 2-5 h to obtain a premixed material.
8. The method for manufacturing a porous ceramic according to any one of claims 6 to 7, wherein the step 4 is specifically:
heating the sintering temperature from room temperature to 250 ℃, and preserving heat, wherein the heating time is 730min, and the preserving heat time is 240min;
heating the sintering temperature from 250 ℃ to 350 ℃, and preserving heat, wherein the heating time is 300min, and the heat preservation time is 60min;
heating the sintering temperature from 350 ℃ to 500 ℃, and preserving heat, wherein the heating time is 150min, and the heat preservation time is 60min;
heating the sintering temperature from 500 ℃ to 900 ℃ for 120min;
heating the sintering temperature from 900 ℃ to 1100 ℃, and preserving the heat, wherein the heating time is 120min, and the heat preservation time is 120min;
and (4) reducing the sintering temperature from 1100 ℃ to room temperature to finish sintering.
9. A porous ceramic produced by the production method according to any one of claims 6 to 8.
10. Use of a porous ceramic according to claim 9 in an aerosol generating device.
CN202110408028.9A 2021-04-15 2021-04-15 Porous ceramic material, manufacturing method, porous ceramic and application Pending CN115215676A (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
CN202110408028.9A CN115215676A (en) 2021-04-15 2021-04-15 Porous ceramic material, manufacturing method, porous ceramic and application
PCT/CN2021/132963 WO2022217932A1 (en) 2021-04-15 2021-11-25 Perforated ceramic material, fabrication method, perforated ceramic and application thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202110408028.9A CN115215676A (en) 2021-04-15 2021-04-15 Porous ceramic material, manufacturing method, porous ceramic and application

Publications (1)

Publication Number Publication Date
CN115215676A true CN115215676A (en) 2022-10-21

Family

ID=83604621

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202110408028.9A Pending CN115215676A (en) 2021-04-15 2021-04-15 Porous ceramic material, manufacturing method, porous ceramic and application

Country Status (2)

Country Link
CN (1) CN115215676A (en)
WO (1) WO2022217932A1 (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115959923A (en) * 2023-01-03 2023-04-14 深圳市卓尔悦电子科技有限公司 Porous ceramic, atomizing core, atomizing device and preparation method of porous ceramic

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101290851A (en) * 2008-06-13 2008-10-22 北京有色金属研究总院 Method for preparing electric vacuum suction element molded by powder injection
CN107324801A (en) * 2017-06-21 2017-11-07 东莞华晶粉末冶金有限公司 A kind of ceramic injection forming material and preparation method thereof
CN110526735A (en) * 2019-09-29 2019-12-03 深圳羽制科技有限公司 A kind of electronic cigarette device porous ceramics and preparation method thereof
CN110742314A (en) * 2019-10-22 2020-02-04 深圳羽制科技有限公司 Electronic cigarette atomization core porous ceramic and preparation method thereof
CN111153686A (en) * 2020-01-14 2020-05-15 东莞市陶陶新材料科技有限公司 Porous ceramic for electronic cigarette, atomizing core containing porous ceramic and preparation method of atomizing core
CN111205104A (en) * 2020-01-14 2020-05-29 东莞市陶陶新材料科技有限公司 Porous ceramic for electronic cigarette and preparation method thereof

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110713379B (en) * 2019-12-02 2023-01-24 湖南福美来电子陶瓷有限公司 Porous ceramic atomizing core and preparation method thereof
CN112592200B (en) * 2020-12-18 2023-06-27 惠州市新泓威科技有限公司 Nanometer porous ceramic for atomizing core and preparation method thereof
CN113149697A (en) * 2021-04-23 2021-07-23 深圳市基克纳科技有限公司 Composition and porous ceramic atomizing core containing continuous glass phase
CN113480327A (en) * 2021-07-16 2021-10-08 深圳市吉迩科技有限公司 Atomizing core, porous ceramic and preparation method of porous ceramic

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101290851A (en) * 2008-06-13 2008-10-22 北京有色金属研究总院 Method for preparing electric vacuum suction element molded by powder injection
CN107324801A (en) * 2017-06-21 2017-11-07 东莞华晶粉末冶金有限公司 A kind of ceramic injection forming material and preparation method thereof
CN110526735A (en) * 2019-09-29 2019-12-03 深圳羽制科技有限公司 A kind of electronic cigarette device porous ceramics and preparation method thereof
CN110742314A (en) * 2019-10-22 2020-02-04 深圳羽制科技有限公司 Electronic cigarette atomization core porous ceramic and preparation method thereof
CN111153686A (en) * 2020-01-14 2020-05-15 东莞市陶陶新材料科技有限公司 Porous ceramic for electronic cigarette, atomizing core containing porous ceramic and preparation method of atomizing core
CN111205104A (en) * 2020-01-14 2020-05-29 东莞市陶陶新材料科技有限公司 Porous ceramic for electronic cigarette and preparation method thereof

Also Published As

Publication number Publication date
WO2022217932A1 (en) 2022-10-20

Similar Documents

Publication Publication Date Title
WO2019223196A1 (en) Oil-permeable porous ceramic, preparation method therefor, and application thereof in electronic cigarette
WO2023284425A1 (en) Atomizing core, porous ceramic, and method for preparing porous ceramic
CN112047753B (en) Porous ceramic and preparation method and application thereof
WO2022135010A1 (en) Porous ceramic atomization core and preparation method therefor, and electronic cigarette
CN110713379B (en) Porous ceramic atomizing core and preparation method thereof
CN111205104A (en) Porous ceramic for electronic cigarette and preparation method thereof
WO2023000573A1 (en) Microporous ceramic atomization core and preparation method therefor
CN110194662B (en) Atomizing core, preparation method thereof and electronic cigarette
CN113149697A (en) Composition and porous ceramic atomizing core containing continuous glass phase
WO2014133077A1 (en) Porous aluminum sintered compact
CN111792922A (en) High-reduction porous ceramic atomizing core and preparation method thereof
CN115215676A (en) Porous ceramic material, manufacturing method, porous ceramic and application
JP2009510266A (en) High porosity metal dual pore porous foam
CN113749305B (en) Porous ceramic atomization core of electronic cigarette and preparation method thereof
CN112679202A (en) Porous ceramic composition, preparation method thereof and electronic cigarette atomization core applying same
CN102266906B (en) Preparation method of easy-to-remove ceramic mold core
CN113563058A (en) Atomizing core, porous ceramic and preparation method of porous ceramic
KR20070096131A (en) Method for manucturing of sintering zirconium-silicate bead and sintering zirconium-silicate bead
CN103801689A (en) Mixed material with high expansion rate for producing porous metallic sintered body
JP2006516678A5 (en)
CN112089104A (en) Manufacturing process of atomizing core and electronic atomizer
CN114149248B (en) Porous ceramic material and preparation method thereof, heating component, atomizer and electronic cigarette
CN101215651B (en) Method for preparing porous foam nickel-titanium shape memory alloy
CN210581002U (en) Atomizing core structure and electronic atomizer
CN210945336U (en) Atomizer

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20221021