CN115193146A - Oil-water layering tank for hydrolysis of dimethyldichlorosilane - Google Patents
Oil-water layering tank for hydrolysis of dimethyldichlorosilane Download PDFInfo
- Publication number
- CN115193146A CN115193146A CN202210830726.2A CN202210830726A CN115193146A CN 115193146 A CN115193146 A CN 115193146A CN 202210830726 A CN202210830726 A CN 202210830726A CN 115193146 A CN115193146 A CN 115193146A
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- China
- Prior art keywords
- cylinder
- water
- separation
- rod
- dimethyldichlorosilane
- Prior art date
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 80
- LIKFHECYJZWXFJ-UHFFFAOYSA-N dimethyldichlorosilane Chemical compound C[Si](C)(Cl)Cl LIKFHECYJZWXFJ-UHFFFAOYSA-N 0.000 title claims abstract description 22
- 238000006460 hydrolysis reaction Methods 0.000 title abstract description 9
- 230000007062 hydrolysis Effects 0.000 title abstract description 7
- 238000000926 separation method Methods 0.000 claims abstract description 67
- 238000010438 heat treatment Methods 0.000 claims abstract description 30
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims abstract description 28
- 229910000041 hydrogen chloride Inorganic materials 0.000 claims abstract description 21
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 claims abstract description 21
- 238000001514 detection method Methods 0.000 claims abstract description 14
- 230000001360 synchronised effect Effects 0.000 claims abstract description 4
- 238000004140 cleaning Methods 0.000 claims description 24
- 230000006835 compression Effects 0.000 claims description 16
- 238000007906 compression Methods 0.000 claims description 16
- 235000017166 Bambusa arundinacea Nutrition 0.000 claims description 8
- 235000017491 Bambusa tulda Nutrition 0.000 claims description 8
- 241001330002 Bambuseae Species 0.000 claims description 8
- 235000015334 Phyllostachys viridis Nutrition 0.000 claims description 8
- 239000011425 bamboo Substances 0.000 claims description 8
- 239000012528 membrane Substances 0.000 claims description 4
- 230000001105 regulatory effect Effects 0.000 claims description 4
- 230000005611 electricity Effects 0.000 claims description 2
- 239000000203 mixture Substances 0.000 abstract description 17
- 230000009286 beneficial effect Effects 0.000 abstract description 2
- 239000007787 solid Substances 0.000 description 11
- 239000000413 hydrolysate Substances 0.000 description 9
- 239000007788 liquid Substances 0.000 description 9
- 235000019198 oils Nutrition 0.000 description 9
- 239000000126 substance Substances 0.000 description 6
- 238000000034 method Methods 0.000 description 5
- 239000005046 Chlorosilane Substances 0.000 description 3
- 108010009736 Protein Hydrolysates Proteins 0.000 description 3
- KOPOQZFJUQMUML-UHFFFAOYSA-N chlorosilane Chemical compound Cl[SiH3] KOPOQZFJUQMUML-UHFFFAOYSA-N 0.000 description 3
- 238000007599 discharging Methods 0.000 description 3
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 description 2
- 238000005188 flotation Methods 0.000 description 2
- 238000005192 partition Methods 0.000 description 2
- 208000034699 Vitreous floaters Diseases 0.000 description 1
- 230000001133 acceleration Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 235000019476 oil-water mixture Nutrition 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 230000008054 signal transmission Effects 0.000 description 1
- 229920002050 silicone resin Polymers 0.000 description 1
- 229920002379 silicone rubber Polymers 0.000 description 1
- 239000004945 silicone rubber Substances 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D36/00—Filter circuits or combinations of filters with other separating devices
- B01D36/003—Filters in combination with devices for the removal of liquids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/30—Accessories for evaporators ; Constructional details thereof
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
- B01D17/02—Separation of non-miscible liquids
- B01D17/0208—Separation of non-miscible liquids by sedimentation
- B01D17/0214—Separation of non-miscible liquids by sedimentation with removal of one of the phases
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
- B01D17/08—Thickening liquid suspensions by filtration
- B01D17/085—Thickening liquid suspensions by filtration with membranes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
- B01D17/12—Auxiliary equipment particularly adapted for use with liquid-separating apparatus, e.g. control circuits
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/11—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with bag, cage, hose, tube, sleeve or like filtering elements
- B01D29/31—Self-supporting filtering elements
- B01D29/35—Self-supporting filtering elements arranged for outward flow filtration
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/88—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor having feed or discharge devices
- B01D29/94—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor having feed or discharge devices for discharging the filter cake, e.g. chutes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D35/00—Filtering devices having features not specifically covered by groups B01D24/00 - B01D33/00, or for applications not specifically covered by groups B01D24/00 - B01D33/00; Auxiliary devices for filtration; Filter housing constructions
- B01D35/16—Cleaning-out devices, e.g. for removing the cake from the filter casing or for evacuating the last remnants of liquid
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Extraction Or Liquid Replacement (AREA)
- Filtration Of Liquid (AREA)
Abstract
The invention discloses a dimethyldichlorosilane hydrolysis oil-water layering tank, which relates to the technical field of oil-water separation and comprises a separation mechanism and a driving mechanism, wherein a filter cylinder is arranged between a support cover and a separation cylinder; the power mechanism drives the drain plug to control the closing of the separation port through the drainage component, the drainage component is synchronous with the movement of the rotating component, a control mechanism is arranged between the PH detection floating block inside the separation cylinder and the heating wire, and the outside of the separation cylinder is connected with the hydrogen chloride cylinder. The invention has the beneficial effects that: the power mechanism controls the driving mechanism and the drainage mechanism at the same time, the matching between the structures is ingenious, and time is provided for water and oil layering; the PH detection floating block is connected with a heating wire, and hydrogen chloride in the mixture is completely evaporated by a control mechanism.
Description
Technical Field
The invention relates to the technical field of oil-water separation, in particular to a dimethyldichlorosilane hydrolysis oil-water layering tank.
Background
Dimethyl dichlorosilane and concentrated hydrochloric acid are subjected to hydrolysis reaction in a hydrolysate reactor to generate a cyclic hydrolysate, which is mainly used for preparing dimethyl ether oil, silicone rubber, silicone resin and the like, and an oil-water mixture containing hydrogen chloride and water is produced after the hydrolysis is finished and needs to be separated.
The Chinese patent with the prior art publication number of CN113996256A discloses a method and a device for treating a dimethyl dichlorosilane hydrolysate, and the method comprises the following steps: performing hydrolysis reaction on dimethyl dichlorosilane and concentrated hydrochloric acid to obtain a hydrolysate; separating the hydrolysate to obtain a first mixture, wherein the first mixture comprises aqueous hydrogen chloride; and absorbing water in the first mixture by using a high-boiling-point substance, wherein the high-boiling-point substance contains chlorosilane. In the method for treating the hydrolysate of dimethyldichlorosilane, dimethyldichlorosilane and the hydrolysate of concentrated hydrochloric acid are separated to obtain a first mixture, the first mixture comprises aqueous hydrogen chloride, water in the first mixture can be absorbed by high-boiling-point substances, chlorosilane is contained in the high-boiling-point substances, and the high-boiling-point substances are difficult to volatilize due to high boiling points, and the chlorosilane in the high-boiling-point substances is rapidly hydrolyzed when meeting water, so that the water in the hydrogen chloride can be removed, the water removal efficiency is high, the water removal effect is good, and new impurities cannot be introduced.
Although water in hydrogen chloride can be removed in the prior art, solids in a hydrolysate cannot be removed mainly aiming at a separated first mixture, and water and oil in the hydrolysate are separated, so that a dimethyldichlorosilane hydrolysate water-oil layering tank is urgently needed.
Disclosure of Invention
Aiming at the technical problems, the technical scheme adopted by the invention is as follows: a dimethyldichlorosilane hydrolysis oil-water layering tank comprises a separation mechanism, a driving mechanism, a drainage mechanism and a heating wire, wherein the separation mechanism comprises a support cover and a separation cylinder, a filter cylinder is arranged between the support cover and the separation cylinder, the filter cylinder is fixedly arranged above the separation cylinder, the heating wire is fixedly wound outside the separation cylinder, a water cylinder is fixedly arranged below the separation cylinder, a power mechanism is arranged on the support cover, the driving mechanism is arranged inside the filter cylinder, the driving mechanism comprises a rotating assembly and a cleaning assembly, the rotating assembly is rotatably arranged inside the filter cylinder, the cleaning assembly is slidably arranged at the bottom of the filter cylinder, the power mechanism drives the cleaning assembly to slide at the bottom of the filter cylinder through the rotating assembly, a baffle is slidably arranged inside the filter cylinder, a driven assembly is arranged between the baffle and the cleaning assembly, and the driven assembly drives the baffle and a water outlet on the water cylinder to be closed; drainage mechanism includes drainage subassembly, drain plug, drainage subassembly sets up in supporting lid top and water drum bottom, the drain plug sets up inside the water drum, the first end slidable mounting of drain plug is on the separation mouth of separation drum bottom, the drain plug second end is connected with drainage subassembly, power unit passes through the closure of drainage subassembly drive drain plug control separation mouth, drainage subassembly is synchronous with rotating assembly's motion, the inside slidable mounting of separation drum has PH to detect the kicking block, PH detects and is provided with control mechanism between kicking block and the heater strip, the separation drum external connection has a hydrogen chloride section of thick bamboo.
Further, the drainage subassembly includes right-angle pole, connecting rod, and the first end fixed mounting of right-angle pole has the arc pole, and arc pole slidable mounting is covered at the support, supports to cover to be provided with the arc support, is provided with compression spring between arc pole and the arc support, and water barrel head portion is provided with slide rail, spring pin, and right-angle pole second end slidable mounting is on the slide rail, and connecting rod rotates connects right-angle pole and drain plug, is provided with compression spring between right-angle pole second end and the spring pin. When the arc pole slides, drive the right angle pole and slide, the right angle pole passes through the connecting rod and drives the drain plug and slide, the closure of control separation mouth, and compression spring assists drainage subassembly and drain plug and resumes initial position.
Further, the runner assembly includes dwang, driven gear, and the dwang rotates to be installed and covers in the support, and fixed mounting has the driving gear on the dwang, and driven gear rotates to be installed in the filter tube bottom, and fixed mounting has accelerating gear on the driven gear, accelerating gear and driving gear meshing. When the rotating rod rotates, the driving gear is driven to rotate, the driving gear drives the accelerating gear to rotate, and the accelerating gear drives the driven gear to rotate.
Further, power unit includes drain bar, clearance pole, and the drain bar rotates to be installed and covers in supporting, and clearance pole fixed mounting is in the drain bar top, and the central line of drain bar and clearance pole is on same straight line, and the contact cooperation of drain bar tip and arc pole, clearance pole and dwang contact cooperation. When the drainage rod rotates, the cleaning rod is driven to rotate, and when the drainage rod drives the arc-shaped rod to slide, the cleaning rod drives the rotating rod to rotate.
Further, the radian of the arc-shaped rod is 60 degrees, the rotating speed of the drainage rod is N, and N =1r/h.
Further, the clearance subassembly includes rack, push pedal, and rack fixed mounting is in the push pedal, rack and driven gear meshing, and push pedal slidable mounting is in the filter cylinder bottom, and the filter cylinder bottom is provided with the filter screen, is provided with reset spring between push pedal and the filter cylinder inner wall, and push pedal both ends symmetry slidable mounting has the regulating plate, is provided with the spring between regulating plate and the push pedal. The rack is driven to move when the driven gear rotates, the rack drives the push plate to slide at the bottom of the filter cartridge, when the push plate moves, the spring deforms, the adjusting plate is in close contact with the inner wall of the filter cartridge, the solid at the bottom of the filter cartridge is fully cleaned, and the reset spring assists the rotating assembly and the cleaning assembly to restore to the initial position.
Further, passive subassembly includes H type frame, slide bar, and H type frame first end rotates to be installed on the push pedal, and H type frame second end rotates to be installed on the baffle, and slide bar slidable mounting is in the cartridge filter outside, and the first end of slide bar is provided with closed stopper, and closed stopper slidable mounting is provided with the rocker between H type frame and the slide bar on the delivery port. The push plate drives the H-shaped frame to move when moving, the H-shaped frame and the rocker drive the baffle to slide on the filter cartridge, the baffle controls the closing of a discharge port on the filter cartridge, the rocker drives the slide bar to slide outside the filter cartridge, and the closing plug controls the closing of a water outlet.
Further, control mechanism includes pointer, heater, and the pointer is connected with PH detection floating block, and the pointer rotates to be installed in the cylinder outside, and fixed mounting has the band pulley on the pointer, and the heater is connected with the heater strip electricity, is provided with the heating button on the heater, is provided with the belt on band pulley and the heating button. PH detects the PH value that the flotation block detected the inside mixture of knockout drum, and PH detects the flotation block and gives the pointer with signal transmission, makes the pointer rotate, and the pointer drives the band pulley and rotates, and the band pulley passes through the belt and drives the heating button and rotate, and heating button drive heater starts, and heater strip heating knockout drum inside mixture when the heater starts.
Further, an air extractor is arranged at the joint of the hydrogen chloride cylinder and the separation cylinder, and an oil-water separation membrane is arranged at a separation port at the bottom of the separation cylinder. The oil-water separation membrane can only allow water to pass through, after the mixture in the separation cylinder is heated, the hydrogen chloride in the mixture is evaporated, and the air extractor sucks the evaporated hydrogen chloride into the hydrogen chloride cylinder.
Compared with the prior art, the invention has the beneficial effects that: (1) The separating mechanism provided by the invention can separate the solid and the liquid of the dimethyl dichlorosilane hydrolysate, so that the water and the oil can be conveniently layered; (2) The power mechanism arranged in the invention controls the driving mechanism and the drainage mechanism simultaneously, the matching between the structures is ingenious, and time is provided for water and oil layering; (3) The PH detection floating block is connected with the heating wire, and hydrogen chloride in the mixture is completely evaporated through the control mechanism; (4) The driving mechanism provided by the invention enables the cleaning component and the baffle plate to move simultaneously, so that the solids in the filter cylinder are fully cleaned.
Drawings
Fig. 1 is a schematic view of a first view of the overall structure of the present invention.
Fig. 2 is a schematic view of the overall structure of the present invention from a second perspective.
Fig. 3 is a schematic view of the overall structure of the present invention with the support cover removed.
Fig. 4 is a schematic view of fig. 3 with the separator removed.
Fig. 5 is a schematic view of fig. 4 with the filter cartridge removed.
Fig. 6 is a partially enlarged view of a portion a in fig. 1.
Fig. 7 is a partially enlarged view of a portion B in fig. 4.
Fig. 8 is a partially enlarged view of a portion C in fig. 4.
Fig. 9 is a partially enlarged view of a portion D in fig. 2.
Fig. 10 is a partially enlarged view of a portion E in fig. 1.
Reference numerals: 1-a separation mechanism; 11-a support cover; 12-a filter cartridge; 13-a separation drum; 131-an oil outlet; 132-a separation port; 14-a water cylinder; 111-a feed port; 112-arc support; 121-a discharge outlet; 122-a filter screen; 123-a separation plate; 141-a water outlet; 142-a slide rail; 143-spring pins; 15-a fixed spring; 16-a fixed pin; 2, a power mechanism; 21-a drain rod; 22-a clearing bar; 211-round pin; 3-a drive mechanism; 31-a rotating assembly; 32-a cleaning assembly; 33-a passive component; 34-a baffle plate; 35-a return spring; 311-rotating rods; 312-a drive gear; 313-an acceleration gear; 314-a driven gear; 321-a rack; 322-push plate; 323-regulating plate; 331-H type frame; 332-a rocker; 333-sliding bar; 3331-closure plug; 4-a drainage mechanism; 41-a drainage assembly; 42-a compression spring; 43-a drain plug; 411-right angle rod; 412-a connecting rod; 413-an arc-shaped rod; 5-a control mechanism; 51-a pointer; 52-a pulley; 53-belts; 54-a heater; 541-heating button; 6-heating wires; a 7-hydrogen chloride cylinder; 8-PH detection of the floaters.
Detailed Description
The technical scheme of the invention is further explained by the specific implementation mode in combination with the attached drawings.
Wherein the showings are for the purpose of illustration only and are shown by way of illustration only and not in actual form, and are not to be construed as limiting the present patent; for a better explanation of the embodiments of the present invention, some parts of the drawings may be omitted, enlarged or reduced, and do not represent the size of an actual product; it will be understood by those skilled in the art that certain well-known structures in the drawings and descriptions thereof may be omitted.
Example (b): as shown in fig. 1-10, the dimethyldichlorosilane hydrolysis oil-water separation tank includes a separation mechanism 1, a driving mechanism 3, a drainage mechanism 4, and a heating wire 6, where the separation mechanism 1 includes a support cover 11 and a separation cylinder 13, a filter cylinder 12 is disposed between the support cover 11 and the separation cylinder 13, the filter cylinder 12 is fixedly mounted above the separation cylinder 13, the heating wire 6 is fixedly wound outside the separation cylinder 13, a water cylinder 14 is fixedly disposed below the separation cylinder 13, a power mechanism 2 is disposed on the support cover 11, the driving mechanism 3 is disposed inside the filter cylinder 12, the driving mechanism 3 includes a rotating component 31 and a cleaning component 32, the rotating component 31 is rotatably mounted inside the filter cylinder 12, the cleaning component 32 is slidably mounted at the bottom of the filter cylinder 12, the power mechanism 2 drives the cleaning component 32 to slide at the bottom of the filter cylinder 12 through the rotating component 31, a baffle 34 is slidably mounted inside the filter cylinder 12, a passive component 33 is disposed between the baffle 34 and the cleaning component 32, and the passive component 33 drives the baffle 34 and a water outlet 141 on the water cylinder 14 to be closed; drainage mechanism 4 includes drainage component 41, drain plug 43, drainage component 41 sets up in support lid 11 top and water section of thick bamboo 14 bottom, drain plug 43 sets up inside water section of thick bamboo 14, drain plug 43 first end slidable mounting is on the isolating port 132 of separating cylinder 13 bottom, drain plug 43 second end is connected with drainage component 41, power unit 2 drives the closure of drain plug 43 control isolating port 132 through drainage component 41, drainage component 41 is synchronous with the motion of rotating assembly 31, the inside slidable mounting of separating cylinder 13 has PH to detect floating block 8, be provided with control mechanism 5 between PH detection floating block 8 and the heater strip 6, separating cylinder 13 external connection has hydrogen chloride section of thick bamboo 7.
As shown in fig. 2, 3, 5, 6, and 9, in the separation mechanism 1, a filter cylinder 12 is fixedly installed below a support cover 11, a separation cylinder 13 is fixedly installed below the filter cylinder 12, a water cylinder 14 is fixedly installed at the bottom of the separation cylinder 13, an oil outlet 131 is arranged on the side surface of the separation cylinder 13, a separation port 132 is arranged at the bottom of the separation cylinder 13, an air extractor is arranged inside the connection between the hydrogen chloride cylinder 7 and the separation cylinder 13, and an oil-water separation membrane is arranged at the separation port 132 and only allows water to pass through; a water outlet 141 is arranged on the water barrel 14, a slide rail 142 and a spring pin 143 are arranged at the bottom of the water barrel 14, a feed port 111 and an arc support 112 are arranged on the support cover 11, a fixing pin 16 is vertically and slidably mounted on the support cover 11, a fixing spring 15 is arranged between the fixing pin 16 and the support cover 11, a first end of the fixing spring 15 is fixedly mounted on the fixing pin 16, and a second end of the fixing spring 15 is fixedly mounted on the support cover 11; the filter cylinder 12 is provided with a discharge port 121, a filter screen 122 and a partition board 123, the power mechanism 2 is rotatably arranged on the support cover 11, the drain rod 21 is rotatably arranged on the support cover 11, the cleaning rod 22 is fixedly arranged above the drain rod 21, the central lines of the drain rod 21 and the cleaning rod 22 are on the same straight line, the drain rod 21 and the power source are fixedly arranged, the power source is arranged inside the support cover 11, the rotation speed of the drain rod 21 is N, N =1r/h, and the drain rod 21 drives the cleaning rod 22 to rotate when rotating; the drain bar 21 is provided with a round pin 211, the round pin 211 is engaged with the end of the fixing pin 16, and the fixing pin 16 restricts the rotation of the drain bar 21.
As shown in fig. 5, 6 and 9, the drainage mechanism 4 is arranged on the support cover 11 and the water drum 14, the drainage mechanism 4 comprises a drainage assembly 41, a compression spring 42 and a drainage plug 43, the drainage assembly 41 comprises a right-angle rod 411, a connecting rod 412 and an arc-shaped rod 413, the arc-shaped rod 413 is fixedly arranged at a first end of the right-angle rod 411, the arc-shaped rod 413 is slidably arranged on the support cover 11, and the radian of the arc-shaped rod is 60 degrees; the initial position of the end of the round pin 211 is located at the second end of the arc-shaped rod 413; the end part of the drainage rod 21 is in contact fit with the arc rod 413, the drainage rod 21 rotates, and when the drainage rod 21 is in contact with the arc rod 413, the arc rod 413 is driven to slide; the second end of the right-angle rod 411 is slidably mounted on the sliding rail 142, the connecting rod 412 is arranged between the right-angle rod 411 and the drain plug 43, the drain plug 43 is arranged inside the water drum 14, the first end of the drain plug 43 is slidably mounted on the separation port 132 at the bottom of the separation drum 13, the first end of the connecting rod 412 is rotatably mounted with the right-angle rod 411, and the second end of the connecting rod 412 is rotatably mounted with the second end of the drain plug 43; be provided with compression spring 42 between arc pole 413 and arc support 112, compression spring 42 first end fixed mounting is on arc pole 413, compression spring 42 second end fixed mounting is on arc support 112, be provided with compression spring 42 between right angle pole 411 second end and the spring pin 143, compression spring 42 first end fixed mounting is on right angle pole 411, compression spring 42 second end fixed mounting is on spring pin 143, when arc pole 413 slides, it slides to drive right angle pole 411, right angle pole 411 passes through connecting rod 412 and drives the slip of drain plug 43, the closure of control separation mouth 132, the supplementary drainage component 41 of compression spring 42 and the recovery initial position of drain plug 43.
As shown in fig. 3, 4, 5, 7, 8, the driving mechanism 3 is disposed inside the filter cartridge 12, and includes a rotating component 31, a cleaning component 32, a driven component 33, and a baffle 34, the rotating component 31 is rotatably mounted inside the filter cartridge 12, the rotating component 31 includes a rotating rod 311, a driving gear 312, an accelerating gear 313, and a driven gear 314, the rotating rod 311 is rotatably mounted on the support cover 11, the driving gear 312 is rotatably mounted inside the support cover 11, the driving gear 312 is fixedly mounted to the rotating rod 311, the rotating rod 311 drives the driving gear 312 to rotate when rotating, the accelerating gear 313 is rotatably mounted above the partition 123, the accelerating gear 313 is engaged with the driving gear 312, the driving gear 312 drives the accelerating gear 313 to rotate, the driven gear 314 is rotatably mounted at the bottom of the filter cartridge 12, and the driven gear 314 is driven to rotate when the accelerating gear 313 rotates.
As shown in fig. 7 and 8, the cleaning assembly 32 includes a rack 321, a push plate 322, and an adjusting plate 323, the rack 321 is fixedly mounted on the push plate 322, the rack 321 is engaged with the driven gear 314, and the driven gear 314 drives the rack 321 to move when rotating; the push plate 322 is slidably mounted at the bottom of the filter cartridge 12, and the rack 321 drives the push plate 322 to slide at the bottom of the filter cartridge 12; a return spring 35 is arranged between the push plate 322 and the inner wall of the filter cartridge 12, when the push plate 322 moves, the spring deforms, and the return spring 35 assists the rotating assembly 31 and the cleaning assembly 32 to recover to the initial positions; adjusting plate 323 symmetry slidable mounting is provided with the spring between adjusting plate 323 and the push pedal 322 at push pedal 322 both ends, makes adjusting plate 323 and cartridge filter 12 inner wall in close contact with, fully clears up the solid of cartridge filter 12 bottom.
As shown in fig. 5 and 8, the passive component 33 includes an H-shaped frame 331, a rocker 332, a sliding rod 333, a first end of the H-shaped frame 331 is rotatably mounted on the pushing plate 322, a second end of the H-shaped frame 331 is rotatably mounted on the baffle 34, the baffle 34 is slidably mounted inside the filter cartridge 12, and the baffle 34 closes the discharge port 121 of the filter cartridge 12; the sliding rod 333 is slidably mounted outside the filter cartridge 12, a first end of the sliding rod 333 is provided with a closing plug 3331, the closing plug 3331 is slidably mounted on the water outlet 141, the cleaning component 32 is arranged between the H-shaped frame 331 and the sliding rod 333, a first end of the rocker 332 is rotatably mounted at a second end of the H-shaped frame 331, and a second end of the rocker 332 is rotatably mounted at a second end of the sliding rod 333; when the push plate 322 moves, the H-shaped frame 331 is driven to move, the H-shaped frame 331 and the rocker 332 drive the baffle 34 to slide on the filter cartridge 12, the baffle 34 controls the closing of the discharge port 121, the rocker 332 drives the slide rod 333 to slide outside the filter cartridge 12, and the closing plug 3331 controls the closing of the water outlet 141.
As shown in fig. 1, 5 and 10, the control mechanism 5 is disposed between the PH detection floating block 8 and the heating wire 6, the pointer 51 is connected to the PH detection floating block 8, the pointer 51 is rotatably mounted outside the separation drum 13, the pointer 51 is fixedly mounted with the pulley 52, the heater 54 is electrically connected to the heating wire 6, the heater 54 is provided with the heating button 541, and the pulley 52 and the heating button 541 are provided with the belt 53. The PH detection floating block 8 detects the PH value of the mixture in the separation cylinder 13, the PH detection floating block 8 transmits a signal to the pointer 51 to enable the pointer 51 to rotate, the pointer 51 drives the belt wheel 52 to rotate, the belt wheel 52 drives the heating button 541 to rotate through the belt 53, the heating button 541 drives the heater 54 to start, and the heating wire 6 heats the mixture in the separation cylinder 13 when the heater 54 starts.
The working principle is as follows: the initial position of the end of the round pin 211 is located at the second end of the arc rod 413, the feed inlet 111 is opened, the mixture of the hydrolysate is poured into the filter cylinder 12, the solid in the mixture is filtered by the filter screen 122 at the bottom of the filter cylinder 12, the mixed liquid falls into the separation cylinder 13, the fixing pin 16 is moved upwards, the fixing spring 15 is extended, the end of the fixing pin 16 is separated from the round pin 211, the power source is started, and the power source drives the power mechanism 2 to rotate.
In the process, the filter screen filters solids, the PH detection floating block 8 floats in the separating cylinder 13 according to the height of the mixed liquid, the PH value of the mixed liquid in the separating cylinder 13 is detected, when the PH value is smaller than 7, hydrogen chloride is proved to exist, the PH detection floating block 8 transmits a signal to the pointer 51, the pointer 51 is driven to rotate, the pointer 51 drives the belt wheel 52 to rotate, the belt wheel 52 drives the heating button 541 to rotate through the belt 53, the heating button 541 drives the heater 54 to start, the heating wire 6 heats the mixed liquid in the separating cylinder 13 when the heater 54 is started, after the mixed liquid in the separating cylinder 13 is heated, the hydrogen chloride in the mixed liquid is evaporated, when the PH value is 7, the heating is stopped, in the process, the air extractor sucks the hydrogen chloride gas into the hydrogen chloride cylinder 7, and the mixed liquid is statically layered in the separating cylinder 13.
After the mixed liquid in the separating cylinder 13 is layered, water is on the lower layer of the separating cylinder 13, oil is on the upper layer of the separating cylinder 13, the end part of the water discharging rod 21 is contacted with the first end of the arc-shaped rod 413, meanwhile, the cleaning rod 22 is contacted with the rotating rod 311, the water discharging rod 21 drives the arc-shaped rod 413 to slide, the arc-shaped rod 413 drives the right-angle rod 411 to slide, the compression spring 42 is compressed, the right-angle rod 411 drives the water discharging plug 43 to slide through the connecting rod 412, the separating opening 132 is opened, and the water on the lower layer in the separating cylinder 13 enters the water cylinder 14 through an oil-water separating film on the separating opening 132; meanwhile, when the rotating rod 311 rotates, the driving gear 312 is driven to rotate, the driving gear 312 drives the accelerating gear 313 to rotate, the accelerating gear 313 drives the driven gear 314 to rotate, when the driven gear 314 rotates, the rack 321 is driven to move, the rack 321 drives the push plate 322 to slide at the bottom of the filter cartridge 12, the return spring 35 extends, and when the push plate 322 moves, the spring deforms, so that the adjusting plate 323 is in close contact with the inner wall of the filter cartridge 12, the solid at the bottom of the filter cartridge 12 is fully cleaned, and the solid is pushed to the discharge port 121; when the push plate 322 moves, the H-shaped frame 331 is driven to move, the H-shaped frame 331 and the rocker 332 drive the baffle 34 to slide on the filter cartridge 12, the discharge port 121 is opened by the baffle 34, the slide rod 333 is driven by the rocker 332 to slide outside the filter cartridge 12, the water outlet 141 is opened by the closing plug 3331, the solid in the filter cartridge 12 leaks out from the discharge port 121, and the water in the water cartridge 14 flows out from the water outlet 141.
When the end of the water drainage rod 21 contacts with the second end of the arc-shaped rod 413, the pH value in the separation cylinder 13 is a hydrogen chloride cylinder 7, the control mechanism 5 and the heating wire 6 stop working, the water-oil separation in the separation cylinder 13 is completed, the solid in the filter cylinder 12 is cleaned up, the water drainage rod 21 continues to rotate, the end of the water drainage rod 21 is disconnected from the second end of the arc-shaped rod 413 and contacts, the compression spring 42, the reset spring 35, the spring between the adjusting plate 323 and the push plate 322, the auxiliary water drainage mechanism 4 and the driving mechanism 3 recover the initial position, the power source is closed, the end of the fixing pin 16 is lifted to be meshed with the round pin 211, the oil outlet 131 is opened, and the oil is discharged from the separation cylinder 13.
The present invention is not limited to the above-described embodiments, and those skilled in the art will be able to make various modifications without creative efforts from the above-described conception and fall within the scope of the present invention.
Claims (9)
1. The utility model provides a dimethyldichlorosilane water oil water layering jar, includes separating mechanism (1), actuating mechanism (3), its characterized in that: the water-saving separation device is characterized by further comprising a drainage mechanism (4) and a heating wire (6), wherein the separation mechanism (1) comprises a supporting cover (11) and a separation cylinder (13), a filter cylinder (12) is arranged between the supporting cover (11) and the separation cylinder (13), the filter cylinder (12) is fixedly installed above the separation cylinder (13), the heating wire (6) is fixedly wound outside the separation cylinder (13), a water cylinder (14) is fixedly arranged below the separation cylinder (13), a power mechanism (2) is arranged on the supporting cover (11), a driving mechanism (3) is arranged inside the filter cylinder (12), the driving mechanism (3) comprises a rotating assembly (31) and a cleaning assembly (32), the rotating assembly (31) is rotatably installed inside the filter cylinder (12), the cleaning assembly (32) is slidably installed at the bottom of the filter cylinder (12), the power mechanism (2) drives the cleaning assembly (32) to slide at the bottom of the filter cylinder (12) through the rotating assembly (31), a baffle (34) is slidably installed inside the filter cylinder (12), a passive assembly (33) is arranged between the baffle (34) and a water outlet of the water cylinder (141) is driven by the passive assembly (33); drainage mechanism (4) are including drainage component (41), drain plug (43), drainage component (41) set up and are being supported lid (11) top and water section of thick bamboo (14) bottom, drain plug (43) set up inside water section of thick bamboo (14), drain plug (43) first end slidable mounting is on isolating port (132) of isolating cylinder (13) bottom, drain plug (43) second end is connected with drainage component (41), power unit (2) are through drainage component (41) drive drain plug (43) control isolating port's (132) closure, drainage component (41) are synchronous with the motion of runner assembly (31), isolating cylinder (13) inside slidable mounting has PH to detect floating block (8), be provided with control mechanism (5) between PH detection floating block (8) and heater strip (6), isolating cylinder (13) external connection has hydrogen chloride section of thick bamboo (7).
2. The dimethyldichlorosilane hydrolyzed oil-water stratified tank of claim 1, wherein: drainage component (41) is including right angle pole (411), connecting rod (412), right angle pole (411) first end fixed mounting has arc pole (413), arc pole (413) slidable mounting is on supporting lid (11), be provided with arc support (112) on supporting lid (11), be provided with compression spring (42) between arc pole (413) and arc support (112), water section of thick bamboo (14) bottom is provided with slide rail (142), spring pin (143), right angle pole (411) second end slidable mounting is on slide rail (142), connecting rod (412) rotate connection right angle pole (411) and drain plug (43), be provided with compression spring (42) between right angle pole (411) second end and spring pin (143).
3. The dimethyldichlorosilane hydrolyzed oil-water stratified tank of claim 2, wherein: the rotating assembly (31) comprises a rotating rod (311) and a driven gear (314), the rotating rod (311) is rotatably installed on the supporting cover (11), a driving gear (312) is fixedly installed on the rotating rod (311), the driven gear (314) is rotatably installed at the bottom of the filter cylinder (12), an accelerating gear (313) is fixedly installed on the driven gear (314), and the accelerating gear (313) is meshed with the driving gear (312).
4. The dimethyldichlorosilane hydrolyzed oil-water stratified tank of claim 3, wherein: power unit (2) include drain bar (21), clearance pole (22), and drain bar (21) rotate to be installed on supporting lid (11), and clearance pole (22) fixed mounting is in drain bar (21) top, and drain bar (21) and the central line of clearance pole (22) are on same straight line, drain bar (21) tip and arc pole (413) contact cooperation, clearance pole (22) and dwang (311) contact cooperation.
5. The dimethyldichlorosilane hydrolyzed oil-water stratified tank of claim 4, wherein: the radian of the arc-shaped rod (413) is 60 degrees, the rotation speed of the drainage rod (21) is N, and N =1r/h.
6. The dimethyldichlorosilane hydrolyzed oil-water stratified tank of claim 3, wherein: clearance subassembly (32) are including rack (321), push pedal (322), rack (321) fixed mounting is on push pedal (322), rack (321) and driven gear (314) meshing, push pedal (322) slidable mounting is in cartridge filter (12) bottom, cartridge filter (12) bottom is provided with filter screen (122), be provided with reset spring (35) between push pedal (322) and cartridge filter (12) inner wall, push pedal (322) both ends symmetry slidable mounting has regulating plate (323), be provided with the spring between regulating plate (323) and push pedal (322).
7. The dimethyldichlorosilane hydrolyzed oil-water stratified tank of claim 6, wherein: the passive component (33) comprises an H-shaped frame (331) and a sliding rod (333), wherein the first end of the H-shaped frame (331) is rotatably installed on the push plate (322), the second end of the H-shaped frame (331) is rotatably installed on the baffle (34), the sliding rod (333) is slidably installed outside the filter cartridge (12), the first end of the sliding rod (333) is provided with a closing plug (3331), the closing plug (3331) is slidably installed on the water outlet (141), and a rocker (332) is arranged between the H-shaped frame (331) and the sliding rod (333).
8. The dimethyldichlorosilane hydrolyzed oil-water stratified tank of claim 1, wherein: control mechanism (5) include pointer (51), heater (54), and pointer (51) are connected with PH detection floating block (8), and pointer (51) rotate to be installed in separating cylinder (13) outside, and fixed mounting has band pulley (52) on pointer (51), and heater (54) are connected with heater strip (6) electricity, are provided with on heater (54) heating button (541), are provided with belt (53) on band pulley (52) and the heating button (541).
9. The dimethyldichlorosilane hydrolyzed oil-water stratified tank of claim 1, wherein: an air extractor is arranged at the joint of the hydrogen chloride cylinder (7) and the separating cylinder (13), and an oil-water separation membrane is arranged at a separation port (132) at the bottom of the separating cylinder (13).
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