CN115094638A - 一种假发后处理工艺及其所用整理剂 - Google Patents
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Abstract
本发明提出了一种假发后处理工艺及其所用整理剂,假发经过清洗后,沥干水分,经过整理剂的处理,定型,烘干,得到最终的假发产品。经过本发明处理的假发,具有良好的柔顺度和悬垂感,提高了发丝的韧性,改善打结的现象,提高了假发的耐水洗性能。
Description
技术领域
本发明属于D06M15/643技术领域,具体涉及一种假发后处理工艺及其所用整理剂。
背景技术
出于对美丽和个性的追求,假发已经逐渐从影视作品、舞台表演进入人们的日常生活。假发在使用过程中容易出现打结、毛糙、掉发、短发的情况,这些情况的出现降低了假发使用时的美观度。中国专利CN103938441B中公开了一种假发滑爽剂及对假发的整理方法,通过加入含巯基乙酸的物质进行假发的定型处理,并通过高温蒸油,让各成分充分附着到发丝表面,提高发丝耐洗性,但是该方法中所用的部分化学品接触空气容易氧化,释放出有毒气体,并且高温蒸油对发丝可能会造成二次损伤。基于此,本发明提出了一种假发后处理工艺及其所用整理剂,以温和的方式提高假发的定型效果和易梳理性、耐水洗性能等。
发明内容
本发明第一个方面提出了一种假发后处理工艺,包括以下步骤:
(1)假发经过3次清洗,去除浮色、油剂;单次清洗时间为1-5min,清洗温度为30-40℃;
(2)假发脱水沥干;
(3)整理剂浸泡处理;假发在整理剂中浸泡处理3次,单次浸泡时间为3-10min,整理剂温度为40-70℃;
(4)平铺打理;假发平铺在金属板上,充分去除水分,打理假发成相应的造型;
(5)烘干;烘干室温度为40-60℃。
在一种优选的实施方式中,所述步骤(1)中假发经过3次清洗,第一次清洗和第二次清洗为清洗剂清洗,第三次清洗为清水清洗。
在一种优选的实施方式中,所述清洗剂中含有除油剂,除油剂占总清洗剂质量的0.1-5%。
在一种优选的实施方式中,所述除油剂含有月桂醇聚醚硫酸酯钠、烷基酰胺丙基甜菜碱,所述月桂醇聚醚硫酸酯钠、烷基酰胺丙基甜菜碱的质量比为2:3。
在一种优选的实施方式中,所述烷基酰胺丙基甜菜碱选自椰油酰胺丙基甜菜碱、月桂酰胺丙基甜菜碱、十八酰胺基丙基甜菜碱、辛基酰胺丙基甜菜碱中的至少一种。
在一种优选的实施方式中,所述烷基酰胺丙基甜菜碱为月桂酰胺丙基甜菜碱。
在一种优选的实施方式中,所述步骤(1)中第一次清洗的时间为5min,清洗温度为40℃,第二次清洗的时间为3min,清洗温度为35℃,第三次清洗的时间为3min,清洗温度为35℃。
在一种优选的实施方式中,所述除油剂占总清洗剂质量的5%。
申请人在假发后处理过程的实验中发现,在清洗阶段,加入特定成分的除油剂,可以有效去除附着于发丝表面的油污和杂质,但是申请人发现如果只用月桂醇聚醚硫酸酯钠进行发丝的去油污,会出现月桂醇聚醚硫酸酯钠和油污共同在发丝表面残留的现象,对于后续的整理、定型造成一定的影响,然而当加入的月桂醇聚醚硫酸酯钠、月桂酰胺丙基甜菜碱的质量比为2:3时,月桂酰胺丙基甜菜碱可以促进月桂醇聚醚硫酸酯钠和油污在水中的溶解度。
在本申请中,步骤(4)中的造型型状没有具体限定,可以根据需要设计。
在一种优选的实施方式中,所述步骤(5)中烘干室的温度为50℃。
本发明第二个方面提出了一种假发后处理工艺的整理剂,所述整理剂包括整理剂A和整理剂B。
在一种优选的实施方式中,所述整理剂A用于第一次浸泡处理,所述整理剂B用于第二次和第三次浸泡处理。
在一种优选的实施方式中,第一次浸泡处理的时间为8min,温度为50℃;第二次浸泡处理的时间为5min,温度为55℃;第三次浸泡处理的时间为5min,温度为50℃。
在一种优选的实施方式中,所述整理剂A的原料包括:烷基膦化物、聚有机硅氧烷、去离子水。
在一种优选的实施方式中,所述整理剂A中烷基膦化物、聚有机硅氧烷、去离子水的质量比为(0.12-0.16):(0.1-1):10。
在一种优选的实施方式中,所述整理剂A中烷基膦化物、聚有机硅氧烷、去离子水的质量比为0.15:0.3:10。
在一种优选的实施方式中,所述聚有机硅氧烷选自氨基聚有机硅氧烷、环氧基聚有机硅氧烷、羟基聚有机硅氧烷、聚醚改性聚有机硅氧烷中的至少一种。
在一种优选的实施方式中,所述聚有机硅氧烷为聚醚改性聚有机硅氧烷。
在一种优选的实施方式中,所述烷基膦化物选自三甲基膦、三异丙基膦、三(2-羧乙基)膦、(2-氯乙基)膦酸二乙酯中的至少一种。
在一种优选的实施方式中,所述烷基膦化物为三(2-羧乙基)膦。
在一种优选的实施方式中,所述整理剂B的原料包括:阳离子羟基硅油、聚有机硅氧烷、氨基酸类物质、丙烯酸酯类聚合物、去离子水。
在一种优选的实施方式中,所述阳离子羟基硅油、聚有机硅氧烷、氨基酸类物质的质量比为(1-2):(1-3):(0.1-1)。
在一种优选的实施方式中,所述阳离子羟基硅油、聚有机硅氧烷、氨基酸类物质的质量比为1.2:3:0.1。
在一种优选的实施方式中,所述丙烯酸酯类聚合物与聚有机硅氧烷的质量比为2:(15-18)。
在一种优选的实施方式中,所述丙烯酸酯类聚合物与聚有机硅氧烷的质量比为2:15。
在一种优选的实施方式中,所述聚有机硅氧烷为氨基聚有机硅氧烷和聚醚改性聚有机硅氧烷的复配物质。
在一种优选的实施方式中,所述氨基聚有机硅氧烷和聚醚改性聚有机硅氧烷的质量比为1:1。
在一种优选的实施方式中,所述丙烯酸酯类聚合物的粘度为1000-15000mPa·s。
在一种优选的实施方式中,所述丙烯酸酯类聚合物的粘度为4000-11000mPa·s,购买于广州胜欣化工科技有限公司。
在一种优选的实施方式中,所述氨基酸类物质为月桂酰肌氨酸钠。
申请人在假发后处理过程的实验中发现,假发经过不同的整理剂处理后,可以提高假发的垂顺度、耐水性能力,并且在后续的造型定型过程中,便于定型。申请人推测可能的原因是,假发先经过整理剂A处理,破坏了发丝中的二硫键,提高发丝的柔软度和可塑性,而后假发经过整理剂B处理,整理剂B中的聚合物附着于发丝表面,通过相互间的交联作用,在发丝表面形成防护膜层,并且发丝中的二硫键在整理剂B中出现重连的趋势,经过烘干后,提高了发丝的定型效果,并且发丝表面的防护膜维持了发丝毛鳞片的闭合状态,降低了发丝间的摩擦力,提高假发的梳理性能,还赋予了假发一定的抗静电能力。
在一种优选的实施方式中,所述整理剂A,按重量份计,包括15份三(2-羧乙基)膦、30份聚醚改性聚有机硅氧烷、1000份去离子水。
在一种优选的实施方式中,所述整理剂B,按重量份计,包括:24份阳离子羟基硅油、30份氨基聚有机硅氧烷、30份聚醚改性聚有机硅氧烷、3份月桂酰肌氨酸钠、8份丙烯酸酯类聚合物、1000份去离子水。
与现有技术相比,本发明具有的有益效果:
假发经过本发明所提供的后处理工艺进行处理后,可以提高假发柔顺度和悬垂感,并且假发经过处理后提高了假发发丝的韧性,改善假发发丝出现打结的现象,于此同时,假发经过特定的整理剂处理后,让发丝表面的毛鳞片处于闭合状态,降低了发丝相互间的摩擦力,提高了假发的耐水洗性能,还赋予了假发发丝一定的防静电效果。
具体实施方式
实施例1
本发明提出了一种假发后处理工艺及其所用整理剂,假发后处理工艺,包括以下步骤:
(1)假发经过3次清洗,去除浮色、油剂;第一次清洗为清洗剂清洗,40℃下清洗5min,第二次清洗为清洗剂清洗,35℃下清洗3min,第三次清洗为清水清洗,35℃下清洗3min;
(2)假发脱水沥干;
(3)整理剂浸泡处理,假发在整理剂中浸泡处理3次;第一次浸泡用整理剂为整理剂A,在50℃下浸泡处理8min,第二次浸泡用整理剂为整理剂B,在55℃下浸泡处理5min,第三次浸泡用整理剂为整理剂B,在50℃下浸泡处理5min;
(4)平铺打理;假发平铺在金属板上,充分去除水分,打理假发成相应的造型;
(5)将假发在50℃下烘干。
其中,清洗剂的原料,按重量份数计,包括:2份月桂醇聚醚硫酸酯钠、3份月桂酰胺丙基甜菜碱、95份去离子水。
其中,整理剂A的原料,按重量份数计,包括:15份三(2-羧乙基)膦、30份聚醚改性聚有机硅氧烷、1000份去离子水。
其中,整理剂B的原料,按重量份数计,包括:24份阳离子羟基硅油、30份氨基聚有机硅氧烷、30份聚醚改性聚有机硅氧烷、3份月桂酰肌氨酸钠、8份份丙烯酸酯类聚合物、1000份去离子水。
阳离子羟基硅油购买于许昌凯特精细化工厂,型号为信捷2#。
氨基聚有机硅氧烷购买于嘉善江南纺织材料有限公司,型号JF-8052。
聚醚改性聚有机硅氧烷购买于扬州市天泰化工有限公司。
丙烯酸酯类聚合物的粘度为4000-11000mPa·s,购买于广州胜欣化工科技有限公司。
实施例2
本发明提出了一种假发后处理工艺及其所用整理剂,假发后处理工艺,包括以下步骤:
(1)假发经过3次清洗,去除浮色、油剂;第一次清洗为清洗剂清洗,40℃下清洗5min,第二次清洗为清洗剂清洗,35℃下清洗3min,第三次清洗为清水清洗,35℃下清洗3min;
(2)假发脱水沥干;
(3)整理剂浸泡处理,假发在整理剂中浸泡处理3次;整理剂为整理剂B,第一次在50℃下浸泡处理8min,第二次在55℃下浸泡处理5min,第三次在50℃下浸泡处理5min;
(4)平铺打理;假发平铺在金属板上,充分去除水分,打理假发成相应的造型;
(5)将假发在50℃下烘干。
其中,清洗剂的原料,按重量份数计,包括:2份月桂醇聚醚硫酸酯钠、98份去离子水。
其中,整理剂B的原料,按重量份数计,包括:24份阳离子羟基硅油、30份氨基聚有机硅氧烷、30份聚醚改性聚有机硅氧烷、3份月桂酰肌氨酸钠、8份丙烯酸酯类聚合物、1000份去离子水。
阳离子羟基硅油购买于许昌凯特精细化工厂,型号为信捷2#。
氨基聚有机硅氧烷购买于嘉善江南纺织材料有限公司,型号JF-8052。
聚醚改性聚有机硅氧烷购买于扬州市天泰化工有限公司。
丙烯酸酯类聚合物的粘度为4000-11000mPa·s,购买于广州胜欣化工科技有限公司。
实施例3
本发明提出了一种假发后处理工艺及其所用整理剂,假发后处理工艺,包括以下步骤:
(1)假发经过3次清水清洗,去除浮色、油剂;单次清洗温度为35℃,单次清洗时间为3min;
(2)假发脱水沥干;
(3)整理剂浸泡处理,假发在整理剂中浸泡处理3次;第一次浸泡用整理剂为整理剂A,在50℃下浸泡处理8min,第二次浸泡用整理剂为整理剂B,在55℃下浸泡处理5min,第三次浸泡用整理剂为整理剂B,在50℃下浸泡处理5min;
(4)平铺打理;假发平铺在金属板上,充分去除水分,打理假发成相应的造型;
(5)将假发在50℃下烘干。
其中,整理剂A的原料,按重量份数计,包括:15份三(2-羧乙基)膦、30份聚醚改性聚有机硅氧烷、1000份去离子水。
其中,整理剂B的原料,按重量份数计,包括:24份阳离子羟基硅油、30份氨基聚有机硅氧烷、30份聚醚改性聚有机硅氧烷、1000份去离子水。
阳离子羟基硅油购买于许昌凯特精细化工厂,型号为信捷2#。
氨基聚有机硅氧烷购买于嘉善江南纺织材料有限公司,型号JF-8052。
聚醚改性聚有机硅氧烷购买于扬州市天泰化工有限公司。
性能测试
将实施例制备得到的假发,选取造型为长直发的假发,进行梳理性、耐水洗性、防静电性测试。数据记录在表1中。
1.梳理性
将假发理顺后放置于倾斜角度为60°的斜面上,让钢梳从假发的发根部自由滑落,记录钢梳下滑距离。
2.耐水洗性
取长度为38cm,重量为20g/条的假发,按照本领域技术人员知晓的假发清洗方式清洗60次后,记录剩余假发的重量。
将20g/条假发按照本领域技术人员知晓的假发清洗方式清洗20次后,自然风干,通过触摸判断手感。当清洗后假发手感与未清洗假发手感相似,等级为A,当清洗后假发手感发涩,等级为B,并根据发涩程度的加深,等级逐渐下降。
3.防静电测试
取长度为30cm,总量为60g的同一批次假发,等重量分成3份,按照实施例中公开的方法,将假发清洗后沥干水分,用动态梳理性测试仪进行头发表面静电压测试,速度为150mm/s,静电压记为V1。将测试后的假发按照实施例中公开的方法进行整理剂处理和后续处理,假发烘干后,用动态梳理性测试仪进行头发表面静电压测试,速度为150mm/s,静电压记为V2。计算静电压差值,差值越大,说明假发抗静电效果越好。
静电压差值=V1-V2。
表1
梳理性cm | 剩余重量g | 触摸手感 | 静电压差值v | |
实施例1 | 35 | 19.95 | A | 1.1 |
实施例2 | 28 | 19.93 | B | 0.9 |
实施例3 | 31 | 19.92 | C | 0.6 |
Claims (10)
1.一种假发后处理工艺,其特征在于,包括以下步骤:
(1)假发经过3次清洗,去除浮色、油剂;单次清洗时间为1-5min,清洗温度为30-40℃;
(2)假发脱水沥干;
(3)整理剂浸泡处理;假发在整理剂中浸泡处理3次,单次浸泡时间为3-10min,整理剂温度为40-70℃;
(4)平铺打理;假发平铺在金属板上,充分去除水分,打理假发成相应的造型;
(5)烘干;烘干室温度为40-60℃。
2.根据权利要求1所述的假发后处理工艺,其特征在于,所述步骤(1)中假发经过3次清洗,第一次清洗和第二次清洗为清洗剂清洗,第三次清洗为清水清洗。
3.根据权利要求2所述的假发后处理工艺,其特征在于,所述清洗剂中含有除油剂,除油剂占总清洗剂质量的0.1-5%。
4.根据权利要求3所述的假发后处理工艺,其特征在于,所述除油剂含有月桂醇聚醚硫酸酯钠、烷基酰胺丙基甜菜碱,所述月桂醇聚醚硫酸酯钠、烷基酰胺丙基甜菜碱的质量比为2:3。
5.一种根据权利要求1-4任一项所述的假发后处理工艺中的整理剂,其特征在于,整理剂包括整理剂A和整理剂B。
6.根据权利要求5所述的整理剂,其特征在于,所述整理剂A用于第一次浸泡处理,所述整理剂B用于第二次和第三次浸泡处理。
7.根据权利要求6所述的整理剂,其特征在于,所述整理剂A的原料包括:烷基膦化物、聚有机硅氧烷、去离子水。
8.根据权利要求6所述的整理剂,其特征在于,所述整理剂B的原料包括:阳离子羟基硅油、聚有机硅氧烷、氨基酸类物质、丙烯酸酯类聚合物、去离子水。
9.根据权利要求7所述的整理剂,其特征在于,所述整理剂A中烷基膦化物、聚有机硅氧烷、去离子水的质量比为(0.12-0.16):(0.1-1):10。
10.根据权利要求8所述的整理剂,其特征在于,所述整理剂B中阳离子羟基硅油、聚有机硅氧烷、氨基酸类物质的质量比为(1-2):(1-3):(0.1-1)。
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