CN115029021A - 一种大粒径、低结构软质炭黑的制备方法 - Google Patents
一种大粒径、低结构软质炭黑的制备方法 Download PDFInfo
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- CN115029021A CN115029021A CN202210721818.7A CN202210721818A CN115029021A CN 115029021 A CN115029021 A CN 115029021A CN 202210721818 A CN202210721818 A CN 202210721818A CN 115029021 A CN115029021 A CN 115029021A
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- 239000006229 carbon black Substances 0.000 title claims abstract description 68
- 229910021384 soft carbon Inorganic materials 0.000 title claims abstract description 20
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims abstract description 82
- 239000007789 gas Substances 0.000 claims abstract description 80
- 238000006243 chemical reaction Methods 0.000 claims abstract description 57
- 239000002245 particle Substances 0.000 claims abstract description 38
- 239000003345 natural gas Substances 0.000 claims abstract description 36
- 238000002156 mixing Methods 0.000 claims abstract description 33
- 239000000571 coke Substances 0.000 claims abstract description 28
- 238000004227 thermal cracking Methods 0.000 claims abstract description 14
- 241000872198 Serjania polyphylla Species 0.000 claims abstract description 13
- 238000010791 quenching Methods 0.000 claims abstract description 12
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000003546 flue gas Substances 0.000 claims abstract description 11
- 230000000171 quenching effect Effects 0.000 claims abstract description 11
- 230000002093 peripheral effect Effects 0.000 claims abstract description 6
- 238000000926 separation method Methods 0.000 claims abstract description 4
- 239000007787 solid Substances 0.000 claims abstract description 4
- 238000000034 method Methods 0.000 claims description 19
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 8
- 229910052739 hydrogen Inorganic materials 0.000 claims description 8
- 239000001257 hydrogen Substances 0.000 claims description 8
- 238000010891 electric arc Methods 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 7
- 238000002679 ablation Methods 0.000 abstract description 4
- 230000003647 oxidation Effects 0.000 abstract description 4
- 238000007254 oxidation reaction Methods 0.000 abstract description 4
- 235000019241 carbon black Nutrition 0.000 description 61
- 239000000047 product Substances 0.000 description 30
- 230000000052 comparative effect Effects 0.000 description 25
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 21
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 18
- 229910052799 carbon Inorganic materials 0.000 description 17
- 238000004939 coking Methods 0.000 description 14
- 239000012265 solid product Substances 0.000 description 13
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- 230000002829 reductive effect Effects 0.000 description 9
- 238000002834 transmittance Methods 0.000 description 7
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 6
- 238000004458 analytical method Methods 0.000 description 6
- 238000001514 detection method Methods 0.000 description 6
- 229910052740 iodine Inorganic materials 0.000 description 6
- 239000011630 iodine Substances 0.000 description 6
- 239000012798 spherical particle Substances 0.000 description 6
- 238000005336 cracking Methods 0.000 description 5
- 238000004220 aggregation Methods 0.000 description 4
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- -1 O-shaped rings Substances 0.000 description 1
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- 239000011229 interlayer Substances 0.000 description 1
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- 238000011031 large-scale manufacturing process Methods 0.000 description 1
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- 238000003199 nucleic acid amplification method Methods 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 230000036961 partial effect Effects 0.000 description 1
- 125000005575 polycyclic aromatic hydrocarbon group Chemical group 0.000 description 1
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- 238000010992 reflux Methods 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
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Images
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/44—Carbon
- C09C1/48—Carbon black
- C09C1/485—Preparation involving the use of a plasma or of an electric arc
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
- Y02P20/129—Energy recovery, e.g. by cogeneration, H2recovery or pressure recovery turbines
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Carbon And Carbon Compounds (AREA)
Abstract
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN115975402A (zh) * | 2022-12-05 | 2023-04-18 | 云南云维飞虎化工有限公司 | 一种采用纯氧提质用炭黑生产设备 |
Citations (13)
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US5997837A (en) * | 1991-12-12 | 1999-12-07 | Kvaerner Technology And Research Ltd. | Method for decomposition of hydrocarbons |
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CN1478765A (zh) * | 2003-07-03 | 2004-03-03 | 太原理工大学 | 制备乙炔和炭黑的方法及装置 |
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CN105017815A (zh) * | 2015-06-04 | 2015-11-04 | 苏州纳康纳米材料有限公司 | 一种低成本和高导电性能的纳米碳材料的制备方法 |
US20160083810A1 (en) * | 2013-06-14 | 2016-03-24 | CCP Technology GmbH | Blast furnace and method for operating a blast furnace |
WO2017034980A1 (en) * | 2015-08-24 | 2017-03-02 | Monolith Materials, Inc. | High temperature heat integration method of making carbon black |
CN107709474A (zh) * | 2015-02-03 | 2018-02-16 | 巨石材料公司 | 炭黑生成*** |
CN109294284A (zh) * | 2018-11-12 | 2019-02-01 | 西南化工研究设计院有限公司 | 一种等离子体裂解富甲烷气制炭黑的方法 |
CN113214683A (zh) * | 2021-04-19 | 2021-08-06 | 淄博职业学院 | 等离子体裂解页岩气制备高品质炭黑的工艺及装置 |
CN113789068A (zh) * | 2021-09-26 | 2021-12-14 | 天津朗缪新材料科技有限公司 | 一种高温超高导电炭黑反应炉及其抽余油生产超高导电炭黑的方法 |
-
2022
- 2022-06-24 CN CN202210721818.7A patent/CN115029021B/zh active Active
Patent Citations (13)
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US5997837A (en) * | 1991-12-12 | 1999-12-07 | Kvaerner Technology And Research Ltd. | Method for decomposition of hydrocarbons |
CN1398780A (zh) * | 2002-08-06 | 2003-02-26 | 中国科学院山西煤炭化学研究所 | 一种裂解烃类生产碳黑和氢气的方法和装置 |
CN1478765A (zh) * | 2003-07-03 | 2004-03-03 | 太原理工大学 | 制备乙炔和炭黑的方法及装置 |
CN102108216A (zh) * | 2010-12-03 | 2011-06-29 | 苏州纳康纳米材料有限公司 | 一种等离子体技术制备导电炭黑和氢气的方法 |
CN102964883A (zh) * | 2012-12-13 | 2013-03-13 | 新疆雅克拉炭黑有限责任公司 | 富氢气气体助产的热裂法炭黑生产工艺 |
CN103160149A (zh) * | 2013-03-28 | 2013-06-19 | 无锡双诚炭黑有限公司 | 一种炭黑反应炉及炭黑生产方法 |
US20160083810A1 (en) * | 2013-06-14 | 2016-03-24 | CCP Technology GmbH | Blast furnace and method for operating a blast furnace |
CN107709474A (zh) * | 2015-02-03 | 2018-02-16 | 巨石材料公司 | 炭黑生成*** |
CN105017815A (zh) * | 2015-06-04 | 2015-11-04 | 苏州纳康纳米材料有限公司 | 一种低成本和高导电性能的纳米碳材料的制备方法 |
WO2017034980A1 (en) * | 2015-08-24 | 2017-03-02 | Monolith Materials, Inc. | High temperature heat integration method of making carbon black |
CN109294284A (zh) * | 2018-11-12 | 2019-02-01 | 西南化工研究设计院有限公司 | 一种等离子体裂解富甲烷气制炭黑的方法 |
CN113214683A (zh) * | 2021-04-19 | 2021-08-06 | 淄博职业学院 | 等离子体裂解页岩气制备高品质炭黑的工艺及装置 |
CN113789068A (zh) * | 2021-09-26 | 2021-12-14 | 天津朗缪新材料科技有限公司 | 一种高温超高导电炭黑反应炉及其抽余油生产超高导电炭黑的方法 |
Non-Patent Citations (2)
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LI J: ""A new grade carbon black produced by thermal plasma process", 《PLASMA SCIENCE & TECHNOLOGY》 * |
罗义文, 漆继红, 唐聪明: ""等离子体裂解天然气制纳米炭黑和乙炔"", 《材料科学与工程学报》 * |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN115975402A (zh) * | 2022-12-05 | 2023-04-18 | 云南云维飞虎化工有限公司 | 一种采用纯氧提质用炭黑生产设备 |
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Inventor after: Wang Cheng Inventor after: Yang Chengpeng Inventor after: Chen Xianhui Inventor after: Chen Feng Inventor after: Xia Weidong Inventor after: Xia Weili Inventor before: Wang Cheng Inventor before: Yang Chengpeng Inventor before: Chen Feng Inventor before: Xia Weidong Inventor before: Xia Weili |
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Effective date of registration: 20240711 Address after: Room 103-b6, embedded R & D building, Advanced Research Institute of China University of science and technology, 5089 Wangjiang West Road, high tech Zone, Hefei City, Anhui Province, 230088 Patentee after: HEFEI TANYI TECHNOLOGY Co.,Ltd. Country or region after: China Patentee after: XINJIANG JUNXIN CHEMICAL CO.,LTD. Patentee after: University of Science and Technology of China Address before: Room 103-b6, embedded R & D building, Advanced Research Institute of China University of science and technology, 5089 Wangjiang West Road, high tech Zone, Hefei City, Anhui Province, 230088 Patentee before: HEFEI TANYI TECHNOLOGY Co.,Ltd. Country or region before: China Patentee before: XINJIANG JUNXIN CHEMICAL CO.,LTD. |
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