CN114946671B - Antibacterial insect-proof deodorizing anti-blocking pet particle and preparation method thereof - Google Patents

Antibacterial insect-proof deodorizing anti-blocking pet particle and preparation method thereof Download PDF

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Publication number
CN114946671B
CN114946671B CN202210544891.1A CN202210544891A CN114946671B CN 114946671 B CN114946671 B CN 114946671B CN 202210544891 A CN202210544891 A CN 202210544891A CN 114946671 B CN114946671 B CN 114946671B
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wasp
powder
fine powder
weight
hive
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CN114946671A (en
Inventor
党菱婧
李梓墨
汪永强
瞿云
岳加蕊
郭云胶
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Foshan Fengyuan Biotechnology Co ltd
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Foshan Fengyuan Biotechnology Co ltd
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01KANIMAL HUSBANDRY; CARE OF BIRDS, FISHES, INSECTS; FISHING; REARING OR BREEDING ANIMALS, NOT OTHERWISE PROVIDED FOR; NEW BREEDS OF ANIMALS
    • A01K1/00Housing animals; Equipment therefor
    • A01K1/015Floor coverings, e.g. bedding-down sheets ; Stable floors
    • A01K1/0152Litter
    • A01K1/0155Litter comprising organic material
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01KANIMAL HUSBANDRY; CARE OF BIRDS, FISHES, INSECTS; FISHING; REARING OR BREEDING ANIMALS, NOT OTHERWISE PROVIDED FOR; NEW BREEDS OF ANIMALS
    • A01K1/00Housing animals; Equipment therefor
    • A01K1/015Floor coverings, e.g. bedding-down sheets ; Stable floors
    • A01K1/0152Litter
    • A01K1/0154Litter comprising inorganic material
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P60/00Technologies relating to agriculture, livestock or agroalimentary industries
    • Y02P60/80Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
    • Y02P60/87Re-use of by-products of food processing for fodder production

Abstract

The invention provides an antibacterial insect-proof stink-proof anti-blocking pet particle and a preparation method thereof. All raw materials and auxiliary materials are safe and environment-friendly, the raw materials are low in price and environment-friendly, the degradation is quick, the powder is fine, and the powder can be directly flushed into a toilet without causing blockage. The wasp honeycomb is light in weight, fluffy and convenient to transport.

Description

Antibacterial insect-proof deodorizing anti-blocking pet particle and preparation method thereof
Technical Field
The invention belongs to the technical field of pet feeds, and particularly relates to an antibacterial insect-proof deodorizing anti-blocking pet particle and a preparation method thereof.
Background
The cat litter (pet particles) is an article for burying feces and urine by a cat fed by the cat, has obvious water absorption performance, agglomeration capacity and taste masking capacity, is a necessary article for feeding the cat in a modern closed environment and space, has high consumption, and is a basic living article for the pet cat. Currently, the varieties of the cat litter mainly sold in the market include bentonite cat litter, beancurd cat litter, crystal cat litter, pine cat litter, paper scrap cat litter, activated carbon cat litter, mineral cat litter and mixed cat litter of the above. The bentonite cat litter and the bentonite-added composite cat litter have the advantages of high use degree, low price, large use replacement amount and good caking property, but have the defects of large dust amount, difficult degradation of the bentonite, environment friendliness and inconvenient treatment. Pine cat litter is the cat litter that utilizes the saw-dust of pine to make, the low price, but the pine cat litter is in use to adsorb urine required time long to can not expand open immediately, not agglomerate after the use, the use amount is big, and inconvenient clearance must cooperate the double-deck cat litter basin of use, because the long condition that can appear urine and directly flow to the second floor cat litter basin that does not adsorb yet in the required time of expansion absorption, also causes the screening to be incomplete easily when handling double-deck cat litter basin, the bad condition of taste performance that hides. The common crystal cat litter is high in price, obvious in water absorption removal effect, not good in covering and taste masking performance, and the silica gel is not easy to degrade and is easy to cause secondary pollution after being abandoned. The bean curd cat litter has the advantages of good caking property and water absorption, large usage amount, convenient treatment and poor performance of covering cat excrement, the raw material is soybean which is a basic use crop for national people, the cost is high, the grain is wasted, artificial spice is needed to be added to cover odor after the preparation is completed, and the added spice is not friendly to the respiratory tract of the cat.
Disclosure of Invention
The first object of the invention is to provide an antibacterial insect-proof deodorizing anti-blocking pet particle, and the second object of the invention is to provide a preparation method of the antibacterial insect-proof deodorizing anti-blocking pet particle.
The first object of the present invention is achieved by: comprises 100-180 parts by weight of wasp hive fine powder, 30-80 parts by weight of corn starch, 8-22 parts by weight of sodium carboxymethyl cellulose and 3-20 parts by weight of sodium bicarbonate.
Preferably, the antibacterial insect-preventing deodorizing anti-blocking pet particles comprise 160 parts by weight of wasp hive fine powder, 40 parts by weight of corn starch, 18 parts by weight of sodium carboxymethyl cellulose and 10 parts by weight of sodium bicarbonate.
Preferably, the antibacterial insect-proof deodorizing anti-blocking pet particle also comprises 120-160 parts by weight of rice hull fine powder.
Preferably, the cat litter is of a long cylindrical granular structure, wherein the diameter is 4-6mm, and the length is 1-2.5cm.
The second object of the present invention is achieved by:
the method comprises the following steps:
(1) Crushing wasp beehives, sieving the powder, and putting the wasp beehive fine powder into a drying oven for baking and sterilizing;
(2) Placing the dried wasp hive fine powder, corn starch, sodium carboxymethyl cellulose and sodium bicarbonate into a stirrer to be uniformly stirred to form mixed powder;
(3) Granulating the mixed powder in a granulator to form mixed granules, sieving the mixed granules, drying the mixed granules in a drying oven, cleaning the powder by a dust remover, and vacuum packaging to form a finished product.
Preferably, before the step (2), the dried and mildew-free rice hulls are further put into a baking oven for baking and disinfection, and the dried rice hulls are crushed and the powder is sieved. And then the wasp hive fine powder, the rice hull fine powder, the corn starch, the sodium carboxymethyl cellulose and the sodium bicarbonate are put into a stirrer to be uniformly stirred, so as to form mixed powder.
Preferably, the sieving step of the wasp hive fine powder is that of a 50-mesh sieve, and the sieving step of the rice hull fine powder is that of a 50-mesh sieve.
Preferably, the wasp hive powder is put into a drying oven for baking and sterilizing, the temperature is 40-70 ℃ and the time is 120-180 minutes.
Preferably, the rice hulls are baked and sterilized in an oven at a temperature of 100-110 ℃ for 60-90 minutes.
Preferably, the mixed particles in the step (3) are put into a drying oven for drying after being sieved, the temperature is 40-70 ℃ and the time is 60-90 minutes.
Compared with the prior art, the invention has the beneficial effects that:
the honeycomb used by the pet particles is derived from wasps such as wasps of wasp family insects, japanese long-foot wasps, hetero-abdomen wasps and the like, and is the waste remained after the wasps are bred and eaten by people such as Yun Guichuan and Hunan. Wasp hives, also called wasps hives, are nests of long-foot wasps in a variety of closely related insects, and wasps are widely living and common in China, and therefore have a great yield. The wasp honeycomb has the advantages of excellent fiber structure, large honeycomb space gap, good water absorption, light material, easy compression and expansion, and has obvious weight advantage compared with the commercial cat litter. Compared with the bean curd cat litter with the same volume, the weight of the bean curd cat litter is reduced by 50%, the bean curd cat litter is convenient to transport and carry, and the weight is light, so that the bean curd cat litter is a main advantage of the bean curd cat litter. The wasp cat litter has another obvious advantage of natural antibacterial property of wasp beehives, and pharmacological research shows that the water extract of the wasp beehives has good treatment and auxiliary treatment effects on diseases caused by bacteria and fungi. The 40-fold diluted honeycomb water extract has strong inhibition effect on staphylococcus aureus, pseudomonas aeruginosa, escherichia coli, bacillus dysenteriae, typhoid bacillus and the like; the composition has obvious inhibition effect on fungi such as aspergillus fumigatus, aspergillus flavus, fusarium solani, moniliforme and the like after 50 times dilution; nidus Vespae contains unique wasp volatile oil, and can expel cestodes. Based on the natural honeycomb characteristics, the finished product is placed at room temperature for three months after the pet particles are prepared, cat litter is observed to have no obvious mildew and worm damage by naked eyes, and microscopic observation has no mildew and worm damage. And then carrying out a bacteriostasis experiment on the finished product, verifying whether the finished product has a bacteriostasis effect after the honeycomb powder is prepared into cat litter, crushing the cat litter of the wasp, extracting the cat litter with an ethyl acetate solution, carrying out a culture dish bacteriostasis circle experiment on the extract, diluting the extract with ethyl acetate to obtain a 1:1 stock solution, carrying out the bacteriostasis experiment with a paper sheet method, using 6 millimeter discs for paper sheets, placing 6 paper sheets immersed in the stock solution in each culture dish, respectively carrying out in vitro bacteriostasis experiment contrast on common staphylococcus aureus and escherichia coli salmonella, and analyzing the experimental data results to obtain the wasp honeycomb cat litter with obvious in vitro bacteriostasis effect. The antibacterial agent has obvious inhibition effects on various strains, and the average antibacterial circle directly reaches 14mm of staphylococcus aureus, 13mm of escherichia coli and 11mm of salmonella respectively, so that the finished pet particle product also keeps good antibacterial and insect repellent effects of the honeycomb from experimental results.
In the mixed cat litter of honeycomb rice hulls, because of natural trace grease components in the wasp honeycomb, the honeycomb and the rice hulls are slightly adhered and independent of each other, the self adhesion reduces the using amount of adhesive carboxymethyl cellulose, urine is encountered after the mixture is mixed with sodium bicarbonate, the sodium bicarbonate releases trace carbon dioxide under the action of moisture, the generated carbon dioxide gas can help pet particles to rapidly and naturally collapse, the surface area is increased after the collapse of the pet particles, the cat litter can be rapidly absorbed by water and is agglomerated, a small amount of corn starch also plays a role in rapid absorption, then the moisture in the corn starch can be absorbed by honeycomb fibers, and the mixture of the corn starch and the pet particles can be rapidly agglomerated. Experiments prove that the pet particles are paved into the height of 3cm in thickness in the cat litter basin, 40ml of water is slowly poured into the cat litter basin, the time for completely absorbing 40ml of water and agglomerating the water is 8 seconds, and the water absorption experiment contrast ratio is higher than the water absorption time of pine cat litter and bean curd cat litter sold in the market. Meanwhile, as the honeycomb powder and the rice hulls are fine fiber powder, after the pet particles added with the rice hulls are manufactured, after the pet particles are absorbed and disintegrated, the fiber powder can be scattered to cover the cat excrement to form a covering surface, the situation that the cat excrement in the bean curd cat litter and the crystal cat litter is not completely covered can not occur, and the excrement can be effectively covered. The wooden fragrance of the honeycomb can also cover the taste of the excrement, and has the function of natural taste masking. On the basis of pure pet particles, the pet particles taking rice hulls as main raw materials are tried to be added, and the anti-bacterial and insect-resistant pet particles have obvious anti-bacterial and insect-resistant properties.
The basic components of the hive, such as plant fibers, propolis, resin and the like, are recorded in the 'compendium of materia medica', the hive has slight smell and sweet and light taste, is externally used for treating superficial skin diseases such as sores and ulcers, acute mastitis, scrofula, skin intractable tinea and the like, has the effect of killing cestodes, and has proved that chemical components such as the hive element and the like contained in the hive have the anti-inflammatory and antibacterial effects, the hive is used as the main raw material of cat litter, and the main components of the hive are fibers and the resin which can be used as natural water absorbing agents and agglomerating agents. The composition of the volatile oil in the honeycomb has light faint scent wood flavor, and has the effect of killing tapeworm, so that the honeycomb and all additives are combined to make the pet particles use the honeycomb as a main raw material to prepare cat litter, so that the cat litter has good taste-blocking property and insecticidal property, is beneficial to the health of cats, is safe and environment-friendly after all raw material auxiliary materials are matched, and reduces the dosage of other auxiliary material additives by utilizing the characteristic that the pet particles are suitable for preparing cat litter. The wasp honeycomb is light in weight, fluffy and convenient to transport.
Description of the embodiments
The invention is further illustrated, but is not limited in any way, by the following examples, and any alterations or modifications based on the teachings of the invention are within the scope of the invention.
Example 1
Crushing clean nidus Vespae purchased in the current year, sieving and sieving the powder. And (3) placing the sieved honeycomb powder into a drying oven for baking and sterilizing for 120-180 minutes at a medium temperature (40-70 ℃) until the water content in the honeycomb powder is not more than 1%. Placing the dried and sterilized honeycomb fine powder, corn starch, sodium carboxymethyl cellulose and sodium bicarbonate into a stirrer to be uniformly stirred to form mixed powder; granulating the mixed powder in a granulator to form mixed granules. And (3) drying the mixed particles in a drying oven, screening, putting the mixed particles into a dust remover to clean the powder, and vacuum packaging to form a finished product.
Example 2
Considering the reduction of the honeycomb usage, more economical raw materials are used for replacing and filling fiber parts, and after clean nidus Vespae purchased in the current year is crushed, the powder is sieved and sieved. And (3) placing the sieved honeycomb powder into a drying oven for baking and sterilizing for 120-180 minutes at a medium temperature (40-70 ℃) until the water content in the honeycomb powder is not more than 1%. Grinding clean and mildew-free rice hulls, sieving the powder, sieving, placing into an oven, baking at 100-110deg.C for 60-90 min to remove excessive water. Placing the dried and sterilized honeycomb fine powder and corn starch, sodium carboxymethyl cellulose, sodium bicarbonate and rice hull fragments into a stirrer to be uniformly stirred to form mixed powder; granulating the mixed powder in a granulator to form mixed granules. And (3) drying the mixed particles in a drying oven, screening, putting the mixed particles into a dust remover to clean the powder, and vacuum packaging to form a finished product.
Example 3:
crushing 1kg of wasp honeycombs by using a grinding machine, sieving the powder by a 50-mesh sieve, and putting the wasp honeycombs fine powder into a drying oven to be baked and sterilized at 40 ℃ for 160 minutes;
adding 400g of corn flour into the dried wasp hive fine powder, and putting 180g of sodium carboxymethylcellulose and 200g of sodium bicarbonate into a stirrer to uniformly stir so as to form mixed powder;
granulating in a granulator, sieving the mixed granules, drying the cat litter granules in a drying oven at 40 ℃ for 70 minutes after sieving, cleaning the powder by a dust remover, and vacuum packaging to form the finished product. The effect is as follows: the cat litter has strong water absorption, dry particles, high hardness and weak use comfort.
Example 4:
crushing 1.5kg wasp honeycomb with a pulverizer, sieving with a 50 mesh sieve, and placing the wasp honeycomb fine powder into a drying oven to be baked and disinfected at 70 ℃ for 120 minutes;
adding 800g of corn flour into the dried wasp hive fine powder, and putting 200g of sodium carboxymethyl cellulose and 200g of sodium bicarbonate into a stirrer to be uniformly stirred to form mixed powder;
granulating in a granulator, sieving the mixed granules, drying the cat litter granules in a drying oven at 100 ℃ for 90 minutes, cleaning the powder by a dust remover, and vacuum packaging to obtain the finished product. The effect is as follows: has strong water absorption, no odor, different particle sizes and short service time.
Example 5:
crushing 1.8kg wasp honeycomb with a pulverizer, sieving with a 50-mesh sieve, and placing the wasp honeycomb fine powder into a drying oven to be baked and disinfected at 70 ℃ for 120 minutes;
adding 600g of corn flour into the dried wasp hive fine powder, and putting 80g of sodium carboxymethyl cellulose and 150g of sodium bicarbonate into a stirrer to uniformly stir so as to form mixed powder;
granulating in a granulator, sieving the mixed granules, drying the cat litter granules in a drying oven at 100 ℃ for 90 minutes, cleaning the powder by a dust remover, and vacuum packaging to obtain the finished product. The effect is as follows: the cat litter has strong water absorption, bad smell near the cat litter, uniform and cylindrical particle size and long service time.
Example 6:
crushing 1.8kg of wasp honeycombs by using a grinding machine, sieving the powder by a 50-mesh sieve, and putting the wasp honeycombs fine powder into a drying oven to be baked and sterilized at 40 ℃ for 180 minutes;
adding 300g of corn flour into the dried wasp hive fine powder, and uniformly stirring 150g of sodium carboxymethylcellulose and 10g of sodium bicarbonate in a stirrer to form mixed powder;
granulating in a granulator, sieving the mixed granules, drying the cat litter granules in a drying oven at 40 ℃ for 90 minutes, cleaning the powder by a dust remover, and vacuum packaging to obtain the finished product.
Example 7;
crushing 1.8kg of wasp honeycombs by using a grinding machine, sieving the powder by a 50-mesh sieve, and putting the wasp honeycombs fine powder into a drying oven to be baked and sterilized at 40 ℃ for 180 minutes;
adding 300g of corn flour into the dried wasp hive fine powder, and putting 80g of sodium carboxymethyl cellulose and 30g of sodium bicarbonate into a stirrer to uniformly stir so as to form mixed powder;
granulating in a granulator, sieving the mixed granules, drying the cat litter granules in a drying oven at 70 ℃ for 60 minutes, cleaning the powder by a dust remover, and vacuum packaging to obtain the finished product.

Claims (9)

1. The antibacterial insect-proof deodorizing anti-blocking pet particle is characterized by comprising 100-180 parts by weight of wasp hive fine powder, 30-80 parts by weight of corn starch, 8-22 parts by weight of sodium carboxymethyl cellulose and 3-20 parts by weight of sodium bicarbonate.
2. The antibacterial insect-resistant deodorizing anti-blocking pet granule according to claim 1, which is characterized by comprising 160 parts by weight of wasp hive fine powder, 40 parts by weight of corn starch, 18 parts by weight of sodium carboxymethyl cellulose and 10 parts by weight of sodium bicarbonate.
3. The antibacterial insect-proof deodorizing anti-blocking pet particle according to claim 1 is characterized by further comprising 120-160 parts by weight of rice hull fine powder.
4. The method for preparing the antibacterial insect-proof deodorizing anti-blocking pet particles according to any one of claims 1-3, which is characterized by comprising the following steps: the method comprises the following steps:
(1) Crushing wasp beehives, sieving the powder, and putting the wasp beehive fine powder into a drying oven for baking and sterilizing;
(2) Placing the dried wasp hive fine powder, corn starch, sodium carboxymethyl cellulose and sodium bicarbonate into a stirrer to be uniformly stirred to form mixed powder;
(3) Granulating the mixed powder in a granulator to form mixed granules, sieving the mixed granules, drying the mixed granules in a drying oven, cleaning the powder by a dust remover, and vacuum packaging to form a finished product.
5. The method for preparing the antibacterial insect-proof deodorizing anti-blocking pet particles according to claim 4, which is characterized in that: before the step (2), the dried and mildew-free rice hulls are put into a baking oven for baking and disinfection, the rice hulls are crushed after being baked, the powder is sieved, and then the wasp honeycomb fine powder, the rice hull fine powder, the corn starch, the sodium carboxymethyl cellulose and the sodium bicarbonate are put into a stirrer for stirring uniformly, so as to form mixed powder.
6. The method for preparing the antibacterial insect-proof deodorizing anti-blocking pet particles according to claim 5, which is characterized in that: the sieving step of the wasp hive fine powder is that the wasp hive fine powder is sieved by a 50-mesh sieve, and the sieving step of the rice hull fine powder is that the wasp hive fine powder is sieved by a 50-mesh sieve.
7. The method for preparing the antibacterial insect-proof deodorizing anti-blocking pet particles according to claim 4, which is characterized in that: and (3) putting the wasp hive fine powder into a drying oven for baking and sterilizing, wherein the temperature is 40-70 ℃ and the time is 120-180 minutes.
8. The method for preparing the antibacterial insect-proof deodorizing anti-blocking pet particles according to claim 5, which is characterized in that: the temperature of baking and sterilizing the rice hulls in the oven is 100-110 ℃ and the time is 60-90 minutes.
9. The method for preparing the antibacterial insect-proof deodorizing anti-blocking pet particles according to claim 4, which is characterized in that: and (3) screening the mixed particles, and then placing the screened mixed particles into a drying oven for drying, wherein the temperature is 40-70 ℃ and the time is 60-90 minutes.
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CN110612913A (en) * 2019-10-28 2019-12-27 合肥学院 High-water-absorptivity easily-agglomerated cat litter with degradation function and preparation method thereof
CN210017392U (en) * 2019-03-19 2020-02-07 上海喵生服装有限公司 Cat sand mat with massage and sand collection functions
CN110841025A (en) * 2019-11-22 2020-02-28 天津市晨辉饲料有限公司 Preparation method of dog food additive for preventing eye diseases and hepatitis
CN111642409A (en) * 2020-06-28 2020-09-11 涿州市浩森再生资源回收有限公司 Novel cat litter with good deodorization performance and preparation method thereof
CN112868542A (en) * 2020-12-31 2021-06-01 广西德壤生态科技有限公司 Biological deodorization tofu cat litter and preparation method thereof
CN113615584A (en) * 2021-09-08 2021-11-09 吉林农业大学 Cat litter made of rice hull plants and preparation method of cat litter

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US5724915A (en) * 1995-07-07 1998-03-10 Sanyo Chemical Industries, Ltd. Material for the treatment of pet excretion and method of producing the same material
CN102821758A (en) * 2010-01-29 2012-12-12 雀巢产品技术援助有限公司 Extruded animal litters having increased absorption rate
CN106614021A (en) * 2016-12-29 2017-05-10 河南时代云通信技术有限公司 Environment-friendly agglomerate type cat litter and preparation method thereof
DE202018103389U1 (en) * 2018-02-20 2019-05-21 Franz Oberleitner Honeycomb flooring
CN210017392U (en) * 2019-03-19 2020-02-07 上海喵生服装有限公司 Cat sand mat with massage and sand collection functions
CN110036926A (en) * 2019-05-23 2019-07-23 南京咕噜材料科技有限公司 A kind of natural plant fibre cat litter and preparation method thereof
CN110612913A (en) * 2019-10-28 2019-12-27 合肥学院 High-water-absorptivity easily-agglomerated cat litter with degradation function and preparation method thereof
CN110841025A (en) * 2019-11-22 2020-02-28 天津市晨辉饲料有限公司 Preparation method of dog food additive for preventing eye diseases and hepatitis
CN111642409A (en) * 2020-06-28 2020-09-11 涿州市浩森再生资源回收有限公司 Novel cat litter with good deodorization performance and preparation method thereof
CN112868542A (en) * 2020-12-31 2021-06-01 广西德壤生态科技有限公司 Biological deodorization tofu cat litter and preparation method thereof
CN113615584A (en) * 2021-09-08 2021-11-09 吉林农业大学 Cat litter made of rice hull plants and preparation method of cat litter

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