CN114774207B - Dry cleaning salt for plush toy and preparation method thereof - Google Patents

Dry cleaning salt for plush toy and preparation method thereof Download PDF

Info

Publication number
CN114774207B
CN114774207B CN202210525944.5A CN202210525944A CN114774207B CN 114774207 B CN114774207 B CN 114774207B CN 202210525944 A CN202210525944 A CN 202210525944A CN 114774207 B CN114774207 B CN 114774207B
Authority
CN
China
Prior art keywords
salt
parts
edible salt
cleaning
plush toy
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN202210525944.5A
Other languages
Chinese (zh)
Other versions
CN114774207A (en
Inventor
汪姣玲
李加兴
岳元媛
刘建平
吴志康
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Xuetian Salt Group Co ltd
Original Assignee
Xuetian Salt Group Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Xuetian Salt Group Co ltd filed Critical Xuetian Salt Group Co ltd
Priority to CN202210525944.5A priority Critical patent/CN114774207B/en
Publication of CN114774207A publication Critical patent/CN114774207A/en
Application granted granted Critical
Publication of CN114774207B publication Critical patent/CN114774207B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02Anionic compounds
    • C11D1/37Mixtures of compounds all of which are anionic
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/04Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium
    • B01J20/046Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium containing halogens, e.g. halides
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B08CLEANING
    • B08BCLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
    • B08B3/00Cleaning by methods involving the use or presence of liquid or steam
    • B08B3/04Cleaning involving contact with liquid
    • B08B3/08Cleaning involving contact with liquid the liquid having chemical or dissolving effect
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02Inorganic compounds ; Elemental compounds
    • C11D3/04Water-soluble compounds
    • C11D3/046Salts
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/38Products with no well-defined composition, e.g. natural products
    • C11D3/382Vegetable products, e.g. soya meal, wood flour, sawdust
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/48Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D2111/00Cleaning compositions characterised by the objects to be cleaned; Cleaning compositions characterised by non-standard cleaning or washing processes
    • C11D2111/10Objects to be cleaned
    • C11D2111/12Soft surfaces, e.g. textile

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Inorganic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Detergent Compositions (AREA)

Abstract

The invention provides a plush toy dry-cleaning salt and a preparation method thereof, wherein the plush toy dry-cleaning salt comprises the following raw materials in parts by weight: 65-95 parts of edible salt, 1-4 parts of plant surfactant, 3-8 parts of decontamination plant extract and 2-8 parts of antibacterial plant extract. The invention adopts the combination of the edible salt and the natural decontamination and bacteriostasis factors, can replace the traditional method of drying after washing, has high cleaning efficiency, can effectively clean dirt such as dust, soil and bacteria attached to plush toys, has good cleaning effect, is safe and nontoxic, and can better ensure the health of infants.

Description

Dry cleaning salt for plush toy and preparation method thereof
Technical Field
The invention belongs to the technical field of daily chemical products, and particularly relates to plush toy dry cleaning salt and a preparation method thereof.
Background
Toys have had a long history in China, and people invented various production tools to meet the demands of social development, and also created toys to meet the physical and mental demands of entertainment after working.
The toy is mainly exported in the world, the production and export amount of the toy is at the top of the world for many years, the toy on the three-way world market is produced in China nowadays, and the produced toy has seven export to the world. The us market research company NPD group 2017 has found that sales growth statistics for the 12 national toy industry, among all toys, plush toys are the fastest growing hot-market class of toys in the global toy market.
The plush toy is made of plush fabric, pp cotton and other textile materials as main fabric, and various fillings are stuffed inside, and can also be called soft toy and stuffed toy. Currently we habitually refer to plush toys as plush toys. For a long time, the biggest problem affecting the sales and recovery of plush toys is easy adsorption of dust and bacterial breeding. During playing, the children chew or even swallow the toy through skin contact, eye contact and chewing, so that certain dust adhered to the fluff is sucked into the lungs or certain bacteria are mistakenly eaten into the body, and the health development of the children is adversely affected. In addition, plush toys are discarded during long play because the surface fills with dirt, and toy factories often refuse to recover because of these hard to handle dirt.
At present, no special plush toy cleaning agent exists in the market, and a laundry detergent is generally used for washing, but because a large amount of filling materials are contained in the plush toy, the moisture is difficult to volatilize completely, bacteria and mould are easy to propagate and breed, and the plush toy is unfavorable for health; the toy is easy to deform, the surface is hardened, and the plush is not fluffy after washing; chemical synthetic substances and essence residues in the liquid laundry detergent can cause certain irritation to the skin of children, have potential safety hazards and pollute the environment.
Salt (namely sodium chloride) is used as the most common seasoning in daily diet, so that the food has salty taste, low price and high safety, and has obvious adsorption effect on dirt. The project is to re-wrap and crystallize large-particle salt and substances such as plant surfactant, natural herbal extract or natural antibacterial factors through a wet coating technology, efficiently remove stains while not reducing the adsorption capacity of the salt, continuously inhibit bacteria, have mild formula, avoid water washing, greatly reduce potential safety hazards, and can be used in combination with a cleaning device to rapidly and efficiently treat toy stains.
Disclosure of Invention
Aiming at the problems, the invention provides the plush toy dry cleaning salt and the preparation method thereof, wherein the edible salt is compounded with the natural decontamination and bacteriostasis factors, so that the plush toy dry cleaning salt can replace the traditional method of drying after washing, has high cleaning efficiency, can effectively clean dirt, soil and bacteria attached to the plush toy, has good cleaning effect, is safe and nontoxic, and can better ensure the health of infants.
The invention is realized by the following technical scheme.
The dry cleaning salt for the plush toy is characterized by comprising the following raw materials in parts by weight: 65-95 parts of edible salt, 1-4 parts of plant surfactant, 3-8 parts of decontamination plant extract and 2-8 parts of antibacterial plant extract.
As a specific technical scheme, the edible salt is refined well mineral salt; the granularity of the edible salt is 14-30 meshes; in the invention, the edible salt is refined well mineral salt; the refined well mineral salt crude salt is obtained from rock salt under deep buried ground bottom rock before 6500 ten thousand years ago, brine is obtained from a drinking water source protection area, brine is purified by a ceramic membrane physical filtration technology, and the refined well mineral salt crude salt is refined by a vacuum steaming crystallization technology, so that the grains are large and uniform; in addition, the applicant finds that the particle size of the raw material edible salt has a great influence on the service performance of the product; if the granularity of the edible salt is too large, the granularity of the finally prepared dry-cleaning salt product is also large, so that the dry-cleaning salt product cannot fully enter between the floss gaps on the surface of the plush toy; in addition, the edible salt accounts for a relatively high proportion in the formula of the product, so that the other auxiliary materials are relatively small, and when the granularity of the edible salt is too large, the other auxiliary materials are difficult to effectively wrap on salt particles in the preparation process of the product, or are easy to fall off after being wrapped, so that the efficacy of the product is affected; if the granularity of the edible salt is too small, the granularity of the finally prepared dry-cleaning salt product is also small, the product is easy to generate dust phenomenon in the preparation process and the cleaning and using process, and the product is also difficult to fall off from plush gaps in the cleaning process; therefore, the invention controls the granularity of the edible salt to be 14-30 meshes, ensures that auxiliary materials can be effectively attached, and simultaneously can control the finally prepared dry-cleaning salt product to effectively enter between plush gaps so as to achieve the purposes of adsorbing dust and stains on plush toys, easily falling off from the plush gaps and avoiding dust pollution during cleaning.
As a specific technical scheme, the plant surfactant is one or a mixture of more of glycoside, amino acid surfactant and betaine; the plant surfactant is extracted from plants, has high safety and has excellent cleaning effect on dirt components on the surfaces of plush.
As a specific technical scheme, the plant surfactant is an amino acid surfactant; the amino acid surfactant is a mixture of disodium cocoyl glutamate and disodium lauryl glutamate; the disodium cocoyl glutamate and the disodium lauryl glutamate belong to amino acid surfactants, have good decontamination and foam increasing capabilities, have certain antistatic and sterilizing capabilities under acidic conditions, have mild components and have good compatibility with skin.
As a specific technical scheme, the decontaminated plant extract is one or a mixture of more of laurel extract, nutmeg extract, gleditsia sinensis lam extract, bitter tea extract, pine needle extract, seaweed extract, soybean extract, coconut extract and sugarcane extract.
As a specific technical scheme, the antibacterial plant extract is one or a mixture of more of aloe extract, mugwort leaf essence, chamomile extract, lavender extract, lemon extract, mandarin orange extract and grapefruit extract.
As a specific technical scheme, the dry-cleaning salt for plush toys comprises the following formula raw materials in parts by weight: 65-95 parts of edible salt, 0.5-2 parts of disodium cocoyl glutamate, 0.5-2 parts of disodium lauryl glutamate, 2-4 parts of bitter tea extract, 1-4 parts of gleditsia sinensis lam extract, 1.5-4 parts of lemon extract and 1.5-4 parts of chamomile extract.
The preparation method of the dry cleaning salt is characterized by comprising the following steps:
(1) Accurately weighing the raw materials according to a formula for standby;
(2) Premixing the raw materials prepared in the step (1) except the edible salt for 5-15 min to obtain a premix; adding water according to the mass ratio of the premix to the feed liquid of 1:2-3 g/g, continuously mixing for 5-15 min, homogenizing, and obtaining auxiliary material slurry for later use;
(3) Transferring the edible salt prepared in the step (1) into a mixing tank, and gradually adding the auxiliary material slurry prepared in the step (2) to the surface of the edible salt in a spray mode for mixing for 10-30 min;
(4) Placing the mixed material in the step (3) into a hot air circulation drying oven, and baking for 1-3 h at 55-70 ℃;
(5) Sieving the baked materials with a 30-mesh sieve, removing residual fine powder in the product, and taking the oversize material to obtain the dry-cleaning salt product.
In the step (3), firstly, carrying out rewetting and granulating treatment on the edible salt prepared in the step (1), and then transferring the edible salt to a mixing tank to be mixed with auxiliary material slurry; the specific method for rewetting and granulating treatment comprises the following steps: a. dissolving edible salt in water, adding 0.8-1.5% of acacia and 2-6% of maltodextrin based on the mass of the edible salt, fully stirring until the acacia and the maltodextrin are completely dissolved, and then spray-drying; b. c, placing the edible salt treated in the step a in a high-humidity environment to enable the edible salt to absorb moisture and agglomerate, then taking the blocky and moisture-absorbing edible salt to crush and screen sequentially, and collecting the edible salt with the granularity of 14-30 meshes; c. vacuum drying the edible salt.
According to the invention, through the rewetting and granulating treatment, the edible salt can form a structure with concave parts on the surface and through holes in the interior, so that the effective adhesion of the follow-up auxiliary materials and the edible salt is facilitated, the auxiliary materials are adhered to the surface and the interior of the edible salt particles, the cleaning effect of the product is improved, and the falling of the auxiliary materials adhered to the surface of the salt particles during the use of the product is avoided to generate dust; wherein, the addition of the acacia gum and the maltodextrin is beneficial to maintaining the shape and structure of salt particles prepared after spray drying.
A method for cleaning a plush toy, comprising the steps of:
(1) Placing the plush toy to be cleaned in a sealable container, adding the dry cleaning salt prepared in the method of claim 8 according to the mass ratio of the plush toy to the dry cleaning salt of 2-5:1 g/g, and sealing the container;
(2) The container filled with the plush toy and the dry cleaning salt is quickly turned over for 5 to 10 minutes, so that the plush toy and the dry cleaning salt are fully contacted and rubbed with each other;
(3) Pouring out the plush toy and the dry-cleaning salt in the container, shaking the plush toy, and shaking the residual dry-cleaning salt on the plush toy.
The invention has the beneficial effects that:
1. The invention is prepared by reasonably matching plant surfactant, decontamination plant extract and antibacterial plant extract with edible salt as main raw materials; the edible salt is used as the most commonly used seasoning, has high safety, is harmless to the health and low in price, has strong adsorption capacity, and can effectively remove plush stains; the plant surfactant, the decontamination plant extract and the bacteriostasis plant extract are all green raw materials, do not irritate skin, can be decomposed naturally, are safe and nontoxic, have good cleaning effect on dust, soil, bacteria and the like adhered to the plush toy, and can not cause the loss and damage of the plush toy. Therefore, when the plush toy for the infant is cleaned by using the product of the invention, the residue and the safety problem in the using process are not worried; in addition, the product of the invention can be directly used for cleaning plush toys, omits the drying process of the plush toys, has high cleaning efficiency and good effect, and does not influence the quality of the plush toys.
2. According to the invention, the improved wet coating technology is utilized to re-wrap and crystallize large-particle salt and natural decontamination and bacteriostasis factors, additives can be uniformly distributed on the surfaces of salt particles to form a monocrystal structure, each salt particle contains a complete customized formula, the uniformity of the particle size of a final product and decontamination and bacteriostasis factors is ensured, the layering problem caused by different particle sizes of raw materials is avoided, and the efficacy and stability of the product are greatly improved.
Detailed Description
The present invention will be further explained in conjunction with the following detailed description, which is to be understood as being given by way of illustration only, but not by way of limitation, and all equivalents of the invention which fall within the spirit of the invention.
Example 1
The dry cleaning salt for plush toys comprises the following raw materials in parts by weight: 65-95 parts of edible salt, 1-4 parts of plant surfactant, 3-8 parts of decontamination plant extract and 2-8 parts of antibacterial plant extract.
Example 2
The dry cleaning salt for plush toys comprises the following raw materials in parts by weight: 65-95 parts of edible salt, 1-4 parts of plant surfactant, 3-8 parts of decontamination plant extract and 2-8 parts of antibacterial plant extract; wherein the edible salt is refined well mineral salt; the plant surfactant is one or a mixture of more of glycoside, amino acid surfactant and betaine; the plant surfactant is an amino acid surfactant; the amino acid surfactant is a mixture of disodium cocoyl glutamate and disodium lauryl glutamate; the decontaminated plant extract is one or more of laurel extract, nutmeg extract, gleditsia sinensis extract, bitter tea extract, pine needle extract, seaweed extract, soybean extract, coconut extract and sugarcane extract; the antibacterial plant extract is one or more of aloe extract, mugwort essence, chamomile extract, lavender extract, lemon extract, mandarin orange extract and grapefruit extract.
Example 3
The plush toy dry-cleaning salt comprises the following raw materials in parts by weight: 65-95 parts of edible salt, 1-4 parts of plant surfactant, 3-8 parts of decontamination plant extract and 2-8 parts of antibacterial plant extract; wherein the edible salt is refined well mineral salt; the plant surfactant is one or a mixture of more of glycoside, amino acid surfactant and betaine; the plant surfactant is an amino acid surfactant; the amino acid surfactant is a mixture of disodium cocoyl glutamate and disodium lauryl glutamate; the decontaminated plant extract is one or more of laurel extract, nutmeg extract, gleditsia sinensis extract, bitter tea extract, pine needle extract, seaweed extract, soybean extract, coconut extract and sugarcane extract; the antibacterial plant extract is one or more of aloe extract, mugwort essence, chamomile extract, lavender extract, lemon extract, mandarin orange extract and grapefruit extract.
Example 4
The dry cleaning salt for plush toys comprises the following raw materials in parts by weight: 65-95 parts of edible salt, 0.5-2 parts of disodium cocoyl glutamate, 0.5-2 parts of disodium lauryl glutamate, 2-4 parts of bitter tea extract, 1-4 parts of gleditsia sinensis lam extract, 1.5-4 parts of lemon extract and 1.5-4 parts of chamomile extract.
Example 5
The plush toy dry-cleaning salt comprises the following raw materials in parts by weight: 65-95 parts of edible salt, 0.5-2 parts of disodium cocoyl glutamate, 0.5-2 parts of disodium lauryl glutamate, 2-4 parts of bitter tea extract, 1-4 parts of gleditsia sinensis lam extract, 1.5-4 parts of lemon extract and 1.5-4 parts of chamomile extract.
Example 6
A preparation method of plush toy dry cleaning salt comprises the following steps:
(1) Accurately weighing the raw materials according to a formula for standby;
(2) Premixing the raw materials prepared in the step (1) except the edible salt for 5-15 min to obtain a premix; adding water according to the mass ratio of the premix to the feed liquid of 1:2-3 g/g, continuously mixing for 5-15 min, homogenizing, and obtaining auxiliary material slurry for later use;
(3) Transferring the edible salt prepared in the step (1) into a mixing tank, and gradually adding the auxiliary material slurry prepared in the step (2) to the surface of the edible salt in a spray mode for mixing for 10-30 min;
(4) Placing the mixed material in the step (3) into a hot air circulation drying oven, and baking for 1-3 h at 55-70 ℃;
(5) Sieving the baked materials with a 30-mesh sieve, removing residual fine powder (namely salt fine powder, auxiliary material fine powder and the like generated in the baking process) in the product, and taking the oversize product to obtain the dry-cleaning salt product.
Example 7
A preparation method of plush toy dry cleaning salt comprises the following steps:
(1) Accurately weighing each raw material according to 65-95 parts of edible salt, 0.5-2 parts of disodium cocoyl glutamate, 0.5-2 parts of disodium lauryl glutamate, 2-4 parts of bitter tea extract, 1-4 parts of gleditsia sinensis lam extract, 1.5-4 parts of lemon extract and 1.5-4 parts of chamomile extract for standby;
(2) Premixing the raw materials prepared in the step (1) except the edible salt for 5-15 min to obtain a premix; adding water according to the mass ratio of the premix to the feed liquid of 1:2-3 g/g, continuously mixing for 5-15 min, homogenizing, and obtaining auxiliary material slurry for later use;
(3) Firstly, carrying out rewetting and granulating treatment on the edible salt prepared in the step (1):
a. Dissolving edible salt in water, adding 0.8-1.5% of acacia and 2-6% of maltodextrin based on the mass of the edible salt, fully stirring until the acacia and the maltodextrin are completely dissolved, and then spray-drying;
b. C, placing the edible salt treated in the step a in a high-humidity environment (the relative humidity is 75% -85%), enabling the hollow edible salt to absorb moisture and agglomerate, then taking the blocky and moisture-absorbing edible salt to crush and screen sequentially, and collecting the edible salt with the granularity of 14-30 meshes;
c. Vacuum drying the edible salt;
Transferring the rewet granulated edible salt to a mixing tank, and gradually adding the auxiliary material slurry prepared in the step (2) to the surface of the edible salt in a spray mode for mixing, wherein the mixing time is 10-30 min;
(4) Placing the mixed material in the step (3) into a hot air circulation drying oven, and baking for 1-3 h at 55-70 ℃;
(5) Sieving the baked materials with a 30-mesh sieve, removing residual fine powder in the product, and taking the oversize material to obtain the dry-cleaning salt product.
Example 8
A preparation method of plush toy dry cleaning salt comprises the following steps:
(1) Accurately weighing each raw material according to 65 parts of edible salt, 2 parts of disodium cocoyl glutamate, 2 parts of disodium lauryl glutamate, 4 parts of bitter tea extract, 4 parts of gleditsia sinensis extract, 4 parts of lemon extract and 4 parts of chamomile extract according to a formula for standby;
(2) Premixing the raw materials prepared in the step (1) except the edible salt for 5min to obtain a premix; adding water according to the mass ratio of the premix to the feed liquid of 1:2g/g, continuously mixing for 15min, homogenizing, and obtaining auxiliary material slurry for later use;
(3) Firstly, carrying out rewetting and granulating treatment on the edible salt prepared in the step (1):
a. Dissolving edible salt in water, adding 1% of acacia and 4% of maltodextrin based on the mass of the edible salt, fully stirring until the acacia and the maltodextrin are completely dissolved, and then spray-drying;
b. C, placing the edible salt treated in the step a in a high-humidity environment (the relative humidity is 75% -85%), enabling the hollow edible salt to absorb moisture and agglomerate, then taking the blocky and moisture-absorbing edible salt to crush and screen sequentially, and collecting the edible salt with the granularity of 14-30 meshes;
c. Vacuum drying the edible salt;
Transferring the rewet granulated edible salt to a mixing tank, and gradually adding the auxiliary material slurry prepared in the step (2) to the surface of the edible salt in a spray mode for mixing for 10min;
(4) Placing the mixed material in the step (3) into a hot air circulation drying oven, and baking for 3 hours at 55 ℃;
(5) Sieving the baked materials with a 30-mesh sieve, removing residual fine powder in the product, and taking the oversize material to obtain the dry-cleaning salt product.
Example 9
A preparation method of plush toy dry cleaning salt comprises the following steps:
(1) Accurately weighing each raw material according to 95 parts of edible salt, 0.5 part of disodium cocoyl glutamate, 0.5 part of disodium lauryl glutamate, 2 parts of bitter tea extract, 1 part of gleditsia sinensis extract, 1.5 parts of lemon extract and 1.5 parts of chamomile extract according to a formula for standby;
(2) Premixing the raw materials prepared in the step (1) except the edible salt for 15min to obtain a premix; adding water according to the mass ratio of the premix to the feed liquid of 1:3g/g, continuously mixing for 5min, homogenizing, and obtaining auxiliary material slurry for later use;
(3) Firstly, carrying out rewetting and granulating treatment on the edible salt prepared in the step (1):
a. Dissolving edible salt in water, adding 1.5% of acacia and 2% of maltodextrin based on the mass of the edible salt, fully stirring until the acacia and the maltodextrin are completely dissolved, and then spray-drying;
b. C, placing the edible salt treated in the step a in a high-humidity environment (the relative humidity is 75% -85%), enabling the hollow edible salt to absorb moisture and agglomerate, then taking the blocky and moisture-absorbing edible salt to crush and screen sequentially, and collecting the edible salt with the granularity of 14-30 meshes;
c. Vacuum drying the edible salt;
Transferring the rewet granulated edible salt to a mixing tank, and gradually adding the auxiliary material slurry prepared in the step (2) to the surface of the edible salt in a spray mode for mixing for 30min;
(4) Placing the mixed material in the step (3) into a hot air circulation drying oven, and baking for 1h at 70 ℃;
(5) Sieving the baked materials with a 30-mesh sieve, removing residual fine powder in the product, and taking the oversize material to obtain the dry-cleaning salt product.
Example 10
A preparation method of plush toy dry cleaning salt comprises the following steps:
(1) Accurately weighing each raw material according to 80 parts of edible salt, 1 part of disodium cocoyl glutamate, 1 part of disodium lauryl glutamate, 4 parts of bitter tea extract, 4 parts of gleditsia sinensis extract, 4 parts of lemon extract and 4 parts of chamomile extract according to a formula for standby;
(2) Premixing the raw materials prepared in the step (1) except the edible salt for 15min to obtain a premix; adding water according to the mass ratio of the premix to the feed liquid of 1:2.5g/g, continuously mixing for 10min, homogenizing, and obtaining auxiliary material slurry for later use;
(3) Firstly, carrying out rewetting and granulating treatment on the edible salt prepared in the step (1):
a. Dissolving edible salt in water, adding 0.8% of acacia and 6% of maltodextrin based on the mass of the edible salt, fully stirring until the acacia and the maltodextrin are completely dissolved, and then spray-drying;
b. C, placing the edible salt treated in the step a in a high-humidity environment (the relative humidity is 75% -85%), enabling the hollow edible salt to absorb moisture and agglomerate, then taking the blocky and moisture-absorbing edible salt to crush and screen sequentially, and collecting the edible salt with the granularity of 14-30 meshes;
c. Vacuum drying the edible salt;
Transferring the rewet granulated edible salt to a mixing tank, and gradually adding the auxiliary material slurry prepared in the step (2) to the surface of the edible salt in a spray mode for mixing for 20min;
(4) Placing the mixed material in the step (3) into a hot air circulation drying oven, and baking for 2 hours at 65 ℃;
(5) Sieving the baked materials with a 30-mesh sieve, removing residual fine powder in the product, and taking the oversize material to obtain the dry-cleaning salt product.
Example 11
(1) Placing the plush toy to be cleaned in a sealable container, adding dry cleaning salt according to the mass ratio of the plush toy to the dry cleaning salt of 2-5:1 g/g, and sealing the container; the container for cleaning can be a pot body with a cover or a thicker plastic bag; when the plush toy has a complex structure and a large surface area, more dry cleaning salt can be added, and the mass ratio of the plush toy to the dry cleaning salt is controlled to be 4-5:1 g/g; when the plush toy has a simple structure and is mostly a flat surface, less dry cleaning salt can be added, and the mass ratio of the plush toy to the dry cleaning salt is controlled to be 2-4:1 g/g;
(2) The container filled with the plush toy and the dry cleaning salt is quickly turned over for 5 to 10 minutes, so that the plush toy and the dry cleaning salt are fully contacted and rubbed with each other;
(3) Pouring out the plush toy and the dry-cleaning salt in the container, shaking the plush toy, and shaking the residual dry-cleaning salt on the plush toy.
Example 12
Investigation of the granularity of the edible salt in the formula of the invention.
1. Experimental materials
Preparing a sample to be cleaned: preparing a plurality of plush toys with the same specification, wherein the plush toys are plush Teddy bear, and the size of the plush toys is 40cm long, 20cm wide and 20cm high (based on the outer packing size); selecting a sunny day, and placing the plush toy in an open air environment for 3 days to enable the plush Teddy Xiong Ziran to be stained with pollutants such as dust, soil, bacteria and the like to serve as the plush toy to be cleaned;
in the embodiment, the dry-cleaning salt product is produced and prepared according to the method of the embodiment 10, wherein the difference is only that after the edible salt is subjected to the rewet and grain finishing treatment, the edible salt with the grain size range of 6-7 meshes, 8-12 meshes, 14-30 meshes, 32-80 meshes and below 80 meshes is collected for subsequent process treatment so as to obtain dry-cleaning salt products respectively prepared by the edible salt with different grain sizes; it can also be understood that the dry cleaning salt products finally prepared are also products of 5 different groups of 6-7 meshes, 8-12 meshes, 14-30 meshes, 32-80 meshes and below 80 meshes respectively in the particle size ranges;
2. Detection index and method
Based on the above 5 groups of dry cleaning salt products, the applicant examined the indexes of their cleaning ability, auxiliary material adhesion rate and residual rate after dry cleaning, and the specific detection method is as follows:
cleaning ability: and selecting 12 product experimenters to form an evaluation group, observing and judging the decontamination capability and softness of the plush toy cleaned by products with different meshes, scoring according to the scoring standard of the table 1, and taking an average value.
Table 1 scoring criteria
Auxiliary material adhesion rate: the sample mass of the premix in step 2 of example 10 was denoted as m 0, the sample mass of the undersize after passing through the 30 mesh sieve in step 5 of example 10 was denoted as m, and the auxiliary attachment rate=100% × (m 0-m)/m0.
Residual ratio after dry cleaning: the mass of the dry-cleaning salt was designated as M 0, the mass of the plush toy was designated as M 1, the mass of the plush toy after the dry-cleaning salt was used was designated as M 2, and the residual rate after the dry cleaning was=100% × (M 0+M1-M2)/M0.
3. Detection result
TABLE 2 influence of the number of edible salt on the cleaning effect of plush toys
As can be seen from Table 2, the number of edible salt has a significant effect on the cleaning effect of the plush toy. When the mesh number of the edible salt is more than 80 meshes (the mesh number is large, the corresponding granularity is small), the auxiliary materials can be effectively and uniformly attached to the surfaces of the edible salt particles due to the large specific surface area of the edible salt, so that the auxiliary materials are high in attachment rate and good in decontamination capability, but the particle size of the product is too small, dust emission is easy to occur in the preparation process and the cleaning and using process of the product, and the product is not easy to fall off from plush gaps in the cleaning process, so that the residual rate is high after dry cleaning, and plush is hard and knotted; as the mesh number of the edible salt is reduced, namely the corresponding granularity is increased, the dust emission is weakened, the residual rate is reduced, the softness is increased, and the comprehensive cleaning effect of the product is optimal when the mesh number is 14-30 meshes; however, when the mesh number is continuously reduced, the granularity of the edible salt is too large, so that the product cannot fully enter between the floss gaps on the surface of the plush toy, and other auxiliary materials are difficult to effectively wrap on salt particles in the preparation process of the product or are easy to fall off after wrapping, so that the adhesion rate of the auxiliary materials of the product is reduced, the detergency is reduced, and the efficacy of the product is affected.
Example 13
The dry cleaning salt of the present invention has a cleaning effect and skin irritation.
1. Experimental materials
Preparing a sample to be cleaned: preparing a plurality of plush toys with the same specification, wherein the plush toys are plush Teddy bear, and the size of the plush toys is 40cm long, 20cm wide and 20cm high (based on the outer packing size); and (3) selecting a sunny day, and placing the plush toy in an open air environment for 3 days so that the plush Teddy Xiong Ziran is adhered with pollutants such as dust, soil, bacteria and the like to serve as the plush toy to be cleaned.
Preparation of a cleaning agent: sample 1 is a commercially available general cleaner (laundry detergent), sample 2 is a commercially available general dry cleaning powder (cloth dry cleaning powder), and sample 3 is a product prepared in example 9 of the present invention.
2. Experimental method
The method for using sample 1 is: dissolving the sample 1 in water, soaking for 30min, rubbing, rinsing for 3 times according to the common cleaning habit, and spin-drying or wringing; typically 30 kg of water is added to 30mL of laundry detergent.
Sample 2 application method: and uniformly spreading the sample 2 on the plush toy, reversely rubbing the wool by using a bath brush for a few minutes, and after the washing is finished, brushing dry-cleaning powder by using a comb.
The using method of the sample 3 is carried out by adopting the method of the embodiment 11, placing the plush toy to be cleaned in a sealable container, adding dry cleaning salt according to the mass ratio of the plush toy to the dry cleaning salt of 3:1g/g, rapidly overturning the sealed container for 5min, pouring out, shaking the plush toy, and shaking the residual dry cleaning salt on the plush toy.
3. Detection index
(1) Cleaning ability and fixation ability: selecting 12 product experimenters to form an assessment group, observing and judging the decontamination capability, softness and color fixing capability of the plush toy cleaned by using three groups of products, scoring according to the scoring standard of the table 1, and then taking an average value, wherein the measurement method is the same as that of example 12;
(2) Skin irritation: the back and spine sides of the test animal are sheared off by the hair before the test, the hair removing range is 3cm multiplied by 3cm respectively, 1g (mL) of the test object is uniformly coated on the skin with the area of 2.5cm multiplied by 2.5cm, four layers of gauze are coated on the skin after the coating, then a layer of non-stimulated plastic film is used for covering, and then the non-stimulated adhesive tape is used for fixing. The other side of the dehaired skin was used as a negative control with sterilized normal saline. After 12h of application, the residue was removed by washing with water. The coating is applied once a day for 14 days continuously, and the conditions of red spots, edema and the like of the coating part are observed and recorded by naked eyes.
Table 3 comparison of cleaning effect and skin irritation of dry cleaning salt for plush toy with conventional method
As is clear from Table 3, the dry cleaning salt for plush toys according to the present invention has little difference in detergency from the conventional cleaning agents and dry cleaning powders on the market, but is excellent in softness after washing, color fixing ability and skin irritation effect. This is due to the fact that in the commercial general cleaners, certain chemical reactions between the detersive ingredients and the dye occur during the cleaning process, resulting in slight discoloration; in addition, the common cleaning agent needs to be cleaned by adding water, so that the cleaning agent can be removed by rinsing, and the residual quantity of the cleaning agent is smaller after the conventional rinsing for 3 times in the embodiment, so that the skin irritation is smaller; the common dry cleaning powder sold in the market is easy to remain and cause irritation to skin due to fine powder, and the phenomena of redness, swelling and the like are generated.

Claims (2)

1. The dry cleaning salt for the plush toy is characterized by comprising the following raw materials in parts by weight: 65-95 parts of edible salt, 0.5-2 parts of disodium cocoyl glutamate, 0.5-2 parts of disodium lauryl glutamate, 2-4 parts of bitter tea extract, 1-4 parts of gleditsia sinensis lam extract, 1.5-4 parts of lemon extract and 1.5-4 parts of chamomile extract;
The preparation method comprises the following steps:
(1) Accurately weighing the raw materials according to a formula for standby;
(2) Premixing other raw materials except edible salt prepared in the step (1) for 5-15 min to obtain a premix; adding water according to the mass ratio of the premix to the feed liquid of 1:2-3 g/g, continuously mixing the mixture for 5-15 min, homogenizing the mixture, and obtaining auxiliary material slurry for later use;
(3) Firstly, carrying out rewetting and granulating treatment on the edible salt prepared in the step (1), transferring the edible salt to a mixing tank, and then gradually adding the auxiliary material slurry prepared in the step (2) to the surface of the edible salt in a spraying mode for mixing for 10-30 min;
The specific method for rewetting and granulating treatment comprises the following steps:
a. Dissolving edible salt in water, adding 0.8-1.5% of acacia and 2-6% of maltodextrin based on the mass of the edible salt, fully stirring until the acacia and the maltodextrin are completely dissolved, and then spray-drying;
b. C, placing the edible salt treated in the step a in a high-humidity environment to enable the edible salt to absorb moisture and agglomerate, then taking blocky moisture-absorbing salt to crush and screen sequentially, and collecting the edible salt with the granularity of 14-30 meshes;
c. Vacuum drying edible salt;
(4) Placing the mixed materials in the step (3) into a hot air circulation drying oven, and baking at 55-70 ℃ for 1-3 h;
(5) Sieving the baked materials with a 30-mesh sieve, removing residual fine powder in the product, and taking the oversize material to obtain the dry-cleaning salt product.
2. The cleaning method of the plush toy is characterized by comprising the following steps:
(1) Placing the plush toy to be cleaned in a sealable container, adding the dry cleaning salt according to the mass ratio of the plush toy to the dry cleaning salt of 2-5:1 g/g, and sealing the container;
(2) The container filled with the plush toy and the dry cleaning salt is quickly turned over for 5 to 10 min, so that the plush toy and the dry cleaning salt are fully contacted and rubbed with each other;
(3) Pouring out the plush toy and the dry-cleaning salt in the container, shaking the plush toy, and shaking the residual dry-cleaning salt on the plush toy.
CN202210525944.5A 2022-05-13 2022-05-13 Dry cleaning salt for plush toy and preparation method thereof Active CN114774207B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202210525944.5A CN114774207B (en) 2022-05-13 2022-05-13 Dry cleaning salt for plush toy and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202210525944.5A CN114774207B (en) 2022-05-13 2022-05-13 Dry cleaning salt for plush toy and preparation method thereof

Publications (2)

Publication Number Publication Date
CN114774207A CN114774207A (en) 2022-07-22
CN114774207B true CN114774207B (en) 2024-05-31

Family

ID=82437212

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202210525944.5A Active CN114774207B (en) 2022-05-13 2022-05-13 Dry cleaning salt for plush toy and preparation method thereof

Country Status (1)

Country Link
CN (1) CN114774207B (en)

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1361510A (en) * 1971-06-15 1974-07-24 Sato Shokuhin Kogyo Kk Processing common salt
SU1117312A1 (en) * 1983-02-24 1984-10-07 Научно-Исследовательский Технохимический Институт Бытового Обслуживания Agent for cleaning soft children's toy
KR19980043563A (en) * 1996-12-04 1998-09-05 성재갑 Toy cleaner composition
CN104450327A (en) * 2013-09-24 2015-03-25 天津一橙垄达环保科技开发有限公司 Natural environment-friendly dry cleaning powder and preparation process thereof
CN205636222U (en) * 2016-03-28 2016-10-12 邯郸学院 Stuffed toy dry cleaner
CN107828563A (en) * 2017-11-07 2018-03-23 重庆市盐业(集团)有限公司 One kind cleaning salt and its preparation and application
CN208450102U (en) * 2018-07-10 2019-02-01 陈剑峰 A kind of decompression children down toy Dry cleaning device
CN110638716A (en) * 2019-11-15 2020-01-03 云南绿新生物药业有限公司 Cannabis diol-containing dry cleaning powder for pets and preparation method thereof

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1361510A (en) * 1971-06-15 1974-07-24 Sato Shokuhin Kogyo Kk Processing common salt
SU1117312A1 (en) * 1983-02-24 1984-10-07 Научно-Исследовательский Технохимический Институт Бытового Обслуживания Agent for cleaning soft children's toy
KR19980043563A (en) * 1996-12-04 1998-09-05 성재갑 Toy cleaner composition
CN104450327A (en) * 2013-09-24 2015-03-25 天津一橙垄达环保科技开发有限公司 Natural environment-friendly dry cleaning powder and preparation process thereof
CN205636222U (en) * 2016-03-28 2016-10-12 邯郸学院 Stuffed toy dry cleaner
CN107828563A (en) * 2017-11-07 2018-03-23 重庆市盐业(集团)有限公司 One kind cleaning salt and its preparation and application
CN208450102U (en) * 2018-07-10 2019-02-01 陈剑峰 A kind of decompression children down toy Dry cleaning device
CN110638716A (en) * 2019-11-15 2020-01-03 云南绿新生物药业有限公司 Cannabis diol-containing dry cleaning powder for pets and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
胶囊型免洗干粉洗发剂的制备及除污效果评价;来士琦等;广东化工;第48卷(第14期);第72-78页 *

Also Published As

Publication number Publication date
CN114774207A (en) 2022-07-22

Similar Documents

Publication Publication Date Title
CN104178379A (en) Natural washing product with strong oil and dirt removal capacity and preparation method of natural washing product with strong oil and dirt removal capacity
CN102041205A (en) Scrub soap and preparation process and formula thereof
CN105012224A (en) Natural shampoo and preparation method thereof
CN106047509A (en) Washing powder and preparation method thereof
CN105176709A (en) Preparation method of plant washing salt powder
JP3610278B2 (en) Processed rice bran
CN105754751A (en) Anti-bacteria and water-saving detergent prepared from pure natural Chinese herbal medicines and plants and preparation method of detergent
CN104212647A (en) Preparation method of pure natural tea seed detergent
CN1036663C (en) Withering tea powder detergent
CN105542974A (en) Skin-care washing powder and preparation method and application thereof
CN105647711A (en) Fruit washing salt and preparation method
CN114774207B (en) Dry cleaning salt for plush toy and preparation method thereof
CN103937629A (en) Washing soap specially used for infants and children
CN105925396A (en) Shell-powder-containing fruit and vegetable washing agent with pesticide removing function
JP3452351B2 (en) Loquat tea production equipment
CN108504461A (en) One kind containing diatomaceous antimicrobial laundry liquid and preparation method thereof
CN111602688A (en) Natural herbal bag for removing mites
CN100430460C (en) Natural scavenging agent for removing residual pesticide on vegetable and fruitage
CN110373274A (en) A kind of dedicated waterless nano liquid detergent of antibacterial anti-mite infant
CN104224577A (en) Whole-plant type hand cleaner and preparation method thereof
CN110343577A (en) A kind of fruits and vegetables washing salt and preparation method thereof
CN112842935B (en) Pet SPA carbonic acid tablet with antibacterial, mite-killing and moisturizing effects and preparation method thereof
CN108084836A (en) A kind of preparation method of dust-proof carpet care agent
CN107236600A (en) A kind of sterilizing skin-protective powdery liquid detergent
KR101420225B1 (en) Foaming composition for washing or cleansing aid and preparation method thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant