CN114737387A - 一种雪尼尔面料的砂洗整理工艺 - Google Patents
一种雪尼尔面料的砂洗整理工艺 Download PDFInfo
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- CN114737387A CN114737387A CN202210573210.4A CN202210573210A CN114737387A CN 114737387 A CN114737387 A CN 114737387A CN 202210573210 A CN202210573210 A CN 202210573210A CN 114737387 A CN114737387 A CN 114737387A
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- 239000004744 fabric Substances 0.000 title claims abstract description 105
- 238000005406 washing Methods 0.000 title claims abstract description 87
- 239000004576 sand Substances 0.000 title claims abstract description 65
- 238000007730 finishing process Methods 0.000 title claims abstract description 21
- 230000000844 anti-bacterial effect Effects 0.000 claims abstract description 47
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 43
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 40
- 230000003647 oxidation Effects 0.000 claims abstract description 40
- 238000007254 oxidation reaction Methods 0.000 claims abstract description 40
- 239000004902 Softening Agent Substances 0.000 claims abstract description 32
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 25
- 238000002360 preparation method Methods 0.000 claims abstract description 18
- 229920000728 polyester Polymers 0.000 claims abstract description 15
- 239000006174 pH buffer Substances 0.000 claims abstract description 14
- 239000002253 acid Substances 0.000 claims abstract description 9
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 70
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 45
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 42
- 238000010438 heat treatment Methods 0.000 claims description 35
- 239000011259 mixed solution Substances 0.000 claims description 35
- 239000002994 raw material Substances 0.000 claims description 29
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 28
- 238000002156 mixing Methods 0.000 claims description 25
- 238000003756 stirring Methods 0.000 claims description 25
- 239000002351 wastewater Substances 0.000 claims description 25
- 239000012286 potassium permanganate Substances 0.000 claims description 24
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 15
- NRTJGTSOTDBPDE-UHFFFAOYSA-N [dimethyl(methylsilyloxy)silyl]oxy-dimethyl-trimethylsilyloxysilane Chemical compound C[SiH2]O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)C NRTJGTSOTDBPDE-UHFFFAOYSA-N 0.000 claims description 15
- 238000001816 cooling Methods 0.000 claims description 15
- 238000001035 drying Methods 0.000 claims description 15
- 239000012188 paraffin wax Substances 0.000 claims description 15
- RFVNOJDQRGSOEL-UHFFFAOYSA-N 2-hydroxyethyl octadecanoate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCCO RFVNOJDQRGSOEL-UHFFFAOYSA-N 0.000 claims description 14
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Natural products OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims description 14
- 229960005070 ascorbic acid Drugs 0.000 claims description 14
- 235000010323 ascorbic acid Nutrition 0.000 claims description 14
- 239000011668 ascorbic acid Substances 0.000 claims description 14
- 239000007822 coupling agent Substances 0.000 claims description 14
- 239000008367 deionised water Substances 0.000 claims description 14
- 229910021641 deionized water Inorganic materials 0.000 claims description 14
- 150000002191 fatty alcohols Chemical class 0.000 claims description 14
- 239000001866 hydroxypropyl methyl cellulose Substances 0.000 claims description 14
- 229920003088 hydroxypropyl methyl cellulose Polymers 0.000 claims description 14
- UFVKGYZPFZQRLF-UHFFFAOYSA-N hydroxypropyl methyl cellulose Chemical compound OC1C(O)C(OC)OC(CO)C1OC1C(O)C(O)C(OC2C(C(O)C(OC3C(C(O)C(O)C(CO)O3)O)C(CO)O2)O)C(CO)O1 UFVKGYZPFZQRLF-UHFFFAOYSA-N 0.000 claims description 14
- 235000010979 hydroxypropyl methyl cellulose Nutrition 0.000 claims description 14
- TYQCGQRIZGCHNB-JLAZNSOCSA-N l-ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(O)=C(O)C1=O TYQCGQRIZGCHNB-JLAZNSOCSA-N 0.000 claims description 14
- 238000000034 method Methods 0.000 claims description 14
- FZHAPNGMFPVSLP-UHFFFAOYSA-N silanamine Chemical compound [SiH3]N FZHAPNGMFPVSLP-UHFFFAOYSA-N 0.000 claims description 14
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 14
- 239000000706 filtrate Substances 0.000 claims description 11
- 239000006004 Quartz sand Substances 0.000 claims description 10
- 238000007599 discharging Methods 0.000 claims description 10
- 239000006185 dispersion Substances 0.000 claims description 10
- 239000012452 mother liquor Substances 0.000 claims description 10
- 239000004094 surface-active agent Substances 0.000 claims description 10
- 238000013268 sustained release Methods 0.000 claims description 10
- 239000012730 sustained-release form Substances 0.000 claims description 10
- 238000004065 wastewater treatment Methods 0.000 claims description 10
- BPMGYFSWCJZSBA-UHFFFAOYSA-N C[SiH](C)O[SiH3] Chemical compound C[SiH](C)O[SiH3] BPMGYFSWCJZSBA-UHFFFAOYSA-N 0.000 claims description 9
- 239000000243 solution Substances 0.000 claims description 9
- 239000007788 liquid Substances 0.000 claims description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 5
- 239000002202 Polyethylene glycol Substances 0.000 claims description 5
- 238000001914 filtration Methods 0.000 claims description 5
- 239000012535 impurity Substances 0.000 claims description 5
- 238000002844 melting Methods 0.000 claims description 5
- 230000008018 melting Effects 0.000 claims description 5
- 229920001223 polyethylene glycol Polymers 0.000 claims description 5
- 239000008213 purified water Substances 0.000 claims description 5
- 229920001030 Polyethylene Glycol 4000 Polymers 0.000 claims description 4
- 239000007853 buffer solution Substances 0.000 claims description 4
- 229940057838 polyethylene glycol 4000 Drugs 0.000 claims description 4
- DPIBHJOCCAFDDL-UHFFFAOYSA-N S(=O)(=O)([O-])[O-].[NH4+].[NH4+].C(C)(=O)O Chemical compound S(=O)(=O)([O-])[O-].[NH4+].[NH4+].C(C)(=O)O DPIBHJOCCAFDDL-UHFFFAOYSA-N 0.000 claims description 3
- NWGKJDSIEKMTRX-AAZCQSIUSA-N Sorbitan monooleate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O NWGKJDSIEKMTRX-AAZCQSIUSA-N 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 3
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 3
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 3
- 239000007974 sodium acetate buffer Substances 0.000 claims description 3
- BHZOKUMUHVTPBX-UHFFFAOYSA-M sodium acetic acid acetate Chemical compound [Na+].CC(O)=O.CC([O-])=O BHZOKUMUHVTPBX-UHFFFAOYSA-M 0.000 claims description 3
- QDWYPRSFEZRKDK-UHFFFAOYSA-M sodium;sulfamate Chemical compound [Na+].NS([O-])(=O)=O QDWYPRSFEZRKDK-UHFFFAOYSA-M 0.000 claims description 3
- 239000004721 Polyphenylene oxide Substances 0.000 claims description 2
- 150000001298 alcohols Chemical class 0.000 claims description 2
- 150000002170 ethers Chemical class 0.000 claims description 2
- -1 ketone compounds Chemical class 0.000 claims description 2
- 125000002467 phosphate group Chemical class [H]OP(=O)(O[H])O[*] 0.000 claims description 2
- 229920000570 polyether Polymers 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 4
- 238000004140 cleaning Methods 0.000 abstract 1
- 239000000975 dye Substances 0.000 description 5
- 230000037303 wrinkles Effects 0.000 description 3
- 238000010521 absorption reaction Methods 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 239000012768 molten material Substances 0.000 description 2
- 230000001954 sterilising effect Effects 0.000 description 2
- 238000004659 sterilization and disinfection Methods 0.000 description 2
- 230000004075 alteration Effects 0.000 description 1
- ALSPKRWQCLSJLV-UHFFFAOYSA-N azanium;acetic acid;acetate Chemical compound [NH4+].CC(O)=O.CC([O-])=O ALSPKRWQCLSJLV-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000005562 fading Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
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Abstract
本发明公开了一种雪尼尔面料的砂洗整理工艺,包括以下步骤:S1.面料入机:将染色后的雪尼尔面料放入耐酸耐氧化的涤纶网袋中,接着放入砂洗专用机中,浴比控制在1:20‑60,在室温下加入pH缓冲体系,控制pH值在4.0‑5.8;S2.氧化助剂制备;S3.砂洗;S4.柔软剂制备;S5.柔软洗;S6.抗菌洗:将S5处理后的雪尼尔面料取出,放入抗菌整理剂中浸轧处理20‑40分钟;S7.清水洗。本发明通过将面料放入耐酸耐氧化的涤纶网袋中,并加入pH缓冲体系,降低了氧化助剂对雪尼尔面料本身的作用,使氧化助剂主要作用于雪尼尔面料的表面及其上面的染料,减少了对雪尼尔面料的损伤以及内部染料的破坏,有效避免了传统砂洗工艺对雪尼尔面料带来的强力损伤。
Description
技术领域
本发明属于雪尼尔面料技术领域,具体涉及一种雪尼尔面料的砂洗整理工艺。
背景技术
砂洗多用一些碱性,氧化性助剂,使衣物洗后有一定褪色效果及陈旧感,若配以石磨,洗后布料表面会产生一层柔和霜白的绒毛,再加入一些柔软剂,可使洗后织物松软、柔和,从而延长衣服寿命。雪尼尔面料由不同细度和强力的短纤维或长丝通过捻合而成的,在雪尼尔面料加工时也需要进行砂洗整理处理。
目前现有的雪尼尔面料的砂洗整理工艺还存在一些的问题:在处理过程中,容易对雪尼尔面料的内部造成损伤以及对内部染料制造成破坏,同时处理后的雪尼尔面料的抗菌性较差,为此我们提出一种雪尼尔面料的砂洗整理工艺。
发明内容
本发明的目的在于提供一种雪尼尔面料的砂洗整理工艺,以解决上述背景技术中提出的问题。
为实现上述目的,本发明提供如下技术方案:一种雪尼尔面料的砂洗整理工艺,包括以下步骤:
S1.面料入机:将染色后的雪尼尔面料放入耐酸耐氧化的涤纶网袋中,接着放入砂洗专用机中,浴比控制在1:20-60,在室温下加入pH缓冲体系,控制pH值在4.0-5.8;
S2.氧化助剂制备:所述氧化助剂选自高锰酸钾缓释剂;
S3.砂洗:将砂洗专用机内升温至50-90℃,在砂洗专用机中加入S2制备氧化助剂进行砂洗,砂洗时间为40-60分钟;
S4.柔软剂制备:所述柔软剂包括以下重量份计的原料组成:八甲基四硅氧烷100-140份,聚乙氧基化脂肪醇40-60份,抗坏血酸3-6份,二甲基二硅氧烷250-350份,乙二醇单硬脂酸酯1-3份、羟丙基甲基纤维素1-3份、碳酸钠1-3份、氨基硅烷偶联剂1-3份、柠檬酸15-30份,去离子水800-1000份;
S5.柔软洗:将S3中砂洗专用机的液体排出,先加入40-60℃的水,再加入S4中制备的柔软剂,柔化处理10-30分钟,脱水、烘干;
S6.抗菌洗:将S5处理后的雪尼尔面料取出,放入抗菌整理剂中浸轧处理20-40分钟;
S7.清水洗:将S6处理后的雪尼尔面料取出,用清水清洗2-4次,烘干。
优选的,所述S1中的pH缓冲体系选用乙酸-乙酸钠缓冲体系或醋酸-醋酸铵缓冲体系或醋酸-硫酸铵缓冲体系。
优选的,所述S2中氧化助剂制备的方法具体为:
S201.原料准备:按以下重量份计取原料,石蜡30-50份,石英砂30-50份,活性炭5-20份,高锰酸钾5-10份;
S202.原料融化:将上述石蜡加入无水乙醇和聚乙二醇的混合液中,加热至60-80℃,搅拌直至石蜡完全融化;
S203.原料混合:在搅拌下依次向S202所得溶液中加入表面活性剂、石英砂、活性炭粉末和高锰酸钾;
S204.将S203得到的熔融态材料冷却即得所述的高锰酸钾缓释剂。
优选的,所述S203中的表面活性剂选自聚乙二醇-4000、司盘80中的至少一种。
优选的,所述S202和S203中的搅拌的转速为200-400rpm,搅拌时间为10-40min。
优选的,所述S4中柔软剂制备的方法包括以下步骤:
S401.原料准备:按以下重量份计取原料,八甲基四硅氧烷100-140份,聚乙氧基化脂肪醇40-60份,抗坏血酸3-6份,二甲基二硅氧烷250-350份,乙二醇单硬脂酸酯1-3份、羟丙基甲基纤维素1-3份、碳酸钠1-3份、氨基硅烷偶联剂1-3份、柠檬酸15-30份,去离子水800-1000份;
S402.制备第一混合溶液:将八甲基四硅氧烷与聚乙氧基化脂肪醇混合,加入氢氧化钠调节PH值为11,以3-6℃/min升温至120-150℃,反应6-10小时,以2-4℃/min降温至40-60℃,滴加抗坏血酸调节PH值降至5,得第一混合溶液;
S403.制备第二混合溶液:将3二甲基二硅氧烷与纯净水混合,加入氢氧化钠调节PH值为12,以1-3℃/min升温至60-80℃,反应10-14小时,以3-6℃/min升温至120-130℃,反应5-8小时,得第二混合溶液;
S404.混合制备柔软剂:将第一混合溶液与第二混合溶液混合,加入氢氧化钠调节PH值为11,以3-6℃/min升温至80-100℃,反应5-8小时,以1-3℃/min降至室温,加入乙二醇单硬脂酸酯、羟丙基甲基纤维素、碳酸钠、氨基硅烷偶联剂、柠檬酸,搅拌均匀,即得柔软剂。
优选的,所述S5中柔化处理的温度控制在40-60℃,烘干温度控制在50-80℃。
优选的,所述S6中抗菌整理剂包括抗菌分散母液、后整理剂和去离子水,所述抗菌分散母液中的纳米抗菌成分占所述抗菌整理液总质量的0.4-1.8wt%,所述后整理剂占所述抗菌整理液总质量的1-4wt%。
优选的,所述后整理剂为氨基磺酸钠、脂肪醇聚氧乙烯醚、烷基酚聚氧乙烯醚、聚醚、磷酸酯类化合物、醇类化合物、酮类化合物和醚类化合物中的一种。
优选的,还包括废水处理,所述废水处理具体为:将废水排放到同一地方,加热废水至90-100℃,保持20-40分钟,趁热过滤除去废水中的杂质得到过滤液,在热的过滤液中加入冷水调节温度后,即可再利用。
与现有技术相比,本发明的有益效果是:
(1)本发明通过将面料放入耐酸耐氧化的涤纶网袋中,并加入pH缓冲体系,降低了氧化助剂对雪尼尔面料本身的作用,使氧化助剂主要作用于雪尼尔面料的表面及其上面的染料,减少了对雪尼尔面料的损伤以及内部染料的破坏,有效避免了传统砂洗工艺对雪尼尔面料带来的强力损伤。
(2)本发明制备的柔软剂为非离子型,对环境污染小,通过该柔软剂处理雪尼尔面料,使得雪尼尔面料的蓬松度得到提高,从而能够增加雪尼尔面料的柔软性能。
(3)本发明通过采用高锰酸钾缓释剂作为氧化助剂,不仅氧化能力强,同时利用高锰酸钾具有杀菌能力,从而方便提高雪尼尔面料的抗菌性。
(4)本发明通过抗菌整理剂对雪尼尔面料进行浸轧,得到雪尼尔面料的柔软性、抗皱性、吸水性以及抗菌性均得到的提高,从而提升了雪尼尔面料的质量。
附图说明
图1为本发明的流程图。
具体实施方式
下面将结合本发明实施例中的附图,对本发明实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例仅仅是本发明一部分实施例,而不是全部的实施例。基于本发明中的实施例,本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例,都属于本发明保护的范围。
实施例1
请参阅图1,本发明提供一种技术方案:一种雪尼尔面料的砂洗整理工艺,包括以下步骤:
S1.面料入机:将染色后的雪尼尔面料放入耐酸耐氧化的涤纶网袋中,接着放入砂洗专用机中,浴比控制在1:20,在室温下加入pH缓冲体系,控制pH值在4.0;
S2.氧化助剂制备:所述氧化助剂选自高锰酸钾缓释剂;
S3.砂洗:将砂洗专用机内升温至50℃,在砂洗专用机中加入S2制备氧化助剂进行砂洗,砂洗时间为40分钟;
S4.柔软剂制备:所述柔软剂包括以下重量份计的原料组成:八甲基四硅氧烷100份,聚乙氧基化脂肪醇40份,抗坏血酸3份,二甲基二硅氧烷250份,乙二醇单硬脂酸酯1份、羟丙基甲基纤维素1份、碳酸钠1份、氨基硅烷偶联剂1份、柠檬酸15份,去离子水800份;
S5.柔软洗:将S3中砂洗专用机的液体排出,先加入40℃的水,再加入S4中制备的柔软剂,柔化处理10分钟,脱水、烘干;
S6.抗菌洗:将S5处理后的雪尼尔面料取出,放入抗菌整理剂中浸轧处理20分钟;
S7.清水洗:将S6处理后的雪尼尔面料取出,用清水清洗2次,烘干。
本实施例中,优选的,所述S1中的pH缓冲体系选用乙酸-乙酸钠缓冲体系。
本实施例中,优选的,所述S2中氧化助剂制备的方法具体为:
S201.原料准备:按以下重量份计取原料,石蜡30份,石英砂30份,活性炭5份,高锰酸钾5份;
S202.原料融化:将上述石蜡加入无水乙醇和聚乙二醇的混合液中,加热至60℃,搅拌直至石蜡完全融化;
S203.原料混合:在搅拌下依次向S202所得溶液中加入表面活性剂、石英砂、活性炭粉末和高锰酸钾;
S204.将S203得到的熔融态材料冷却即得所述的高锰酸钾缓释剂。
本实施例中,优选的,所述S203中的表面活性剂选自聚乙二醇-4000。
本实施例中,优选的,所述S202和S203中的搅拌的转速为200rpm,搅拌时间为10min。
本实施例中,优选的,所述S4中柔软剂制备的方法包括以下步骤:
S401.原料准备:按以下重量份计取原料,八甲基四硅氧烷100份,聚乙氧基化脂肪醇40份,抗坏血酸3份,二甲基二硅氧烷250份,乙二醇单硬脂酸酯1份、羟丙基甲基纤维素1份、碳酸钠1份、氨基硅烷偶联剂1份、柠檬酸15份,去离子水800份;
S402.制备第一混合溶液:将八甲基四硅氧烷与聚乙氧基化脂肪醇混合,加入氢氧化钠调节PH值为11,以3℃/min升温至120℃,反应6小时,以2℃/min降温至40℃,滴加抗坏血酸调节PH值降至5,得第一混合溶液;
S403.制备第二混合溶液:将3二甲基二硅氧烷与纯净水混合,加入氢氧化钠调节PH值为12,以1℃/min升温至60℃,反应10小时,以3℃/min升温至120℃,反应5小时,得第二混合溶液;
S404.混合制备柔软剂:将第一混合溶液与第二混合溶液混合,加入氢氧化钠调节PH值为11,以3℃/min升温至80℃,反应5小时,以1℃/min降至室温,加入乙二醇单硬脂酸酯、羟丙基甲基纤维素、碳酸钠、氨基硅烷偶联剂、柠檬酸,搅拌均匀,即得柔软剂。
本实施例中,优选的,所述S5中柔化处理的温度控制在40℃,烘干温度控制在50℃。
本实施例中,优选的,所述S6中抗菌整理剂包括抗菌分散母液、后整理剂和去离子水,所述抗菌分散母液中的纳米抗菌成分占所述抗菌整理液总质量的0.4wt%,所述后整理剂占所述抗菌整理液总质量的1wt%。
本实施例中,优选的,所述后整理剂为氨基磺酸钠。
本实施例中,优选的,还包括废水处理,所述废水处理具体为:将废水排放到同一地方,加热废水至90℃,保持20分钟,趁热过滤除去废水中的杂质得到过滤液,在热的过滤液中加入冷水调节温度后,即可再利用。
实施例2
请参阅图1,本发明提供一种技术方案:一种雪尼尔面料的砂洗整理工艺,包括以下步骤:
S1.面料入机:将染色后的雪尼尔面料放入耐酸耐氧化的涤纶网袋中,接着放入砂洗专用机中,浴比控制在1:60,在室温下加入pH缓冲体系,控制pH值在5.8;
S2.氧化助剂制备:所述氧化助剂选自高锰酸钾缓释剂;
S3.砂洗:将砂洗专用机内升温至90℃,在砂洗专用机中加入S2制备氧化助剂进行砂洗,砂洗时间为60分钟;
S4.柔软剂制备:所述柔软剂包括以下重量份计的原料组成:八甲基四硅氧烷140份,聚乙氧基化脂肪醇60份,抗坏血酸6份,二甲基二硅氧烷350份,乙二醇单硬脂酸酯3份、羟丙基甲基纤维素3份、碳酸钠3份、氨基硅烷偶联剂3份、柠檬酸30份,去离子水1000份;
S5.柔软洗:将S3中砂洗专用机的液体排出,先加入60℃的水,再加入S4中制备的柔软剂,柔化处理30分钟,脱水、烘干;
S6.抗菌洗:将S5处理后的雪尼尔面料取出,放入抗菌整理剂中浸轧处理40分钟;
S7.清水洗:将S6处理后的雪尼尔面料取出,用清水清洗4次,烘干。
本实施例中,优选的,所述S1中的pH缓冲体系选用醋酸-醋酸铵缓冲体系。
本实施例中,优选的,所述S2中氧化助剂制备的方法具体为:
S201.原料准备:按以下重量份计取原料,石蜡50份,石英砂50份,活性炭20份,高锰酸钾10份;
S202.原料融化:将上述石蜡加入无水乙醇和聚乙二醇的混合液中,加热至80℃,搅拌直至石蜡完全融化;
S203.原料混合:在搅拌下依次向S202所得溶液中加入表面活性剂、石英砂、活性炭粉末和高锰酸钾;
S204.将S203得到的熔融态材料冷却即得所述的高锰酸钾缓释剂。
本实施例中,优选的,所述S203中的表面活性剂选自司盘80。
本实施例中,优选的,所述S202和S203中的搅拌的转速为400rpm,搅拌时间为40min。
本实施例中,优选的,所述S4中柔软剂制备的方法包括以下步骤:
S401.原料准备:按以下重量份计取原料,八甲基四硅氧烷140份,聚乙氧基化脂肪醇60份,抗坏血酸6份,二甲基二硅氧烷350份,乙二醇单硬脂酸酯3份、羟丙基甲基纤维素3份、碳酸钠3份、氨基硅烷偶联剂3份、柠檬酸30份,去离子水1000份;
S402.制备第一混合溶液:将八甲基四硅氧烷与聚乙氧基化脂肪醇混合,加入氢氧化钠调节PH值为11,以6℃/min升温至150℃,反应10小时,以4℃/min降温至60℃,滴加抗坏血酸调节PH值降至5,得第一混合溶液;
S403.制备第二混合溶液:将3二甲基二硅氧烷与纯净水混合,加入氢氧化钠调节PH值为12,以3℃/min升温至80℃,反应14小时,以6℃/min升温至130℃,反应8小时,得第二混合溶液;
S404.混合制备柔软剂:将第一混合溶液与第二混合溶液混合,加入氢氧化钠调节PH值为11,以6℃/min升温至100℃,反应8小时,以3℃/min降至室温,加入乙二醇单硬脂酸酯、羟丙基甲基纤维素、碳酸钠、氨基硅烷偶联剂、柠檬酸,搅拌均匀,即得柔软剂。
本实施例中,优选的,所述S5中柔化处理的温度控制在60℃,烘干温度控制在80℃。
本实施例中,优选的,所述S6中抗菌整理剂包括抗菌分散母液、后整理剂和去离子水,所述抗菌分散母液中的纳米抗菌成分占所述抗菌整理液总质量的1.8wt%,所述后整理剂占所述抗菌整理液总质量的4wt%。
本实施例中,优选的,所述后整理剂为脂肪醇聚氧乙烯醚。
本实施例中,优选的,还包括废水处理,所述废水处理具体为:将废水排放到同一地方,加热废水至100℃,保持40分钟,趁热过滤除去废水中的杂质得到过滤液,在热的过滤液中加入冷水调节温度后,即可再利用。
实施例3
请参阅图1,本发明提供一种技术方案:一种雪尼尔面料的砂洗整理工艺,包括以下步骤:
S1.面料入机:将染色后的雪尼尔面料放入耐酸耐氧化的涤纶网袋中,接着放入砂洗专用机中,浴比控制在1:40,在室温下加入pH缓冲体系,控制pH值在4.8;
S2.氧化助剂制备:所述氧化助剂选自高锰酸钾缓释剂;
S3.砂洗:将砂洗专用机内升温至70℃,在砂洗专用机中加入S2制备氧化助剂进行砂洗,砂洗时间为50分钟;
S4.柔软剂制备:所述柔软剂包括以下重量份计的原料组成:八甲基四硅氧烷120份,聚乙氧基化脂肪醇50份,抗坏血酸4份,二甲基二硅氧烷300份,乙二醇单硬脂酸酯2份、羟丙基甲基纤维素2份、碳酸钠2份、氨基硅烷偶联剂2份、柠檬酸25份,去离子水900份;
S5.柔软洗:将S3中砂洗专用机的液体排出,先加入50℃的水,再加入S4中制备的柔软剂,柔化处理20分钟,脱水、烘干;
S6.抗菌洗:将S5处理后的雪尼尔面料取出,放入抗菌整理剂中浸轧处理30分钟;
S7.清水洗:将S6处理后的雪尼尔面料取出,用清水清洗3次,烘干。
本实施例中,优选的,所述S1中的pH缓冲体系选用醋酸-硫酸铵缓冲体系。
本实施例中,优选的,所述S2中氧化助剂制备的方法具体为:
S201.原料准备:按以下重量份计取原料,石蜡40份,石英砂40份,活性炭15份,高锰酸钾8份;
S202.原料融化:将上述石蜡加入无水乙醇和聚乙二醇的混合液中,加热至70℃,搅拌直至石蜡完全融化;
S203.原料混合:在搅拌下依次向S202所得溶液中加入表面活性剂、石英砂、活性炭粉末和高锰酸钾;
S204.将S203得到的熔融态材料冷却即得所述的高锰酸钾缓释剂。
本实施例中,优选的,所述S203中的表面活性剂选自聚乙二醇-4000。
本实施例中,优选的,所述S202和S203中的搅拌的转速为300rpm,搅拌时间为30min。
本实施例中,优选的,所述S4中柔软剂制备的方法包括以下步骤:
S401.原料准备:按以下重量份计取原料,八甲基四硅氧烷120份,聚乙氧基化脂肪醇50份,抗坏血酸4份,二甲基二硅氧烷300份,乙二醇单硬脂酸酯2份、羟丙基甲基纤维素2份、碳酸钠2份、氨基硅烷偶联剂2份、柠檬酸20份,去离子水900份;
S402.制备第一混合溶液:将八甲基四硅氧烷与聚乙氧基化脂肪醇混合,加入氢氧化钠调节PH值为11,以4℃/min升温至140℃,反应8小时,以3℃/min降温至50℃,滴加抗坏血酸调节PH值降至5,得第一混合溶液;
S403.制备第二混合溶液:将3二甲基二硅氧烷与纯净水混合,加入氢氧化钠调节PH值为12,以2℃/min升温至70℃,反应12小时,以5℃/min升温至125℃,反应7小时,得第二混合溶液;
S404.混合制备柔软剂:将第一混合溶液与第二混合溶液混合,加入氢氧化钠调节PH值为11,以4℃/min升温至90℃,反应6小时,以2℃/min降至室温,加入乙二醇单硬脂酸酯、羟丙基甲基纤维素、碳酸钠、氨基硅烷偶联剂、柠檬酸,搅拌均匀,即得柔软剂。
本实施例中,优选的,所述S5中柔化处理的温度控制在50℃,烘干温度控制在60℃。
本实施例中,优选的,所述S6中抗菌整理剂包括抗菌分散母液、后整理剂和去离子水,所述抗菌分散母液中的纳米抗菌成分占所述抗菌整理液总质量的1.4%,所述后整理剂占所述抗菌整理液总质量的3wt%。
本实施例中,优选的,所述后整理剂为烷基酚聚氧乙烯醚。
本实施例中,优选的,还包括废水处理,所述废水处理具体为:将废水排放到同一地方,加热废水至95℃,保持30分钟,趁热过滤除去废水中的杂质得到过滤液,在热的过滤液中加入冷水调节温度后,即可再利用。
本发明的原理及优点:本发明通过将面料放入耐酸耐氧化的涤纶网袋中,并加入pH缓冲体系,降低了氧化助剂对雪尼尔面料本身的作用,使氧化助剂主要作用于雪尼尔面料的表面及其上面的染料,减少了对雪尼尔面料的损伤以及内部染料的破坏,有效避免了传统砂洗工艺对雪尼尔面料带来的强力损伤;本发明制备的柔软剂为非离子型,对环境污染小,通过该柔软剂处理雪尼尔面料,使得雪尼尔面料的蓬松度得到提高,从而能够增加雪尼尔面料的柔软性能;通过采用高锰酸钾缓释剂作为氧化助剂,不仅氧化能力强,同时利用高锰酸钾具有杀菌能力,从而方便提高雪尼尔面料的抗菌性;通过抗菌整理剂对雪尼尔面料进行浸轧,得到雪尼尔面料的柔软性、抗皱性、吸水性以及抗菌性均得到的提高,从而提升了雪尼尔面料的质量。
选取传统的砂洗工艺的雪尼尔面料和本发明砂洗工艺的雪尼尔面料进行以下实验,实验内容和结果如下表
通过各项实验可以发现,实施例1、实施例2和实施例3中砂洗处理的雪尼尔面料的柔软性、抗皱性、吸水性以及抗菌性皆得到提高,且实施例3为最佳实施例。
尽管已经示出和描述了本发明的实施例,对于本领域的普通技术人员而言,可以理解在不脱离本发明的原理和精神的情况下可以对这些实施例进行多种变化、修改、替换和变型,本发明的范围由所附权利要求及其等同物限定。
Claims (10)
1.一种雪尼尔面料的砂洗整理工艺,其特征在于:包括以下步骤:
S1.面料入机:将染色后的雪尼尔面料放入耐酸耐氧化的涤纶网袋中,接着放入砂洗专用机中,浴比控制在1:20-60,在室温下加入pH缓冲体系,控制pH值在4.0-5.8;
S2.氧化助剂制备:所述氧化助剂选自高锰酸钾缓释剂;
S3.砂洗:将砂洗专用机内升温至50-90℃,在砂洗专用机中加入S2制备氧化助剂进行砂洗,砂洗时间为40-60分钟;
S4.柔软剂制备:所述柔软剂包括以下重量份计的原料组成:八甲基四硅氧烷100-140份,聚乙氧基化脂肪醇40-60份,抗坏血酸3-6份,二甲基二硅氧烷250-350份,乙二醇单硬脂酸酯1-3份、羟丙基甲基纤维素1-3份、碳酸钠1-3份、氨基硅烷偶联剂1-3份、柠檬酸15-30份,去离子水800-1000份;
S5.柔软洗:将S3中砂洗专用机的液体排出,先加入40-60℃的水,再加入S4中制备的柔软剂,柔化处理10-30分钟,脱水、烘干;
S6.抗菌洗:将S5处理后的雪尼尔面料取出,放入抗菌整理剂中浸轧处理20-40分钟;
S7.清水洗:将S6处理后的雪尼尔面料取出,用清水清洗2-4次,烘干。
2.根据权利要求1所述的一种雪尼尔面料的砂洗整理工艺,其特征在于:所述S1中的pH缓冲体系选用乙酸-乙酸钠缓冲体系或醋酸-醋酸铵缓冲体系或醋酸-硫酸铵缓冲体系。
3.根据权利要求1所述的一种雪尼尔面料的砂洗整理工艺,其特征在于:所述S2中氧化助剂制备的方法具体为:
S201.原料准备:按以下重量份计取原料,石蜡30-50份,石英砂30-50份,活性炭5-20份,高锰酸钾5-10份;
S202.原料融化:将上述石蜡加入无水乙醇和聚乙二醇的混合液中,加热至60-80℃,搅拌直至石蜡完全融化;
S203.原料混合:在搅拌下依次向S202所得溶液中加入表面活性剂、石英砂、活性炭粉末和高锰酸钾;
S204.将S203得到的熔融态材料冷却即得所述的高锰酸钾缓释剂。
4.根据权利要求3所述的一种雪尼尔面料的砂洗整理工艺,其特征在于:所述S203中的表面活性剂选自聚乙二醇-4000、司盘80中的至少一种。
5.根据权利要求3所述的一种雪尼尔面料的砂洗整理工艺,其特征在于:所述S202和S203中的搅拌的转速为200-400rpm,搅拌时间为10-40min。
6.根据权利要求1所述的一种雪尼尔面料的砂洗整理工艺,其特征在于:所述S4中柔软剂制备的方法包括以下步骤:
S401.原料准备:按以下重量份计取原料,八甲基四硅氧烷100-140份,聚乙氧基化脂肪醇40-60份,抗坏血酸3-6份,二甲基二硅氧烷250-350份,乙二醇单硬脂酸酯1-3份、羟丙基甲基纤维素1-3份、碳酸钠1-3份、氨基硅烷偶联剂1-3份、柠檬酸15-30份,去离子水800-1000份;
S402.制备第一混合溶液:将八甲基四硅氧烷与聚乙氧基化脂肪醇混合,加入氢氧化钠调节PH值为11,以3-6℃/min升温至120-150℃,反应6-10小时,以2-4℃/min降温至40-60℃,滴加抗坏血酸调节PH值降至5,得第一混合溶液;
S403.制备第二混合溶液:将3二甲基二硅氧烷与纯净水混合,加入氢氧化钠调节PH值为12,以1-3℃/min升温至60-80℃,反应10-14小时,以3-6℃/min升温至120-130℃,反应5-8小时,得第二混合溶液;
S404.混合制备柔软剂:将第一混合溶液与第二混合溶液混合,加入氢氧化钠调节PH值为11,以3-6℃/min升温至80-100℃,反应5-8小时,以1-3℃/min降至室温,加入乙二醇单硬脂酸酯、羟丙基甲基纤维素、碳酸钠、氨基硅烷偶联剂、柠檬酸,搅拌均匀,即得柔软剂。
7.根据权利要求1所述的一种雪尼尔面料的砂洗整理工艺,其特征在于:所述S5中柔化处理的温度控制在40-60℃,烘干温度控制在50-80℃。
8.根据权利要求1所述的一种雪尼尔面料的砂洗整理工艺,其特征在于:所述S6中抗菌整理剂包括抗菌分散母液、后整理剂和去离子水,所述抗菌分散母液中的纳米抗菌成分占所述抗菌整理液总质量的0.4-1.8wt%,所述后整理剂占所述抗菌整理液总质量的1-4wt%。
9.根据权利要求8所述的一种雪尼尔面料的砂洗整理工艺,其特征在于:所述后整理剂为氨基磺酸钠、脂肪醇聚氧乙烯醚、烷基酚聚氧乙烯醚、聚醚、磷酸酯类化合物、醇类化合物、酮类化合物和醚类化合物中的一种。
10.根据权利要求1所述的一种雪尼尔面料的砂洗整理工艺,其特征在于:还包括废水处理,所述废水处理具体为:将废水排放到同一地方,加热废水至90-100℃,保持20-40分钟,趁热过滤除去废水中的杂质得到过滤液,在热的过滤液中加入冷水调节温度后,即可再利用。
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