CN114703362B - 一种含钒含铬原料联合钠化焙烧的方法 - Google Patents
一种含钒含铬原料联合钠化焙烧的方法 Download PDFInfo
- Publication number
- CN114703362B CN114703362B CN202210261844.6A CN202210261844A CN114703362B CN 114703362 B CN114703362 B CN 114703362B CN 202210261844 A CN202210261844 A CN 202210261844A CN 114703362 B CN114703362 B CN 114703362B
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- Prior art keywords
- vanadium
- chromium
- raw materials
- clinker
- sodium
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 229910052720 vanadium Inorganic materials 0.000 title claims abstract description 104
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 title claims abstract description 104
- 239000011651 chromium Substances 0.000 title claims abstract description 94
- 229910052804 chromium Inorganic materials 0.000 title claims abstract description 94
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 title claims abstract description 90
- 239000002994 raw material Substances 0.000 title claims abstract description 55
- 238000000034 method Methods 0.000 title claims abstract description 34
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 title claims abstract description 15
- 239000011734 sodium Substances 0.000 title claims abstract description 15
- 229910052708 sodium Inorganic materials 0.000 title claims abstract description 15
- 238000002386 leaching Methods 0.000 claims abstract description 44
- 239000012065 filter cake Substances 0.000 claims abstract description 26
- WFISYBKOIKMYLZ-UHFFFAOYSA-N [V].[Cr] Chemical compound [V].[Cr] WFISYBKOIKMYLZ-UHFFFAOYSA-N 0.000 claims abstract description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 22
- 238000000605 extraction Methods 0.000 claims abstract description 21
- 238000003756 stirring Methods 0.000 claims abstract description 15
- 238000002156 mixing Methods 0.000 claims abstract description 13
- 238000001914 filtration Methods 0.000 claims abstract description 9
- 239000000706 filtrate Substances 0.000 claims abstract description 8
- 239000000047 product Substances 0.000 claims abstract description 8
- 159000000000 sodium salts Chemical class 0.000 claims abstract description 8
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 7
- 238000005406 washing Methods 0.000 claims abstract description 7
- 239000000463 material Substances 0.000 claims abstract description 4
- 238000002791 soaking Methods 0.000 claims abstract description 3
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 56
- ZSIAUFGUXNUGDI-UHFFFAOYSA-N hexan-1-ol Chemical compound CCCCCCO ZSIAUFGUXNUGDI-UHFFFAOYSA-N 0.000 claims description 45
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 28
- 239000012074 organic phase Substances 0.000 claims description 24
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 16
- 150000003242 quaternary ammonium salts Chemical class 0.000 claims description 14
- LZZYPRNAOMGNLH-UHFFFAOYSA-M Cetrimonium bromide Chemical compound [Br-].CCCCCCCCCCCCCCCC[N+](C)(C)C LZZYPRNAOMGNLH-UHFFFAOYSA-M 0.000 claims description 13
- KHSLHYAUZSPBIU-UHFFFAOYSA-M benzododecinium bromide Chemical compound [Br-].CCCCCCCCCCCC[N+](C)(C)CC1=CC=CC=C1 KHSLHYAUZSPBIU-UHFFFAOYSA-M 0.000 claims description 13
- 239000003085 diluting agent Substances 0.000 claims description 13
- -1 vanadium sodium carbonate-sodium bicarbonate Chemical compound 0.000 claims description 13
- 239000011259 mixed solution Substances 0.000 claims description 12
- 239000000243 solution Substances 0.000 claims description 11
- 239000007788 liquid Substances 0.000 claims description 10
- BJQHLKABXJIVAM-UHFFFAOYSA-N bis(2-ethylhexyl) phthalate Chemical compound CCCCC(CC)COC(=O)C1=CC=CC=C1C(=O)OCC(CC)CCCC BJQHLKABXJIVAM-UHFFFAOYSA-N 0.000 claims description 9
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 8
- 239000000843 powder Substances 0.000 claims description 8
- 239000011780 sodium chloride Substances 0.000 claims description 8
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 8
- 235000011152 sodium sulphate Nutrition 0.000 claims description 8
- 238000000926 separation method Methods 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 5
- 239000003054 catalyst Substances 0.000 claims description 4
- 150000001875 compounds Chemical class 0.000 claims description 4
- 239000003350 kerosene Substances 0.000 claims description 3
- 239000004615 ingredient Substances 0.000 claims description 2
- 230000002035 prolonged effect Effects 0.000 claims description 2
- 238000011084 recovery Methods 0.000 abstract description 4
- 238000004064 recycling Methods 0.000 abstract description 3
- 239000002920 hazardous waste Substances 0.000 abstract 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 14
- 239000002893 slag Substances 0.000 description 9
- 229910052742 iron Inorganic materials 0.000 description 7
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 6
- 239000002699 waste material Substances 0.000 description 6
- 229910000831 Steel Inorganic materials 0.000 description 5
- 239000003795 chemical substances by application Substances 0.000 description 5
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N iron oxide Inorganic materials [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 5
- NDLPOXTZKUMGOV-UHFFFAOYSA-N oxo(oxoferriooxy)iron hydrate Chemical compound O.O=[Fe]O[Fe]=O NDLPOXTZKUMGOV-UHFFFAOYSA-N 0.000 description 5
- 239000010959 steel Substances 0.000 description 5
- NQVBEJRSQQSHFS-UHFFFAOYSA-H [V+5].C([O-])([O-])=O.[Na+].C([O-])([O-])=O.C([O-])([O-])=O Chemical compound [V+5].C([O-])([O-])=O.[Na+].C([O-])([O-])=O.C([O-])([O-])=O NQVBEJRSQQSHFS-UHFFFAOYSA-H 0.000 description 3
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 3
- 235000017557 sodium bicarbonate Nutrition 0.000 description 3
- 229910052500 inorganic mineral Inorganic materials 0.000 description 2
- 235000010755 mineral Nutrition 0.000 description 2
- 239000011707 mineral Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000004321 preservation Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000012670 alkaline solution Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000004568 cement Substances 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000000658 coextraction Methods 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000005272 metallurgy Methods 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000002912 waste gas Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B1/00—Preliminary treatment of ores or scrap
- C22B1/02—Roasting processes
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/04—Extraction of metal compounds from ores or concentrates by wet processes by leaching
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/22—Treatment or purification of solutions, e.g. obtained by leaching by physical processes, e.g. by filtration, by magnetic means, or by thermal decomposition
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/44—Treatment or purification of solutions, e.g. obtained by leaching by chemical processes
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/20—Obtaining niobium, tantalum or vanadium
- C22B34/22—Obtaining vanadium
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/30—Obtaining chromium, molybdenum or tungsten
- C22B34/32—Obtaining chromium
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B7/00—Working up raw materials other than ores, e.g. scrap, to produce non-ferrous metals and compounds thereof; Methods of a general interest or applied to the winning of more than two metals
- C22B7/006—Wet processes
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Metallurgy (AREA)
- Mechanical Engineering (AREA)
- Organic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Geochemistry & Mineralogy (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Processing Of Solid Wastes (AREA)
Abstract
Description
Claims (3)
Priority Applications (1)
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CN202210261844.6A CN114703362B (zh) | 2022-03-17 | 2022-03-17 | 一种含钒含铬原料联合钠化焙烧的方法 |
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CN202210261844.6A CN114703362B (zh) | 2022-03-17 | 2022-03-17 | 一种含钒含铬原料联合钠化焙烧的方法 |
Publications (2)
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CN114703362A CN114703362A (zh) | 2022-07-05 |
CN114703362B true CN114703362B (zh) | 2024-04-05 |
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CN202210261844.6A Active CN114703362B (zh) | 2022-03-17 | 2022-03-17 | 一种含钒含铬原料联合钠化焙烧的方法 |
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Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103614566A (zh) * | 2013-12-13 | 2014-03-05 | 重庆大学 | 一种从转炉钒铬渣中提取钒和铬的方法 |
CN107619941A (zh) * | 2017-10-30 | 2018-01-23 | 攀钢集团攀枝花钢铁研究院有限公司 | 从钒铬渣中分离钒与铬的方法 |
CN108179265A (zh) * | 2018-01-29 | 2018-06-19 | 东北大学 | 一种从含铬钒物料中分离提取钒的方法 |
CN109055724A (zh) * | 2018-10-11 | 2018-12-21 | 攀钢集团钒钛资源股份有限公司 | 从铬钒矿/渣中提取钒和铬的方法 |
CN109182768A (zh) * | 2018-10-25 | 2019-01-11 | 攀钢集团攀枝花钢铁研究院有限公司 | 从钒铬渣中分离钒与铬的方法 |
CN110512097A (zh) * | 2019-09-25 | 2019-11-29 | 河钢股份有限公司承德分公司 | 一种提高钠化焙烧过程钒渣中钒的转化率的方法 |
CN111235409A (zh) * | 2020-03-09 | 2020-06-05 | 广西大学 | 一种从含钒碳酸钠浸出液中萃取钒的方法 |
WO2021155441A1 (en) * | 2020-02-07 | 2021-08-12 | Avanti Materials Ltd | Recovery of vanadium from alkaline slag materials |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US7175818B2 (en) * | 2002-02-07 | 2007-02-13 | Lynntech, Inc. | Extraction of metals with diquaternary ammonium salts |
-
2022
- 2022-03-17 CN CN202210261844.6A patent/CN114703362B/zh active Active
Patent Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103614566A (zh) * | 2013-12-13 | 2014-03-05 | 重庆大学 | 一种从转炉钒铬渣中提取钒和铬的方法 |
CN107619941A (zh) * | 2017-10-30 | 2018-01-23 | 攀钢集团攀枝花钢铁研究院有限公司 | 从钒铬渣中分离钒与铬的方法 |
CN108179265A (zh) * | 2018-01-29 | 2018-06-19 | 东北大学 | 一种从含铬钒物料中分离提取钒的方法 |
CN109055724A (zh) * | 2018-10-11 | 2018-12-21 | 攀钢集团钒钛资源股份有限公司 | 从铬钒矿/渣中提取钒和铬的方法 |
CN109182768A (zh) * | 2018-10-25 | 2019-01-11 | 攀钢集团攀枝花钢铁研究院有限公司 | 从钒铬渣中分离钒与铬的方法 |
CN110512097A (zh) * | 2019-09-25 | 2019-11-29 | 河钢股份有限公司承德分公司 | 一种提高钠化焙烧过程钒渣中钒的转化率的方法 |
WO2021155441A1 (en) * | 2020-02-07 | 2021-08-12 | Avanti Materials Ltd | Recovery of vanadium from alkaline slag materials |
CN111235409A (zh) * | 2020-03-09 | 2020-06-05 | 广西大学 | 一种从含钒碳酸钠浸出液中萃取钒的方法 |
Non-Patent Citations (2)
Title |
---|
有机胺类萃取剂构效关系及其萃钒的研究进展;陈子杨;叶国华;左琪;谢禹;张豪;;钢铁钒钛(第03期);第8-15页 * |
钒铬渣钠化焙烧同步提取钒和铬;付自碧;蒋霖;李明;伍珍秀;;钢铁钒钛(第04期);第1-6页 * |
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