CN114668093A - Efficient extracting device for effective ingredients of codonopsis pilosula and codonopsis pilosula beverage - Google Patents
Efficient extracting device for effective ingredients of codonopsis pilosula and codonopsis pilosula beverage Download PDFInfo
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- CN114668093A CN114668093A CN202210606839.4A CN202210606839A CN114668093A CN 114668093 A CN114668093 A CN 114668093A CN 202210606839 A CN202210606839 A CN 202210606839A CN 114668093 A CN114668093 A CN 114668093A
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- 241000007126 Codonopsis pilosula Species 0.000 title claims abstract description 46
- 235000013361 beverage Nutrition 0.000 title claims abstract description 26
- 239000004615 ingredient Substances 0.000 title abstract description 10
- 238000000605 extraction Methods 0.000 claims abstract description 35
- 238000003756 stirring Methods 0.000 claims abstract description 26
- 238000007789 sealing Methods 0.000 claims abstract description 25
- 241000756943 Codonopsis Species 0.000 claims abstract description 21
- 238000001125 extrusion Methods 0.000 claims abstract description 18
- 230000001954 sterilising effect Effects 0.000 claims abstract description 15
- CHHHXKFHOYLYRE-UHFFFAOYSA-M 2,4-Hexadienoic acid, potassium salt (1:1), (2E,4E)- Chemical compound [K+].CC=CC=CC([O-])=O CHHHXKFHOYLYRE-UHFFFAOYSA-M 0.000 claims abstract description 9
- 239000004302 potassium sorbate Substances 0.000 claims abstract description 9
- 235000010241 potassium sorbate Nutrition 0.000 claims abstract description 9
- 229940069338 potassium sorbate Drugs 0.000 claims abstract description 9
- UNXHWFMMPAWVPI-UHFFFAOYSA-N Erythritol Natural products OCC(O)C(O)CO UNXHWFMMPAWVPI-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000004386 Erythritol Substances 0.000 claims abstract description 7
- 229940009714 erythritol Drugs 0.000 claims abstract description 7
- UNXHWFMMPAWVPI-ZXZARUISSA-N erythritol Chemical compound OC[C@H](O)[C@H](O)CO UNXHWFMMPAWVPI-ZXZARUISSA-N 0.000 claims abstract description 7
- 235000019414 erythritol Nutrition 0.000 claims abstract description 7
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 claims abstract description 6
- FFRBMBIXVSCUFS-UHFFFAOYSA-N 2,4-dinitro-1-naphthol Chemical compound C1=CC=C2C(O)=C([N+]([O-])=O)C=C([N+]([O-])=O)C2=C1 FFRBMBIXVSCUFS-UHFFFAOYSA-N 0.000 claims abstract description 6
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000001630 malic acid Substances 0.000 claims abstract description 6
- 235000011090 malic acid Nutrition 0.000 claims abstract description 6
- 239000007788 liquid Substances 0.000 claims description 17
- 238000004140 cleaning Methods 0.000 claims description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
- 239000004480 active ingredient Substances 0.000 claims description 9
- 238000004806 packaging method and process Methods 0.000 claims description 5
- 238000009835 boiling Methods 0.000 claims description 3
- 238000007599 discharging Methods 0.000 claims description 3
- 238000004659 sterilization and disinfection Methods 0.000 claims description 3
- 238000011049 filling Methods 0.000 claims description 2
- 238000010025 steaming Methods 0.000 claims description 2
- 238000007689 inspection Methods 0.000 claims 1
- 238000002156 mixing Methods 0.000 claims 1
- 239000002244 precipitate Substances 0.000 claims 1
- 206010012601 diabetes mellitus Diseases 0.000 abstract description 2
- 238000001514 detection method Methods 0.000 description 15
- 239000000463 material Substances 0.000 description 10
- 239000000203 mixture Substances 0.000 description 9
- 238000009924 canning Methods 0.000 description 8
- 238000001914 filtration Methods 0.000 description 8
- 238000000034 method Methods 0.000 description 8
- 150000004676 glycans Chemical class 0.000 description 6
- 229920001282 polysaccharide Polymers 0.000 description 6
- 239000005017 polysaccharide Substances 0.000 description 6
- 239000002994 raw material Substances 0.000 description 5
- 238000002791 soaking Methods 0.000 description 5
- 229920002472 Starch Polymers 0.000 description 4
- 230000005540 biological transmission Effects 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 4
- 239000012535 impurity Substances 0.000 description 4
- 230000033001 locomotion Effects 0.000 description 4
- 239000008213 purified water Substances 0.000 description 4
- 239000008107 starch Substances 0.000 description 4
- 235000019698 starch Nutrition 0.000 description 4
- 241000894006 Bacteria Species 0.000 description 3
- 238000010411 cooking Methods 0.000 description 3
- BEFDCLMNVWHSGT-UHFFFAOYSA-N ethenylcyclopentane Chemical compound C=CC1CCCC1 BEFDCLMNVWHSGT-UHFFFAOYSA-N 0.000 description 3
- 238000005086 pumping Methods 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 239000004334 sorbic acid Substances 0.000 description 3
- 235000010199 sorbic acid Nutrition 0.000 description 3
- 229940075582 sorbic acid Drugs 0.000 description 3
- 206010028980 Neoplasm Diseases 0.000 description 2
- 238000005265 energy consumption Methods 0.000 description 2
- 230000036039 immunity Effects 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
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- 238000002360 preparation method Methods 0.000 description 2
- 230000001105 regulatory effect Effects 0.000 description 2
- 102000006587 Glutathione peroxidase Human genes 0.000 description 1
- 108700016172 Glutathione peroxidases Proteins 0.000 description 1
- 206010020772 Hypertension Diseases 0.000 description 1
- WSMYVTOQOOLQHP-UHFFFAOYSA-N Malondialdehyde Chemical compound O=CCC=O WSMYVTOQOOLQHP-UHFFFAOYSA-N 0.000 description 1
- 229930182558 Sterol Natural products 0.000 description 1
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 1
- 229930006000 Sucrose Natural products 0.000 description 1
- 102000019197 Superoxide Dismutase Human genes 0.000 description 1
- 108010012715 Superoxide dismutase Proteins 0.000 description 1
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- 210000004369 blood Anatomy 0.000 description 1
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- 210000004556 brain Anatomy 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 229940118019 malondialdehyde Drugs 0.000 description 1
- 238000010172 mouse model Methods 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 210000002966 serum Anatomy 0.000 description 1
- 150000003432 sterols Chemical class 0.000 description 1
- 235000003702 sterols Nutrition 0.000 description 1
- 239000005720 sucrose Substances 0.000 description 1
- 230000001360 synchronised effect Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
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- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/38—Other non-alcoholic beverages
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
- A23L2/60—Sweeteners
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/125—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives containing carbohydrate syrups; containing sugars; containing sugar alcohols; containing starch hydrolysates
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B30—PRESSES
- B30B—PRESSES IN GENERAL
- B30B9/00—Presses specially adapted for particular purposes
- B30B9/02—Presses specially adapted for particular purposes for squeezing-out liquid from liquid-containing material, e.g. juice from fruits, oil from oil-containing material
- B30B9/04—Presses specially adapted for particular purposes for squeezing-out liquid from liquid-containing material, e.g. juice from fruits, oil from oil-containing material using press rams
- B30B9/06—Presses specially adapted for particular purposes for squeezing-out liquid from liquid-containing material, e.g. juice from fruits, oil from oil-containing material using press rams co-operating with permeable casings or strainers
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Abstract
The invention discloses a high-efficiency extraction device for effective ingredients of codonopsis pilosula and a codonopsis pilosula beverage, wherein the extraction device comprises a bottom plate, an electric boiler is fixed on the bottom plate, a power supply is fixed on the electric boiler, a sealing plate is arranged at the upper end of the electric boiler, a discharge pipe is fixed on one side of the lower end of the electric boiler, a fixed barrel is fixed on the lower surface of the sealing plate, a rotating plate is rotatably arranged on the fixed barrel, filter screens are fixed on the fixed barrel and the rotating plate, a collection box is fixed on the upper surface of the bottom plate, and an extrusion mechanism is arranged on the upper surface of the sealing plate. Adding erythritol, VC, malic acid and potassium sorbate into the radix Codonopsis extractive solution obtained by the extraction device, circularly stirring, and sterilizing to obtain radix Codonopsis beverage. The advantages are that: the one-time extraction is carried out in a sealed environment by one-time feeding, time and labor are saved, and the efficient extraction of the effective components in the codonopsis pilosula is realized. The radix codonopsitis beverage has uniform and transparent properties and golden yellow color, maintains the specific natural properties of the product, is suitable for people with diabetes and the like to drink, and is safe and reliable.
Description
Technical Field
The invention relates to the extraction of effective ingredients of codonopsis pilosula, in particular to a device and a process for efficiently extracting the effective ingredients of codonopsis pilosula and a preparation method of a beverage thereof.
Background
Radix codonopsitis (Codonopsis pilosula Nannf) is a traditional Chinese medicinal material in China, can be used as both medicine and food, and has activities of resisting oxidation, tonifying qi and blood, resisting tumor, regulating immunity and the like. Research shows that the active ingredients of the codonopsis pilosula comprise active molecules such as polysaccharide, sterol and the like. The Codonopsis pilosula polysaccharide has activities of resisting oxidation, resisting tumor, regulating immunity, etc., such as obvious reduction of malondialdehyde and brown content in brain in blood serum of aging model mice treated by the Codonopsis pilosula polysaccharide, and obvious increase of activities of superoxide dismutase and glutathione peroxidase. However, health beverages containing codonopsis pilosula active ingredients are currently on the market, such as: patent numbers: ZL201210035217.7, name: the codonopsis pilosula health-care beverage and the preparation method thereof have long extraction process flow, fussy feeding and time and labor waste. In addition, effective components in the codonopsis pilosula can be quickly extracted by boiling, the codonopsis pilosula is directly put into a pot in the existing method, a large amount of time is consumed by the method, and the components cannot be completely and efficiently extracted.
Disclosure of Invention
Aiming at the problems in the prior art, the invention provides a device for efficiently extracting active ingredients of codonopsis pilosula and a codonopsis pilosula beverage.
The technical scheme adopted by the invention is as follows: a high-efficiency extraction process of effective components of radix codonopsis, specifically comprises the following steps:
s1, raw material pretreatment: soaking dried radix Codonopsis in water for 2-3 hr, cleaning, and cutting into 1-2cm segments;
s2, dynamic extraction: adopt high-efficient extraction element to draw, once only be 1 according to the solid-to-liquid ratio in this jar: 420 and 500, adding the radix codonopsis and purified water into the segments, heating to 115 and 120 ℃, and circularly extracting for 3-4 hours by steaming and boiling, so that the effective components of the medicinal materials are fully and effectively extracted;
s3, filtering and removing impurities: and filtering the obtained extracting solution through a filter, and removing starch, particles and material residues in the extracting solution to obtain the codonopsis pilosula extracting solution.
The method for preparing the codonopsis pilosula beverage by adopting the extraction process specifically comprises the following steps:
s4, circulating stirring: pumping the radix codonopsitis extracting solution into a stirring tank, adding erythritol, VC, malic acid and potassium sorbate, installing circulating pipelines at the upper part and the lower part of the stirring tank, enabling liquid at the lower part of the stirring tank to enter from the upper part of the stirring tank, circularly stirring the liquid from bottom to top at the temperature of 110-;
s5, canning and sterilizing: filling the mixture obtained in the step S4, sterilizing the mixture in a sterilization kettle at the temperature of 120-140 ℃ for 0.3-0.4h after canning, and then inspecting and packaging the mixture to obtain the finished product of the codonopsis pilosula health care beverage.
The invention provides a device for efficiently extracting active ingredients of codonopsis pilosula, which adopts the following technical scheme: high-efficient extraction element of codonopsis pilosula active ingredient, comprising a base plate, fixed surface is equipped with electric boiler on the bottom plate, the last fixed power ware that is equipped with of electric boiler, the electric boiler upper end is equipped with the closing plate, the fixed discharging pipe that is equipped with in electric boiler lower extreme one side, closing plate lower fixed surface is equipped with fixed bucket, it is equipped with the rotor plate to rotate on the fixed bucket, all fixed being equipped with the filter screen on fixed bucket and the rotor plate, fixed surface is equipped with the collection box on the bottom plate, the closing plate upper surface is equipped with extrusion mechanism.
Preferably, the extrusion mechanism includes the connecting rod, the connecting rod runs through the closing plate, the fixed extrusion piece that is equipped with of connecting rod lower extreme, the extrusion piece is circular, the fixed mount that is equipped with in connecting rod upper end, the fixed limiting plate that is equipped with in mount both ends, the fixed two pairs of circular poles that are equipped with of closing plate upper surface, the circular pole runs through the limiting plate, the fixed spring that is equipped with of limiting plate lower surface, the spring lower extreme is connected with closing plate upper surface fixed.
Preferably, the upper surface of the sealing plate is fixedly provided with a supporting block, one side of the upper end of the supporting block is fixedly provided with a first motor, the other side of the upper end of the supporting block is fixedly provided with a rotating shaft, one end of the rotating shaft is fixedly connected with the output end of the first motor, the other end of the rotating shaft is fixedly provided with an elliptical block, and the outer wall of the elliptical block is attached to the fixing frame.
Preferably, a cleaning ring is fixedly arranged in the rotating plate, a central shaft is rotatably arranged on the fixing barrel and fixedly connected with one side of the rotating plate, a third motor is fixedly arranged on the sealing plate, the output end of the third motor is fixedly connected with the central shaft, and a feeding pipe is fixedly arranged on one side of the fixing barrel.
Preferably, the upper surface of the bottom plate is rotatably provided with a fixed column, one side of the upper end of the fixed column is provided with a lifting groove, a threaded rod is arranged in the lifting groove in a rotating mode, a fixed rod is arranged in the lifting groove in a sliding mode, one end of the fixed rod is connected with the threaded rod in a threaded mode, the other end of the fixed rod is fixedly connected with the sealing plate, a second motor is fixedly arranged at the upper end of the fixed column, and the output end of the second motor is fixedly connected with the threaded rod.
Preferably, the extrusion block is positioned in the fixed barrel, and the connecting rod is positioned in the center of the sealing plate.
Preferably, the upper end of the feeding pipe penetrates through the sealing plate.
Compared with the prior art, the invention has the beneficial effects that:
1. the invention carries out leaching before pretreatment and cleaning, not only ensures thorough and clean cleaning, but also directly adds an efficient extraction device for cooking and extraction during subsequent extraction without soaking, thereby saving energy consumption.
2. The invention adopts one-time feeding in a sealed environment for one-time extraction, and compared with the prior art, the invention saves the complex process of multiple feeding, saves time and labor, saves labor cost and energy consumption; the dynamic extraction process is carried out at about 120 ℃, and the preliminary sterilization effect is achieved.
3. The invention adopts dry radix codonopsitis as raw material, the active ingredient content of the radix codonopsitis is high, and the high-efficiency extraction of the effective ingredient in the radix codonopsitis is realized through the high-efficiency extraction device.
4. The product of the invention contains erythritol instead of sucrose, has uniform quality and good taste, is suitable for people with diabetes, hypertension, children and the like, and is safe and reliable.
5. The health-care beverage only containing the radix codonopsitis nutrient components prepared by the extraction method has uniform and transparent shape and golden yellow color, keeps the specific natural property of the product, is not added with any pigment, has good taste and is safe to drink.
6. According to the invention, the rotating shaft and the elliptical block are driven to rotate by the first motor, the fixed frame and the connecting rod are driven to move by the rotation of the elliptical block, the movement is limited by the circular rod, and the lower-end extrusion block is driven by the connecting rod to extrude the codonopsis pilosula, so that effective ingredients can be extracted more quickly.
Drawings
FIG. 1 is a schematic structural view of the present invention,
figure 2 is a schematic view of the structure of the extrusion mechanism of the present invention,
FIG. 3 is a schematic view of a rotating plate according to the present invention.
In the figure: 1. a base plate; 11. an electric boiler; 12. a power supply; 13. a sealing plate; 14. a discharge pipe; 15. fixing the barrel; 16. a rotating plate; 17. a filter screen; 18. a collection box; 2. an extrusion mechanism; 21. a connecting rod; 22. extruding the block; 23. a fixed mount; 24. a limiting plate; 25. a circular rod; 26. a spring; 3. a support block; 31. a first motor; 32. a rotating shaft; 33. an elliptical block; 4. cleaning a ring; 41. a third motor; 42. a feed pipe; 43. a central shaft; 5. fixing a column; 51. a lifting groove; 52. a threaded rod; 53. fixing the rod; 54. a second motor.
Detailed Description
The present invention is further illustrated by, but is not limited to, the following examples.
Example 1
A high-efficiency extraction process of effective components of radix codonopsis, specifically comprises the following steps:
s1, raw material pretreatment: soaking dried radix Codonopsis in water for 2 hr, cleaning, and cutting into 2cm segments;
s2, dynamic extraction: adopt high-efficient extraction element to draw, once only according to solid-to-liquid ratio 1 in toward this jar: 450, adding segmented codonopsis pilosula and purified water, heating to 120 ℃, and circularly extracting for 4 hours by cooking, so that the effective ingredients of the medicinal materials are fully and effectively extracted;
s3, filtering and removing impurities: filtering the obtained extractive solution with a filter, and removing starch, particulate matter and residue to obtain radix Codonopsis extractive solution with golden color.
The method for preparing the codonopsis pilosula beverage by adopting the extraction process specifically comprises the following steps:
s4, circulating stirring: 31000mL of the codonopsis pilosula extracting solution is pumped into a stirring tank, 1.73kg of erythritol, 0.0003kg of VC, 0.035kg of malic acid and 0.01kg of potassium sorbate are added, circulating pipelines are installed at the upper part and the lower part of the stirring tank, so that liquid at the lower part of the stirring tank enters from the upper part of the stirring tank, the liquid is prevented from crystallizing from bottom to top, and the stirring is circularly carried out at 110 ℃ for 2 hours to obtain a mixture;
s5, canning and sterilizing: canning the mixture, sterilizing at 120 deg.C for 0.3 hr in a sterilizing kettle, inspecting, and packaging to obtain radix Codonopsis health beverage.
The beverage is golden yellow and is transparent liquid with uniform properties, no precipitant floccule appears after being placed for 24 hours according to the detection of GB/T31326, the soluble solid (20 ℃ refractometry) is not less than 0.5 percent according to the detection of GB/T12143, and the crude polysaccharide is not less than 0.4g/100g according to the detection of SN/T4260-; according to GB5009.28-2016 detection, potassium sorbate (calculated by sorbic acid) is less than or equal to 0.5 g/kg; according to GB 5009.12 detection, lead (calculated as Pb) is less than or equal to 0.3 mg/L. The total number of detected colonies in GB 4789.2 is 450 CFU/g, coliform bacteria in GB 4789.3 is less than 10 CFU/g, and mould in GB 4789.15 is less than 10 CFU/g.
Example 2
A high-efficiency extraction process of effective components of radix codonopsis, specifically comprises the following steps:
s1, raw material pretreatment: soaking dried radix Codonopsis in water for 3 hr, cleaning, and cutting into 1cm segments;
s2, dynamic extraction: adopt high-efficient extraction element to draw, once only according to solid-to-liquid ratio 1 in toward this jar: 500, adding segmented codonopsis pilosula and purified water, heating to 115 ℃, and circularly extracting for 3 hours by stewing, so that the effective ingredients of the medicinal materials are fully and effectively extracted;
s3, filtering and removing impurities: filtering the obtained extractive solution with a filter, and removing starch, particulate matter and residue to obtain radix Codonopsis extractive solution with golden color.
The method for preparing the codonopsis pilosula beverage by adopting the extraction process specifically comprises the following steps:
s4, circulating stirring: pumping 62000mL of radix codonopsis extract into a stirring tank, adding 3.6kg of erythritol, 0.0006kg of VC0.0006kg of malic acid and 0.025kg of potassium sorbate, installing circulating pipelines at the upper part and the lower part of the stirring tank, so that liquid at the lower part of the stirring tank enters from the upper part of the stirring tank, and circularly stirring the liquid from bottom to top at 135 ℃ for 3.5 hours to obtain a mixture;
s5, canning and sterilizing: canning the mixture, sterilizing at 125 deg.C for 0.4 hr in a sterilizing kettle, inspecting, and packaging to obtain radix Codonopsis health beverage.
The beverage is golden yellow and is transparent liquid with uniform properties, no precipitant floccule appears after being placed for 24 hours according to the detection of GB/T31326, the soluble solid (20 ℃ refractometry) is not less than 0.5 percent according to the detection of GB/T12143, and the crude polysaccharide is not less than 0.4g/100g according to the detection of SN/T4260-; according to GB5009.28-2016 detection, potassium sorbate (calculated by sorbic acid) is less than or equal to 0.5 g/kg; according to GB 5009.12 detection, lead (calculated as Pb) is less than or equal to 0.3 mg/L. The total number of detected colonies in GB 4789.2 is 450 CFU/g, coliform bacteria in GB 4789.3 is less than 10 CFU/g, and mould in GB 4789.15 is less than 10 CFU/g.
Example 3
A high-efficiency extraction process of effective components of radix codonopsis, specifically comprises the following steps:
s1, raw material pretreatment: soaking dried radix Codonopsis in water for 2.5 hr, cleaning, and cutting into 1.5cm segments;
s2, dynamic extraction: adopt high-efficient extraction element to draw, once only according to solid-to-liquid ratio 1 in toward this jar: 420, adding segmented codonopsis pilosula and purified water, heating to 120 ℃, and circularly extracting for 3 hours by cooking, so that the effective ingredients of the medicinal materials are fully and effectively extracted;
s3, filtering and removing impurities: and filtering the obtained extracting solution through a filter to remove starch, particles and material residues in the extracting solution to obtain the codonopsis pilosula extracting solution which is light yellow in color.
The extraction process is applied to the extraction of the effective components of the codonopsis pilosula.
The method for preparing the codonopsis pilosula beverage by adopting the extraction process specifically comprises the following steps:
s4, circulating stirring: pumping 93000mL of radix Codonopsis extract into a stirring tank, adding 4.8kg of erythritol, 0.0009kg of VC, 0.095kg of malic acid and 0.026kg of potassium sorbate, installing circulating pipelines at the upper and lower parts of the stirring tank, allowing liquid at the lower part of the stirring tank to enter from the upper part of the stirring tank, and circularly stirring the liquid at 135 ℃ from bottom to top for 3.5h to obtain a mixture;
s5, canning and sterilizing: canning the mixture, sterilizing at 140 deg.C for 0.3h in a sterilizing kettle, inspecting, and packaging to obtain radix Codonopsis health beverage.
The beverage is golden yellow and is transparent liquid with uniform properties, no precipitant floccule appears after being placed for 24 hours according to the detection of GB/T31326, the soluble solid (20 ℃ refractometry) is not less than 0.5 percent according to the detection of GB/T12143, and the crude polysaccharide is not less than 0.4g/100g according to the detection of SN/T4260-; according to GB5009.28-2016 detection, potassium sorbate (calculated by sorbic acid) is less than or equal to 0.5 g/kg; according to GB 5009.12 detection, lead (calculated as Pb) is less than or equal to 0.3 mg/L. The total number of detected colonies in GB 4789.2 is 450 CFU/g, coliform bacteria in GB 4789.3 is less than 10 CFU/g, and mould in GB 4789.15 is less than 10 CFU/g.
Example 4
As shown in fig. 1-3, the device for efficiently extracting active ingredients from codonopsis pilosula provided by the present invention comprises a bottom plate 1, an electric boiler 11 is fixedly disposed on the upper surface of the bottom plate 1, a power supply 12 is fixedly disposed on the electric boiler 11, a sealing plate 13 is disposed at the upper end of the electric boiler 11, a discharge pipe 14 is fixedly disposed at one side of the lower end of the electric boiler 11, a fixed barrel 15 is fixedly disposed at the lower surface of the sealing plate 13, a rotating plate 16 is rotatably disposed on the fixed barrel 15, filter screens 17 are fixedly disposed on the fixed barrel 15 and the rotating plate 16, a cleaning ring 4 is fixedly disposed in the rotating plate 16, a central shaft 43 is rotatably disposed on the fixed barrel 15, the central shaft 43 is fixedly connected to one side of the rotating plate 16, a third motor 41 is fixedly disposed on the sealing plate 13, an output end of the third motor 41 is fixedly connected to the central shaft 43, a feeding pipe 42 is fixedly disposed at one side of the fixed barrel 15, and an upper end of the feeding pipe 42 penetrates through the sealing plate 13, the upper surface of the bottom plate 1 is fixedly provided with a collection box 18, the upper surface of the sealing plate 13 is provided with an extrusion mechanism 2, a proper amount of water is added into the electric boiler 11, materials are fed into a fixed barrel 15 through a feeding pipe 42, a power supply 12 is connected with an external power supply to heat the electric boiler 11, the codonopsis pilosula in the fixed barrel 15 is extruded through the extrusion mechanism 2, the codonopsis pilosula is separated through a filter screen 17 to extract effective components more quickly, finally the effective components are discharged through a discharge pipe 14, the sealing plate 13 is lifted to drive the fixed barrel 15 to leave the electric boiler 11, a transmission motor drives the fixed column 5 to rotate, the fixed barrel 15 is moved to the upper part of the collection box 18, a central shaft 43 is driven to rotate through rotation of a third motor 41 to rotate the rotating plate 16, the rotating plate 16 drives the cleaning ring 4 to synchronously move, the materials in the fixed barrel 15 are taken out and fall into the collection box 18, the transmission motor is positioned inside the bottom plate 1, and the output end of the transmission motor is connected with the fixing column 5.
The extruding mechanism 2 comprises a connecting rod 21, the connecting rod 21 penetrates through a sealing plate 13, an extruding block 22 is fixedly arranged at the lower end of the connecting rod 21, the extruding block 22 is circular, a fixing frame 23 is fixedly arranged at the upper end of the connecting rod 21, limiting plates 24 are fixedly arranged at two ends of the fixing frame 23, two pairs of circular rods 25 are fixedly arranged on the upper surface of the sealing plate 13, the circular rods 25 penetrate through the limiting plates 24, springs 26 are fixedly arranged on the lower surfaces of the limiting plates 24, the lower end of each spring 26 is fixedly connected with the upper surface of the sealing plate 13, the extruding block 22 is positioned in a fixed barrel 15, the connecting rod 21 is positioned at the central position of the sealing plate 13, a supporting block 3 is fixedly arranged on the upper surface of the sealing plate 13, a first motor 31 is fixedly arranged on one side of the upper end of the supporting block 3, a rotating shaft 32 is fixedly arranged on the other side of the upper end of the supporting block 3, one end of the rotating shaft 32 is fixedly connected with the output end of the first motor 31, an elliptical block 33 is fixedly arranged on the other end of the rotating shaft 32, the outer wall of the elliptical block 33 is attached to the fixing frame 23, the first motor 31 drives the rotating shaft 32 and the elliptical block 33 to rotate, the elliptical block 33 rotates to drive the fixing frame 23 and the connecting rod 21 to move, the movement is limited through the circular rod 25, and the connecting rod 21 drives the lower end extrusion block 22 to extrude the codonopsis pilosula.
The working principle is as follows: firstly, adding a proper amount of water into an electric boiler 11, connecting a power supply 12 with an external power supply to heat the electric boiler 11, then driving a rotating shaft 32 and an elliptical block 33 to rotate through a first motor 31, driving a fixing frame 23 and a connecting rod 21 to move through the rotation of the elliptical block 33, limiting the movement through a circular rod 25, driving a lower-end extrusion block 22 to extrude and filter codonopsis pilosula to extract effective components more quickly through the connecting rod 21, driving a threaded rod 52 to rotate through a second motor 54, driving a fixing rod 53 to move along a lifting groove 51 through the threaded rod 52, driving a sealing plate 13 to move upwards through the fixing rod 53, driving a fixing barrel 15 to move upwards along with the sealing plate 13, enabling the fixing barrel 15 to be positioned outside the electric boiler 11, driving a fixing column 5 to rotate through a transmission motor, enabling the fixing barrel 15 to move above a collecting box 18, and driving a central shaft 43 to rotate through the rotation of a third motor 41, the rotating plate 16 is rotated, and the rotating plate 16 drives the cleaning ring 4 to move synchronously, so that the material in the fixed barrel 15 is taken out and falls into the collecting box 18.
Claims (6)
1. The utility model provides a high-efficient extraction element of codonopsis pilosula active ingredient, includes bottom plate (1), its characterized in that: bottom plate (1) upper surface is fixed and is equipped with electric boiler (11), the fixed power ware (12) that is equipped with on electric boiler (11), electric boiler (11) upper end is equipped with closing plate (13), electric boiler (11) lower extreme one side is fixed and is equipped with discharging pipe (14), closing plate (13) lower fixed surface is equipped with fixed bucket (15), it is equipped with rotor plate (16) to rotate on fixed bucket (15), all fixed being equipped with filter screen (17) on fixed bucket (15) and rotor plate (16), bottom plate (1) upper surface is fixed and is equipped with collection box (18), closing plate (13) upper surface is equipped with extrusion mechanism (2), to adding suitable water in electric boiler (11), is 1 according to solid-to-liquid ratio: 420 and 500. the codonopsis pilosula which is soaked for 2 to 3 hours, cleaned and cut into sections of 1 to 2cm is sent into a fixed barrel (15) through a feeding pipe (42), a power supply is connected with an external power supply, the electric boiler (11) is heated, the temperature is increased by 115 and 120 ℃, steaming and boiling are circulated and extracted for 3 to 4 hours, the codonopsis pilosula in the fixed barrel (15) is extruded through an extrusion mechanism (2), the codonopsis pilosula is isolated through a filter screen (17), effective components are extracted rapidly, and finally the effective components are discharged through a discharging pipe (14).
2. The device for extracting the effective components of the codonopsis pilosula according to claim 1, is characterized in that: extrusion mechanism (2) include connecting rod (21), connecting rod (21) run through closing plate (13), fixed extrusion piece (22) that is equipped with of connecting rod (21) lower extreme, extrusion piece (22) are circularly, fixed mount (23) that is equipped with in connecting rod (21) upper end, fixed limiting plate (24) that is equipped with in mount (23) both ends, fixed surface is equipped with two pairs of round bars (25) on closing plate (13), limiting plate (24) are run through in round bar (25), fixed surface is equipped with spring (26) under limiting plate (24), fixed surface is connected on spring (26) lower extreme and closing plate (13).
3. The device for efficiently extracting the active ingredients of the codonopsis pilosula according to claim 1 or 2, which is characterized in that: the sealing plate is characterized in that a supporting block (3) is fixedly arranged on the upper surface of the sealing plate (13), a first motor (31) is fixedly arranged on one side of the upper end of the supporting block (3), a rotating shaft (32) is fixedly arranged on the other side of the upper end of the supporting block (3), one end of the rotating shaft (32) is fixedly connected with the output end of the first motor (31), an elliptical block (33) is fixedly arranged on the other end of the rotating shaft (32), and the outer wall of the elliptical block (33) is attached to the fixing frame (23).
4. The device for extracting the effective components of the codonopsis pilosula according to claim 3, wherein: the cleaning device is characterized in that a cleaning ring (4) is fixedly arranged in the rotating plate (16), a central shaft (43) is rotatably arranged on the fixed barrel (15), the central shaft (43) is fixedly connected with one side of the rotating plate (16), a third motor (41) is fixedly arranged on the sealing plate (13), the output end of the third motor (41) is fixedly connected with the central shaft (43), and a feeding pipe (42) is fixedly arranged on one side of the fixed barrel (15).
5. A radix codonopsitis beverage prepared from radix codonopsitis effective components prepared by the device according to claim 4 is prepared by mixing and stirring the radix codonopsitis effective component extracting solution with erythritol, VC, malic acid and potassium sorbate, and then sequentially carrying out filling, sterilization, inspection and packaging to obtain the radix codonopsitis beverage, and is characterized in that: the total number of colonies of the radix Codonopsis beverage is 450 CFU/g, the coliform is less than 10 CFU/g, and the mould is less than 10 CFU/g.
6. The Codonopsis beverage of claim 5, wherein: the radix Codonopsis beverage is golden yellow, is uniform transparent liquid, and has no floccule precipitate after standing for 24 hr.
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CN215542750U (en) * | 2021-07-05 | 2022-01-18 | 福州九阳化工有限公司 | Centrifugal filtering device for preparing silicon oxide |
CN216088647U (en) * | 2021-08-12 | 2022-03-22 | 龙陵县鹏翔茶叶加工厂 | Fixation device suitable for tea processing |
CN216296902U (en) * | 2021-08-31 | 2022-04-15 | 江苏晶河电子科技有限公司 | Adhesive dispensing device with excellent thixotropy and adhesion |
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JP3005899B1 (en) * | 1998-10-14 | 2000-02-07 | 清水市農業協同組合 | Beverage production equipment |
CN101167587A (en) * | 2006-10-26 | 2008-04-30 | 好事植物饮品(北京)有限公司 | Health beverage and its preparation method |
CN102626247A (en) * | 2012-04-09 | 2012-08-08 | 云南知味园食品有限公司 | Making method of blood replenishing and qi regulating health care nutrient drinks |
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CN215542750U (en) * | 2021-07-05 | 2022-01-18 | 福州九阳化工有限公司 | Centrifugal filtering device for preparing silicon oxide |
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CN216296902U (en) * | 2021-08-31 | 2022-04-15 | 江苏晶河电子科技有限公司 | Adhesive dispensing device with excellent thixotropy and adhesion |
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