CN114642621B

CN114642621B - Abelmoschus manihot flower mask, preparation method and application thereof

Info

Publication number: CN114642621B
Application number: CN202210489126.4A
Authority: CN
Inventors: 唐川
Original assignee: Guangzhou Heyan Hemei Biological Engineering Co ltd
Current assignee: Guangzhou Heyan Hemei Biological Engineering Co ltd
Priority date: 2022-05-06
Filing date: 2022-05-06
Publication date: 2024-06-07
Anticipated expiration: 2042-05-06
Also published as: CN114642621A

Abstract

The application discloses a flower facial mask of abelmoschus manihot in the technical field of cosmetics, which comprises 0.8-1.3% of plant extracts by mass percent, wherein the plant extracts are extracted and separated by a supercritical CO ₂ fluid technology, and the plant extracts comprise 0.1-0.2% of cactus stem extract, 0.6-0.9% of flower extract of abelmoschus manihot and 0.1-0.2% of radix puerariae extract. The application has the functions of moisturizing, removing spots, repairing and fading scars, diminishing inflammation and inhibiting bacteria, and can effectively permeate deep skin, balance grease secretion, shrink pores, improve skin quality and make skin smooth and fine through the synergistic effect of the three plant extracts.

Description

Abelmoschus manihot flower mask, preparation method and application thereof

Technical Field

The invention relates to the technical field of cosmetics, in particular to a flower face mask of abelmoschus manihot, a preparation method and application thereof.

Background

With the improvement of the living standard of people, consumers, especially female consumers, have higher requirements on skin care, and the consumers are fashionable in returning to nature and green; in addition, the cosmetic added with the plant components has small molecular weight, so that the cosmetic can quickly permeate into the skin and play the role of repairing the skin. Therefore, the "green cosmeceuticals" with plant extract active ingredients have met with unprecedented development opportunities.

Abelmoschus manihot is a dry corolla of Abelmoschus manihot of Abelmoschus of Malvaceae, and is used for treating carbuncle, swelling, and scald due to fire and water. The main chemical components of the flower of sunset abelmoschus are flavonoid compounds such as hyperin, quercetin-3-O-beta-D-glucoside, isoquercitrin and the like, and modern pharmacological researches prove that the compound has various pharmacological activities such as improving renal function, resisting inflammation, relieving fever and pain, protecting heart and cerebral ischemia injury and the like, and has wide development prospect and research significance.

Disclosure of Invention

Aiming at the defects of the prior art, the invention designs a mask of the flos Abelmoschi Manihot extract.

The invention aims to provide an abelmoschus manihot flower mask which comprises 0.8-1.3% of plant extracts by mass percent, wherein the plant extracts are extracted and separated by a supercritical CO ₂ fluid technology, and the plant extracts comprise 0.1-0.2% of cactus stem extract, 0.6-0.9% of abelmoschus manihot flower extract and 0.1-0.2% of radix puerariae extract.

Further, the plant extract comprises 0.15% of cactus stem extract, 0.753% of flos Abelmoschi Manihot extract, and 0.15% of radix Puerariae extract.

Further, when preparing the flos Abelmoschi Manihot extract, cleaning flos Abelmoschi Manihot, pulverizing, extracting with supercritical CO ₂ under 60% ethanol, concentrating, decolorizing, spray drying, and sieving with 100 mesh sieve.

Further, when preparing the cactus stem extract, the cactus is cleaned, selected, dried and crushed, extracted by supercritical CO ₂ in the presence of water, concentrated, decolorized, spray-dried and screened by a 100-mesh sieve.

Further, when the kudzuvine root extract is prepared, kudzuvine root is cleaned, selected, dried and crushed, the kudzuvine root is decocted and extracted for 2 times, the decoction time is 3 hours and 1 hour respectively, the two filtrates are combined, the filtrate is kept stand for 2 hours and filtered, concentrated, extracted by supercritical CO ₂, concentrated, decolorized, spray-dried and screened by a 100-mesh sieve.

Further, the raw materials also comprise a water phase and an oil phase, wherein the water phase list comprises the following components in percentage by mass:

the oil phase list comprises the following components in percentage by mass:

further, the daily essence comprises 0.03% by mass.

The invention also provides a preparation method of the abelmoschus manihot facial mask, which is characterized in that: during the specific preparation, all water phase raw materials are added into a water phase pot according to a proportion, the temperature is controlled at 75-80 ℃, and the water phase material A is obtained after stirring for 20 min;

all oil phase raw materials are added into an oil phase pot in proportion, the temperature is controlled at 75-80 ℃, and after stirring is carried out for 30min, an oil phase material B is obtained;

Vacuumizing the emulsifying pot, preheating to 60-70 ℃, firstly sucking the water phase material A into the emulsifying pot, stirring, sucking the oil phase material B, continuing stirring for 10min after sucking, and then feeding into a homogenizing tank;

Adding flos Abelmoschi Manihot extract, radix Puerariae extract, and radix et caulis Opuntiae Dillenii stem extract into emulsifying pot at a certain proportion, stirring for 15min; when the temperature of the materials is cooled to 45-50 ℃, adding daily essence according to a proportion, and uniformly stirring to obtain the flos Abelmoschi Manihot essence;

and bagging the mask paper and the flos Abelmoschi Manihot essence to obtain the flos Abelmoschi Manihot mask.

Further, in the preparation, the stirring speed is 800-2000 rmp.

The invention further aims to provide application of the abelmoschus manihot essence in preparing skin care products

The working principle and the beneficial effects of the invention are as follows:

1. The plant extract of the invention abandons the traditional extraction processing technology, adopts the current very advanced supercritical CO ₂ fluid technology for extraction and separation, and the processed product has high purity and no residue.

2. The compound facial mask essence emulsion prepared from the flower extract of abelmoschus manihot, the root extract of kudzu vine and the stem extract of cactus and other components has the effects of moisturizing, removing freckles, repairing and fading scars, diminishing inflammation and inhibiting bacteria, and meanwhile, through the synergistic effect of the three plant extracts, the deep skin can be effectively permeated, the secretion of grease is balanced, pores are contracted, the skin quality is improved, and the skin is smooth and fine.

Drawings

FIG. 1 is a process flow diagram of the flower face mask of Abelmoschus manihot of the present invention;

FIG. 2 is a process flow diagram of the flos Abelmoschi Manihot extract of FIG. 1;

FIG. 3 is a process flow diagram of the cactus stem extract of FIG. 1;

FIG. 4 is a process flow diagram of the radix Puerariae extract of FIG. 1.

Detailed Description

The following is a further detailed description of the embodiments:

The preparation method of the flower face mask of the abelmoschus manihot comprises the following specific steps of:

S1, preparation of an extract: when the flos Abelmoschi Manihot extract is prepared as shown in figure 2, cleaning flos Abelmoschi Manihot, pulverizing, extracting with supercritical CO ₂ under 60% ethanol, concentrating, collecting paste, decolorizing with decolorizing agent, spray drying, pulverizing, sieving with 100 mesh sieve, and packaging, wherein the steps from paste collection to packaging are performed in 10 ten thousand clean areas;

when the cactus stem extract is prepared as shown in fig. 3, the cactus is cleaned, dried and crushed, extracted by a supercritical CO ₂ technology in the presence of water, concentrated, paste is collected, decolorized by a decolorizing agent, finally spray-dried, crushed and sieved by a 100-mesh sieve, and a finished product is packaged for later use, wherein the steps from paste collection to finished product packaging are carried out in a 10-ten thousand clean area;

As shown in fig. 4, in preparing the radix puerariae extract, radix puerariae is cleaned, dried and crushed, decocted for 2 times, and each time is 10 times of water, the decoction time is 3 hours and 1 hour respectively, the two filtrates are combined, and the mixture is kept stand for 2 hours for filtering, concentrated, the clear paste is extracted by using supercritical CO ₂, then concentrated, the paste is collected, decolorized by using a decolorizing agent, finally spray-dried, crushed and filtered through a 100-mesh sieve, and the finished product is packaged for later use, wherein the steps from the paste collection to the finished product packaging are carried out in a 10-ten thousand clean area in the stages of paste collection and finished product packaging.

The addition ratio of the extracts is as follows: 0.15% of cactus stem extract, 0.753% of abelmoschus manihot flower extract and 0.15% of radix puerariae extract.

S2, preparing and adding the water phase raw materials: all the water phase raw materials are added into a water phase pot in proportion, the temperature is controlled at 75-80 ℃, the stirring speed is 800rmp, and the stirring time is 20min, so as to obtain a water phase raw material A;

Wherein the water phase raw material list comprises the following components in percentage by mass:

s3, preparing and adding the oil phase raw materials in proportion: all oil phase raw materials of the formula are added into an oil phase pot according to a proportion, the temperature is controlled at 75-80 ℃, the stirring speed is 2000rmp, and the stirring time is 30min, so as to obtain a water phase raw material B;

the oil phase raw material list comprises the following components in percentage by mass:

S4, emulsifying, homogenizing and adding daily essence: vacuumizing the emulsifying pot, preheating to 60-70 ℃, firstly sucking the water phase material A into the emulsifying pot, sucking the oil phase material B at the stirring speed of 2000rmp, and stirring for 10min after sucking; adding proportionally prepared additive C (flos Abelmoschi Manihot extract, radix Puerariae extract, and radix et caulis Opuntiae Dillenii stem extract) into homogenizing tank, stirring at 2000rmp for 15min; when the temperature of the materials is cooled to 45-50 ℃, adding 0.03 mass percent of daily essence, stirring for 10min at the stirring speed of 2000rmp to obtain flos Abelmoschi Manihot essence, and discharging and checking for later use;

s5, bagging and filling: packaging the tencel facial mask paper into a bag, filling the flos Abelmoschi Manihot essence according to the filling amount, and sealing to obtain the final product.

Example 2 differs from example 1 only in that: 0.1% of cactus stem extract, 0.6% of abelmoschus manihot flower extract, 0.1% of kudzuvine root extract, 88.897% of water and the balance of raw materials.

Example 3 differs from example 1 only in that: 0.2% of cactus stem extract, 0.9% of abelmoschus manihot flower extract, 0.2% of kudzuvine root extract, 88.397% of water and the proportion of the rest raw materials is unchanged.

The flos Abelmoschi Manihot essence of examples 1-3 was tested according to the standard, and the test results were as follows:

appearance: a white flowable mask liquid;

pH value: 6 to 7.5

Viscosity (25 ℃,2# and 30 r/min) is 30-100 mpa;

stability (cold resistance): keeping 24H in a refrigerator at (-8+ -2deg.C), and recovering to room temperature without layering, color-changing and taste-changing;

stability (heat resistance): keeping for 24H in a constant temperature box at the temperature of (40+/-1), and recovering the room temperature without layering, color changing and smell changing;

And (3) centrifugal examination: 2000r/min,30min without layering;

Colony count: < 10CFU/g;

Mould and yeast: < 10CFU/g;

heat-resistant coliform group: undetected;

Staphylococcus aureus: undetected;

pseudomonas aeruginosa: not detected.

Product skin irritation experiments:

60 volunteers were collected to evaluate the product quality, and the experimental results were as follows:

Table 1 shows the number of people with skin allergy

The skin of volunteers has no allergic phenomena such as erythema, eschar or edema, etc., which further indicates that the product has high safety.

Comparative example 1 differs from example 1 in that the plant extract is 0.8% of the flower extract of abelmoschus manihot.

Comparative example 2 was different from example 1 in that the plant extract was 0.8% of the pueraria extract.

Comparative example 3 differs from example 1 in that the plant extract is 0.8% cactus stem extract.

Comparative example 4 differs from example 1 only in that the extract of flower of Abelmoschus manihot, the extract of Pueraria lobata, and the extract of stem of Opuntia Dillenii are all conventional aqueous extracts.

In order to demonstrate the advantages of the technical solutions provided by the present application, the following provides the technical solutions provided by examples 1 to 3 of the present application and comparative experimental effects of the technical solutions provided by comparative examples 1 to 4.

Product moisturizing effect verification experiment: 70 volunteers (20-30 years old) were recruited to examine skin moisture values using the product. Every 10 people are one group, the first 3 groups are 7 groups, the mask of the embodiment 1-3 is used as an experimental group, the comparative example 1-4 groups are comparison groups in the prior art, before the product is smeared, skin is washed by warm water, the average value (W1) of each group of skin moisture values is detected, the product is smeared, the average value (W2) of each group of skin moisture values is detected after the product is dried, the average value (W3) of each group of skin moisture values is detected after the product is smeared for 3 hours, and the experimental result is as follows:

table 1 shows the moisture measurement before and after application to the skin

The detection result shows that the skin moisture value after the product is smeared is about 1.5 times of that before the product is smeared, the moisture value after 3 hours is higher than that before the product is smeared, the average value of the skin moisture value of the average value of the skin moisture value after the control group is smeared for 3 hours is reduced quickly, the average value difference between the average value of the skin moisture value and the moisture value before the product is not smeared is smaller, and therefore, the moisture retention and water supplementing effect of the plant extract with single component is poorer, and the effect of the plant extract with conventional water extraction is also poorer than that of the plant extract with the conventional water extraction is enough to prove that the moisture retention and water supplementing effect is more obvious after the plant extract with the invention is extracted by supercritical CO ₂, and the plant extract with the single component has the synergistic effect.

Mask freckle removing experiment

1. Selecting an object: 300 women with age of 25-40 years and different degrees of pigments such as chloasma, butterfly spot and the like on the face are selected, wherein 150 women are 25-30 years old, 100 women are 30-35 years old and 50 women are 35-40 years old.

2. Mask sample: the mask of example 1 and the mask of comparative example 4 were used as samples for the current mask freckle-removing experiment.

3. The experimental method comprises the following steps: after cleaning skin every night before sleeping, the facial mask is stuck on the face for 20 minutes, the facial mask paper is removed, and the facial mask is continuously used for 6 months.

4. Curative effect judgment criteria: basic cure: the visual stain is basically disappeared; the effect is shown: visual stain resolved by more than 60%; the method is effective: visual stain resolved by more than 20%; invalidation: visual stain resolved less than 20%.

Table 2 shows statistics of freckle removing effect of facial mask

As can be seen from Table 2, both example 1 and comparative example 4 had a good freckle removing effect on women of ages 25 to 40, and women aged between ages 25 to 30 had a best effect by applying the freckle removing mask of the present invention, which was higher than women aged between ages 30 to 40. Comparative examples 1 and 4 found that the facial mask of the plant extract extracted by supercritical CO ₂ technique was better in the freckle removing effect.

The foregoing is merely exemplary embodiments of the present application, and specific structures and features that are well known in the art are not described in detail herein. It should be noted that modifications and improvements can be made by those skilled in the art without departing from the structure of the present application, and these should also be considered as the scope of the present application, which does not affect the effect of the implementation of the present application and the utility of the patent. The protection scope of the present application is subject to the content of the claims, and the description of the specific embodiments and the like in the specification can be used for explaining the content of the claims.

Claims

1. The flower mask is characterized by comprising 0.8% of plant extracts by mass, wherein the plant extracts are extracted and separated by a supercritical CO ₂ fluid technology, and the plant extracts comprise 0.1% of cactus stem extract, 0.6% of flower extract and 0.1% of radix puerariae extract; when the kudzuvine root extract is prepared, kudzuvine root is cleaned, selected, dried and crushed, decocted and extracted for 2 times, wherein the decoction time is 3 hours and 1 hour respectively, the two filtrates are combined, and the filtrate is filtered after standing for 2 hours, concentrated and extracted by supercritical CO ₂, and then concentrated, decolorized and spray-dried and passes through a 100-mesh sieve; when preparing flos Abelmoschi Manihot extract, cleaning flos Abelmoschi Manihot, pulverizing, extracting with supercritical CO ₂ under 60% ethanol, concentrating, decolorizing, spray drying, and sieving with 100 mesh sieve; when preparing the cactus stem extract, cleaning, selecting, drying and pulverizing the cactus, extracting with supercritical CO ₂ in the presence of water, concentrating, decolorizing, spray drying, and sieving with 100 mesh sieve.

2. The abelmoschus manihot mask as claimed in claim 1, wherein: the raw materials also comprise a water phase and an oil phase, wherein the water phase list comprises the following components in percentage by mass:

88.397 to 88.897 percent of water

Glycerol 3.65%

Propylene glycol 0.045%

Glycerol polyether-200.05%

1, 6-Hexanediol 0.035%

Diglycerol 2%

Trehalose sulfate sodium 0.02%

Carbomer 0.1%

P-hydroxyacetophenone 0.25%

Nicotinamide 0.8%

Ceramide EOP0.02%

1, 2-Pentanediol 0.5%

Allantoin 0.05%

EDTA disodium 0.02%

Dipotassium glycyrrhizinate 0.005%

Cetyl hydroxyethyl cellulose 0.1%

Hyaluronic acid 0.012%

Sodium citrate 0.22%

Hydrolyzed hyaluronic acid 0.013%

0.15% Of tapioca starch

Potassium sorbate 0.014%

0.25% Of aspergillus/glucose/soybean/starch fermentation product filtrate;

the oil phase list comprises the following components in percentage by mass:

PEG/PPG-19/19 polydimethylsiloxane 0.0165%

Polyacrylate-100.011%

Acrylic acid (esters)/C10-30 alkanol acrylate cross-linked polymer 0.012%

Saccharide isomer 0.25%

Magnesium hydroxide 0.0055%

PEG-60 hydrogenated castor oil PCA isostearate 0.1%

Phenoxyethanol 0.01%

Squalane 0.25%

Nipagin ester 0.03%

PEG-10 wild soyasterol 0.25%

Cetyl ethyl hexanoate 0.026%

Hydrogenated lecithin 0.014%

Coconut oil 0.22%

0.085% Of frankincense thyme oil

Sodium benzoate 0.015%

Polyglycerol-3 diisostearate 0.018%

Sea buckthorn seed oil 0.25%

Tocopherol 0.15%

Phenyl trimethicone 0.25%.

3. The abelmoschus manihot mask as claimed in claim 2, wherein: also comprises 0.03 percent of daily essence by mass percent.

4. A method for preparing a flower of abelmoschus manihot mask according to claim 3, wherein the method comprises the following steps: during the specific preparation, all water phase raw materials are added into a water phase pot in proportion, the temperature is controlled to be 75-80 ℃, and the water phase raw material A is obtained after stirring for 20 min;

All oil phase raw materials are added into an oil phase pot in proportion, the temperature is controlled to be 75-80 ℃, and after stirring is carried out for 30min, an oil phase material B is obtained;

adding flos Abelmoschi Manihot extract, radix Puerariae extract, and radix et caulis Opuntiae Dillenii stem extract into homogenizing tank at a certain proportion, and stirring for 15min; when the temperature of the materials is cooled to 45-50 ℃, adding daily essence according to a proportion, and uniformly stirring to obtain the flos Abelmoschi Manihot essence;

5. The method for preparing the abelmoschus manihot mask according to claim 4, wherein the method comprises the following steps of: during preparation, the stirring speed is 800-2000 rmp.

6. The use of the flos Abelmoschi Manihot essence obtained in the preparation method of the flos Abelmoschi Manihot mask according to any one of claims 4 or 5 for preparing skin care products.