CN114522648A - Mixing reactor for automatically and rapidly mixing solution and construction method - Google Patents

Mixing reactor for automatically and rapidly mixing solution and construction method Download PDF

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Publication number
CN114522648A
CN114522648A CN202210368841.2A CN202210368841A CN114522648A CN 114522648 A CN114522648 A CN 114522648A CN 202210368841 A CN202210368841 A CN 202210368841A CN 114522648 A CN114522648 A CN 114522648A
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China
Prior art keywords
liquid
mixing
reaction
weir
box body
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Pending
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CN202210368841.2A
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Chinese (zh)
Inventor
苟志远
查笑乐
刘长东
刘昌林
吴秋廷
杨飞
张波
罗以超
王福海
李祖强
陈向华
赖力
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Panzhihua Pangang Group Design & Research Institute Co ltd
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Panzhihua Pangang Group Design & Research Institute Co ltd
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Priority to CN202210368841.2A priority Critical patent/CN114522648A/en
Publication of CN114522648A publication Critical patent/CN114522648A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J14/00Chemical processes in general for reacting liquids with liquids; Apparatus specially adapted therefor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/006Baffles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/001Feed or outlet devices as such, e.g. feeding tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/008Feed or outlet control devices
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/02Feed or outlet devices; Feed or outlet control devices for feeding measured, i.e. prescribed quantities of reagents
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2204/00Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices
    • B01J2204/002Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices the feeding side being of particular interest
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/20Recycling

Abstract

The invention discloses a mixing reactor for automatically and rapidly mixing a solution and a construction method, and belongs to the technical field of design and manufacture of salt chemical production process equipment. Provides a mixing reactor capable of rapidly and automatically mixing various solutions uniformly and a construction method thereof. The mixing reactor comprises a reaction tank, a weir-turning type mixing mechanism and a liquid conveying piping system, wherein the weir-turning type mixing mechanism is arranged in the reaction tank, a solution to be mixed is input into the weir-turning type mixing mechanism through the liquid conveying piping system to be mixed and turned out to the reaction tank for reaction, and a mixed solution after the reaction is finished is output out of the reaction tank through the liquid conveying piping system. The construction method comprises the steps of inputting different types of liquid into the open sleeve through the liquid input pipe, mixing the liquid in the open sleeve in a weir turning mode, entering the box body to react in the weir turning process, and finally outputting the liquid to the reaction tank through the liquid output pipe to complete the mixing and reaction of various liquids in the mixing reactor.

Description

Mixing reactor for automatically and rapidly mixing solution and construction method
Technical Field
The invention relates to a mixing reactor, in particular to a mixing reactor for automatically and quickly mixing a solution, and belongs to the technical field of design and manufacture of salt chemical production process equipment. The invention also relates to a construction method for mixed liquid reaction by adopting the mixed reactor.
Background
The main raw material for producing the titanium sponge and the titanium dioxide in China is TiCl4, and the TiCl4 mainly adopts a molten salt chlorination process and a boiling chlorination process. Aiming at the condition that W (Ca + Mg) in the titanium slag raw material is more than 5 percent, the most suitable process at present is a molten salt chlorination process. The generation of a large amount of Cl-containing waste residues (waste salts for short) by the chlorination of the molten salt is commonly adopted at present. Through research and development, the developed new waste salt treatment process needs to effectively mix various waste liquids generated in production, so that the multiple waste liquids are quickly and uniformly mixed in a reactor, elements such as Fe, Mn, Ca, Mg and the like are gradually separated, and finally NaCl is recycled and returned to a molten salt chlorination furnace for use.
Disclosure of Invention
The technical problem to be solved by the invention is as follows: provides a mixing reactor capable of rapidly and automatically mixing various solutions uniformly and a construction method for adopting the mixing reactor to mix liquid for reaction.
The technical scheme adopted for solving the technical problems is as follows: the utility model provides a mixed reactor for automatic quick mixing of solution, mixed reactor include the reaction tank, turn over weir formula mixing mechanism and liquid delivery piping, turn over weir formula mixing mechanism and arrange the reaction tank in, the solution that needs to mix passes through liquid delivery piping input turn over weir formula mixing mechanism in mix and turn out to the reaction tank in react, the mixed liquid after the reaction is accomplished passes through liquid delivery piping output the reaction tank.
Furthermore, the reaction tank is composed of a closable box body, the weir-turning type mixing mechanism is arranged in the box body, a liquid input pipe of the liquid conveying pipe system extends into the box body from the middle upper part of the box body, and a liquid output pipe of the liquid conveying pipe system is communicated with the box body from the lower part of the box body.
The preferable mode of the scheme is that the inner surface of the box body is provided with a lining glass fiber reinforced plastic anticorrosive layer, the top of the box body is provided with a reaction gas outlet and a liquid input pipe arrangement hole, and the reaction gas outlet and the liquid input pipe arrangement hole are uniformly provided with a detachable sealing cover.
Further, the lining glass fiber reinforced plastic anticorrosive coating is a 9-cloth 10-coating structural glass fiber reinforced plastic anticorrosive coating arranged on the inner surface of the box body.
The preferred mode of the above scheme is that the weir-turning mixing mechanism is an open casing arranged in the box body, the distance from the tail end of each liquid input pipe for conveying different liquids to the bottom of the open casing is less than the pipe diameter of the liquid input pipe, and the distance from the open upper opening of the open casing to the bottom of the box body is not less than two thirds of the height of the box body.
Furthermore, control valves are arranged on a liquid input pipe and a liquid output pipe of the liquid conveying pipe system, the top of the box body is detachably sealed through a cover plate, and a reaction gas outlet and liquid input pipe arrangement holes are uniformly arranged on the cover plate.
The construction method comprises the steps of inputting different types of liquid into the open sleeve through the liquid input pipe, mixing the liquid in the open sleeve in a weir turning mode, entering the box body to react in the weir turning process, and finally outputting the liquid to the reaction tank through the liquid output pipe to complete the mixing and reaction of the various types of liquid in the mixing reactor.
Further, the stay time of the mixed liquid in the box body is longer than or equal to the reaction time of various liquids.
In a preferred embodiment of the above-described embodiment, the reaction time is obtained by an external reaction test.
Furthermore, the staying time of various liquids in the box body is controlled by the control valves arranged on the liquid output pipe and the liquid input pipe so as to control the amount of the input and/or output liquid.
The invention has the beneficial effects that: the technical scheme that this application provided is through setting up one set including the reaction tank, turning over the mixed reactor of weir formula mixing mechanism and liquid delivery piping, and will turn over weir formula mixing mechanism and arrange the reaction tank in, then pass through the solution that needs to mix liquid delivery piping input turn over weir formula mixing mechanism in mix and turn over to the reaction tank in react, the mixed liquid after the reaction is accomplished passes through liquid delivery piping output the reaction tank. Because the technical scheme that this application provided adopts each liquid that liquid conveying piping system will need to mix to import simultaneously turns over weir formula mixing mechanism to realize the mixing of stirring completion various liquid between the different liquid at this turns over weir formula mixing mechanism through the form that turns over the weir formula, changed prior art and need can't effectively mix or need set up the current situation that large-scale mixing tank adds agitating unit and just can mix a large amount of different liquid, reached quick automatic liquid to multiple needs reaction and mixed the purpose. The method creates conditions for separating elements such as Fe, Mn, Ca, Mg and the like from the waste salt through reaction treatment and finally realizing the recovery of NaCl and returning the NaCl to the fused salt chlorination furnace for use.
Drawings
FIG. 1 is a simplified structural diagram of a mixing reactor for automatic and rapid mixing of a solution according to the present invention.
Labeled as: the device comprises a reaction tank 1, a weir-turning type mixing mechanism 2, a liquid conveying pipe system 3, a liquid input pipe 4, a liquid output pipe 5, a reaction gas outlet 6, a liquid input pipe arrangement hole 7, a control valve 8 and a cover plate 9.
Detailed Description
Fig. 1 shows a mixing reactor capable of rapidly and automatically mixing a plurality of solutions according to the present invention. The mixing reactor comprises a reaction tank 1, a weir-turning type mixing mechanism 2 and a liquid conveying piping system 3, wherein the weir-turning type mixing mechanism 2 is arranged in the reaction tank 1, a solution to be mixed is input into the weir-turning type mixing mechanism 2 through the liquid conveying piping system 3 to be mixed and turned out to the reaction tank 1 for reaction, and a mixed solution after the reaction is finished is output out of the reaction tank 1 through the liquid conveying piping system 3. The construction method comprises the steps of inputting different types of liquid into the open sleeve through the liquid input pipe 4, mixing the liquid in the open sleeve in a weir turning mode, entering the box body in the weir turning process to react, and finally outputting the liquid out of the reaction tank through the liquid output pipe 5 to complete mixing and reaction of various liquids in the mixing reactor. The technical scheme that this application provided is through setting up one set including the reaction tank, turning over the mixed reactor of weir formula mixing mechanism and liquid delivery piping, and will turn over weir formula mixing mechanism and arrange the reaction tank in, then pass through the solution that needs to mix liquid delivery piping input turn over weir formula mixing mechanism in mix and turn over to the reaction tank in react, the mixed liquid after the reaction is accomplished passes through liquid delivery piping output the reaction tank. Because the technical scheme that this application provided adopts each liquid that liquid conveying piping system will need to mix to import simultaneously turns over weir formula mixing mechanism to realize the mixing of stirring completion various liquid between the different liquid at this turns over weir formula mixing mechanism through the form that turns over the weir formula, changed prior art and need can't effectively mix or need set up the current situation that large-scale mixing tank adds agitating unit and just can mix a large amount of different liquid, reached quick automatic liquid to multiple needs reaction and mixed the purpose. The method creates conditions for separating elements such as Fe, Mn, Ca, Mg and the like from the waste salt through reaction treatment and finally realizing the recovery of NaCl and returning the NaCl to the fused salt chlorination furnace for use.
In the above embodiment, in order to simplify the structure of each part of the present application, facilitate the manufacture, assembly and use, and improve the mixing effect, the reaction tank 1 of the present application is composed of a closable tank body, the weir-turning mixing mechanism 2 is disposed in the tank body, the liquid input pipe 4 of the liquid conveying piping system 3 extends into the tank body from the middle upper part of the tank body, and the liquid output pipe 5 of the liquid conveying piping system is communicated with the tank body from the lower part of the tank body. The weir-turning type mixing mechanism 2 is an open casing arranged in the box body, the distance from the tail end of each liquid input pipe 4 for conveying different liquids to the bottom of the open casing is smaller than the pipe diameter of the liquid input pipe 4, and the distance between the open upper opening of the open casing and the bottom of the box body is not smaller than two thirds of the height of the box body. And the liquid input pipe 4 and the liquid output pipe 5 of the liquid conveying pipe system 3 are both provided with a control valve 8, the top of the box body is detachably sealed by a cover plate 9, and the reaction gas outlet 6 and the liquid input pipe arrangement hole 7 are both arranged on the cover plate 9. Correspondingly, all have the characteristics of corrosivity in order to adapt to this application various liquid that need mix, in order to prolong the life of this application mixing reactor, be provided with inside lining glass steel anticorrosive coating on the internal surface of box, be provided with reaction gas discharge port 6 and liquid input pipe arrangement hole 7 at the top of box reaction gas discharge port 6 with liquid input pipe arrangement hole 7 on the equipartition have placed detachable sealed lid. At the moment, the lining glass fiber reinforced plastic anticorrosive coating is a 9-cloth 10-coating structural glass fiber reinforced plastic anticorrosive coating arranged on the inner surface of the box body.
Further, in order to improve the reaction effect, the stay time of the mixed liquid in the box body is longer than or equal to the reaction time of various liquids. In this case, the reaction time is determined by an external reaction test. The staying time of various liquids in the box body is adopted to control the amount of the liquid input and/or output by control valves arranged on the liquid output pipe 5 and the liquid input pipe 4.
DETAILED DESCRIPTION OF EMBODIMENT (S) OF INVENTION
The main content of the invention is as follows:
1. the invention is suitable for acidic solution, and is anticorrosive by lining glass fiber reinforced plastic in a reactor, and adopting 9 cloth and 10 coatings;
2. the invention arranges a sleeve in a reaction tank, and inserts a plurality of solution feed pipes into the bottom of the sleeve to ensure that the solution turns upwards and overflows the sleeve, and forms a 'turning weir' to ensure that the solution is fully mixed, then flows downwards in the reaction tank and is discharged out of a reactor at the bottom of a container;
3. the external reaction tank calculates the retention time of the solution in the reactor according to the reaction time, thereby effectively solving the chemical reaction effect;
4. setting other reaction discharge holes at the top of the molten pool, and effectively treating the gas;
5. a flow control system is arranged on the feeding system, and the proportioning problem is solved through a regulating valve.
Example one
According to the invention, through researching material properties and process conditions, a reactor for quickly and automatically mixing various solutions is developed, and the purposes of quickly mixing and effectively controlling reaction rate are achieved.
The first step is as follows: selecting materials according to working conditions;
the second step is that: according to the process requirements, calculating the mixing time of the solution in the reactor, designing the length of a sleeve and the like;
the third step: the reactor specifications are designed according to the process requirements, the length of the sleeve and the reaction time in the reactor.

Claims (10)

1. A mixing reactor that is used for automatic quick mixing of solution which characterized in that: the mixing reactor comprises a reaction tank (1), a weir-turning type mixing mechanism (2) and a liquid conveying piping system (3), wherein the weir-turning type mixing mechanism (2) is arranged in the reaction tank (1), a solution needing to be mixed is input into the weir-turning type mixing mechanism (2) through the liquid conveying piping system (3) to be mixed and turned out to the reaction tank (1) for reaction, and a mixed solution after the reaction is finished is output from the reaction tank (1) through the liquid conveying piping system (3).
2. The mixing reactor for automatic and rapid blending of solutions according to claim 1, characterized in that: the reaction tank (1) is composed of a closable tank body, the weir-turning type mixing mechanism (2) is arranged in the tank body, a liquid input pipe (4) of the liquid conveying pipe system (3) extends into the tank body from the middle upper part of the tank body, and a liquid output pipe (5) of the liquid conveying pipe system is communicated with the tank body from the lower part of the tank body.
3. The mixing reactor for automatic and rapid blending of solutions according to claim 2, characterized in that: the inner surface of the box body is provided with a lining glass fiber reinforced plastic anticorrosive layer, the top of the box body is provided with a reaction gas outlet (6) and a liquid input pipe arrangement hole (7), and detachable sealing covers are uniformly distributed on the reaction gas outlet (6) and the liquid input pipe arrangement hole (7).
4. The mixing reactor for automatic and rapid blending of solutions according to claim 3, characterized in that: the lining glass fiber reinforced plastic anticorrosive coating is a 9-cloth 10-coating structural glass fiber reinforced plastic anticorrosive coating arranged on the inner surface of the box body.
5. The mixing reactor for automatic rapid blending of solutions according to claim 1, 2, 3 or 4, characterized in that: the weir-turning type mixing mechanism (2) is an open sleeve arranged in the box body, the distance from the tail end of each liquid input pipe (4) for conveying different liquids to the bottom of the open sleeve is smaller than the pipe diameter of the liquid input pipe (4), and the distance between the open upper opening of the open sleeve and the bottom of the box body is not smaller than two thirds of the height of the box body.
6. The mixing reactor for automatic and rapid blending of solutions according to claim 5, characterized in that: control valves (8) are arranged on a liquid input pipe (4) and a liquid output pipe (5) of the liquid conveying pipe system (3), the top of the box body is detachably sealed through a cover plate (9), and reaction gas discharge ports (6) and liquid input pipe arrangement holes (7) are uniformly arranged on the cover plate (9).
7. The construction method for reacting the mixed liquid in the mixing reactor of claim 6, wherein: the construction method comprises the steps of inputting different types of liquid into the open sleeve through the liquid input pipe (4), mixing the liquid in the open sleeve in a weir turning mode, entering the box body to react in the weir turning process, and finally outputting the liquid to the reaction tank through the liquid output pipe (5) to complete the mixing and reaction of various liquids in the mixing reactor.
8. The construction method according to claim 7, wherein: the stay time of the mixed liquid in the box body is longer than or equal to the reaction time of various liquids.
9. The construction method according to claim 8, wherein: the reaction duration is determined by external reaction tests.
10. The construction method according to claim 9, wherein: the staying time of various liquids in the box body is controlled by the control valves arranged on the liquid output pipe (5) and the liquid input pipe (4) to control the amount of the input and/or output liquid.
CN202210368841.2A 2022-04-08 2022-04-08 Mixing reactor for automatically and rapidly mixing solution and construction method Pending CN114522648A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202210368841.2A CN114522648A (en) 2022-04-08 2022-04-08 Mixing reactor for automatically and rapidly mixing solution and construction method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202210368841.2A CN114522648A (en) 2022-04-08 2022-04-08 Mixing reactor for automatically and rapidly mixing solution and construction method

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CN114522648A true CN114522648A (en) 2022-05-24

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Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1198448A (en) * 1966-11-03 1970-07-15 Wool Ind Res Association Methods and Apparatus for Mixing and Dispensing Solutions
CN1170628A (en) * 1996-02-27 1998-01-21 普拉塞尔技术有限公司 Improved reactor system
CN1195897A (en) * 1997-02-03 1998-10-14 松下电器产业株式会社 Manufacturing method of active materials for positive electrode in alkaline storage batteries
CN101274249A (en) * 2007-03-28 2008-10-01 中国石油大学(北京) Novel liquid-liquid heterophase reactor
CN103611454A (en) * 2013-12-05 2014-03-05 北京国科安达科技发展有限公司 Pneumatic stirring device and stirring method thereof
CN203572771U (en) * 2013-11-25 2014-04-30 武汉钢铁(集团)公司 Atomic absorption spectrometer mixing sample introduction device
KR20160055410A (en) * 2014-11-10 2016-05-18 주식회사 포스코 Apparatus for mixing solution
CN107727559A (en) * 2017-09-12 2018-02-23 合肥通用机械研究院 A kind of corrosion testing apparatus and the method using the device
CN108273452A (en) * 2018-01-30 2018-07-13 浙江工业大学 A kind of grease epoxidation reactor
CN208906035U (en) * 2018-08-23 2019-05-28 江西国化实业有限公司 A kind of medication chemistry apparatus for combining liquids
CN114259972A (en) * 2022-01-07 2022-04-01 四川宝生药业发展有限公司 Liquid-liquid two-phase mixing device of chlorine dioxide enhanced reactor

Patent Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1198448A (en) * 1966-11-03 1970-07-15 Wool Ind Res Association Methods and Apparatus for Mixing and Dispensing Solutions
CN1170628A (en) * 1996-02-27 1998-01-21 普拉塞尔技术有限公司 Improved reactor system
CN1195897A (en) * 1997-02-03 1998-10-14 松下电器产业株式会社 Manufacturing method of active materials for positive electrode in alkaline storage batteries
CN101274249A (en) * 2007-03-28 2008-10-01 中国石油大学(北京) Novel liquid-liquid heterophase reactor
CN203572771U (en) * 2013-11-25 2014-04-30 武汉钢铁(集团)公司 Atomic absorption spectrometer mixing sample introduction device
CN103611454A (en) * 2013-12-05 2014-03-05 北京国科安达科技发展有限公司 Pneumatic stirring device and stirring method thereof
KR20160055410A (en) * 2014-11-10 2016-05-18 주식회사 포스코 Apparatus for mixing solution
CN107727559A (en) * 2017-09-12 2018-02-23 合肥通用机械研究院 A kind of corrosion testing apparatus and the method using the device
CN108273452A (en) * 2018-01-30 2018-07-13 浙江工业大学 A kind of grease epoxidation reactor
CN208906035U (en) * 2018-08-23 2019-05-28 江西国化实业有限公司 A kind of medication chemistry apparatus for combining liquids
CN114259972A (en) * 2022-01-07 2022-04-01 四川宝生药业发展有限公司 Liquid-liquid two-phase mixing device of chlorine dioxide enhanced reactor

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