CN114469811A

CN114469811A - Collagen anti-wrinkle repair mask and production process

Info

Publication number: CN114469811A
Application number: CN202210150299.3A
Authority: CN
Inventors: 王菲菲
Original assignee: Beijing Yanzhisu Biotechnology Co ltd
Current assignee: Beijing Yanzhisu Biotechnology Co ltd
Priority date: 2022-02-18
Filing date: 2022-02-18
Publication date: 2022-05-13

Abstract

The invention provides a collagen anti-wrinkle repair mask and a production process, which relate to the technical field of liquid mask processing and comprise the following raw materials: purified water, butanediol, herba Portulacae extract, glycerol, 1, 3-propylene glycol, 1, 2-hexanediol, caprylyl hydroximic acid, panthenol, allantoin, arginine, and carbomer. According to the invention, through reasonable matching of purified water, butanediol, purslane extract, glycerol, 1, 3-propanediol, 1, 2-hexanediol, caprylyl hydroximic acid, panthenol, allantoin, arginine, carbomer, collagen, dipotassium glycyrrhizinate, hydrolyzed sclerotium rolfsii gum, acrylic acid (ester) copolymer and sodium alginate, the prepared liquid facial mask has the effects of moisturizing, soothing, repairing, resisting photoaging, resisting oxidation, enhancing skin hydration capacity and the like, and is rich in effect and good in effect.

Description

Collagen anti-wrinkle repair mask and production process

Technical Field

The invention relates to the technical field of liquid mask processing, in particular to a collagen anti-wrinkle repair mask and a production process thereof.

Background

The skin is a fragile part in a human body, and people pay attention to skin care all the time, the traditional liquid facial mask generally only has the effect of protecting the skin for a short time, the nourishing effect is poor, the skin characteristics of people of various ages are different, and the existing liquid facial mask has a single protection effect and a poor effect on a user. The facial mask is a carrier of a beauty care product, and can temporarily isolate the outside air and dust to improve the skin temperature, expand the pores of the skin, promote the secretion and metabolism of sweat glands and remove the products of surface cell metabolism by covering the facial mask on the face for a short time. Moisture in the facial mask permeates into the horny layer of the skin epidermis to keep the skin durable, natural, bright and elastic, so the facial mask is favored in beauty maintenance of girls.

Disclosure of Invention

Aiming at the defects of the prior art, the invention provides a collagen anti-wrinkle repair mask and a production process thereof, and solves the problems of single protection effect and poor effect of the existing liquid mask on a user.

Technical scheme

In order to achieve the purpose, the invention is realized by the following technical scheme: a liquid facial mask prepared by a vacuum emulsification method comprises the following raw materials in percentage: comprises the following raw materials in percentage by weight: purified water (or water for injection) is added to 100%, butanediol 2.5-3.0%, herba Portulacae extract 0.02-0.03%, glycerol 1-3%, 1, 3-propylene glycol 0.5-0.6%, 1, 2-hexanediol 0.2-0.3%, caprylyl hydroximic acid 0.04-0.05%, panthenol 0.5-1.0%, allantoin 0.2-0.5%, arginine 0.1-0.2%, carbomer 0.1-0.2%, collagen 0.1-0.2%, dipotassium glycyrrhizinate 0.05-0.08%, hydrolyzed Sclerotinia sclerotiorum (Sclerotinum) 0.03-0.04%, acrylic acid (ester) copolymer 0.0005-0.001%, and sodium alginate 0.0003-0.0005%.

Preferably, the collagen anti-wrinkle repair mask and the production process thereof comprise the following steps:

s1, adding purified water into a reaction container through a flowmeter, and sequentially adding hydrolyzed sclerotium rolfsii gum, acrylic acid (ester) copolymer, sodium alginate and carbomer into the reaction container for mixing and dissolving; standing for 6h to completely swell the solution to obtain a solution A;

s2, adding purified water into the reaction container through a flowmeter, then weighing the allantoin, collagen and dipotassium glycyrrhizinate raw materials with corresponding percentages, adding the raw materials into the reaction container, dissolving the raw materials until the raw materials are transparent, and obtaining a solution B after dissolving;

s3, sequentially weighing butanediol, purslane extract, glycerol, 1, 3-propanediol, 1, 2-hexanediol, caprylyl hydroximic acid and panthenol, adding into a reaction container, stirring until the materials are dissolved, adding the solution B into the reaction container, and mixing at the mixing speed of 25 revolutions per minute for 10 minutes to obtain a solution C;

s4, adding the solution A into the solution C, mixing, adding arginine, mixing at the rotation speed of 25r/min for 10min, and then placing the mixed solution into a reaction container for deaeration at the rotation speed of 20 r/min, wherein the vacuum pressure of the reaction container is not less than 0.06mpa, and the deaeration time is 20 min;

s5, conveying the intermediate to a laboratory for detecting sensory indexes, carrying out ozone disinfection on the product plastic bags and the film carrier materials, bagging the film carrier materials by using equipment according to requirements, filling according to rules to obtain intermediate products, packaging the products in a warehouse, carrying out finished product inspection, and warehousing after the finished products are qualified.

Preferably, in the step S1, the stirring speed of the reaction vessel is 25r/min, and the stirring time is 40 minutes.

Preferably, in the step S2, the rotation speed of the reaction vessel is 25 rpm, and the mixing time is 40 minutes.

Preferably, the reaction vessel is one of a vacuum emulsification reaction kettle and a stainless steel barrel.

The invention has the following advantages and beneficial effects:

the invention provides a collagen anti-wrinkle repair mask and a production process thereof.A purified water (or an injection water), butanediol, a purslane extract, glycerol, 1, 3-propanediol, 1, 2-ethanediol, caprylyl hydroximic acid, panthenol, allantoin, arginine, carbomer, collagen, dipotassium glycyrrhizinate, hydrolyzed sclerotium rolfsii gum, an acrylic acid (ester) copolymer and sodium alginate are reasonably matched for use, so that the prepared liquid mask has the effects of moisturizing, soothing, repairing, light aging resistance, oxidation resistance, skin hydration capacity enhancement and the like, and is rich in effect and good in effect.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

Example 1

The embodiment of the invention provides a collagen anti-wrinkle repair mask and a production process thereof, wherein the collagen anti-wrinkle repair mask comprises the following raw materials in percentage by weight: purified water (or water for injection) is added to 100 percent, butanediol is 2.5 percent, purslane extract is 0.02 percent, glycerol is 1 percent, 1, 3-propylene glycol is 0.5 percent, 1, 2-hexanediol is 0.2 percent, caprylyl hydroximic acid is 0.04 percent, panthenol is 0.5 percent, allantoin is 0.2 percent, arginine is 0.1 percent, carbomer is 0.1 percent, collagen is 0.1 percent, dipotassium glycyrrhizinate is 0.05 percent, hydrolyzed sclerotium rolfsii gum is 0.03 percent, acrylic acid (ester) copolymer is 0.0005 percent, sodium alginate is 0.0003 percent, butanediol has better moisturizing effect, and the proportion of water grasping is small and has certain bacteriostasis effect at the same time as butanediol is a small-molecule moisturizing component; the purslane extract can reduce the secretion of inflammatory factors interleukin and has certain anti-inflammatory effect, so that the purslane extract can relieve skin inflammation and inhibit skin itch caused by dryness, meanwhile, the purslane extract has obvious improvement effect on skin allergy generated by long-term use of hormone cosmetics, also has various stimulation effects on the skin from the outside, and is an effective anti-allergic component; the panthenol has stable property and good permeability, is easy to penetrate skin barriers, is used as a humectant and a skin conditioner in a nutrient solution, effectively enhances the moisturizing effect of the nutrient solution, relieves the dryness of the skin, enhances the hydration capability of the skin, and also has certain anti-inflammatory and repairing effects; allantoin not only can promote the water absorption capacity of the outermost layer of skin and hair, but also is beneficial to the hydrophilicity of keratin molecules; arginine belongs to basic amino acid, is mainly used for conditioning dry skin in cosmetics, and can keep skin moisture, smooth skin and reduce the peeling of scurf by the synergistic effect of fruit acid, trehalose and the like with the moisturizing effect; carbomers, known collectively as acrylics, are a common cosmetic additive.

A collagen anti-wrinkle repair mask and a production process thereof comprise the following steps:

s1, adding purified water into the vacuum emulsification reaction kettle through a flowmeter, and sequentially adding hydrolyzed sclerotium rolfsii gum, acrylic acid (ester) copolymer, sodium alginate and carbomer into the vacuum emulsification reaction kettle for mixing and dissolving; standing for 6h to completely swell the solution to obtain a solution A;

s2, adding purified water into the vacuum emulsification reaction kettle through a flowmeter, then weighing allantoin, collagen and dipotassium glycyrrhizinate materials in corresponding percentages, adding the materials into the vacuum emulsification reaction kettle to dissolve the materials until the materials are transparent, and obtaining a solution B after dissolution;

s3, sequentially weighing butanediol, purslane extract, glycerol, 1, 3-propanediol, 1, 2-hexanediol, caprylyl hydroximic acid and panthenol, adding into a reaction container, stirring until the materials are dissolved, adding the solution B into the reaction container, and mixing at the mixing speed of 25 revolutions per minute for 10min to obtain a solution C;

s4, adding the solution A into the solution C, mixing, adding arginine, mixing at the rotation speed of 25r/min for 10min, placing the mixed solution into a vacuum emulsification reaction kettle, and defoaming, wherein the rotation speed of the vacuum emulsification reaction kettle is 20 r/min, the vacuum pressure of the vacuum emulsification reaction kettle is not less than 0.06mpa, and the defoaming time is 20 min;

In the step S1, the stirring speed of the vacuum emulsification reaction kettle is 25r/min, and the stirring time is 40 minutes.

In the step S2, the rotation speed of the vacuum emulsification reactor is 25 rpm, and the mixing time is 40 minutes.

Example 2

The embodiment of the invention provides a collagen anti-wrinkle repair mask and a production process thereof, wherein the collagen anti-wrinkle repair mask comprises the following raw materials in percentage by weight: purified water (or water for injection) is added to 100 percent, butanediol is 3.0 percent, purslane extract is 0.03 percent, glycerol is 3 percent, 1, 3-propylene glycol is 0.6 percent, 1, 2-hexanediol is 0.3 percent, caprylyl hydroximic acid is 0.05 percent, panthenol is 1.0 percent, allantoin is 0.5 percent, arginine is 0.2 percent, carbomer is 0.2 percent, collagen is 0.2 percent, dipotassium glycyrrhizinate is 0.08 percent, hydrolyzed sclerotium rolfsii gum is 0.04 percent, acrylic acid (ester) copolymer is 0.001 percent, sodium alginate is 0.0005 percent, butanediol has better moisturizing effect, and butanediol is a small molecular moisturizing component, so the proportion of water grasping is small, and a certain bacteriostasis effect is achieved; the purslane extract can reduce the secretion of inflammatory factors, namely interleukin, has a certain anti-inflammatory effect, so that the inflammation of skin is relieved, and the skin itch caused by dryness is inhibited; the panthenol has stable property and good permeability, is easy to penetrate skin barriers, is used as a humectant and a skin conditioner in a nutrient solution, effectively enhances the moisturizing effect of the nutrient solution, relieves the dryness of the skin, enhances the hydration capability of the skin, and also has certain anti-inflammatory and repairing effects; allantoin not only can promote the water absorption capacity of the outermost layer of skin and hair, but also is beneficial to the hydrophilicity of keratin molecules; arginine belongs to basic amino acid, is mainly used for conditioning dry skin in cosmetics, and can keep skin moisture, smooth skin and reduce the peeling of scurf by the synergistic effect of fruit acid, trehalose and the like with the moisturizing effect; carbomers, known collectively as acrylics, are a common cosmetic additive.

The carbomer is added into the mask, so that the nutrient solution has the following effects, namely, the irritation and the damage of substances with irritation to skin and mucous membrane can be reduced; secondly, the resistance of the skin to ultraviolet rays can be enhanced, and the damage of the ultraviolet rays to the skin can be reduced; third, carbomer has certain looseness, and is a slightly acidic substance with extremely strong dilutability, so that a proper amount of carbomer can be added when the gel or the cosmetic is prepared, the viscosity of the substances is reduced, and the stability of the effective substances can be maintained; fourthly, carbomer is a natural medicinal component and can sterilize and diminish inflammation; the dipotassium glycyrrhizinate can neutralize or reduce toxic substances of cosmetics and also can prevent certain allergic reactions of the cosmetics; the hydrolyzed sclerotium rolfsii gum is added into skin nutrition, so that the liquid mask has the effects of moisturizing and nourishing, and has the effects of repairing, resisting inflammation, resisting oxidation and the like.

s1, adding purified water into a stainless steel barrel through a flowmeter, and sequentially adding hydrolyzed sclerotium rolfsii gum, acrylic acid (ester) copolymer, sodium alginate and carbomer into the stainless steel barrel for mixing and dissolving; standing for 6h to completely swell the solution to obtain a solution A;

s2, adding purified water into a stainless steel barrel through a flowmeter, then weighing the allantoin, collagen and dipotassium glycyrrhizinate raw materials in corresponding percentages, adding the raw materials into the stainless steel barrel, dissolving the raw materials until the raw materials are transparent, and obtaining a solution B after dissolving;

s4, adding the solution A into the solution C, mixing, adding arginine, mixing at the rotation speed of 25r/min for 10min, and then placing the mixed solution into a stainless steel barrel for deaeration, wherein the rotation speed of the stainless steel barrel is 20 r/min, the vacuum pressure of the stainless steel barrel is not less than 0.06mpa, and the deaeration time is 20 min;

In the step S1, the stirring speed of the stainless steel barrel is 25r/min, and the stirring time is 40 minutes.

In the step S2, the rotation speed of the stainless steel barrel is 25 rpm, and the mixing time is 40 minutes.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

1. EXAMPLES evaluation of product safety

The safety of the product was examined with reference to the microorganism examination method, the skin patch test-skin closed patch test in technical Specification for cosmetic safety (2015 edition), and the chick chorioallantoic membrane test for eye irritation/corrosion of cosmetics, and the results were as follows:

TABLE 1 safety evaluation test results

2. EXAMPLES in vitro antioxidant testing of the product

The DPPH powder 2mg is precisely weighed, the weighing is quick and the light is avoided, a container is prepared in advance and is wrapped by aluminum foil paper, and the aluminum foil paper is dissolved by 50ml of absolute ethyl alcohol. Test example 1 and example 2 samples were diluted to 50% and 25% concentration solutions. Sequentially adding samples, and incubating for 30min at 37 ℃ by a shaking table. The absorbance was measured by a microplate reader (wavelength 517nm), and the clearance was calculated.

TABLE 2 clearance of DPPH free radicals

DPPH clearance ═ [ (a-D) - (C-D) ]/(a-D) × 100%, where a: 100uLDPPH +100uL of absolute ethyl alcohol; b: blank; c: 100uLDPPH +100uL sample; d: 100uL of sample +100uL of absolute ethanol.

1, 1-diphenyl-2-trinitrophenylhydrazine (DPPH for short) is a stable long-life free radical, and the ethanol solution of the free radical is dark purple and has strong absorption near 517 nm. In the presence of free radical scavengers, the light absorption of the DPPH ethanol solution is reduced due to its one-electron pairing. The degree of discoloration of the DPPH ethanol solution is linear with the number of electrons it receives, and thus the ability of the test sample to scavenge free radicals, i.e., the magnitude of antioxidant activity, can be evaluated. Free radicals are natural products of human metabolic processes, and attack skin cell membranes, destroy the elasticity and flexibility of the cell membranes, cause skin cells to accelerate aging, cause the skin to relax, lose elasticity, generate wrinkles and show aging signs. The samples of the embodiment 1 and the embodiment 2 have stronger free radical scavenging capacity, wherein the antioxidant effect of the sample of the embodiment 2 is more obvious.

3. EXAMPLES evaluation test of human body efficacy of the product

32 volunteers (female healthy volunteers with facial skin non-abnormalities between the ages of 25 and 60 years) were selected and randomly divided equally into two groups, using the samples of example 1 and example 2, respectively, for 4 weeks continuously, and the return visit test was performed after 4 weeks after the use of the product. The test indexes are respectively as follows: moisture content of skin stratum corneum, moisture loss amount through skin, skin elasticity R2, wrinkle number, and skin redness differentiation value. The results of the tests are shown in Table 3 for 4 weeks after continuous use of the product.

Table 3 change in test index after 4 weeks of continuous use of the product (n ═ 16)

The moisture content of the skin stratum corneum is increased to prove that the test sample has the effects of moisturizing and moistening, the reduction of the moisture loss of the skin proves that the test sample has the effect of repairing the skin barrier, and the increase of the skin elasticity value proves that the test sample has the effect of enhancing the skin elasticity and firmness; the reduction in the number of wrinkles demonstrates the anti-wrinkle efficacy of the test sample, and the reduction in the skin redness score demonstrates the soothing efficacy of the test sample. The data in table 3 show that both example 1 and example 2 have certain moisturizing, repairing, firming and anti-wrinkle effects, and example 2 has a better comprehensive effect.

4. EXAMPLES volunteer self-assessment of products

The volunteers were asked to investigate their product perception, with score 1 indicating very different consent, score 2 indicating more different consent, score 3 indicating neither different nor consent, score 4 indicating more consent, and score 5 indicating very good consent. The statistical results are expressed as the sum of the percentages of "4 over comparative" and "5 over very similar" after 28 days of use of the product, and are shown in Table 4.

Table 4 statistical table of volunteer feeling after 4 weeks of continuous use of the product (n ═ 16)

After the product is continuously used for 4 weeks, the volunteers have obvious feelings on the moisturizing effect, the redness improving effect, the skin smoothing effect, the fine line fading effect, the dryness and tightness relieving effect and the like of the samples in the examples 1 and 2, the comprehensive effect of the example 2 is better, and all feelings reach 100 percent identity (4 points or 5 points).

Claims

1. A liquid facial mask prepared by a vacuum emulsification method is characterized in that: the composite material comprises the following raw materials in percentage by weight: purified water is added to 100%, butanediol 2.5-3.0%, herba Portulacae extract 0.02-0.03%, glycerol 1-3%, 1, 3-propylene glycol 0.5-0.6%, 1, 2-hexanediol 0.2-0.3%, caprylyl hydroximic acid 0.04-0.05%, panthenol 0.5-1.0%, allantoin 0.2-0.5%, arginine 0.1-0.2%, carbomer 0.1-0.2%, collagen 0.1-0.2%, dipotassium glycyrrhizinate 0.05-0.08%, hydrolyzed Sclerotinia sclerotiorum 0.03-0.04%, acrylic acid (ester) copolymer 0.0005-0.001%, and sodium alginate 0.0003-0.0005%.

2. The collagen anti-wrinkle repair mask as claimed in claim 1 and the production process thereof, wherein: the method comprises the following steps:

3. The collagen anti-wrinkle repair mask as claimed in claim 2 and the production process thereof, wherein: in the step S1, the stirring speed of the reaction vessel is 25r/min, and the stirring time is 40 minutes.

4. The collagen anti-wrinkle repair mask as claimed in claim 2 and the production process thereof, wherein: in the step S2, the rotation speed of the reaction vessel is 25 rpm, and the mixing time is 40 minutes.

5. The collagen anti-wrinkle repair mask as claimed in claim 2 and the production process thereof, wherein: the reaction vessel is one of a vacuum emulsification reaction kettle and a stainless steel barrel.