CN114468132A - Mushroom cooking liquor extract feed additive and preparation method thereof - Google Patents

Mushroom cooking liquor extract feed additive and preparation method thereof Download PDF

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Publication number
CN114468132A
CN114468132A CN202210233426.6A CN202210233426A CN114468132A CN 114468132 A CN114468132 A CN 114468132A CN 202210233426 A CN202210233426 A CN 202210233426A CN 114468132 A CN114468132 A CN 114468132A
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China
Prior art keywords
feed additive
filter residue
extract
cooking liquor
extract feed
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CN202210233426.6A
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Chinese (zh)
Inventor
刘超英
王冶
朱津津
岳宗阳
禹航
杨新峰
刘浩
袁雄艳
陈佳慧
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Huanghuai University
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Huanghuai University
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Priority to CN202210233426.6A priority Critical patent/CN114468132A/en
Publication of CN114468132A publication Critical patent/CN114468132A/en
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K10/00Animal feeding-stuffs
    • A23K10/30Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K20/00Accessory food factors for animal feeding-stuffs
    • A23K20/10Organic substances
    • A23K20/105Aliphatic or alicyclic compounds
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K20/00Accessory food factors for animal feeding-stuffs
    • A23K20/10Organic substances
    • A23K20/163Sugars; Polysaccharides
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K20/00Accessory food factors for animal feeding-stuffs
    • A23K20/20Inorganic substances, e.g. oligoelements
    • A23K20/28Silicates, e.g. perlites, zeolites or bentonites
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K40/00Shaping or working-up of animal feeding-stuffs
    • A23K40/10Shaping or working-up of animal feeding-stuffs by agglomeration; by granulation, e.g. making powders
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/02Solvent extraction of solids
    • B01D11/0288Applications, solvents

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Polymers & Plastics (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Zoology (AREA)
  • Animal Husbandry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Molecular Biology (AREA)
  • Mycology (AREA)
  • Physiology (AREA)
  • Inorganic Chemistry (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)
  • Preparation Of Fruits And Vegetables (AREA)

Abstract

The invention discloses a mushroom cooking liquor extract feed additive and a preparation method thereof, belonging to the technical field of additives, the mushroom extract feed additive is prepared from mushroom, a carrier, a preservative and an outer protective material, the mushroom is cleaned, aired and cut up for standby, the cut-up mushroom is placed in an alcohol extraction tank, primary liquid and filter residue are extracted, the filter residue in S2 is placed in the alcohol extraction tank, secondary liquid and filter residue are extracted, the filter residue in S3 is placed in the alcohol extraction tank, tail liquid and filter residue are extracted, the filter residue is removed, the primary liquid, the secondary liquid and the tail liquid are mixed, distilled and concentrated to prepare extract, the extract is placed in an atomization drier for atomization drying to prepare powder, the preservative and the carrier are placed in a stirring device together for stirring, so that the powder, the preservative and the carrier are fully mixed together and placed in a granulator for granulation, the additive can be effectively prevented from losing efficacy due to erosion of water vapor in a storage process, the quality of the additive is guaranteed.

Description

Mushroom cooking liquor extract feed additive and preparation method thereof
Technical Field
The invention relates to the technical field of additives, in particular to a shiitake cooking liquor extract feed additive and a preparation method thereof.
Background
The additive comprises various chemical additives such as feed additives, food additives, concrete additives, engine oil additives and the like.
The feed additive is a small amount or trace substance added in the production, processing and using processes of feed, and the feed additive is small in dosage but remarkable in effect. The feed additive is a raw material inevitably used in modern feed industry, and has obvious effects on strengthening the nutritive value of basic feed, improving the production performance of animals, ensuring the health of the animals, saving the feed cost, improving the quality of animal products and the like.
The shiitake mushroom feed additive is prepared by extracting the shiitake mushroom after cooking, so that the existing shiitake mushroom feed additive is not easy to store, is easy to contact moisture in the air in the storage process, causes additive failure and seriously affects the quality of the additive.
Disclosure of Invention
The invention aims to provide a shiitake mushroom cooking liquor extract feed additive and a preparation method thereof, and aims to solve the problems that the existing shiitake mushroom feed additive provided in the background art is not easy to store, and is easy to contact with moisture in the air in the storage process, so that the additive loses efficacy, and the quality of the additive is seriously influenced.
In order to achieve the purpose, the invention provides the following technical scheme: a feed additive of the extract of the digestion liquid of lentinus edodes is prepared from lentinus edodes, carrier, antiseptic and external protecting material.
Preferably, the carrier is formed by mixing pine needle powder, attapulgite, silicon dioxide and maltodextrin in a weight ratio of 1:1-2:0.7-0.9: 0.6-0.8.
Preferably, the preservative is monosodium fumarate.
Preferably, the outer protective material is formed by mixing food-grade hydrophobic material and edible alkali, and the weight ratio of the food-grade hydrophobic material to the edible alkali is 1: 1-1.5.
A preparation method of a mushroom cooking liquor extract feed additive comprises the following steps:
s1: cleaning Lentinus Edodes, air drying, and cutting into pieces;
s2: placing the cut mushrooms into an alcohol extraction tank, adding 95% ethanol which is 8-10 times of the total weight of the mushrooms, boiling for 7-8 hours under the steam pressure of 0.9-1 MPa, and extracting a primary liquid and filter residues;
s3: placing the filter residue in S2 in an alcohol extraction tank, adding 95% ethanol 1-2 times of the total weight of the filter residue, boiling for 1-2 hr under 0.9-1 MPa, and extracting the secondary solution and the filter residue;
s4: placing the filter residue in the step S3 in an alcohol extraction tank, adding 95% ethanol 1-2 times of the total weight of the filter residue, boiling for 1-2 hours under the vapor pressure of 0.9-1 MPa, extracting the tail liquid and the filter residue, and removing the filter residue;
s5: mixing the primary liquid, the secondary liquid and the tail liquid, distilling and concentrating to obtain an extract;
s6: putting the extract into an atomization drying machine for atomization drying, wherein the air inlet temperature is 190-;
s7: putting the powder, the preservative and the carrier into a stirring device together for stirring for 1-2 hours at the stirring temperature of 50-60 ℃ and the stirring pressure of 0.5-0.7 MPa, so that the powder, the preservative and the carrier are fully mixed together and put into a granulator for granulation;
s8: and (3) placing the prepared granules and the outer protective material into a mixer for rolling, wherein the rolling temperature is 30-45 ℃, so that the outer protective material is uniformly adhered to the surfaces of the granules, and the lentinus edodes extract additive is prepared.
Compared with the prior art, the invention has the beneficial effects that: the invention can effectively prevent the additive from losing efficacy caused by the erosion of water vapor in the storage process, and ensure the quality of the additive, the outer protective material is formed by mixing food-grade hydrophobic material and edible alkali, the outer protective material is coated on the outer layer of the additive, and the additive is prevented from being eroded by the water vapor through the hydrophobic material, so that the quality of the additive is effectively ensured.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The invention provides a mushroom cooking liquor extract feed additive which can effectively prevent the additive from losing efficacy caused by the erosion of water vapor in the storage process and ensure the quality of the additive, the mushroom extract feed additive is prepared from mushrooms, a carrier, a preservative and an outer protective material, wherein the carrier is prepared by mixing pine needle powder, attapulgite, silicon dioxide and maltodextrin in a weight ratio of 1:1-2:0.7-0.9:0.6-0.8, the preservative is monosodium fumarate, the outer protective material is prepared by mixing food-grade hydrophobic material and dietary alkali in a weight ratio of 1:1-1.5, the outer protective material is prepared by mixing food-grade hydrophobic material and dietary alkali, the outer protective material is coated on the outer layer of the additive, the hydrophobic material prevents the additive from being eroded by the water vapor, the quality of the additive is effectively ensured, and the dietary alkali is added into the outer protective material, after the additive is used by livestock, the edible alkali is neutralized with the gastric acid phase, so that the external protective material can be quickly decomposed, and the additive can be conveniently absorbed by the livestock.
The invention also provides a preparation method of the mushroom cooking liquor extract feed additive, which comprises the following steps:
s1: cleaning Lentinus Edodes, air drying, and cutting into pieces;
s2: placing the cut mushrooms into an alcohol extraction tank, adding 95% ethanol which is 8-10 times of the total weight of the mushrooms, boiling for 7-8 hours under the steam pressure of 0.9-1 MPa, and extracting a primary liquid and filter residues;
s3: placing the filter residue in S2 in an alcohol extraction tank, adding 95% ethanol 1-2 times of the total weight of the filter residue, boiling for 1-2 hr under 0.9-1 MPa, and extracting the secondary solution and the filter residue;
s4: placing the filter residue in the step S3 in an alcohol extraction tank, adding 95% ethanol 1-2 times of the total weight of the filter residue, boiling for 1-2 hours under the vapor pressure of 0.9-1 MPa, extracting the tail liquid and the filter residue, and removing the filter residue;
s5: mixing the primary liquid, the secondary liquid and the tail liquid, distilling and concentrating to obtain an extract;
s6: putting the extract into an atomization drying machine for atomization drying, wherein the air inlet temperature is 190-;
s7: putting the powder, the preservative and the carrier into a stirring device together for stirring for 1-2 hours at the stirring temperature of 50-60 ℃ and the stirring pressure of 0.5-0.7 MPa, so that the powder, the preservative and the carrier are fully mixed together and put into a granulator for granulation;
s8: and (3) placing the prepared granules and the outer protective material into a mixer for rolling, wherein the rolling temperature is 30-45 ℃, so that the outer protective material is uniformly adhered to the surfaces of the granules, and the lentinus edodes extract additive is prepared.
Example 1
S1: cleaning Lentinus Edodes, air drying, and cutting into pieces;
s2: placing the cut mushrooms into an alcohol extraction tank, adding 95% ethanol which is 8 times of the total weight of the mushrooms, boiling for 7 hours under the steam pressure of 0.9 MPa, and extracting a primary solution and filter residues;
s3: placing the filter residue in the S2 into an alcohol extraction tank, adding 95% ethanol 1 time of the total weight of the filter residue, boiling for 1 hour under the vapor pressure of 0.9 MPa, and extracting secondary liquid and the filter residue;
s4: placing the filter residue in the step S3 in an alcohol extraction tank, adding 95% ethanol 1 time of the total weight of the filter residue, boiling for 1 hour under the vapor pressure of 0.9 MPa, extracting the tail liquid and the filter residue, and removing the filter residue;
s5: mixing the primary liquid, the secondary liquid and the tail liquid, distilling and concentrating to obtain an extract;
s6: putting the extract into an atomization drying machine for atomization drying, wherein the air inlet temperature is 190 ℃, the air outlet temperature is 100 ℃, and powder is prepared;
s7: putting the powder, the preservative and the carrier into a stirring device together for stirring for 1 hour at the stirring temperature of 50 ℃ and under the stirring pressure of 0.5 MPa, so that the powder, the preservative and the carrier are fully mixed together and put into a granulator for granulation;
s8: the prepared particles and the outer protection material are placed in a mixer to be rolled, the temperature of the rolled material is 30 ℃, so that the outer protection material is uniformly adhered to the surfaces of the particles to prepare the mushroom extract additive, the outer protection material is coated on the outer layer of the additive, the additive is prevented from being corroded by water vapor through the hydrophobic material, the quality of the additive is effectively guaranteed, and dietary alkali is added into the outer protection material.
Example 2
S1: cleaning Lentinus Edodes, air drying, and cutting into pieces;
s2: placing the cut mushrooms into an alcohol extraction tank, adding 95% ethanol which is 8 times of the total weight of the mushrooms, boiling for 8 hours under the steam pressure of 0.9 MPa, and extracting a primary solution and filter residues;
s3: placing the filter residue in S2 in an alcohol extraction tank, adding 95% ethanol 1-2 times of the total weight of the filter residue, boiling for 2 hr under 1 MPa, and extracting the secondary liquid and the filter residue;
s4: placing the filter residue in the step S3 in an alcohol extraction tank, adding 95% ethanol 2 times of the total weight of the filter residue, boiling for 1 hour under the vapor pressure of 0.9 MPa, extracting the tail liquid and the filter residue, and removing the filter residue;
s5: mixing the primary liquid, the secondary liquid and the tail liquid, distilling and concentrating to obtain an extract;
s6: putting the extract into an atomization drying machine for atomization drying, wherein the air inlet temperature is 190 ℃, the air outlet temperature is 100 ℃, and powder is prepared;
s7: putting the powder, the preservative and the carrier into a stirring device together for stirring, wherein the stirring time is 2 hours, the stirring temperature is 50 ℃, and the stirring pressure is 0.7 MPa, so that the powder, the preservative and the carrier are fully mixed together and put into a granulator for granulation;
s8: the prepared particles and the outer protection material are placed in a mixer to be rolled, the rolling temperature is 45 ℃, so that the outer protection material is uniformly adhered to the surfaces of the particles to prepare the mushroom extract additive, the outer protection material is coated on the outer layer of the additive, the additive is prevented from being corroded by water vapor through the hydrophobic material, the quality of the additive is effectively guaranteed, and dietary alkali is added into the outer protection material, and after the mushroom extract additive is used by domestic animals, the dietary alkali is neutralized with gastric acid phase, so that the outer protection material can be quickly decomposed, and the additive can be conveniently absorbed by the domestic animals.
Example 3
S1: cleaning Lentinus Edodes, air drying, and cutting into pieces;
s2: placing the cut mushrooms into an alcohol extraction tank, adding 95 percent ethanol which is 10 times of the total weight of the mushrooms, boiling for 8 hours under the steam pressure of 1 MPa, and extracting a primary solution and filter residues;
s3: placing the filter residue in the S2 into an alcohol extraction tank, adding 95% ethanol 2 times of the total weight of the filter residue, boiling for 2 hours under the vapor pressure of 1 MPa, and extracting secondary liquid and the filter residue;
s4: placing the filter residue in the step S3 in an alcohol extraction tank, adding 95% ethanol 2 times of the total weight of the filter residue, boiling for 2 hours under the vapor pressure of 1 MPa, extracting the tail liquid and the filter residue, and removing the filter residue;
s5: mixing the primary liquid, the secondary liquid and the tail liquid, distilling and concentrating to obtain an extract;
s6: putting the extract into an atomization drying machine for atomization drying, wherein the air inlet temperature is 200 ℃, the air outlet temperature is 110 ℃, and powder is prepared;
s7: putting the powder, the preservative and the carrier into a stirring device together for stirring, wherein the stirring time is 2 hours, the stirring temperature is 60 ℃, and the stirring pressure is 0.7 MPa, so that the powder, the preservative and the carrier are fully mixed together and put into a granulator for granulation;
s8: the prepared particles and the outer protection material are placed in a mixer to be rolled, the rolling temperature is 45 ℃, so that the outer protection material is uniformly adhered to the surfaces of the particles to prepare the mushroom extract additive, the outer protection material is coated on the outer layer of the additive, the additive is prevented from being corroded by water vapor through the hydrophobic material, the quality of the additive is effectively guaranteed, and dietary alkali is added into the outer protection material, and after the mushroom extract additive is used by domestic animals, the dietary alkali is neutralized with gastric acid phase, so that the outer protection material can be quickly decomposed, and the additive can be conveniently absorbed by the domestic animals.
While the invention has been described above with reference to an embodiment, various modifications may be made and equivalents may be substituted for elements thereof without departing from the scope of the invention. In particular, the various features of the embodiments disclosed herein may be used in any combination, provided that there is no structural conflict, and the combinations are not exhaustively described in this specification merely for the sake of brevity and conservation of resources. Therefore, it is intended that the invention not be limited to the particular embodiments disclosed, but that the invention will include all embodiments falling within the scope of the appended claims.

Claims (5)

1. A shiitake mushroom cooking liquor extract feed additive is characterized in that: the shiitake mushroom extract feed additive is prepared from shiitake mushrooms, a carrier, a preservative and an external protection material.
2. The shiitake mushroom cooking liquor extract feed additive as claimed in claim 1, wherein the shiitake mushroom cooking liquor extract feed additive comprises: the carrier is formed by mixing pine needle powder, attapulgite, silicon dioxide and maltodextrin in a weight ratio of 1:1-2:0.7-0.9: 0.6-0.8.
3. The shiitake mushroom cooking liquor extract feed additive as claimed in claim 2, wherein the shiitake mushroom cooking liquor extract feed additive comprises: the preservative is monosodium fumarate.
4. The shiitake mushroom cooking liquor extract feed additive as claimed in claim 3, wherein the shiitake mushroom cooking liquor extract feed additive comprises: the outer protective material is formed by mixing food-grade hydrophobic material and edible alkali, and the weight ratio of the food-grade hydrophobic material to the edible alkali is 1: 1-1.5.
5. A method for preparing a shiitake mushroom extract feed additive according to claim 1, characterized in that: the preparation method of the mushroom extract feed additive comprises the following steps:
s1: cleaning Lentinus Edodes, air drying, and cutting into pieces;
s2: placing the cut mushrooms into an alcohol extraction tank, adding 95% ethanol which is 8-10 times of the total weight of the mushrooms, boiling for 7-8 hours under the steam pressure of 0.9-1 MPa, and extracting a primary liquid and filter residues;
s3: placing the residue in S2 in an alcohol extraction tank, adding 95% ethanol 1-2 times of the total weight of the residue, boiling for 1-2 hr under 0.9-1 MPa, and extracting the secondary solution and residue;
s4: placing the filter residue in the step S3 in an alcohol extraction tank, adding 95% ethanol 1-2 times of the total weight of the filter residue, boiling for 1-2 hours under the vapor pressure of 0.9-1 MPa, extracting the tail liquid and the filter residue, and removing the filter residue;
s5: mixing the primary liquid, the secondary liquid and the tail liquid, distilling and concentrating to obtain an extract;
s6: putting the extract into an atomization drying machine for atomization drying, wherein the air inlet temperature is 190-;
s7: putting the powder, the preservative and the carrier into a stirring device together for stirring for 1-2 hours at the stirring temperature of 50-60 ℃ and the stirring pressure of 0.5-0.7 MPa, so that the powder, the preservative and the carrier are fully mixed together and put into a granulator for granulation;
s8: and (3) placing the prepared granules and the outer protective material into a mixer for rolling, wherein the rolling temperature is 30-45 ℃, so that the outer protective material is uniformly adhered to the surfaces of the granules, and the lentinus edodes extract additive is prepared.
CN202210233426.6A 2022-03-10 2022-03-10 Mushroom cooking liquor extract feed additive and preparation method thereof Pending CN114468132A (en)

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Application Number Priority Date Filing Date Title
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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102144726A (en) * 2010-02-08 2011-08-10 上海农昊生物技术研究所 Mushroom extract feed additive and preparation method thereof
CN103599082A (en) * 2013-04-05 2014-02-26 黑龙江福和华星制药集团股份有限公司 Omeprazole and sodium bicarbonate core-covering tablet
CN107535717A (en) * 2017-09-07 2018-01-05 高计会 It is a kind of to be used to treat solid feed of rabbit diarrheb and preparation method thereof
CN108782968A (en) * 2018-07-28 2018-11-13 厦门同欣荣饲料科技有限公司 A kind of rheum officinale fish meal and preparation method thereof
CN110463849A (en) * 2019-08-28 2019-11-19 隋传吉 A kind of feed for pet and its manufacture craft

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102144726A (en) * 2010-02-08 2011-08-10 上海农昊生物技术研究所 Mushroom extract feed additive and preparation method thereof
CN103599082A (en) * 2013-04-05 2014-02-26 黑龙江福和华星制药集团股份有限公司 Omeprazole and sodium bicarbonate core-covering tablet
CN107535717A (en) * 2017-09-07 2018-01-05 高计会 It is a kind of to be used to treat solid feed of rabbit diarrheb and preparation method thereof
CN108782968A (en) * 2018-07-28 2018-11-13 厦门同欣荣饲料科技有限公司 A kind of rheum officinale fish meal and preparation method thereof
CN110463849A (en) * 2019-08-28 2019-11-19 隋传吉 A kind of feed for pet and its manufacture craft

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