CN114405431B - Multi-connected chemical synthesis reactor - Google Patents
Multi-connected chemical synthesis reactor Download PDFInfo
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- CN114405431B CN114405431B CN202210075669.1A CN202210075669A CN114405431B CN 114405431 B CN114405431 B CN 114405431B CN 202210075669 A CN202210075669 A CN 202210075669A CN 114405431 B CN114405431 B CN 114405431B
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- 238000003786 synthesis reaction Methods 0.000 title claims abstract description 12
- 239000007788 liquid Substances 0.000 claims abstract description 117
- 238000006243 chemical reaction Methods 0.000 claims abstract description 66
- 230000005540 biological transmission Effects 0.000 claims abstract description 29
- 239000002699 waste material Substances 0.000 claims abstract description 18
- 238000007599 discharging Methods 0.000 claims abstract description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 21
- 229910001868 water Inorganic materials 0.000 claims description 21
- 238000001125 extrusion Methods 0.000 claims description 5
- 238000004064 recycling Methods 0.000 claims 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract description 54
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 abstract description 38
- 239000001569 carbon dioxide Substances 0.000 abstract description 19
- 229910002092 carbon dioxide Inorganic materials 0.000 abstract description 19
- 239000013049 sediment Substances 0.000 abstract description 11
- 238000011084 recovery Methods 0.000 abstract description 7
- 239000000243 solution Substances 0.000 description 44
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 18
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 10
- 239000004579 marble Substances 0.000 description 10
- 229910000019 calcium carbonate Inorganic materials 0.000 description 9
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 7
- 239000012528 membrane Substances 0.000 description 7
- 238000002156 mixing Methods 0.000 description 6
- 239000001110 calcium chloride Substances 0.000 description 5
- 229910001628 calcium chloride Inorganic materials 0.000 description 5
- 229910000029 sodium carbonate Inorganic materials 0.000 description 5
- 238000003756 stirring Methods 0.000 description 5
- 230000001105 regulatory effect Effects 0.000 description 4
- 230000005484 gravity Effects 0.000 description 3
- 238000010030 laminating Methods 0.000 description 3
- 239000007789 gas Substances 0.000 description 2
- 239000011259 mixed solution Substances 0.000 description 2
- 238000003825 pressing Methods 0.000 description 2
- 238000005096 rolling process Methods 0.000 description 2
- 239000011550 stock solution Substances 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 238000003723 Smelting Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005242 forging Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 239000002912 waste gas Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
- B01J19/20—Stationary reactors having moving elements inside in the form of helices, e.g. screw reactors
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J14/00—Chemical processes in general for reacting liquids with liquids; Apparatus specially adapted therefor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J16/00—Chemical processes in general for reacting liquids with non- particulate solids, e.g. sheet material; Apparatus specially adapted therefor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/002—Avoiding undesirable reactions or side-effects, e.g. avoiding explosions, or improving the yield by suppressing side-reactions
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/50—Carbon dioxide
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The invention relates to the technical field of chemical synthesis, in particular to a multi-connected chemical synthesis reactor, which comprises a reaction device, wherein the section of the reaction device is a shell, a waste residue recovery box is fixed at the left side of the inside of the bottom end of the shell, a waste liquid recovery box is fixed in the middle of the inside of the bottom end of the shell, a discharging mechanism is fixedly connected above the waste liquid recovery box, a screw shaft and a pushing rod are respectively arranged at the left side and the right side of the discharging mechanism, two ends of the screw shaft and the pushing rod respectively penetrate through the shell, the right end of the discharging mechanism is movably connected with a transmission mechanism, the upper end of the transmission mechanism is connected with an air pipe of the reaction box through a piston, a liquid storage box is fixed at the top of the reaction box, and a liquid outlet pipe in the liquid storage mechanism is fixedly connected at the left side of the liquid storage box. The sediment can react with part of hydrochloric acid in the solution, carbon dioxide generated by the reaction can flow back to the reaction box along with the liquid containing pipe, the air outlet pipe flows out, and then the air is collected, so that the sediment in the solution can be reacted again, carbon dioxide is generated, and the carbon dioxide is recycled.
Description
Technical Field
The invention relates to the technical field of chemical synthesis, in particular to a multi-connection chemical synthesis reactor.
Background
The existing chemical reaction synthesizer mainly aims at chemical reaction, caCO 3 +2HCL＝CO 2 ↑+H 2 O+CaCl 2 The carbon dioxide is collected and metered to be extracted, the collected carbon dioxide is pure, the carbon dioxide produced at present is high-temperature forged calcium carbonate, waste gas generated after combustion is easy to harm the environment while resources are utilized, the purity of the carbon dioxide generated by forging the calcium carbonate is not high, and the calcination of the calcium carbonate can generate reducing carbon in a smelting furnace, so that certain potential safety hazard exists.
Disclosure of Invention
Aiming at the problems in the prior art, the invention provides a multi-connected chemical synthesis reactor.
The technical scheme adopted for solving the technical problems is as follows: the utility model provides a many allies oneself with chemical synthesis reactor, includes reaction unit, reaction unit section is the shell, the inside left side fixed waste residue of bottom of shell retrieves the box, the inside middle fixed waste liquid of bottom of shell retrieves the box, and the outer end right side of reaction unit is being connected a motor, the top fixed connection discharge mechanism of box is retrieved to the waste liquid, screw axis and ejector pin are installed respectively on the left side and the right side of discharge mechanism, and see screw axis and ejector pin's both ends head and pass the shell respectively, the right-hand member swing joint drive mechanism of discharge mechanism, the drive mechanism upper end is connected through the air pipe of piston and reaction box, the fixed receiver in top of reaction box, the drain pipe in the left side fixed connection receiver of receiver.
Preferably, the reaction box comprises a liquid storage box, the air pipe is connected at liquid storage box top fixedly, and the drain pipe in the left side fixed connection stock solution mechanism of liquid storage box, the fluid-discharge tube is being connected to the lower extreme of liquid storage box, the fluid-discharge tube is located the inside of reaction box, the left and right sides of fluid-discharge tube is standing to hold the box, and holds the bottom of box and be fixed in the bottom of reaction box, hold the outside of box and offer a hole all around, a filter screen is fixed in the hole inside, the top right side of the inside of reaction box is even fixedly connected with the outlet duct, the lower extreme swing joint rotary drum of reaction box, no. two holes have been seted up to the semi-cylindrical surface of rotary drum, no. two filter screens are installed to the inboard in No. two holes, the rotary drum below is being connected with the liquid-holding tube.
Preferably, the liquid containing pipe lower extreme fixed connection ejection of compact box, the (mixing) shaft is being connected to inside intermediate junction of ejection of compact box, the left side inner wall at the inside intermediate position of ejection of compact box is connected to the left side one end of (mixing) shaft, and the transmission shaft of intermediate position in ejection of compact box is connected to the one end on the right side of (mixing) shaft, the notch has been seted up at the top of ejection of compact box, and the left side at the top of ejection of compact box is connected the inlet pipe, screw axis and pushing rod are installed respectively in the bottom left side and the right side of ejection of compact box, screw axis intermediate position is equipped with the internal screw thread.
Preferably, the ejector pin is being connected on ejector pin right side, ejector pin right-hand member laminating No. one is taking out the pole, no. one is taking out the pole inside and is being fixed No. two ejector pins, no. two ejector pins right-hand member laminating No. two are taking out the pole, no. one is taking out pole and No. two is taking out pole left side port departments and is being fixed with the movable block, the movable block below is fixed with extrusion spring, no. one is taking out pole and No. two is taking out pole right side port punishment and is equipped with the locating hole.
Preferably, the left end of the transmission shaft is fixedly connected with a first motor, the right end of the transmission shaft is fixedly connected with a second belt pulley, a crankshaft is fixedly connected between the transmission shaft and the second belt pulley, the crankshaft is movably connected with a push rod, the upper end of the push rod is fixedly connected with a piston, two sides of the piston are clung to a plug wall, an air inlet is vertically arranged at the right end of the plug wall, the air inlet penetrates through a shell, a belt is in rolling connection with the upper part of the second belt pulley, the other end of the belt is connected with the first belt pulley, and the first belt pulley is movably connected with a rotary drum.
Preferably, the drain pipe one end fixed connection liquid storage box, and the other end fixed connection water pump, the feed liquor pipe is being connected to water pump below fixed connection, and the feed liquor pipe passes the liquid reserve tank, top, and the end department laminating liquid reserve tank's of feed liquor pipe bottom, water pump and No. two motor fixed connection, no. two motor fixed placement in the top of liquid reserve tank.
The invention has the beneficial effects that:
(1) When the solution in the liquid containing tube starts to flow into the discharging box from two sides, excessive sodium carbonate solution exists in the discharging box, at the moment, the sodium carbonate solution reacts with the calcium chloride solution to regenerate calcium carbonate sediment, the mixed solution in the discharging box is stirred along with a stirring shaft in a transmission mechanism under the drive of a first motor, so that the solution can quickly generate calcium carbonate sediment, and because hydrochloric acid solution exists in the discharging box, after the calcium carbonate sediment is generated, the sediment reacts with part of hydrochloric acid in the solution, carbon dioxide generated by the reaction flows back into the reaction box along with the liquid containing tube again and flows out through an air outlet pipe, and then gas is collected, so that the sediment in the solution is conveniently reacted again to generate carbon dioxide, and the carbon dioxide is recycled.
(2) According to the invention, a certain amount of marble blocks are put into the accommodating box in the reaction box, the second motor is started, the water pump is driven to rotate by the second motor, the hydrochloric acid solution starts to be extracted from the liquid storage box, the hydrochloric acid solution is sent into the liquid storage box through the liquid outlet pipe, the hydrochloric acid solution in the liquid storage box starts to be collected towards the liquid outlet pipe, and the hydrochloric acid solution starts to drop downwards under the action of gravity, then the hydrochloric acid solution starts to perform chemical reaction with the marble blocks in the accommodating box to generate carbon dioxide, calcium chloride and water, and carbon dioxide generated by the reaction is converged in the reaction box and then converged to the top and is discharged from the air outlet pipe at the right end of the top of the reaction box, so that dangerous generation can be effectively avoided.
Drawings
The invention is further illustrated by the following figures in conjunction with the accompanying drawings and examples.
FIG. 1 is a schematic diagram of the overall structure of the present invention;
FIG. 2 is a cross-sectional view of the reaction apparatus shown in FIG. 1;
FIG. 3 is a schematic view of the containment box mechanism of FIG. 2;
FIG. 4 is a schematic view of the drum mechanism shown in FIG. 2;
FIG. 5 is an enlarged view of the portion A shown in FIG. 2;
FIG. 6 is an enlarged view at B shown in FIG. 2;
FIG. 7 is a schematic view of the screw shaft mechanism shown in FIG. 2;
FIG. 8 is a schematic view of the moving block mechanism shown in FIG. 2;
in the figure: 1. a reaction device; 11. a housing; 12. a waste residue recovery box; 13. a waste liquid recovery box; 14. a motor I; 2. a reaction cassette; 21. a liquid storage box; 22. a liquid discharge pipe; 23. a housing case; 231. a first filter screen; 232. a first hole; 24. an air outlet pipe; 25. a rotating drum; 251. a second filter screen; 252. a second hole; 26. an air tube; 3. a discharging mechanism; 31. a discharge box; 32. a stirring shaft; 33. a screw shaft; 331. an internal thread; 34. a pushing rod; 341. a first drawing rod; 342. a second drawing rod; 343. a first ejector rod; 344. a second ejector rod; 345. a moving block; 346. extruding a spring; 347. positioning holes; 35. a feed pipe; 36. a liquid containing tube; 4. a transmission mechanism; 41. a transmission shaft; 42. a push rod; 43. a first belt wheel; 44. a second belt wheel; 45. a belt; 46. an air inlet; 461. a piston; 462. a stopper wall; 47. a crankshaft; 5. a liquid storage mechanism; 51. a motor II; 52. a water pump; 53. a liquid inlet pipe; 54. a liquid outlet pipe; 55. a liquid storage tank.
Detailed Description
The technical means, the creation features, the achievement of the purpose and the effect of the present invention are easy to understand, and are further described below in connection with the specific embodiments.
As shown in fig. 1 to 8, the multi-joint chemical synthesis reactor of the present invention is characterized in that: including reaction unit 1, reaction unit 1 section is shell 11, the inside left side fixed waste residue of bottom of shell 11 retrieves box 12, the inside middle fixed waste liquid of bottom of shell 11 retrieves box 13, and the outer end right side of reaction unit 1 is being connected with motor number one 14, the top fixed connection discharge mechanism 3 of box 13 is retrieved to waste liquid, screw shaft 33 and pushing rod 34 are installed respectively on the left side and the right side of discharge mechanism 3, and see screw shaft 33 and pushing rod 34's both ends head and pass shell 11 respectively, the right-hand member swing joint drive mechanism 4 of discharge mechanism 3, drive mechanism 4 upper end is connected through piston 461 and reaction box 2's air tube 26, the fixed receiver 21 in top of reaction box 2, the left side fixed connection of receiver 21 goes out the liquid pipe 54 in the receiver 5.
Specifically, the reaction box 2 includes the liquid storage box 21, the air pipe 26 is connected at liquid storage box 21 top fixed connection, and the drain pipe 54 in the left side fixed connection stock solution mechanism 5 of liquid storage box 21, the drain pipe 22 is being connected to the lower extreme of liquid storage box 21, the drain pipe 22 is located the inside of reaction box 2, the left and right sides of drain pipe 22 is standing and is holding box 23, and holds the bottom of box 23 and be fixed in the bottom of reaction box 2, hold the outside of box 23 and offer a hole 232 all around, a hole 232 internally fixed filter screen 231, the top right side of the inside of reaction box 2 is even fixedly connected with outlet duct 24, the lower extreme swing joint rotary drum 25 of reaction box 2, no. two holes 252 have been seted up to rotary drum 25 semicircle face, no. two filter screens 251 are installed to the inboard of No. two holes 252, rotary drum 25 below is being connected with liquid holding pipe 36. During specific operation, firstly marble blocks need to be put into the accommodating box 23 from the second inlet on the right side of the top of the reaction device 1, a certain amount of marble blocks need to be put into the accommodating box 23 in the reaction box 2, afterwards, the water pump 52 is driven to rotate by the second motor 51 through the second motor 51, the hydrochloric acid solution is pumped from the liquid storage tank 55 through the liquid outlet pipe 54 and is fed into the liquid storage box 21, then the hydrochloric acid solution in the liquid storage box 21 begins to be converged towards the liquid discharge pipe 22, under the action of gravity, and begins to drop downwards, then the hydrochloric acid solution begins to react with the marble blocks accommodating the box 23 to generate carbon dioxide, calcium chloride and water, because the top of the reaction box 2 is closed, carbon dioxide generated by the reaction converges in the reaction box 2, then converges to the top, and begins to be discharged from the air outlet pipe 24 on the right end of the top of the reaction box 2, but as the reaction box 2 is reacted, the solution of calcium chloride and water is generated, the rotary drum 25 is driven to rotate through the transmission mechanism 4, one surface of the rotary drum 25 is closed, when the rotary drum 25 is turned to the surface, the hydrochloric acid solution does not flow into the liquid inlet pipe 36, and the liquid outlet pipe 36 is also can not flow into the liquid outlet pipe 36, and the liquid outlet pipe 36 is connected to the liquid outlet pipe 36, and the liquid flow into the liquid inlet pipe 36.
Specifically, the liquid containing tube 36 lower extreme fixed connection ejection of compact box 31, the (mixing) shaft 32 is being connected to the inside intermediate junction of ejection of compact box 31, the left side inner wall at the inside intermediate position of ejection of compact box 31 is being connected to the left side one end of (mixing) shaft 32, and the transmission shaft 41 in the intermediate position of ejection of compact box 31 is connected to the one end on the right side of (mixing) shaft 32, the notch has been seted up at the top of ejection of compact box 31, and the left side at the top of ejection of compact box 31 is connected inlet pipe 35, screw shaft 33 and pushing rod 34 are installed respectively to the bottom left side and the right side of ejection of compact box 31, screw shaft 33 intermediate position is equipped with internal thread 331. When the marble is added from the right end of the top of the reaction device 1, the mixed sodium carbonate solution is added at the left inlet, so when the solution in the liquid containing tube 36 flows into the discharge box 31 from both sides, excessive sodium carbonate solution exists in the discharge box 31, at the moment, the sodium carbonate solution reacts with the calcium chloride solution to regenerate calcium carbonate sediment, the mixed solution in the discharge box 31 is stirred along with the stirring shaft 32 in the transmission mechanism 4 under the drive of the motor No. 1, the solution can be quickly generated into calcium carbonate sediment, hydrochloric acid solution also exists in the discharge box 31, after the calcium carbonate sediment is generated, the sediment can react with part of hydrochloric acid in the solution, carbon dioxide generated by the reaction can flow back into the reaction box 2 along with the liquid containing tube 36, and flows out through the air outlet tube 24, then gas is collected, after one end time, the left side of the bottom of the discharge box 31 is screwed with a rotation, the screw shaft 33 is screwed out from the inside of the internal thread 331, the screw shaft 33 is pushed out from the end of the screw shaft 33 to the end of the screw shaft, at the moment, the screw shaft is pushed out of the screw shaft 33 is pushed against the end of the screw shaft, at the moment, the screw shaft is pushed out of the screw shaft 33 is pushed out, the screw shaft is pushed into the notch 13, the filter membrane is pushed out, the waste liquid enters the filter membrane 13, and flows into the filter membrane through the notch, and flows into the filter membrane 13, and flows into the filter membrane, and enters the filter membrane, and flows into the filter membrane.
Specifically, the right side of the pushing rod 34 is connected with a first ejector rod 343, the right end of the first ejector rod 343 is attached to a first drawing rod 341, a second ejector rod 344 is fixed inside the first drawing rod 341, the right end of the second ejector rod 344 is attached to a second drawing rod 342, moving blocks 345 are fixed at left side ports of the first drawing rod 341 and the second drawing rod 342, extrusion springs 346 are fixed below the moving blocks 345, and positioning holes 347 are respectively formed at right side ports of the first drawing rod 341 and the second drawing rod 342. In particular, when the collected carbon dioxide is sufficient, the device stops working, at this time, by manually starting to screw the screw shaft 33, the screw shaft 33 is screwed out to the outside around the internal thread 331, the end of the screw shaft 33 is from the starting abutting notch to the leaking notch, the notch is continuously increased along with the continuous screwing, the screwing is stopped after a period of time, the solution in the discharging box 31 is continuously flowed from the notch to the waste liquid recovery box 13, then, the second suction rod 342 is started to be withdrawn again, when the second suction rod 342 is horizontally moved to the right side inside the first suction rod 341, the end moving block 345 of the second suction rod 342 is pressed against the first suction rod 341 due to the pressing of the internal pressing spring 346, with the right movement of the second drawer 342 until the moving block 345 at the end of the second drawer starts to be inserted into the positioning hole 347 of the first drawer 341, at this time, the second drawer 342 and the first drawer 341 are integrated, and similarly, when the moving block 345 at one end of the first drawer 341 moves to the right until the moving block 345 of the first drawer 341 starts to be inserted into the positioning hole 347 on the right side of the pushing rod 34, at this time, the pushing rod 34, the first drawer 341 and the second drawer 342 are coupled into a whole, at this time, by pushing the second drawer 342, the end of the pushing rod 34 is moved to the left, some of the precipitated particles and larger precipitates in the discharge box 31 are pushed to move to the notch, and then drop to the waste residue recovery box 12.
Specifically, the left end of the transmission shaft 41 is fixedly connected with the first motor 14, the right end of the transmission shaft is fixedly connected with the second belt pulley 44, a crankshaft 47 is fixedly connected between the transmission shaft 41 and the second belt pulley 44, the end of the crankshaft 47 is movably connected with a push rod 42, the upper end of the push rod 42 is fixedly connected with a piston 461, two sides of the piston 461 are tightly attached to a plug wall 462, an air inlet 46 is vertically arranged at the right end of the plug wall 462, the air inlet 46 penetrates through the shell 11, a belt 45 is connected above the second belt pulley 44 in a rolling manner, the other end of the belt 45 is connected with the first belt pulley 43, and the first belt pulley 43 is movably connected with the rotary drum 25. When the liquid storage box 21 starts to be injected with hydrochloric acid solution, the first motor 14 is started, the first motor 14 drives the transmission shaft 41 to start to rotate, the transmission shaft 41 drives the crankshaft 47 to rotate, the crankshaft 47 is sleeved with the movable push rod 42, the other end of the push rod 42 is connected with the movable piston 461, when the transmission shaft 41 rotates, the crankshaft 47 rotates up and down in the circumferential direction, the crankshaft 47 moves the piston 461 up and down in a reciprocating manner through the push rod 42, the right side of the piston 461 is provided with the row of air inlets 46, so that the air pressure in the liquid storage box 21 can be regulated, the piston 461 moves up and down in a reciprocating manner under the driving of the crankshaft 47, on the one hand, the air pressure of the air pipe 26 can be controlled, on the other hand, the air inlet 46 can be blocked during upward extrusion, so that the air pressure of the air pipe 26 is controlled by the piston 461, the speed of the piston 461 can be regulated, the hydrochloric acid flow can be regulated, the rotation of the stirring shaft 32 in the discharging box 31 can be driven along with the rotation of the first motor 14, the solution in the discharging box 31 can be fully reacted, the inner solution can be further rotated, the transmission shaft 41 can be driven by the belt 45 to rotate the rotary drum 25, the rotary drum 25 can be controlled, and the volume of the liquid can be further controlled, and the flow of the rotary drum 25 can be controlled, and the volume of the liquid can be further controlled, and the rotary drum 25 can be further controlled, and the volume can be controlled.
Specifically, one end of the liquid outlet pipe 54 is fixedly connected with the liquid storage box 21, the other end of the liquid outlet pipe is fixedly connected with the water pump 52, the lower part of the water pump 52 is fixedly connected with the liquid inlet pipe 53, the liquid inlet pipe 53 penetrates through the liquid storage box 55, the top of the liquid inlet pipe 53 is attached to the bottom of the liquid storage box 55, the water pump 52 is fixedly connected with the motor No. two 51, and the motor No. two 51 is fixedly arranged at the top of the liquid storage box 55. In specific operation, after a certain amount of marble is added into the accommodating box 23, at this time, the second motor 51 is turned on, the second motor 51 drives the water pump 52 to operate, at this time, the water pump 52 starts to extract the hydrochloric acid solution from the liquid storage tank 55, and then the hydrochloric acid solution is sent into the liquid storage box 21 through the liquid outlet pipe 54, so as to continuously provide the hydrochloric acid solution for the liquid storage box 21.
The working principle of the multi-connected chemical synthesis reactor provided by the invention is as follows:
firstly, marble blocks need to be placed into the accommodating box 23 from the second inlet on the right side of the top of the reaction device 1, a certain amount of marble blocks need to be placed into the accommodating box 23 in the reaction box 2, then, the water pump 52 is driven to rotate by the second motor 51 through the second motor 51, the hydrochloric acid solution is started to be extracted from the liquid storage box 55 by the water pump 52 and is sent into the liquid storage box 21 through the liquid outlet pipe 54, then, the hydrochloric acid solution in the liquid storage box 21 starts to be collected towards the liquid discharge pipe 22, under the action of gravity, and begins to drop downwards, then, the hydrochloric acid solution starts to perform chemical reaction with the marble blocks accommodating box 23, carbon dioxide, calcium chloride and water are generated by the reaction, the carbon dioxide generated by the reaction is converged in the reaction box 2, then, the carbon dioxide is converged at the top, the air outlet pipe 24 at the right end of the top of the reaction box 2 is started to be discharged, but as the reaction box 2 is performed, the solution of calcium chloride and water is generated, the solution is driven to rotate by the transmission mechanism 4, one surface of the liquid storage box 25 is closed, when the reaction box 2 is rotated to the closed, the hydrochloric acid solution is enabled to flow into the liquid outlet pipe 36 through the liquid inlet pipe 36, the liquid outlet pipe 36 is opened to the liquid outlet pipe 36, the hydrochloric acid solution is not enabled to flow into the liquid outlet pipe 36, and the liquid outlet pipe 36 is connected to the liquid outlet pipe 36 is opened to the liquid outlet pipe 36, and the liquid flow into the liquid outlet pipe 36.
In addition, when the solution storage box 21 starts to be injected with the hydrochloric acid solution, the first motor 14 is started, the first motor 14 drives the transmission shaft 41 to start to rotate, the transmission shaft 41 drives the crankshaft 47 to rotate, the crankshaft 47 is sleeved with the movable push rod 42, the other end of the push rod 42 is connected with the movable piston 461, when the transmission shaft 41 rotates, the crankshaft 47 rotates up and down circumferentially, the crankshaft 47 reciprocates the piston 461 up and down through the push rod 42, as the right side of the piston 461 is provided with the row of air inlets 46, the air pressure inside the solution storage box 21 can be regulated, so that the descending speed of the hydrochloric acid solution is controlled, the piston 461 is driven by the crankshaft 47 to reciprocate up and down, on the one hand, the air pressure of the air pipe 26 can be controlled, on the other hand, the air inlet 46 can be blocked during upward extrusion, so that the air pressure of the air pipe 26 is controlled by the piston 461, the adjustment of the speed of the piston 461 can be realized, the adjustment of the flow of the hydrochloric acid can be realized, the rotation of the stirring shaft 32 inside the discharge box 31 can be driven along with the rotation of the first motor 14, the solution inside the discharge box 31 is fully reacted, the inner solution can be driven to rotate, and the transmission shaft 41 can be driven to rotate through the belt 45, so that the flow of the liquid can be further controlled to flow into the rotary drum 25, and the discharge box 25 can be further controlled, and the flow of the discharge box can be controlled, and the flow of the liquid can be further controlled, and the flow and the volume of the discharge box can be controlled, and the flow can be controlled, and the volume can be controlled.
The foregoing has shown and described the basic principles, principal features and advantages of the invention. It will be understood by those skilled in the art that the present invention is not limited to the foregoing examples, and that the foregoing description and description are merely illustrative of the principles of this invention, and various changes and modifications may be made without departing from the spirit and scope of the invention, which is defined in the appended claims. The scope of the invention is defined by the appended claims and equivalents thereof.
Claims (2)
1. A multiple chemical synthesis reactor, characterized by: the waste liquid recycling device comprises a reaction device (1), wherein the section of the reaction device (1) is a shell (11), a waste residue recycling box (12) is fixed at the left side inside the bottom end of the shell (11), a waste liquid recycling box (13) is fixed in the middle inside the bottom end of the shell (11), a first motor (14) is connected to the right side of the outer end of the reaction device (1), a discharging mechanism (3) is fixedly connected to the upper side of the waste liquid recycling box (13), a screw shaft (33) and a pushing rod (34) are respectively arranged at the left side and the right side of the discharging mechanism (3), two ends of the screw shaft (33) and the pushing rod (34) are seen to penetrate through the shell (11) respectively, a transmission mechanism (4) is movably connected to the right end of the discharging mechanism (3), the upper end of the transmission mechanism (4) is connected with an air pipe (26) of the reaction box (2) through a piston (461), a liquid storage box (21) is fixed at the top of the reaction box (2), and a liquid pipe (54) in a liquid storage mechanism (5) is fixedly connected to the left side of the liquid storage box (21).
The reaction box (2) comprises a liquid storage box (21), an air pipe (26) is fixedly connected to the top of the liquid storage box (21), a liquid outlet pipe (54) in a liquid storage mechanism (5) is fixedly connected to the left side of the liquid storage box (21), a liquid discharge pipe (22) is connected to the lower end of the liquid storage box (21), the liquid discharge pipe (22) is located inside the reaction box (2), a containing box (23) is vertically arranged on the left side and the right side of the liquid discharge pipe (22), the bottom of the containing box (23) is fixed to the bottom of the reaction box (2), a first hole (232) is formed in the periphery of the outer side of the containing box (23), a first filter screen (231) is fixed inside the first hole (232), a second hole (252) is fixedly connected to the right side of the top end of the inside of the reaction box (2), a second hole (252) is formed in a semi-cylindrical surface of the rotary drum (25), a second filter screen (251) is mounted on the inner side of the second hole (252), and the second filter screen (251) is connected to the lower side of the rotary drum (25).
The liquid containing tube (36) lower extreme fixed connection ejection of compact box (31), inside intermediate junction (mixer shaft (32) of ejection of compact box (31), the left side inner wall in the inside intermediate position of ejection of compact box (31) is connected to left side one end of mixer shaft (32), and the transmission shaft (41) in the intermediate position of ejection of compact box (31) is connected to the one end on the right side of mixer shaft (32), the notch has been seted up at the top of ejection of compact box (31), and inlet pipe (35) are connected on the left side at the top of ejection of compact box (31), screw shaft (33) and pushing rod (34) are installed respectively to the bottom left side and the right side of ejection of compact box (31), screw shaft (33) intermediate position is equipped with internal thread (331);
the right side of the pushing rod (34) is connected with a first ejector rod (343), the right end of the first ejector rod (343) is attached to a first drawing rod (341), a second ejector rod (344) is fixed inside the first drawing rod (341), the right end of the second ejector rod (344) is attached to a second drawing rod (342), moving blocks (345) are fixed at the left side ports of the first drawing rod (341) and the second drawing rod (342), extrusion springs (346) are fixed below the moving blocks (345), and positioning holes (347) are respectively formed in the right side ports of the first drawing rod (341) and the second drawing rod (342);
the utility model discloses a motor (14) is fixed connection in transmission shaft (41) left end, no. two band pulleys (44) are fixed connection in the right-hand member, fixed connection bent axle (47) in the middle of transmission shaft (41) and No. two band pulleys (44), bent axle (47) end swing joint push rod (42), piston (461) are fixed connection in push rod (42) upper end, and piston (461) both sides are hugged closely and are stopped up wall (462), vertical range air inlet (46) of stopper wall (462) right-hand member, and air inlet (46) pass shell (11), no. two band pulleys (44) top roll connection belt (45), no. one band pulley (43) are connected to the other end of belt (45), no. one band pulley (43) and rotary drum (25) swing joint.
2. A multiple chemical synthesis reactor according to claim 1, wherein: the drain pipe (54) one end fixedly connected with liquid storage box (21), and other end fixed connection water pump (52), liquid inlet pipe (53) are connected to water pump (52) below fixed connection, and liquid inlet pipe (53) pass liquid reserve tank (55), the top, and the bottom of liquid reserve tank (55) is laminated to the end department of liquid inlet pipe (53), water pump (52) and No. two motor (51) fixed connection, and No. two motor (51) fixed place in the top of liquid reserve tank (55).
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| CN202210075669.1A CN114405431B (en) | 2022-01-22 | 2022-01-22 | Multi-connected chemical synthesis reactor |
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| CN114405431A (en) | 2022-04-29 |
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