CN114149872A - 一种新型洗衣粉及其制备方法 - Google Patents
一种新型洗衣粉及其制备方法 Download PDFInfo
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- 239000000843 powder Substances 0.000 title claims abstract description 73
- 238000005406 washing Methods 0.000 title claims abstract description 53
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 239000002245 particle Substances 0.000 claims abstract description 24
- 239000002250 absorbent Substances 0.000 claims abstract description 17
- 230000002745 absorbent Effects 0.000 claims abstract description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 17
- 239000003963 antioxidant agent Substances 0.000 claims abstract description 15
- 230000003078 antioxidant effect Effects 0.000 claims abstract description 15
- 239000000835 fiber Substances 0.000 claims abstract description 15
- 239000004367 Lipase Substances 0.000 claims abstract description 13
- 102000004882 Lipase Human genes 0.000 claims abstract description 13
- 108090001060 Lipase Proteins 0.000 claims abstract description 13
- 229910000503 Na-aluminosilicate Inorganic materials 0.000 claims abstract description 13
- 108091005804 Peptidases Proteins 0.000 claims abstract description 13
- 239000004365 Protease Substances 0.000 claims abstract description 13
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 claims abstract description 13
- GVGUFUZHNYFZLC-UHFFFAOYSA-N dodecyl benzenesulfonate;sodium Chemical compound [Na].CCCCCCCCCCCCOS(=O)(=O)C1=CC=CC=C1 GVGUFUZHNYFZLC-UHFFFAOYSA-N 0.000 claims abstract description 13
- PMYUVOOOQDGQNW-UHFFFAOYSA-N hexasodium;trioxido(trioxidosilyloxy)silane Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[O-][Si]([O-])([O-])O[Si]([O-])([O-])[O-] PMYUVOOOQDGQNW-UHFFFAOYSA-N 0.000 claims abstract description 13
- 235000019421 lipase Nutrition 0.000 claims abstract description 13
- 239000002736 nonionic surfactant Substances 0.000 claims abstract description 13
- 229920001467 poly(styrenesulfonates) Polymers 0.000 claims abstract description 13
- 229940051841 polyoxyethylene ether Drugs 0.000 claims abstract description 13
- 229920000056 polyoxyethylene ether Polymers 0.000 claims abstract description 13
- 235000012217 sodium aluminium silicate Nutrition 0.000 claims abstract description 13
- 239000000429 sodium aluminium silicate Substances 0.000 claims abstract description 13
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000001509 sodium citrate Substances 0.000 claims abstract description 13
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 claims abstract description 13
- 229940080264 sodium dodecylbenzenesulfonate Drugs 0.000 claims abstract description 13
- 239000003205 fragrance Substances 0.000 claims abstract description 9
- 239000002002 slurry Substances 0.000 claims description 33
- 239000000203 mixture Substances 0.000 claims description 29
- 238000003756 stirring Methods 0.000 claims description 27
- 239000000686 essence Substances 0.000 claims description 20
- 239000000463 material Substances 0.000 claims description 12
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 8
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 8
- 239000003795 chemical substances by application Substances 0.000 claims description 8
- 239000008187 granular material Substances 0.000 claims description 7
- 238000001816 cooling Methods 0.000 claims description 6
- 238000001914 filtration Methods 0.000 claims description 6
- 230000001007 puffing effect Effects 0.000 claims description 6
- 239000007787 solid Substances 0.000 claims description 6
- 238000001694 spray drying Methods 0.000 claims description 6
- 239000000126 substance Substances 0.000 claims description 6
- 238000005303 weighing Methods 0.000 claims description 6
- 238000000576 coating method Methods 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- 239000011347 resin Substances 0.000 claims description 4
- 229920005989 resin Polymers 0.000 claims description 4
- 239000011780 sodium chloride Substances 0.000 claims description 4
- 229960001922 sodium perborate Drugs 0.000 claims description 4
- 159000000000 sodium salts Chemical class 0.000 claims description 4
- YKLJGMBLPUQQOI-UHFFFAOYSA-M sodium;oxidooxy(oxo)borane Chemical compound [Na+].[O-]OB=O YKLJGMBLPUQQOI-UHFFFAOYSA-M 0.000 claims description 4
- 239000012467 final product Substances 0.000 claims description 3
- 238000000034 method Methods 0.000 claims description 3
- 102000004190 Enzymes Human genes 0.000 claims description 2
- 108090000790 Enzymes Proteins 0.000 claims description 2
- 102000004317 Lyases Human genes 0.000 claims description 2
- 108090000856 Lyases Proteins 0.000 claims description 2
- 239000004372 Polyvinyl alcohol Substances 0.000 claims description 2
- GVJHHUAWPYXKBD-UHFFFAOYSA-N d-alpha-tocopherol Natural products OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims description 2
- 238000000354 decomposition reaction Methods 0.000 claims description 2
- 238000004090 dissolution Methods 0.000 claims description 2
- MCPKSFINULVDNX-UHFFFAOYSA-N drometrizole Chemical compound CC1=CC=C(O)C(N2N=C3C=CC=CC3=N2)=C1 MCPKSFINULVDNX-UHFFFAOYSA-N 0.000 claims description 2
- 229930003935 flavonoid Natural products 0.000 claims description 2
- 150000002215 flavonoids Chemical class 0.000 claims description 2
- 235000017173 flavonoids Nutrition 0.000 claims description 2
- 150000008442 polyphenolic compounds Chemical class 0.000 claims description 2
- 235000013824 polyphenols Nutrition 0.000 claims description 2
- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 2
- 239000002994 raw material Substances 0.000 claims description 2
- 229960001295 tocopherol Drugs 0.000 claims description 2
- 229930003799 tocopherol Natural products 0.000 claims description 2
- 235000010384 tocopherol Nutrition 0.000 claims description 2
- 239000011732 tocopherol Substances 0.000 claims description 2
- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 claims description 2
- MRBKEAMVRSLQPH-UHFFFAOYSA-N 3-tert-butyl-4-hydroxyanisole Chemical compound COC1=CC=C(O)C(C(C)(C)C)=C1 MRBKEAMVRSLQPH-UHFFFAOYSA-N 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 5
- 230000003647 oxidation Effects 0.000 abstract description 5
- 238000007254 oxidation reaction Methods 0.000 abstract description 5
- 238000004140 cleaning Methods 0.000 abstract description 4
- 230000007774 longterm Effects 0.000 abstract description 2
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- 239000003599 detergent Substances 0.000 description 2
- 230000004075 alteration Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- CZBZUDVBLSSABA-UHFFFAOYSA-N butylated hydroxyanisole Chemical compound COC1=CC=C(O)C(C(C)(C)C)=C1.COC1=CC=C(O)C=C1C(C)(C)C CZBZUDVBLSSABA-UHFFFAOYSA-N 0.000 description 1
- 239000012459 cleaning agent Substances 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/83—Mixtures of non-ionic with anionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/02—Preparation in the form of powder by spray drying
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/0005—Other compounding ingredients characterised by their effect
- C11D3/0036—Soil deposition preventing compositions; Antiredeposition agents
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/0005—Other compounding ingredients characterised by their effect
- C11D3/0084—Antioxidants; Free-radical scavengers
-
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/046—Salts
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/08—Silicates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
- C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
- C11D3/1246—Silicates, e.g. diatomaceous earth
- C11D3/128—Aluminium silicates, e.g. zeolites
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
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- C11D3/3746—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/3749—Polyolefins; Halogenated polyolefins; Natural or synthetic rubber; Polyarylolefins or halogenated polyarylolefins
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- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
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Abstract
本发明公开了一种新型洗衣粉，该洗衣粉的组成以及各组分的百分比含量为：磺酸化聚苯乙烯10‑15％、铝硅酸钠5‑12％、二硅酸钠5‑10％、脂肪醇聚氧乙烯醚1‑4％、十二烷基苯磺酸钠3‑5％、非离子型表面活性剂12‑16％、纤维防垢剂5‑7％、蛋白酶1‑3％、脂肪酶1‑4％、柠檬酸钠4‑6％、膨化粉7‑9％、混合颗粒香精6‑15％、紫外线吸收剂1‑3％、抗氧化剂0.5‑2％，余量为水。本发明还公开了一种新型洗衣粉的制备方法，能够优化制备工艺，提高品控效果。本发明所制备的洗衣服，具有良好的清洗效果，能够达到甚至超过一般标准，并且使用本发明洗衣粉清洗的衣物具有明显的香味，香味具有多个层次，能够缓缓散发，持久留香；本发明的洗衣粉具有良好的抗氧化性，能够满足家庭长时间使用的要求。
Description
技术领域
本发明涉及清洁剂相关技术领域，具体为一种新型洗衣粉及其制备方法。
背景技术
随着人们生活水平的提高，人们有更好的条件来改善居住环境以及个人卫生，长期处于干净整洁的环境中，不仅能够促进人们的健康，还能使人身心愉悦。而人们除了保证自身身体的干净之外，一般还需要保证衣物的干净，洗衣粉以及洗衣液是目前最主要的两种衣物清洗剂，其能够产生泡沫，去除衣物上沾染的各种污渍，并且留下一定的香味，受到很多人的喜爱。
洗衣粉相对来说性价比更高，因此应用更为广泛，但是目前市面上的很多洗衣粉通常成分较为简单，不仅清洗效果一般，还难以留住香味，不易受到消费者的喜爱，竞争力不足。同时洗衣粉在储存的过程中，受到阳光的长时间直射时，很容易出现氧化的情况，造成变质。鉴于此，我们提出一种新型洗衣粉及其制备方法。
发明内容
本发明的目的在于提供一种新型洗衣粉及其制备方法，以解决背景技术中提出的问题。
为实现目的，本发明提供如下技术方案，一种新型洗衣粉，该洗衣粉的组成以及各组分的百分比含量为：磺酸化聚苯乙烯10-15％、铝硅酸钠5-12％、二硅酸钠5-10％、脂肪醇聚氧乙烯醚1-4％、十二烷基苯磺酸钠3-5％、非离子型表面活性剂12-16％、纤维防垢剂5-7％、蛋白酶1-3％、脂肪酶1-4％、柠檬酸钠4-6％、膨化粉7-9％、混合颗粒香精6-15％、紫外线吸收剂1-3％、抗氧化剂0.5-2％，余量为水。
优选的，所述纤维防垢剂为混合制剂，由树脂、钠盐、过硼酸钠、氯化钠、分解酶、聚乙稀醇、乙醇和水混合组成，各组份的配合比例是：树脂占6-10％，钠盐占0.2-0.4％，过硼酸钠占0.3-0.5％，氯化钠占0.3-0.5％，分解酶占0.4-0.6％，乙醇占约5％，余量为水。
优选的，所述混合颗粒香精包括有三种及以上香味，且混合颗粒香精利用植物香精为原料制成颗粒，并在其上包裹包衣，并且不同种类的植物香精包裹不同厚度的包衣，具有不同的溶解层级。
优选的，所述紫外线吸收剂采用紫外线吸收剂UV-P和紫外线吸收剂UV-O的混合物。
优选的，所述抗氧化剂采用茶多酚(TP)、生育酚、黄酮类、丁基羟基茴香醚中的一种或多种。
一种新型洗衣粉的制备方法，该制备方法为：按比例称取磺酸化聚苯乙烯、铝硅酸钠、二硅酸钠、脂肪醇聚氧乙烯醚、十二烷基苯磺酸钠，全部组合一起，倒入浆料搅拌机中，加水后进行搅拌，转速800-1000转/分钟的状态下，搅拌40-60分钟，随后再加入非离子型表面活性剂、纤维防垢剂、蛋白酶、脂肪酶、柠檬酸钠、膨化粉、紫外线吸收剂、抗氧化剂，加速至1000-1200转/分钟，搅拌90分钟，制成洗衣粉浆料，然后转入温控密封式搅拌机中搅拌，控制温控搅拌机的温度在50℃-80℃，搅拌时间为60-120分钟，然后用10目网过滤，除去粒度过大的固体物，随后将浆料输入到高压温控喷雾器中，喷雾干燥成空心颗粒，凉后输送到软体搅拌机中，加入混合颗粒香精进行软体搅拌，搅拌时间为60-120分钟，制得洗衣粉。
与现有技术相比，本发明的有益效果是：
1.本发明所制备的洗衣服，具有良好的清洗效果，能够达到甚至超过一般标准，并且使用本发明洗衣粉清洗的衣物具有明显的香味，香味具有多个层次，能够缓缓散发，持久留香，足以受到消费者的喜爱，提高市场竞争力；
2.本发明的洗衣粉经过100h阳光直射的检测，氧化率低于2％，具有良好的抗氧化性，能够满足家庭长时间使用的要求。
具体实施方式
下面对本发明实施例中的技术方案进行清楚、完整地描述，显然，所描述的实施例仅仅是本发明一部分实施例，而不是全部的实施例。基于本发明中的实施例，本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例，都属于本发明保护的范围。
本发明提供一种技术方案：下面结合具体实施方式对本专利的技术方案作进一步详细地说明。
一种新型洗衣粉，该洗衣粉的组成以及各组分的百分比含量为：磺酸化聚苯乙烯10-15％、铝硅酸钠5-12％、二硅酸钠5-10％、脂肪醇聚氧乙烯醚1-4％、十二烷基苯磺酸钠3-5％、非离子型表面活性剂12-16％、纤维防垢剂5-7％、蛋白酶1-3％、脂肪酶1-4％、柠檬酸钠4-6％、膨化粉7-9％、混合颗粒香精6-15％、紫外线吸收剂1-3％、抗氧化剂0.5-2％，余量为水。
一种新型洗衣粉的制备方法，该制备方法为：按比例称取磺酸化聚苯乙烯、铝硅酸钠、二硅酸钠、脂肪醇聚氧乙烯醚、十二烷基苯磺酸钠，全部组合一起，倒入浆料搅拌机中，加水后进行搅拌，转速800-1000转/分钟的状态下，搅拌40-60分钟，随后再加入非离子型表面活性剂、纤维防垢剂、蛋白酶、脂肪酶、柠檬酸钠、膨化粉、紫外线吸收剂、抗氧化剂，加速至1000-1200转/分钟，搅拌90分钟，制成洗衣粉浆料，然后转入温控密封式搅拌机中搅拌，控制温控搅拌机的温度在50℃-80℃，搅拌时间为60-120分钟，然后用10目网过滤，除去粒度过大的固体物，随后将浆料输入到高压温控喷雾器中，喷雾干燥成空心颗粒，凉后输送到软体搅拌机中，加入混合颗粒香精进行软体搅拌，搅拌时间为60-120分钟，制得洗衣粉。
具体实施例1
一种新型洗衣粉，该洗衣粉的组成以及各组分的百分比含量为：磺酸化聚苯乙烯12％、铝硅酸钠6％、二硅酸钠8％、脂肪醇聚氧乙烯醚3％、十二烷基苯磺酸钠4％、非离子型表面活性剂15％、纤维防垢剂7％、蛋白酶2％、脂肪酶2％、柠檬酸钠4％、膨化粉9％、混合颗粒香精6％、紫外线吸收剂3％、抗氧化剂2％，余量为水。
一种新型洗衣粉的制备方法，该制备方法为：按比例称取磺酸化聚苯乙烯、铝硅酸钠、二硅酸钠、脂肪醇聚氧乙烯醚、十二烷基苯磺酸钠，全部组合一起，倒入浆料搅拌机中，加水后进行搅拌，转速800转/分钟的状态下，搅拌60分钟，随后再加入非离子型表面活性剂、纤维防垢剂、蛋白酶、脂肪酶、柠檬酸钠、膨化粉、紫外线吸收剂、抗氧化剂，加速至1200转/分钟，搅拌90分钟，制成洗衣粉浆料，然后转入温控密封式搅拌机中搅拌，控制温控搅拌机的温度在60℃，搅拌时间为100分钟，然后用10目网过滤，除去粒度过大的固体物，随后将浆料输入到高压温控喷雾器中，喷雾干燥成空心颗粒，凉后输送到软体搅拌机中，加入混合颗粒香精进行软体搅拌，搅拌时间为60分钟，制得洗衣粉。
具体实施例2
一种新型洗衣粉，该洗衣粉的组成以及各组分的百分比含量为：磺酸化聚苯乙烯15％、铝硅酸钠11％、二硅酸钠8％、脂肪醇聚氧乙烯醚3％、十二烷基苯磺酸钠3％、非离子型表面活性剂15％、纤维防垢剂6％、蛋白酶3％、脂肪酶4％、柠檬酸钠5％、膨化粉7％、混合颗粒香精15％、紫外线吸收剂2％、抗氧化剂0.5％，余量为水。
一种新型洗衣粉的制备方法，该制备方法为：按比例称取磺酸化聚苯乙烯、铝硅酸钠、二硅酸钠、脂肪醇聚氧乙烯醚、十二烷基苯磺酸钠，全部组合一起，倒入浆料搅拌机中，加水后进行搅拌，转速1000转/分钟的状态下，搅拌50分钟，随后再加入非离子型表面活性剂、纤维防垢剂、蛋白酶、脂肪酶、柠檬酸钠、膨化粉、紫外线吸收剂、抗氧化剂，加速至1100转/分钟，搅拌90分钟，制成洗衣粉浆料，然后转入温控密封式搅拌机中搅拌，控制温控搅拌机的温度在80℃，搅拌时间为120分钟，然后用10目网过滤，除去粒度过大的固体物，随后将浆料输入到高压温控喷雾器中，喷雾干燥成空心颗粒，凉后输送到软体搅拌机中，加入混合颗粒香精进行软体搅拌，搅拌时间为80分钟，制得洗衣粉。
具体实施例3
一种新型洗衣粉，该洗衣粉的组成以及各组分的百分比含量为：磺酸化聚苯乙烯13％、铝硅酸钠11％、二硅酸钠8％、脂肪醇聚氧乙烯醚4％、十二烷基苯磺酸钠3％、非离子型表面活性剂15％、纤维防垢剂6％、蛋白酶2％、脂肪酶4％、柠檬酸钠6％、膨化粉9％、混合颗粒香精10％、紫外线吸收剂3％、抗氧化剂1％，余量为水。
一种新型洗衣粉的制备方法，该制备方法为：按比例称取磺酸化聚苯乙烯、铝硅酸钠、二硅酸钠、脂肪醇聚氧乙烯醚、十二烷基苯磺酸钠，全部组合一起，倒入浆料搅拌机中，加水后进行搅拌，转速900转/分钟的状态下，搅拌60分钟，随后再加入非离子型表面活性剂、纤维防垢剂、蛋白酶、脂肪酶、柠檬酸钠、膨化粉、紫外线吸收剂、抗氧化剂，加速至1000转/分钟，搅拌90分钟，制成洗衣粉浆料，然后转入温控密封式搅拌机中搅拌，控制温控搅拌机的温度在70℃，搅拌时间为120分钟，然后用10目网过滤，除去粒度过大的固体物，随后将浆料输入到高压温控喷雾器中，喷雾干燥成空心颗粒，凉后输送到软体搅拌机中，加入混合颗粒香精进行软体搅拌，搅拌时间为80分钟，制得洗衣粉。
对以上三个实施例制备的洗衣粉进行性能检测，均具有良好的清洗效果，完全能够达到甚至超过标准，同时经过100h阳光直射的检测，以上三个实施例制备的洗衣粉氧化率均低于2％，具有良好的抗氧化性，能够满足家庭长时间使用的要求；并且，使用以上方法制备的洗衣粉清洗的衣物具有明显的香味，香味具有多个层次，能够缓缓散发，持久留香。
尽管已经示出和描述了本发明的实施例，对于本领域的普通技术人员而言，可以理解在不脱离本发明的原理和精神的情况下可以对这些实施例进行多种变化、修改、替换和变型，本发明的范围由所附权利要求及其等同物限定。
Claims (6)
1.一种新型洗衣粉，其特征在于：该洗衣粉的组成以及各组分的百分比含量为：磺酸化聚苯乙烯10-15％、铝硅酸钠5-12％、二硅酸钠5-10％、脂肪醇聚氧乙烯醚1-4％、十二烷基苯磺酸钠3-5％、非离子型表面活性剂12-16％、纤维防垢剂5-7％、蛋白酶1-3％、脂肪酶1-4％、柠檬酸钠4-6％、膨化粉7-9％、混合颗粒香精6-15％、紫外线吸收剂1-3％、抗氧化剂0.5-2％，余量为水。
2.根据权利要求1所述的一种新型洗衣粉，其特征在于：所述纤维防垢剂为混合制剂，由树脂、钠盐、过硼酸钠、氯化钠、分解酶、聚乙稀醇、乙醇和水混合组成，各组份的配合比例是：树脂占6-10％，钠盐占0.2-0.4％，过硼酸钠占0.3-0.5％，氯化钠占0.3-0.5％，分解酶占0.4-0.6％，乙醇占约5％，余量为水。
3.根据权利要求2所述的一种新型洗衣粉，其特征在于：所述混合颗粒香精包括有三种及以上香味，且混合颗粒香精利用植物香精为原料制成颗粒，并在其上包裹包衣，并且不同种类的植物香精包裹不同厚度的包衣，具有不同的溶解层级。
4.根据权利要求3所述的一种新型洗衣粉，其特征在于：所述紫外线吸收剂采用紫外线吸收剂UV-P和紫外线吸收剂UV-O的混合物。
5.根据权利要求4所述的一种新型洗衣粉，其特征在于：所述抗氧化剂采用茶多酚(TP)、生育酚、黄酮类、丁基羟基茴香醚中的一种或多种。
6.一种根据权利要求1-5任意一项所述的新型洗衣粉的制备方法，其特征在于：该制备方法为：按比例称取磺酸化聚苯乙烯、铝硅酸钠、二硅酸钠、脂肪醇聚氧乙烯醚、十二烷基苯磺酸钠，全部组合一起，倒入浆料搅拌机中，加水后进行搅拌，转速800-1000转/分钟的状态下，搅拌40-60分钟，随后再加入非离子型表面活性剂、纤维防垢剂、蛋白酶、脂肪酶、柠檬酸钠、膨化粉、紫外线吸收剂、抗氧化剂，加速至1000-1200转/分钟，搅拌90分钟，制成洗衣粉浆料，然后转入温控密封式搅拌机中搅拌，控制温控搅拌机的温度在50℃-80℃，搅拌时间为60-120分钟，然后用10目网过滤，除去粒度过大的固体物，随后将浆料输入到高压温控喷雾器中，喷雾干燥成空心颗粒，凉后输送到软体搅拌机中，加入混合颗粒香精进行软体搅拌，搅拌时间为60-120分钟，制得洗衣粉。
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