CN114085068A - Aluminum ash light brick and preparation method thereof - Google Patents
Aluminum ash light brick and preparation method thereof Download PDFInfo
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- CN114085068A CN114085068A CN202111532588.1A CN202111532588A CN114085068A CN 114085068 A CN114085068 A CN 114085068A CN 202111532588 A CN202111532588 A CN 202111532588A CN 114085068 A CN114085068 A CN 114085068A
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- aluminum ash
- brick
- aluminum
- ash
- parts
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- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 title claims abstract description 82
- 229910052782 aluminium Inorganic materials 0.000 title claims abstract description 80
- 239000011449 brick Substances 0.000 title claims abstract description 61
- 238000002360 preparation method Methods 0.000 title abstract description 11
- 239000002956 ash Substances 0.000 claims abstract description 67
- 238000000498 ball milling Methods 0.000 claims abstract description 17
- 239000000203 mixture Substances 0.000 claims abstract description 14
- 239000000843 powder Substances 0.000 claims abstract description 11
- 239000002994 raw material Substances 0.000 claims abstract description 11
- 239000010881 fly ash Substances 0.000 claims abstract description 10
- 229910052500 inorganic mineral Inorganic materials 0.000 claims abstract description 9
- 239000011707 mineral Substances 0.000 claims abstract description 9
- 239000002245 particle Substances 0.000 claims abstract description 9
- 238000005245 sintering Methods 0.000 claims abstract description 9
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 7
- 238000002156 mixing Methods 0.000 claims abstract description 6
- 238000003825 pressing Methods 0.000 claims abstract description 6
- 238000001816 cooling Methods 0.000 claims abstract description 3
- 230000003068 static effect Effects 0.000 claims abstract description 3
- 239000000463 material Substances 0.000 claims description 7
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims description 6
- 239000004327 boric acid Substances 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 238000000034 method Methods 0.000 claims description 5
- 238000000465 moulding Methods 0.000 claims description 5
- 239000002893 slag Substances 0.000 claims description 5
- WUKWITHWXAAZEY-UHFFFAOYSA-L calcium difluoride Chemical group [F-].[F-].[Ca+2] WUKWITHWXAAZEY-UHFFFAOYSA-L 0.000 claims description 3
- 239000010436 fluorite Substances 0.000 claims description 3
- 230000008569 process Effects 0.000 claims description 3
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 2
- 238000000926 separation method Methods 0.000 claims description 2
- 239000004927 clay Substances 0.000 abstract description 10
- 238000012216 screening Methods 0.000 abstract description 8
- 230000000694 effects Effects 0.000 abstract description 6
- 239000004566 building material Substances 0.000 abstract description 5
- 239000011148 porous material Substances 0.000 abstract description 4
- 238000000227 grinding Methods 0.000 abstract 1
- 238000001354 calcination Methods 0.000 description 6
- 239000000654 additive Substances 0.000 description 5
- 230000000996 additive effect Effects 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 238000009413 insulation Methods 0.000 description 3
- 239000012258 stirred mixture Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- PMHQVHHXPFUNSP-UHFFFAOYSA-M copper(1+);methylsulfanylmethane;bromide Chemical compound Br[Cu].CSC PMHQVHHXPFUNSP-UHFFFAOYSA-M 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 238000009776 industrial production Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 2
- 238000004321 preservation Methods 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 1
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 1
- 241000565357 Fraxinus nigra Species 0.000 description 1
- 238000003723 Smelting Methods 0.000 description 1
- 235000011941 Tilia x europaea Nutrition 0.000 description 1
- 239000011469 building brick Substances 0.000 description 1
- 238000005266 casting Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000003009 desulfurizing effect Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 238000007667 floating Methods 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
- 239000011464 hollow brick Substances 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000004571 lime Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 239000011819 refractory material Substances 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000002910 solid waste Substances 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/132—Waste materials; Refuse; Residues
- C04B33/138—Waste materials; Refuse; Residues from metallurgical processes, e.g. slag, furnace dust, galvanic waste
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/132—Waste materials; Refuse; Residues
- C04B33/135—Combustion residues, e.g. fly ash, incineration waste
- C04B33/1352—Fuel ashes, e.g. fly ash
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/74—Physical characteristics
- C04B2235/77—Density
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/60—Production of ceramic materials or ceramic elements, e.g. substitution of clay or shale by alternative raw materials, e.g. ashes
Abstract
The invention discloses an aluminum ash light brick and a preparation method thereof, wherein the aluminum ash light brick is prepared from the following raw materials in parts by weight: 50-70 parts of aluminum ash, 15-20 parts of fly ash, 20-30 parts of mineral powder and 1-3 parts of auxiliary agent, obtaining a proper particle size after ball milling and screening the aluminum ash, and then uniformly mixing the aluminum ash, the mineral powder and the auxiliary agent; then pouring the mixture into a grinding tool, and pressing and forming the mixture by a static pressure machine; and demolding, sintering and cooling to obtain the light brick with low density and uniform size. Compared with the traditional clay brick, the lightweight brick taking the aluminum ash as the main raw material has lower density and higher strength, can effectively reduce the bearing of a building, and has good heat-insulating and sound-insulating effects due to the uniform pore structure, thereby replacing the clay brick or the common lightweight brick to a certain extent as a novel building material.
Description
Technical Field
The invention belongs to the technical field of building materials, relates to a resource utilization method of industrial solid waste, and particularly relates to an aluminum ash light brick and a preparation method thereof.
Background
The aluminum ash (also called aluminum slag ash or aluminum slag) is a kind of dross generated in the primary and secondary aluminum industrial production, is the main loss part of liquid raw aluminum in the electrolytic aluminum production, mainly comes from infusible inclusion floating on the surface of aluminum melt in the casting process, additive and substance generated by physical and chemical reaction with the additive, and is in loose ash shape. The aluminum ash produced during the liquid primary aluminum processing process generally contains 30-70% of metallic aluminum, and is generally called lime or primary aluminum ash, and can be used as a raw material for secondary aluminum industrial production. The secondary aluminum industry is primarily concerned with the recovery of aluminum from various wastes (e.g., primary aluminum ash, aluminum scrap, etc. from aluminum processing). The waste produced by the secondary aluminum industry typically contains 5% to 20% metallic aluminum and a large amount of soluble salts, commonly referred to as black ash. The aluminum ash contains a plurality of substances which are directly or indirectly harmful to the environment, and the direct discarding can cause environmental pollution; the aluminum ash is a renewable resource with comprehensive utilization value, and secondary energy sources such as aluminum, salt, aluminum oxide and the like can be recycled from the aluminum ash; it can also be used as raw material for refractory material, road and building material, and desulfurizing agent for steel-smelting.
The bricks traditionally used in the construction industry are mostly formed by evenly stirring clay and other auxiliary materials and then forming the mixture by a briquetting machine and then firing the mixture. Traditional brick is heavier when building a wall, and is hard when building a wall, and the inevitable bearing burden that has increased the building, and the wall that this brick was built simultaneously gives sound insulation, keeps warm, the effect of taking precautions against earthquakes is poor, and anti-seismic performance is low. In addition, the preparation raw materials need a large amount of clay, which has great negative effects on natural resources and ecological balance.
As a result, the brick sintered by the aluminum ash has more porous structures, compared with the traditional solid brick, the weight of the aluminum ash light brick is only 60% -70%, the density is obviously reduced, and compared with the hollow brick, the brick has the advantages of compact structure and good strength. The reactive aluminum nitride contained in the aluminum ash raw material is decomposed after high-temperature sintering, and the nitrogen and other halogen elements in the reactive aluminum nitride are volatilized in a gas form, so that the dangerous characteristic of the aluminum ash is eliminated. In addition, the aluminum ash sintered brick has a porous structure, has the effects of sound insulation, noise reduction, heat preservation and shock resistance when being used for building walls, is particularly suitable for non-bearing walls of commercial places and entertainment places, and is an excellent building brick.
Disclosure of Invention
In order to solve the problems in the prior art, the invention aims to provide an aluminum ash lightweight brick and a preparation method thereof, the lightweight brick taking aluminum ash as a main raw material has lower density and higher strength, can effectively reduce the load bearing of a building, and has good heat preservation and sound insulation effects due to a uniform pore structure, so that the lightweight brick replaces a clay brick or a common lightweight brick to a certain extent as a novel building material.
The invention uses fine aluminum ash to sinter high-strength light bricks, wherein the aluminum ash contains high aluminum oxide. The high-strength light-weight brick is prepared by ball milling the aluminum ash, winnowing and screening to obtain the aluminum ash with proper particle size, mixing the aluminum ash with the fly ash, the mineral powder and the auxiliary agent, and sintering.
The purpose of the invention is realized by the following technical scheme:
an aluminum ash light brick is prepared from the following raw materials in parts by weight:
preferably, the aluminum ash is ball-milled, and the ball-milling process parameters are as follows: the ball milling revolution is 300 and 2500 revolutions per minute, and the ball milling time is 0.5 to 2 hours; then passing through a wind separation sieve, the particle size is 200-400 meshes.
Preferably, the particle size of the fly ash is 300-600 meshes, and the content of alumina is lower than 35 wt%.
Preferably, the ore fines are of the type S75, S95 or S105 ore fines.
Preferably, the auxiliary agent is fluorite tailing slag or boric acid.
According to the invention, the fluorite tailing slag or boric acid is added, so that the sintering temperature of the light brick can be effectively reduced, and the pore density of the light brick can be increased.
The invention also provides a preparation method of the aluminum ash light brick, which comprises the following steps:
(1) uniformly mixing the aluminum ash, the mineral powder, the fly ash and the auxiliary agent in a stirring tank according to a set proportion to obtain a mixture;
(2) pouring the mixture into a mold, pressing and molding the material through a static pressure machine, delivering the molded material into a sintering kiln, sintering at the temperature of 900-1050 ℃, cooling, and demolding to obtain the aluminum ash light brick.
The invention has the advantages and effects that:
the invention takes the aluminum ash as the main raw material, the aluminum ash generates weak reaction with water at normal temperature, and can release gases such as ammonia gas and the like at high temperature to form uniform air holes in the material, thereby effectively reducing the density of the material.
The aluminum ash is mixed with the fly ash and the mineral powder, then the sintering temperature is further reduced and the pore density of the light brick is increased under the cooperation of the auxiliary agent, so that the aluminum ash light brick with lower density and higher strength can be obtained.
Compared with the traditional clay brick, the light brick taking the aluminum ash as the main raw material has lower density and higher strength, and can effectively reduce the bearing of a building, thereby replacing the clay brick or the common light brick to a certain extent as a novel building material.
Drawings
FIG. 1 is a flow chart of the preparation process of the aluminum ash lightweight brick of the invention.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments of the present invention will be clearly and completely described below.
Example 1
An aluminum ash light brick and a preparation method thereof are as follows:
(1) ball milling, winnowing and screening the aluminum ash, wherein the ball milling speed of the aluminum ash is 1500 rpm, the ball milling time is 1.5 hours, and the screening particle size is 200-400 meshes;
(2) uniformly mixing 55 parts of aluminum ash, 15 parts of fly ash, 28 parts of mineral powder and 1 part of boric acid additive according to parts by weight, wherein the stirring speed is 240 revolutions per minute;
(3) adding 6 parts of water into the stirred mixture, pouring the mixture into a mold, and pressing and molding the mixture;
(4) placing the pressed aluminum ash brick blocks for 24 hours and then demoulding;
(5) and (3) putting the demolded aluminum ash bricks into a kiln for calcining, wherein the calcining temperature is 1000 ℃.
Example 2
An aluminum ash light brick and a preparation method thereof are as follows:
(1) ball milling, winnowing and screening the aluminum ash, wherein the ball milling speed of the aluminum ash is 1200 r/min, the ball milling time is 2 hours, and the screening particle size is 200-400 meshes;
(2) uniformly mixing 60 parts of aluminum ash, 15 parts of fly ash, 22 parts of mineral powder and 1 part of boric acid additive in parts by weight, wherein the stirring speed is 240 revolutions per minute;
(3) adding 6 parts of water into the stirred mixture, pouring the mixture into a mold, and pressing and molding the mixture;
(4) placing the pressed aluminum ash brick blocks for 24 hours and then demoulding;
(5) and (3) putting the demolded aluminum ash bricks into a kiln for calcining, wherein the calcining temperature is 1000 ℃.
Example 3
An aluminum ash light brick and a preparation method thereof are as follows:
(1) ball milling, winnowing and screening the aluminum ash, wherein the ball milling speed of the aluminum ash is 1800 rpm, the ball milling time is 1.8 hours, and the screening particle size is 200-400 meshes;
(2) according to the weight portion, 65 portions of aluminum ash, 18 portions of fly ash, 25 portions of mineral powder and 2 portions of boric acid additive are uniformly mixed, and the stirring speed is 240 r/m;
(3) adding 6 parts of water into the stirred mixture, pouring the mixture into a mold, and pressing and molding the mixture;
(4) placing the pressed aluminum ash brick blocks for 24 hours and then demoulding;
(5) and putting the demolded aluminum ash bricks into a kiln for calcining, wherein the calcining temperature is 950 ℃.
TABLE 1 comparison of main Properties of the lightweight bricks according to the invention
The compressive strength of the clay brick purchased from the market is 18.2MPa, and the bulk density is 2085kg/m3The compressive strength of the baking-free light brick prepared in the embodiments 1 to 3 is 11.5MPa to 12.5MPa, which is lower than that of a sintered clay brick, but the compressive strength of the baking-free light brick meets the MU10 standard value of GB5101-2003, and the baking-free light brick can be used for non-load-bearing walls; the bulk density is 1030kg/m3~1070kg/m3Much lower than the bulk density of the fired clay brick.
The light brick prepared by the invention has the characteristics of light weight, good strength and high temperature resistance.
It is only a preferred embodiment of the present invention and is not intended to limit the present invention, and various modifications and changes may be made to the present invention by those skilled in the art. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (6)
2. the aluminum ash light brick as claimed in claim 1, wherein the aluminum ash is ball milled first, and the ball milling process parameters are as follows: the ball milling revolution is 300 and 2500 revolutions per minute, and the ball milling time is 0.5 to 2 hours; then passing through a wind separation sieve, the particle size is 200-400 meshes.
3. The aluminum ash lightweight brick as claimed in claim 1, wherein the particle size of the fly ash is 300-600 mesh, and the content of alumina is less than 35 wt%.
4. The aluminum ash lightweight brick as claimed in claim 1, wherein the ore powder type is S75, S95 or S105 ore powder.
5. The aluminum ash lightweight brick according to claim 1, wherein the auxiliary is fluorite tailing slag or boric acid.
6. The method for preparing an aluminum ash lightweight brick according to any one of claims 1 to 5, which comprises the steps of:
(1) uniformly mixing the aluminum ash, the mineral powder, the fly ash and the auxiliary agent in a stirring tank according to a set proportion to obtain a mixture;
(2) pouring the mixture into a mold, pressing and molding the material through a static pressure machine, delivering the molded material into a sintering kiln, sintering at the temperature of 900-1050 ℃, cooling, and demolding to obtain the aluminum ash light brick.
Priority Applications (1)
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CN202111532588.1A CN114085068A (en) | 2021-12-15 | 2021-12-15 | Aluminum ash light brick and preparation method thereof |
Applications Claiming Priority (1)
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CN202111532588.1A CN114085068A (en) | 2021-12-15 | 2021-12-15 | Aluminum ash light brick and preparation method thereof |
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CN114085068A true CN114085068A (en) | 2022-02-25 |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN114644506A (en) * | 2022-04-08 | 2022-06-21 | 福建省德化县合和陶瓷技术开发有限公司 | Environment-friendly high-whiteness domestic ceramic product and preparation process thereof |
CN115432997A (en) * | 2022-10-18 | 2022-12-06 | 中南大学 | Ceramic-based molten salt composite phase-change heat storage material and preparation method thereof |
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CN114644506A (en) * | 2022-04-08 | 2022-06-21 | 福建省德化县合和陶瓷技术开发有限公司 | Environment-friendly high-whiteness domestic ceramic product and preparation process thereof |
CN115432997A (en) * | 2022-10-18 | 2022-12-06 | 中南大学 | Ceramic-based molten salt composite phase-change heat storage material and preparation method thereof |
CN115432997B (en) * | 2022-10-18 | 2023-08-22 | 中南大学 | Ceramic-based fused salt composite phase-change heat storage material and preparation method thereof |
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